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Composite Structures 83 (2008) 413–428


www.elsevier.com/locate/compstruct

Failure analysis of low velocity impact on thin composite


laminates: Experimental and numerical approaches
a,*
Volnei Tita , Jonas de Carvalho b, Dirk Vandepitte c

a
Department of Materials, Aeronautical and Automobilist Engineering, Engineering School of São Carlos, University of São Paulo, Av.
Trabalhador São-Carlense 400, 13566-590 São Carlos, SP, Brazil
b
Department of Mechanical Engineering, Engineering School of São Carlos, University of São Paulo,
Av. Trabalhador São-Carlense 400, São Carlos 13566-590, SP, Brazil
c
Department of Mechanical Engineering, PMA Division, Katholieke Universiteit Leuven, Belgium

Available online 26 June 2007

Abstract

The dynamic behavior of composite laminates is very complex because there are many concurrent phenomena during composite lam-
inate failure under impact load. Fiber breakage, delaminations, matrix cracking, plastic deformations due to contact and large displace-
ments are some effects which should be considered when a structure made from composite material is impacted by a foreign object. Thus,
an investigation of the low velocity impact on laminated composite thin disks of epoxy resin reinforced by carbon fiber is presented. The
influence of stacking sequence and energy impact was investigated using load–time histories, displacement–time histories and energy–
time histories as well as images from NDE. Indentation tests results were compared to dynamic results, verifying the inertia effects when
thin composite laminate was impacted by foreign object with low velocity. Finite element analysis (FEA) was developed, using Hill’s
model and material models implemented by UMAT (User Material Subroutine) into software ABAQUSTM, in order to simulate the fail-
ure mechanisms under indentation tests.
 2007 Elsevier Ltd. All rights reserved.

Keywords: Composite laminates; Low velocity impact; NDE; Indentation tests; Finite element analysis

1. Introduction should change the material and/or architecture of the com-


ponent. However, changes in the architecture can cause
During the last years, criteria of automobile and aircraft increase of costs and/or of weights, reducing the perfor-
projects have been more and more rigorous for component mance of the structure. The weight increase is not attractive
developed in order to absorb impact energy. Research on for the aircraft development, because it reduces the aircraft
the development of structural components with high crash- performance. Nowadays, many kinds of components have
worthiness has been carried out not only by the automobile been made using composite materials, because these mate-
and aeronautics industries, but also by naval, trains and rials can absorb a high amount of impact energy and can
elevators industries. The project concept for structural guarantee the survival of the passengers.
components with high crashworthiness depends on the However, the dynamic behavior of composite laminates
crash resistance concept described by Kindervater and is very complex, because there are many concurrent phe-
Georgi [1]. The crash resistance concept is based on the nomena during composite laminate failure under impact
energy absorption capacity and structural integrity. For load. Fiber breakage, delaminations, matrix cracking, plas-
developing a project that reaches these requirements, it tic deformations due to the contact and large displacements
are some effects which should be considered when a struc-
*
Corresponding author. Tel.: +55 16 3373 8612; fax: +55 16 3373 9590. ture made from composite material is impacted by a for-
E-mail address: voltita@sc.usp.br (V. Tita). eign object. Therefore, it is very common to find research

0263-8223/$ - see front matter  2007 Elsevier Ltd. All rights reserved.
doi:10.1016/j.compstruct.2007.06.003
414 V. Tita et al. / Composite Structures 83 (2008) 413–428

works about this issue at the literature, for example: Oñate


et al. [2]; Cairns and Lagace [3]; Farley and Jones [4]; Haug
and De Rouvray [5]; Belingardi et al. [6]; Collombet et al.
[7]; Gottesman and Girshovich [8]; Vicente et al. [9]; Kin-
dervater et al. [10]; Kostopoulos et al. [11]; Lopresto and
Caprino [12]; Naik and Shrirao [13]; De Morais et al.
[14]; Mitrevski et al. [15]; Mikkor et al. [16]; Mamalis
et al. [17]; Kim and Chung [18]; Zhao and Cho [19].
This work shows an experimental investigation and
numerical results of the low velocity impact on thin com-
posite laminates plates of epoxy resin reinforced (matrix)
by carbon fiber (reinforcement). This study describes the
technology to manufacture the specimens and the set-ups
of equipments to make dynamic experimental tests (using
a drop-tower instrumented) and to realize non-destructive
evaluation (NDE) (using ultrasonic C-scan), as well as
the finite element model and UMAT subroutine imple-
mented into software ABAQUSTM to simulate the failure
mechanisms of the composite laminate. Afterwards, several
issues are discussed:

• Experimental results as load–time, displacement–time Fig. 1. (a) Composite failure mechanisms: intra-ply and inter-ply failures
and energy–time histories of the laminate plate impacted and (b) Intra-ply damages (by Anderson [20]).
under low velocity, considering different stacking
sequence and different impact energies;
• Experimental results as images from non-destructive on the in-service temperature. Thus, the polymeric matrix
evaluation (NDE) of laminate damaged after impact can present a fragile or a plastic behavior (mechanism 5).
test, using NDE by ultrasonic C-scan technique; Other intra-ply failure mechanisms are shown in Fig. 1.
• Experimental results as load–displacement of the lami- Mechanism 1 is called ‘‘Pull-Out’’ and occurs when the
nate under indentation test (quasi-static loading), con- interface between fiber and matrix is weak. So, the fiber
sidering the same stacking sequence used during is pulled out of the matrix after the debonding mechanism
impact test and the same maximum force level reached (mechanism 3) occurs. If the interface between fiber and
at impact tests; matrix is strong, the fiber is not pulled out of the matrix
• Comparison between experimental results from impact and mechanism 2 called ‘‘Fiber Bridging’’ occurs.
and indentation tests; The inter-ply failure called delamination occurs, in
• Comparison between indentation tests results and finite many cases, after intra-ply damages, i.e., the evolution of
element model results, using Hill’s model and two mate- intra-ply damages propagates the delaminations, because
rial models implemented by UMAT. the regions damaged at the ply propagates when the load
increases and the cracks at two adjacent plies (with differ-
ent orientation angle) join for creating a discrete failure
2. Composite failure mechanisms between them. At that moment, the interlaminar shear
increases strongly and the delamination process initiates.
Composite laminate structures were made from the This failure mechanism is very common to occur during
stacking of plies, which contains a polymeric matrix rein- impact events. According to Abrate [21], there is a charac-
forced by fibers. Therefore, composite laminate shows teristic shape for the plate thickness when the laminate suf-
two failure modes: fers impact loading. For thick laminates, the damage
occurs at the outer plies, which contact to the impacter,
1. Intra-ply failure mode: damages at fibers, polymeric because the structure is less flexible. The damages at those
matrix and/or interface between fibers and matrix. plies occur due to the high contact stress values and prop-
2. Inter-ply failure mode: delaminations between plies. agate to the inner plies, promoting delaminations. The del-
aminations increase the flexibility of the structure and new
The intra-ply damage at fibers is shown by mechanism 4 intra-ply damages occur close to the delaminations. The
(Fig. 1) that is the fiber rupture. However, the fiber failure intra-ply damage evolution increases the interlaminar shear
mode depends on the type of loading, because compression that promotes new discrete damage between adjacent plies,
loads can induce micro-buckling, but tensile loads can forming a ‘‘pine tree’’ shape at the plate thickness. This
induce rupture of fibers. The intra-ply damage at the progressive failure process stops when the impact energy
matrix depends on the ductility of the polymer, as well as is insufficient to activate any failure mechanism. For thin
V. Tita et al. / Composite Structures 83 (2008) 413–428 415

