POTASSIUM IODIDE

TITLE

A laboratory group report for Pharmaceutical Chemistry 1

Class Schedule: PHARM 114L 3:30-5:30 MWF

Prepared by Group 3

*Group Members Contribution Signature

1. ALIM, Mia Franz
2. ANCERO, Angelica L.
3. BALNEG, Joyce R.
4. BALUYOT, Leianne Wichelle
5. BAUZON, Raechell Anne
6. BILLEDO, Monica Lai
7. BOADO, Patricia Anne L.
Preparation and Identification of Potassium iodide
Preparation of Potassium iodide
Preparation of Potassium iodide
Labelled the Potassium iodide product
Preparation of Potassium iodide
Identification of Potassium iodide
Preparation and identification of potassium iodide;
prepared the group report for identification tests.

Excellent(25pts) Good(20pts) Satisfactory(15pts) Needs Improvement

(10pts)
Analytical Results □ □ □ □
Questions for □ □ □ □
Research

Comments, Suggestions, Deductions:

Total Deductions:

Total Score:
Identification Test for Potassium iodide (photo documentation)

1. Add a pinch of the salt in water and stir.

Result: The salt was dissolved, thus, making it soluble in water.

Prepared Potassium iodide by the group Commercial Potassium iodide

2. To the above solution, add silver nitrate T.S.

Result: Formation of yellow precipitate of AgI

Prepared Potassium iodide by the group Commercial Potassium iodide

3. To another solution of the salt, add hydrochloric acid or sulfuric acid.

Result: Formation of white precipitate.
Rationale: The reagents used was concentrated Hydrochloric acid and Sulfuric acid, thus, no formation of white
precipitate formed. The reagents that was supposed to be used is diluted HCl and sulfuric dioxide gas.
Reference: http://ncert.nic.in/ncerts/l/kelm207.pdf
Prepared Potassium iodide by the group Commercial Potassium iodide
Hydrochloric acid Hydrochloric acid

Sulfuric acid Sulfuric acid


*Group Members
8. ALIM, Mia Franz
9. ANCERO, Angelica L.
10. BALNEG, Joyce R.
11. BALUYOT, Leianne Wichelle
12. BAUZON, Raechell Anne
13. BILLEDO, Monica Lai
14. BOADO, Patricia Anne L.
Excellent(25pts)
Analytical Results
Questions for
Research
Comments, Suggestions, Deductions:
POTASSIUM BITARTRATE
TITLE
A laboratory group report for Pharmaceutical Chemistry 1
Class Schedule: PHARM 114L 3:30-5:30 MWF
Prepared by Group 3
Contribution Signature
Preparation and Identification of Potassium bitartrate
Preparation of Potassium bitartrate
Preparation of Potassium bitartrate
Preparation of Potassium bitartrate
Preparation of Potassium bitartrate
Labelled the Potassium bitartrate product and prepared the
group report
Labelled the Potassium bitartrate product and prepared the
group report
Good(20pts) Satisfactory(15pts) Needs Improvement
(10pts)
□ □ □ □
□ □ □ □
Total Deductions:
Total Score:
Identification Test for Potassium bitartrate (photo documentation)

1. Heat the crystals at high temperature.

Result: Ash-like forming chars

Prepared Potassium bitartrate by the group Commercial Potassium bitartrate

2. Dissolve the residue in water and perform the Beilstein’s test.

Result: Negative result for Beilstein’s test.

Prepared Potassium bitartrate by the group Commercial Potassium bitartrate

3. Prepare a saturated aqueous solution of potassium bitartrate, neutralized with sodium hydroxide, add silver
nitrate T.S.
To the precipitated formed, dissolve it with ammonia T.S. and the solution warmed.
Result: Silver mirror/metallic silver is deposited along the inner walls of the test tube.

Prepared Potassium bitartrate by the group Commercial Potassium bitartrate

4. Prepare a 1% resorcinol solution in a hydrochloric acid. Add a few drops of this solution to a dry salt of potassium
bitartrate. Then add 3 mL of sulfuric acid and slowly heat the solution.
Result: Rose-red color is formed; after heating, it becomes colorless.

Prepared Potassium bitartrate by the group Commercial Potassium bitartrate

4. Acidify a tartarate solution with acetic acid. Add a few drops of ferrous sulfate T.S. and hydrogen peroxide T.S.,
then add an excess of sodium hydroxide T.S.
Result: Purple/violet color of solution.

Prepared Potassium bitartrate by the group Commercial Potassium bitartrate

 SODIUM CITRATE
TITLE

A laboratory group report for Pharmaceutical Chemistry 1

Class Schedule: PHARM 114L 3:30-5:30 MWF

Prepared by Group 3

*Group Members Contribution Signature

15. ALIM, Mia Franz
16. ANCERO, Angelica L.
17. BALNEG, Joyce R.
18. BALUYOT, Leianne Wichelle
19. BAUZON, Raechell Anne
20. BILLEDO, Monica Lai
21. BOADO, Patricia Anne L.
Preparation of Sodium citrate
Preparation of Sodium citrate
Preparation of Sodium citrate
Identification Test for Sodium citrate
Identification of Sodium citrate
Labelled the Sodium citrate and prepared the group report
Labelled the Sodium citrate and prepared the group report
for the identification tests.

Excellent(25pts) Good(20pts) Satisfactory(15pts) Needs Improvement

(10pts)
Analytical Results □ □ □ □
Questions for □ □ □ □
Research

Comments, Suggestions, Deductions:

Total Deductions:

Total Score:
Identification Test for Sodium Citrate (photo documentation)

1. Perform Belstein’s Test.

Result: Negative result for Belstein’s test.

Prepared Sodium Citrate by the group Commercial Sodium Citrate

2. Test for citrate ion

2a. Prepare 1:10 solution of the compound; add excess calcium chloride T.S. and heat.
Result: white granular precipitate of calcium citrate settles out
Chemical Reaction: Na3C6H5O7 + CaCl2 —> Ca(CH3COO)3 + NaCl

Prepared Sodium Citrate by the group Commercial Sodium Citrate

2b. Prepare 5 ml of sodium citrate solution and add 0.5 ml mercuric sulfate T.S. Heat the solution and add
dropwise Potassium permanganate T.S.
Result: formation of white precipitate

Prepared Sodium Citrate by the group Commercial Sodium Citrate