This document provides procedures for preparing two coordination compounds: bis(acetylacetonato)diaquanickel(II) and tris(acetylacetonato)iron(III). For bis(acetylacetonato)diaquanickel(II), nickel sulfate is dissolved in water and added to an acetylacetone and sodium hydroxide solution. The product is recrystallized in ethanol and filtered. For tris(acetylacetonato)iron(III), iron(III) chloride is dissolved in water and precipitated with ammonium hydroxide before being heated with acetylacetone to form the product, which is then filtered.
Original Description:
Preparation of Bis(acetylacetonato)diaquanickel(II)
Preparation of Tris(acetylacetonato)iron(III)
This document provides procedures for preparing two coordination compounds: bis(acetylacetonato)diaquanickel(II) and tris(acetylacetonato)iron(III). For bis(acetylacetonato)diaquanickel(II), nickel sulfate is dissolved in water and added to an acetylacetone and sodium hydroxide solution. The product is recrystallized in ethanol and filtered. For tris(acetylacetonato)iron(III), iron(III) chloride is dissolved in water and precipitated with ammonium hydroxide before being heated with acetylacetone to form the product, which is then filtered.
This document provides procedures for preparing two coordination compounds: bis(acetylacetonato)diaquanickel(II) and tris(acetylacetonato)iron(III). For bis(acetylacetonato)diaquanickel(II), nickel sulfate is dissolved in water and added to an acetylacetone and sodium hydroxide solution. The product is recrystallized in ethanol and filtered. For tris(acetylacetonato)iron(III), iron(III) chloride is dissolved in water and precipitated with ammonium hydroxide before being heated with acetylacetone to form the product, which is then filtered.