laminates, the damages occur at the opposite plies that con- Temperature Pressure Vacuum
tact to the impacter, because the structure is more flexible. 4 0.0
The damage at those plies occurs due to the high flexural 120

stress values and propagate to the inner plies, promoting


delaminations. The delaminations increase the flexibility 100 3 -0.2

Pressure [bar]
of the structure and new intra-ply damage occurs close to

Vaccum [bar]
Temperature [°C]
the delaminations. The intra-ply damages evolution 80
-0.4
increases the interlaminar shears that promotes new dis- 2
crete damage between adjacent plies, forming a ‘‘reverse 60
pine tree’’ shape at the plate thickness. This progressive -0.6
failure process stops when the impact energy is insufficient 40 1
to activate any failure mechanism. Besides, according to
Abrate [21], the delaminated plies show the damage shape 20
-0.8

like a ‘‘peanut shape’’ oriented in the same direction of the 0


fibers in each ply. 0 30 60 90 120 150
time [minutes]

3. Failure analysis approaches Fig. 2. Cure cycle.

3.1. Experimental analysis


tower. Table 1 shows the values for dimensions of square
American Society for Testing and Materials (ASTM) specimen, as well as, impact mass (m), height of falling
standards were followed to manufacture the specimens impact mass (h), impact velocity (mo) and impact energy
and to realize the experimental tests. It is important to note (Ei). The specimens were fixed by two circular steel disks
that the fabrication of the specimens and the experimental that had a hole with a diameter of 80 mm. Thus, in fact, cir-
tests was executed at Leuven Composites Processing Cen- cular composite plates with boundary clamped by two cir-
tre (LCPC) of Katholieke Universiteit Leuven (Belgium). cular steel disks attached (using four bolts under torque
The prepreg M10 (epoxy resin reinforced by carbon fiber equaling 27 Nm) were evaluated under impact conditions
unidirectional) from Hexcel was used for manufacturing specified in Table 1. The geometry of the aluminium dart
of the composite plates. (hemisphere; radius equal to 8 mm) with a mass of
After the hand-lay-up process used to stack the plies, the 0.0513 kg is according to ASTM D5628-96 [22] (FD
composite plate was put in the auto-clave with vacuum sys- Method) summarised in Table 1. The support of mass
tem set to 0.8 Bar (0.08 MPa). According to Hexcel, and the load cell of the drop-tower with the aluminium dart
the complete cure cycle for M10 occurs when this material have a total mass of 1.205 kg shown in Table 1. The instru-
is processed at 120 C, under a pressure with range from mented drop-tower has an optic sensor fixed at the base
0.3 to 5.0 Bar for 60 min (Fig. 2). After the curing process, and a LED (‘‘light emitting diode’’) attached to the support
the composite plates were cut on square shapes (length and of the mass, which permits to measure the displacement of
width of 120 mm and thickness of 1.8 mm), using diamond the impactor support in function of the time (si(t)) shown in
saw in order to guarantee the tolerances specified by Fig. 3. Thus, numerical methods to derive the displacement
standards. measured were applied in order to obtain the velocity (mi(t))
For the impact tests under low velocity, drop-tests were and acceleration of the support during the impact event.
realized following the specifications by FD Method On the other hand, the load cell measures the force during
described on the ASTM D5628-96 [22] and using a drop- the impact event (Fexp(t)) shown in Fig. 3. The load cell was

Table 1
Specifications for drop-tests
Stacking sequence Length (mm) Thickness (mm) m (kg) h (m) mo (m/s) Ei (J)
[0]10 120 1.8 1.205 0.5 3.13 5.91
120 1.8 1.205 0.2 1.98 2.36
[0/90/0/90/0]s 120 1.8 1.205 0.5 3.13 5.91
120 1.8 1.205 0.2 1.98 2.36
[+45/45/+45/0/90]s 120 1.8 1.205 0.5 3.13 5.91
120 1.8 1.205 0.2 1.98 2.36
120 1.8 2.205 0.5 3.13 10.82
120 1.8 2.205 0.2 1.98 4.33
Impactor material Mass (kg) Nose shape Radius of impactor (mm)
Aluminium 0.0513 Hemispherical 8.0
416 V. Tita et al. / Composite Structures 83 (2008) 413–428

Fig. 3. Drop-tower at LCPC of Katholieke Universiteit Leuven: kinematic energy (impact energy level), absorbed energy and elastic energy.

