Roll No"

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Total No. of Questions: 101

B. Pharmacy (Sem.- l')

PHARMACEUTTCAL ANALYSIS - I
SUBJEqTCODE : PHM - 1.1.1(2k9Batch
PaperID : [D01a5l
[Note : Pleasefill subjectcodeand paperlD on OMRI

Time : 03 Hours Maximum Marks : 80

Instructionto Candidates:
l) Section- A is Compulsory.
2) Attemptany Four questionsfrom Section- B.
3) AttemptanyThree questionsfrom Section- C.

Section- A
QI) (15x2=30)
a) Standard
deviation.
b) StudenL
t-test.
c) Conjugateacidandconjugatebase.
d) Precislon.
e) Selfinciicato:.

D Blanktitration.
'
g) Co-precipitation.
h) Digestion.

D Salthydrolysis.

) Titrationcurve.
k) Oxidationnumber.
l) reductionpotential.
Standard
m) Colloidssolution.
n) Acidimetry
o) Buffersolution.
2eI
J-e60[8r P.TO.
 Section - B
(4 x S :20)

Q2) Discussvarioustheoriesof neutralizattonindicator.

Q3) Discusstitration curve of weak acid with weak base.

Q4) DescribeIdometricand Iodimetric assayswith suitableexamples.

QS) What is the critical role playedby commonion effect in gravimetricanalysis?

Explain.

Q6) Explain role of solubility product in precipitationreactionsgoverning

argentimetrictitration methods.

Section- C
(3 x 10:30)
Q7) What arethe two majortypesof error encounteredin pharmaceuticalanalysis?
Explainwith suitableexamples.

QS) What is Volhard'smethod of argentimetrictitration? Explain it with the help

of equationandthe precautionsinvolved in it.

'
Q9) Describemeasurement ofelectrodepotentialandits applicationin determining
equilibrium constantof redox reaction.

QI0) Writeshortnoteson :
(a) Organicprecipitant.
(b) Titrationof polyproticacid.

SSOS

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