plugged on a KistlerTM amplifier (model 5007) that sends The experimental impact force Fexp is measured during
signal to the computer. In the computer, there is a system the impact event. Thus, it is possible to evaluate the impact
for data acquisition with 11 bits, three channels for input energy, which reaches the composite plate, as well as the
data and sampling frequency set to 19 kHz. Thus, the absorbed energy and the elastic energy (Fig. 3).
acceleration of the load cell was obtained dividing the force The absorbed energy could be understood as ‘‘released
measured by the impact mass. Numerical methods to inte- energy’’, because the failure mechanisms activated during
grate the acceleration measured were applied in order to the impact event release energy. However, the literature
obtain the velocity and displacement of the load cell during considers these release energies as a fraction of impact
the impact event. In fact, not only the dimensions of the energy, which is absorbed by the structure and is not trans-
support and numerical methods to derive, but also the formed on elastic vibrations (elastic energy).
measurements of the load cell and numerical methods to Fig. 3 shows that the absorbed energy from measure-
integrate produce errors on the calculated displacement, ments can be calculated using
velocity and acceleration of the dart. Therefore, in order KEðtÞ ¼ Ee þ Ea ; ð4Þ
to minimize the errors, both measures (from load cell and
from support) were used to determine the displacement, where KEi is the kinematic energy; Ee is the elastic energy
velocity and acceleration of the dart. and Ea is the absorbed energy.
If an object with mass m impacts a composite plate with In other words, the impact energy E(t) transferred from
a velocity mo, the impact energy of the impacter Ei can be the object to the target (composite laminate plate) is
expressed by absorbed by the failure mechanisms activated. Thus, each
failure mechanism, i.e., intra-ply failures and/or delamina-
mv2o tions absorb a fraction of impact energy. Therefore, the
Ei ¼ : ð1Þ
2 amount and the type of failure mechanisms activated will
Besides, the kinematic energy KE(t) transferred from affect the absorbed energy values. However, the amount
object to the target (composite laminate plate) can be and the type of failure mechanisms activated depend on
expressed by some factors:
2
mv2o mðvi ðtÞÞ • Mass and velocity of the impacter (impact energy level);
KEðtÞ ¼  ; ð2Þ
2 2 • Geometry of the impacter;
where the velocity of the impacter mi(t) can be obtained by • Geometry of the structure;
Z • Type of fiber and/or matrix used for manufacturing of
1 t the composite structure;
vi ðtÞ ¼ vo  F exp dt: ð3Þ
m 0 • Stacking sequence of the plies.
V. Tita et al. / Composite Structures 83 (2008) 413–428 417

For this work, the influence of the impact energy level captured is a superposition of the damaged regions on
and the stacking sequence was verified. each layer, i.e., all failure mechanisms are projected in
The indentation tests were realized using a universal the same plane. Despite this limitation, it was possible
machine equipment in order to produce a quasi-static load- to identify the principal failure mechanisms at composite
ing under a velocity of 10 mm/min on the specimens with plates impacted.
the same geometry and the same boundary conditions used
for drop-tests. Thus, each circular composite plate was 3.2. Description of material models
loaded from zero to the maximum force value reached at
respective drop-test. After that, the load was removed till First, a material model, defined as Material Model I,
zero under a velocity of 10 mm/min. was developed in order to simulate only the intra-ply dam-
According to Abrate [21], non-destructive evaluation age mechanisms, using laminated shell elements and plane
techniques can be used to determine the principal failure stress state. After that, a more complex material model,
mechanisms that occur when a composite structure is defined as Material Model II, was developed in order to
impacted. However, the destructive evaluation techniques simulate the intra-ply and inter-ply damage mechanisms,
are used in order to verify more details about failure using laminated solid elements and 3D stress state. Both
mechanisms. In fact, non-destructive and destructive tech- material models were implemented as a UMAT subroutine
niques are used in conjunction to improve the information into software ABAQUSTM [23].
quality, increasing the accuracy of inspection results, but Table 2 shows the Material Model I used finite element
this approach also increases the costs. In this work, only analysis with shell elements. It is important to note that a
the NDE by ultrasonic C-scan technique was used, failure criteria associated to a type of failure constitutes
because this technique is applied on large scale by aero- the Material Model. Table 3 shows an explicit definition
nautic industries. The C-scan equipment was set with for all symbols.
the frequency of 5 MHz and set to cover a square area The failure criteria for the Material Model I is based on
(length is equal to 30 mm) of the composite plate works published by: Yamada and Sun [24]; Hashin [25,26];
impacted by the dart, using the increment for scanning Chang and Chang [27,28].
of 298.4 lm. According to the failure (fiber or matrix failure), there
Some C-scan equipment can be used to inspect the is a degradation law in order to reduce the material prop-
extension of damage at a specific layer. Thus, it is possible erties of the failure ply based on the works published by:
to determine with accuracy the location and the extent of Chang and Chang [27,28]; Chang et al. [29]; Chang and
the delaminations. However, the ultrasonic C-scan equip- Lessard [30]. For the matrix and fiber failure, E22 and
ment at LCPC of Katholieke Universiteit Leuven (Bel- m12 are reduced to zero. However, E11 is not reduced,
gium) did not offer that tool. Therefore, the image considering the matrix failure, but this property and

Table 2
Material Model I for shell element
Material Model I
Failure Criteria Type of failure Degradation law
 2     
r1 eF > 1 ! damage Fiber compression A
¼ e2F Edf
11 ! E11 exp  H
Xc eF 6 1 ! no damage Ao
   
A
Gdf
12 ! G12 exp  H
 2 Ao
r1 ð2r212 =G12 Þ þ ð3ar412 Þ Fiber tension
þ ¼ e2F ; i:e:; Edf
22 ! 0
XT ð2S 212 =G12 Þ þ ð3aS 412 Þ
 2  mdf
12 ! 0
r1 F1 eF > 1 ! damage
þ ¼ e2F
XT F2 eF 6 1 ! no damage

 2 " 2 # 
r2 YC r2 F 1 eM > 1 ! damage Matrix compression Edm
11 ! E11
þ 1 þ ¼ e2M
2S 23 2S 23 YC F2 eM 6 1 ! no damage Edm
22 ! 0

mdm
12 ! 0
 2 
r2 F1 eM > 1 ! damage Matrix tension
þ ¼ e2M
YT F2 eM 6 1 ! no damage
418 V. Tita et al. / Composite Structures 83 (2008) 413–428

Table 3 more for Eq. (5). Thus, it is not verified that the Young
Definition for the symbols of Material Models I and II modulus reduces suddenly, which is very reasonable for
Symbol Definition indentation tests.
r1 Component stress acting at fiber direction However, G12 degradation law is also updated according
r2 Component stress acting at normal to the fiber to the non-linear behavior of the shear stress at planes 1–2.
r3 Component stress acting at normal to the ply plane Thus, G12 is the updated shear modulus, which is calculated
r12 Shear stress acting at the ply plane
r13 Shear stress acting transverse to the ply plane
using the tangent of the curve shear stress–shear strain:
r23 Shear stress acting transverse to the ply plane 1
XT Strength value parallel to the fiber under tension G12 ¼ 1
; ð6Þ
XC Strength value parallel to the fiber under compression G12
þ 3ar212
YT Strength value normal to the fiber under tension
YC Strength value normal to the fiber under compression where a represents the value provided by the stress tensor
ZT Strength value normal to the ply plane under tension component of the fourth order shown by Hahn and Tsai
S12 Strength value for shear at the ply plane [32].
S13 Strength value for shear transverse to the ply plane
S23 Strength value for shear transverse to the ply plane
Table 4 shows the Material Model II used for simulation
eF Failure index for the fiber finite element analysis with solid elements. It is important
eM Failure index for the matrix to note that a failure criteria associated to a type of failure
edela Failure index for delamination constitutes the Material Model. The Failure Criteria
E11 Young modulus at fiber direction applied is based on works published by: Hashin [25,26];
E22 Young modulus at normal to the fiber
m12 Poisson’s ratio
Liu et al. [33]; Kermanidis et al. [34]; Dávila and Camanho
df Modulus degradeted after fiber damage [35]; Dávila et al. [36]; Kostopoulos et al. [11]. Table 3
dm Modulus degradeted after matrix damage shows an explicit definition for all symbols.
dela Modulus degradeted after delamination According to the failure (delamination, fiber or matrix
failure), there is a degradation law in order to reduce the
material properties of the failure ply based on the works
G12 are reduced for fiber failure, based on an exponential published by: Chang and Chang [27,28] and Kermanidis
decaying et al. [34]. For the matrix and fiber failure, intra-ply failure,
   
df A the degradation law is the same applied for the Material
P ¼ P exp  H ; ð5Þ Model I. For delamination, inter-ply failure, the degrada-
Ao
tion factors are the following:
where P is the property to be reduced, A is the area of the
damage zone; Ao is the area of the interaction zone of the d dela
1 ¼ d dela
2 ¼ d dela
3 ¼ d dela
4 ¼ d dela
5 ¼ 0:01: ð7Þ
fiber failure that was obtained from Chang and Chang
[27,28] and from Shahid and Chang [31]. Finally, H is a Finally, Table 5 shows the material data used during the
parameter, which controls the level of the property degra- finite element analysis.
dation and it is obtained using reverse analysis.
Fig. 4 shows the E11 degradation law for Chang and 3.3. Finite element analysis
Chang [27,28] and for the present work, where b is the Wei-
bull distribution parameter. The parameter H is similar to The finite element analysis, using UMAT subroutines,
parameter b, but the degradation phenomenon is slightly was realized to evaluate the performance of Material
Model I and II to predict the composite structure behavior.
Numerical results as force–displacement graphs were com-
pared to experimental results from indentation tests.
E11 Chang-Chang
β =2.0 Material Model I (Table 2) and II (Table 4) were imple-
1.00E+011
β =3.5 mented by UMAT subroutine into software ABAQUSTM
β =5.0 [23], because some failure criteria adopted for these material
8.00E+010 β =8.0
Present work models were used by other researchers, but the combination
6.00E+010 H=0.5 of the failure criteria is a new investigation and the degrada-
H=1.0 tion law proposed in Eq. (5) is a new investigation, too.
E11 [Pa]

H=1.5
The stacking sequences investigated are shown in Table
df

4.00E+010
1, in order to evaluate the influence of the fiber orientation
2.00E+010 on the composite structure behavior, and, to evaluate the
material models performance for predicting the composite
0.00E+000 structure behavior.
First of all, a synthesis of the contact problem will be
0.0 0.5 1.0 1.5 2.0 2.5 3.0 3.5 4.0
shown. After that, details of the finite element models will
A/A o
be shown, like the geometry, the mesh, and boundary con-
Fig. 4. E11 degradation laws. ditions and mainly the material model.
V. Tita et al. / Composite Structures 83 (2008) 413–428 419

Table 4
Material Model II for solid element
Material Model II
Failure Criteria Type of failure Degradation law

      
r1 eF > 1 ! damage Fiber compression A
¼ e2F Edf
11 ! E 11 exp  H
XC eF 6 1 ! no damage Ao
   
A
Gdf
12 ! G12 exp  H
 2  2  Fiber tension Ao
r1 r13 F1 eF > 1 ! damage
þ þ ¼ e2F Edf
22 ! 0
XT S 12 F2 eF 6 1 ! no damage
V df
12 ! 0

" 2 #
1 2 YC ðr2 þ r3 Þ 1 Matrix compression Edm
11 ! E11
ðr2 þ r3 Þ þ 1 þ 2 ðr223  r2 r3 Þ
4S 223 2S 23 YC S 23 Edm
22 ! 0
 2 
r13 F1 eM > 1 ! damage V dm
12 ! 0
þ þ ¼ e2M
S 12 F2 eM 6 1 ! no damage

 2 Matrix tension
1 2 1 2 r13
ðr2 þ r3 Þ þ 2 ðr23  r2 r3 Þ þ
Y 2T S 23 S 12

F1 eM > 1 ! damage
þ ¼ e2M
F2 eM 6 1 ! no damage

 2  2  2  Delamination dela
r3 r13 r23 2
edela > 1 ! failure Edela
33 ! d 1 E 33
þ þ ¼ edela
ZT S 13 Z 23 edela 6 1 ! no damage Gdela dela
23 ! d 2 G23
dela
Gdela
13 ! d 3 G13
dela
V dela
23 ! d 4 V 23
dela
V dela
13 ! d 5 V 13

Table 5 ABAQUSTM provides a type of contact model called ‘‘expo-


Material data used for simulations
nential contact’’, where the contact forces are activated
Elastic properties Strength values when the hemisphere penetrates the disk for a distance of
E11 127 GPa XT 1400 MPa Co, providing a pressure Po. For this work, Co was taken
E22 = E33 10 GPa XC 930 MPa to be 104 mm and Po was 102 N/m2.
G12 = G13 5.4 GPa YT 47 MPa
G23 3.05 GPa YC 130 MPa
For the finite element analysis, two types of finite ele-
m12 = m13 0.34 ZT 62.3 MPa ment models were developed. The first model was created
m23 0.306 S12 = S13 53 MPa using shell elements (S4) with four nodes and four integra-
S23 89 MPa tion points [23] in order to simulate the plane stress at the
laminate. The nodes at the edge of the model were fixed in
order to simulate the circular disk clamped (Fig. 5a). The
For the contact problem, it is very important to evaluate second model was created, using solid elements (C3D8)
the work produced by contact forces Fc on the contact sur- with eight nodes and four integration points in order to
face Sc in the equilibrium equations. Thus, during each simulate the 3D state of stress at laminate. The solid had
iteration i, the contact algorithm of software ABAQUSTM three elements per thickness and the nodes at the edge of
verifies the contact occurrence in order to evaluate the con- the model were fixed (Fig. 5b). It is important to note that
tact forces Fc. In this work, a circular disk was used in a for the shell model, as well as for the solid model, the exter-
clamped set-up under a load applied at the centre, using nal surface of the indention hemisphere was simulated as a
a hemisphere, which contacts the composite disk. Software rigid surface, which contacted the central region of the
420 V. Tita et al. / Composite Structures 83 (2008) 413–428

two steps (normal to the disk). For the first step, the load-
ing phase was simulated, i.e., the hemisphere was displaced
from the initial position (very close to the disk) to the final
position (maximum displacement verified at the experimen-
tal test). For the second step, the unloading phase was sim-
ulated, i.e., the hemisphere was displaced from the initial
position, which was equal to the final position of the first
step, to the final position, which was equal to the initial
position of the first step.
Two material models were implemented as UMAT sub-
routine into software ABAQUSTM. Model I was used for
the shell element model (Table 2) and Model II was used
for the solid element model (Table 3). Fig. 6 shows that
the software ABAQUSTM manages all calculation proce-
dures, and the user can recover components of the stress
tensor for each iteration i. After that, the stress tensor for
each integration point is read by the UMAT subroutine
in order to be used in a failure criteria. If failure does not
occur then the updated stress tensor is equal to the original
stress tensor. Thus, this tensor comes back to the principal
calculus procedure in order to form the internal forces vec-
tor, which will be compared to the external forces vector.
The result of this comparison will produce residues (R) that
will be compared to a specified tolerance. If R is higher
than the tolerance, a new iteration will be necessary.
However, if failure occurs then a degradation law is
applied on the elastic properties of the ply, according to
the type of failure (Tables 2 and 3). Therefore, the consti-
tutive tensor must be corrected and the stress tensor will
Fig. 5. Finite element models: (a) Shell element S4 and (b) Solid element
be updated before to return to software ABAQUSTM. Then,
C3D8.
R is calculated with the internal and external forces vector
disk. There was a node associated to the rigid surface where in order to be compared to the threshold that is set to indi-
the boundary conditions were imposed in order to simulate cate convergence. If there is convergence, then a new incre-
the displacement at the z-direction of the hemisphere in ment of load occurs, otherwise, the software ABAQUSTM

New Increment

BEGIN

Calculus of Stress Tensor


Equilibrium at iteration i
for the integration point

Aplication of Calculusof Residual (R)


Damage Criteria

Yes
R < Tolerance?
No
Failure? Original Stress Tensor
No
Yes
Yes
Aplication of the Convergence?
Updated Stress Tensor
Degradation Law
No

Corrected END
Constitutive Tensor
Subroutine UMAT ABAQUS ®

Fig. 6. UMAT subroutine and software ABAQUSTM.


V. Tita et al. / Composite Structures 83 (2008) 413–428 421

checks the convergence. During the iterations for only one a 2500
load step, it is expected that R decreases. If R increases, Stacking Sequence: [0]10
then the solution produces divergence, and the procedure
Ei =5.91J
stops. Frequently, the divergence occurs, because the mate- 2000
rial properties have high degradation, and the structure
does not have enough stiffness to support the loads
1500
imposed. Other critical parameter, which can cause diver-

Force [N]
gence in non-linear finite element analysis, is the time step
applied on the simulations. For the initial time increment, a
1000
value of 0.05 was used, which would be modified as
required, because the automatic time stepping scheme Ei =2.36J
was set on. For the time period of the step, 7 was used. 500
For the minimum and maximum time increment allowed,
0.0001 and 0.5, respectively were chosen. Finally, for the
maximum number of increments in a step, 100 was chosen. 0
0 1 2 3 4 5 6 7
time [ms]
4. Results and discussion
b
First, the impact test results are shown (force–time, dis- 6
placement–time and energy–time graphics) and images
from ultrasonic C-scan technique. Second, the indentation 5
test results are shown, comparing the force–displacement
graphs between quasi-static and impact loading. Finally, 4
the finite element results are shown, comparing the force–
E(t) [J]

Impact Level = 5.91J


displacement graphs between numerical and experimental 3 Impact Level = 2.36J
results.
The stacking sequences investigated are shown in Table 2
1, in order to evaluate the influence of the fiber orientation
on the composite structure behavior, and, to evaluate the
1
material models performance for predicting the composite
structure behavior.
0
0 1 2 3 4 5 6 7 8
4.1. Impact test results and NDE images time [ms]

Fig. 7. Experimental impact results for laminate [0]10.


4.1.1. Experimental impact results for laminate [0]10
Fig. 7a shows force–time graphics for composite plates
with stacking sequence [0]10, considering two impact energy energy of 5.91 J. Based on Fig. 3 and Eq. (4), it is verified
levels (5.91 J and 2.36 J). There is a region with oscillations that specimens have absorbed energy equal to 4.42 J, so
of high frequency (in the initial phase of contact from 0 to only 25% of the impact energy is converted to elastic
1 ms) due to initial contact between specimen and dart at vibrations.
force–time graph (Fig. 7a). From 2 ms, there are some However, the specimens impacted by 2.36 J have just
oscillations with more intensity that show damage 1.2 J for absorbed energy (Fig. 7b), converting 50% of
occurred, not only for specimens under Ei of 5.91 J, where the impact energy to elastic vibrations. Thus, the specimens
maximum impact force is 2250 N, but also for specimens impacted by 2.36 J show less failure mechanisms. This
under Ei of 2.36 J, where maximum impact force is observation can be confirmed, using the images from ultra-
1300 N. Due to the stacking sequence [0]10, the principal sonic C-scan technique.
failure mechanism is matrix rupture, slightly reducing the Fig. 8 shows the ultrasonic C-scan images for composite
global stiffness of the structure. Therefore, there is no plates with stacking sequence [0]10, considering the impact
abrupt drop of the impact force value after the progressive energies of 5.91 J and 2.36 J. Specimens impacted by 5.91 J
damage process initiation (Fig. 7a). The contact time show damage more concentrated close to the impact region
depends on the impact energy level; so, the contact time (Fig. 8a). However, specimens impacted by 2.36 J show
is longer (6 ms) for specimens impacted by impact energy damage more distributed at the matrix represented by
of 2.36 J than by impact energy of 5.91 J. Thus, for high cracks oriented to the fibers (Fig. 8b). Besides, it was
contact time, the mechanical behavior of the specimen observed that some fibers fail at the opposite side of the
tends to quasi-static response. impact for the specimens impacted at 5.91 J. This observa-
Fig. 7b shows the energy–time graph for composite tion can explain why these specimens absorbed 75% of the
plates with stacking sequence [0]10, considering the impact impact energy, where the failure mechanisms of fibers
422 V. Tita et al. / Composite Structures 83 (2008) 413–428

a 3500 Stacking Sequence: [0/90/0/90/0]s

3000 Ei =5.91J

2500

2000

Force [N]
1500

Ei =2.36J
1000

500

0
0 1 2 3 4 5
time [ms]

b
6

Fig. 8. Experimental impact results for laminate [0]10: (a) energy–time for 4
5.91 J and 2.36 J and (b) C-scan images.
E(t) [J]

3
Impact Level = 5.91J
release more energy than failure mechanisms of the matrix. Impact Level = 2.36J
Because the energy to rupture the fibers is higher than the 2
energy to crack the polymer matrix.
1
4.1.2. Experimental impact results for laminate [0/90/0/90/
0]s 0
0 1 2 3 4 5 6
Fig. 9a shows force–time graphics for composite plates
time [ms]
with stacking sequence [0/90/0/90/0]s, considering two
impact energy levels (5.91 J and 2.36 J). Fig. 9. Experimental impact results for laminate [0/90/0/90/0]s.
There is a region with oscillations of high frequency
(from 0 to 1.2 ms) due to initial contact between specimen
and dart in the force–time graph (Fig. 9a). From 1.8 ms,
there are some small oscillations that show damage, not
only for specimens under Ei of 5.91 J (where maximum
impact force is 3000 N), but also for specimens under Ei
of 2.36 J (where maximum impact force is 1750 N). Due
to the stacking sequence [0/90/0/90/0]s, the main failure
mechanisms are the matrix rupture and delaminations,
reducing the global stiffness of the structure. Therefore,
there is no abrupt drop of the impact force value after
the progressive damage process initiation (Fig. 9a). The
contact time depends on the impact energy level; so, the
contact time is higher (4.5 ms) for specimens impacted by
impact energy of 2.36 J than by impact energy of 5.91 J.
Thus, for high contact time, the mechanical behavior of
the specimen tends to quasi-static response. Fig. 10. Experimental impact results for laminate [0/90/0/90/0]s: (a)
Fig. 9b shows the energy–time graph for composite energy–time for 5.91 J and 2.36 J and (b) C-scan images.
plates with stacking sequence [0/90/0/90/0]s, considering
the impact energy of 5.91 J. It is verified that specimens energy (Fig. 9b), converting 75% of the impact energy to
have absorbed energy of 3.96 J, so only 33% of the impact elastic vibrations. Thus, the specimens impacted by 2.36 J
energy is converted to elastic vibrations. However, the show less failure mechanisms. This observation can be con-
specimens impacted by 2.36 J have just 0.58 J for absorbed firmed, using the images from ultrasonic C-scan technique.
V. Tita et al. / Composite Structures 83 (2008) 413–428 423

Fig. 10 shows the ultrasonic C-scan images for compos- by a mass of 2.205 kg with an impact energy of 4.33 J
ite plates with stacking sequence [0/90/0/90/0]s, considering and 10.82 J show that the contact time is higher than the
the impact energy of 5.91 J (Fig. 10a) and 2.36 J (Fig. 10b). specimens impacted by a mass of 1.205 kg (Fig. 11).
Due to the stacking sequence [0/90/0/90/0]s, there are more Fig. 12 shows the energy–time graph for composite
layers oriented at 0 than at 90, so, there are more cracks plates with stacking sequence [+45/45/+45/0/90]s, con-
aligned to 0. Besides, there are ‘‘peanut shapes’’, which sidering the impact energy equal to 5.91 J. Specimens have
represent delaminations, at both directions (0 and 90). absorbed 4.0 J of energy, so only 32% of the impact energy
The area damaged for the specimens impacted by 5.91 J is converted to elastic vibrations. The specimens impacted
(340 mm2) is larger than the specimens impacted by by 10.82 J have the highest absorbed energy, because
2.36 J (150 mm2). This calculus can explain why the speci- 8.8 J was absorbed by many failure mechanisms. On the
mens impacted by 2.36 J absorbed just 25% of the impact other hand, the specimens impacted by 2.36 J have a very
energy. Many failure mechanisms cannot be activated for low absorbed energy level (0.8 J), converting 66% of the
the stacking sequence equal [0/90/0/90/0]s by this impact impact energy to elastic vibrations. Finally, the specimens
energy level, and the mechanical behavior of the specimen impacted by 4.33 J show that the absorbed energy is
tends to elastic response. 2.6 J, converting only 40% of the impact energy to elastic
vibrations. Thus, the specimens impacted by 2.36 J show
4.1.3. Experimental impact results for laminate [+45/45/ less failure mechanisms. This observation can be con-
+45/0/90]s firmed, using the images from ultrasonic C-scan.
Fig. 11 shows force–time graphs for composite plates Fig. 13 shows the ultrasonic C-scan images for compos-
with stacking sequence [+45/45/+45/0/90]s, considering ite plates with stacking sequence [+45/45/+45/0/90]s,
four impact energy levels (2.36 J, 4.33 J, 5.91 J and 10.82 J). considering the impact energy levels of 5.91 J (Fig. 13a),
The dynamic responses for the specimens impacted by 2.36 J (Fig. 13b), 10.82 J (Fig. 13c) and 4.33 J (Fig. 13d).
5.91 J and by 10.82 J are very similar. They reach a maxi- Due to the stacking sequence [+45/45/+45/0/90]s,
mum impact force of 3300 N and 4500 N, respectively. there are more layers oriented at +45 than at other direc-
However, dynamic responses are very different for the spec- tion, so there are more cracks aligned to +45. Besides,
imens impacted by 2.36 J and by 4.33 J, which reaches a there are ‘‘peanut shapes’’, which represent delaminations
maximum impact force of 1900 N at 2.36 J and 2500 N at at four directions (0, +45, 45 and 90). The areas dam-
4.33 J (Fig. 11). Besides, the specimens impacted by aged for the specimens impacted by 5.91 J (360 mm2) and
5.91 J and by 10.82 J show many oscillations close to the by 10.82 J (450 mm2) are larger than the specimens
maximum impact force that represent many types of failure impacted by 2.36 J (165 mm2) and by 4.33 J (211 mm2).
mechanisms, for example: cracks at the matrix, delamina- This explains why the specimens impacted by 10.82 J
tions between layers oriented at 0/90 and at 45/0, as absorbed 81% of the impact energy, where many failure
well as, some fiber rupture. However, there are just some mechanisms are activated for the stacking sequence [+45/
oscillations close to the maximum impact force for speci- 45/+45/0/90]s by this impact energy level. The mechani-
mens impacted by 2.36 J and by 4.33 J (Fig. 11) that repre- cal behavior of the specimen tends to a completely inelastic
sent a small amount of damage. In fact, the specimens response where the dart is almost retained by the composite
impacted by lower energy have a response that tends to plate.
quasi-static response. However, the specimens impacted
12
5000 Stacking Sequence: [+45/-45/+45/0/90]s 11

4500 Ei =10.82J 10

4000 E i =5.91J 9

8 Impact Level = 5.91J


3500
7 Impact Level = 2.36J
3000
E(t) [J]

6 Impact Level = 10.82J


Force [N]

2500 E i =4.33J
5 Impact Level = 4.33J
2000 4

1500
Ei =2.36J 3

2
1000
1
500
0
0 0 1 2 3 4 5 6 7
0 1 2 3 4 5 6 time [ms]
time [ms]
Fig. 12. Experimental impact results for laminate [+45/45/+45/0/90]s
Fig. 11. Experimental impact results for laminate [+45/45/+45/0/90]s. Energy–time for 5.91 J; 2.36 J; 10.82 J; 4.33 J.
424 V. Tita et al. / Composite Structures 83 (2008) 413–428

indentation curves do not show the oscillations inherent


for the dynamic response obtained from drop-tests. Besides,
when the load reaches the maximum force, which is equal to
the maximum force obtained at drop-test, the indentation
curves do not show oscillations because failure mechanisms
of the composite plate are activated. Thus, for the same
level of load, the indentation curves show lower displace-
ment than impact curves, because, there are more failure
mechanisms activated during the impact event than quasi-
static event. Besides, the failure mechanisms for composite
plate under quasi-static loading concentrate closer to the
region where the dart contacts the specimen. However,
the failure mechanisms shown by plates impacted are more
distributed.
Therefore, the failure mechanisms for a composite plate
under impact loading reduce the global stiffness of the
structure more than the concentrated failure mechanisms.
This observation explains why the slope of indentation
curve is very different of the slope presented by the impact
curve, in the unloading step.

4.2.2. Experimental indentation results for laminate [0/90/0/


90/0]s
Fig. 15 shows the force–displacement graphics for com-
Fig. 13. Experimental impact results for laminate [+45/45/+45/0/90]s: posite plates with stacking sequence [0/90/0/90/0]s. In gen-
C-scan images. eral, in the initial phases of the loading step, the
indentation and the impact curves have about the same
slope that represents non-linear behavior due to the contact
4.2. Indentation test results interaction between the disks and the aluminium dart
(hemisphere). However, the indentation curves do not
4.2.1. Experimental indentation results for laminate [0]10 show the oscillations inherent for the dynamic response
Fig. 14 shows the force–displacement graphs for com- obtained from drop-tests. Besides, when the load reaches
posite plates with stacking sequence [0]10. In general, in the maximum force, which is equal to the maximum force
the initial phases of loading, the indentation and the impact obtained at drop-test, the indentation curves do not show
curves have about the same slope that represents non-linear oscillations due to intra-ply failures and delaminations
behavior due to the contact phenomenon. However, the activated.

Indentation Test (Fmax = 2,250 N)


2500 Indentation Test (Fmax = 3,000 N)
Indentation Test (Fmax = 1,300 N) 3500
Indentation Test (Fmax = 1,750 N)

3000
2000

2500

1500
2000
Force [N]

Force [N]

1000 Impact Test 1500


(Fmax = 2,250 N) Impact Test
1000 (Fmax = 3,000 N)
500
500
Impact Test Impact Test
(Fmax = 1,300 N) (Fmax = 1,750 N)
0 0
0 1 2 3 4 5 6 7 0 1 2 3 4 5
displacement [mm] displacement [mm]

Fig. 14. Experimental indentation results for laminate [0]10 maximum Fig. 15. Experimental indentation results for laminate [0/90/0/90/0]s
force at: 2250 N and 1300 N. maximum force at: 3000 N and 1750 N.
V. Tita et al. / Composite Structures 83 (2008) 413–428 425

Fig. 15 shows for the same level of load that the inden- event (more distributed) and by quasi-static event (more
tation curve has lower displacement than impact curves, concentrated).
because there are more failure mechanisms activated dur-
ing the impact event than during the quasi-static event. 4.3. Finite element results
However, Fig. 15 shows that the slope of indentation curve
is similar to the slope presented by the impact curve not 4.3.1. Numerical results for laminate [0]10
only in the loading step, but also in the unloading step. Fig. 17a shows that the Material Model I can simulate
The specimens impacted by 2.36 J (maximum impact force the indentation test, during the loading phase when param-
equal to 1750 N) just absorbed 25% of the impact energy eter H is 1.2.
and the mechanical behavior of the specimen tends to elas- However, the maximum load simulated is higher than
tic response. Therefore, many failure mechanisms are not the experimental maximum load, and, the initial phase of
activated for the stacking sequence which is equal to [0/ unloading is not simulated very well. Material Model I
90/0/90/0]s by neither impact event nor indentation test. can simulate the final of phase unloading, but the perma-
nent strain is not represented when the polymer matrix
4.2.3. Experimental indentation results for laminate [+45/ exhibits plastic deformation under the rigid hemisphere.
45/+45/0/90]s This phenomenon can be verified in Fig. 17b, that shows
Fig. 16 shows the force–displacement graphs for com- a stress concentration at the centre of the disk, because
posite plates with stacking sequence [+45/45/+45/0/ the contact interaction between the disk and the rigid hemi-
90]s. Fig. 16 shows that the indentation and the impact sphere causes contact press and contact stress.
curves have different slopes. The specimens with stacking In order to simulate the permanent strain, Hill’s Crite-
sequence [+45/45/+45/0/90]s impacted show many types rion, implemented in software ABAQUSTM [23], provides
of failure mechanisms that are distributed at composite good results at the final phase of unloading. However,
plate. the loading phase cannot be represented, because Hill’s
However, the failure mechanisms for a composite plate
under quasi-static loading are concentrated close to the
region where the dart contacts the specimen. These failure
2500
mechanisms reduce the structure global stiffness less than Material Model I (H=1.2)
the distributed failure mechanisms. Hill's Criterion
However, Fig. 16 shows that the slope of the indentation 2000
Indentation Test
curve is similar to the slope of the impact curve not only in
the loading step, but also in the unloading step. The spec- 1500
Force [N]

imens impacted by 2.36 J (maximum impact force equal to


1900 N) converted 66% of the impact energy to elastic 1000
vibrations. Although the slopes of the two curves are sim-
ilar, there is an offset between both curves due to the differ-
500
ence between the failure mechanisms shown by impact

0
Indentation Test (Fmax = 3,300 N) 0 1 2 3 4 5 6
Indentation Test (Fmax = 1,900 N) displacement [mm]
3500

3000

2500
Force [N]

2000

1500 Impact Test


(Fmax = 3,300 N)
1000

500 Impact Test


(Fmax = 1,900 N)
0
0 1 2 3 4 5
displacement [mm]

Fig. 16. Experimental indentation results for laminate [+45/45/+45/0/ Fig. 17. Numerical indentation results for laminate [0]10: (a) force–
90]s maximum force at: 3300 N and 1900 N. displacement and (b) stress distribution.
426 V. Tita et al. / Composite Structures 83 (2008) 413–428

Criterion cannot represent the failure mechanisms shown ing and in the unloading phases (Fig. 18). In fact, the
by the composite structure. Besides, the maximum load permanent strain for the laminate [0/90/0/90/0]s is lower
simulated is much lower than the experimental maximum than the laminate [0]10 due to the stacking sequence.
load (Fig. 17a). It is important to note for finite element models on shell
It is important to note for finite element models on shell elements, the maximum number of iterations is equal to 8.
elements, the maximum number of iterations is equal to 10. For solid elements, the maximum number of iterations is
For solid elements, the maximum number of iterations is equal to 8, too.
equal to 9.
4.3.3. Numerical results for laminate [+45/45/+45/0/90]s
4.3.2. Numerical results for laminate [0/90/0/90/0]s Fig. 19 shows that Material Model I cannot simulate the
Fig. 18 shows that the Material Model I can simulate indentation test very well, during the loading and unload-
the indentation test, during the loading and unloading ing phases when parameter H is 1.2. However, the maxi-
phases when parameter H is equal to 1.6. Besides, the mum load simulated is quite similar to the experimental
maximum load simulated is quite similar to the experi- maximum load. The simulated load values for 1.5 mm up
mental maximum load. However, the simulated load val- to 3.2 mm for the displacement are very different from
ues for 1.5 mm up to 3.0 mm for the displacement is the experimental load values, because delaminations occur
very different from the experimental load values, because for the laminate [+45/45/+45/0/90]s and the shear stres-
delaminations occur for the laminate [0/90/0/90/0]s and ses increase due to the stacking sequence, providing a
the Material Model I cannot simulate this phenomenon. non-linear behavior. Any material degradation law is not
Any material degradation law is not activated and the activated and the simulated load values are higher than
simulated load values are higher than the experimental the experimental load values. The model correlates with
load values. The model correlates with the experimental the experimental test when displacement is close to
test when displacement reaches 3.5 mm, because fiber fail- 3.5 mm, because fiber failures occur and the degradation
ures occur and the degradation law decreases the material law decreases the material properties. In order to improve
properties. In order to improve the results during the the results during the loading phase, the Material Model II
loading phase, the Material Model II is applied to simu- is applied to simulate the delaminations. Fig. 19 shows that
late the delaminations. Fig. 18 shows that Material Model Material Model II cannot simulate very well the indenta-
II can simulate the indentation test during the loading and tion test during the loading and unloading phases, when
unloading phases, when parameter H is set to 0.4. Corre- parameter H is equal to 0.3, because the non-linear behav-
lation with experimental results is better than with Mate- ior caused by the shear stresses is not simulated with accu-
rial Model I. racy. Finally, in order to simulate the permanent strain,
Material Model I cannot simulate the final unloading Hill’s Criterion, implemented in software ABAQUSTM
phase due to the permanent strain at the disk centre when [23], provides poor results too (Fig. 19).
the polymer matrix exhibits plastic deformation under the It’s important to note for finite element models on shell
rigid hemisphere. In order to simulate the permanent elements, the maximum number of iterations is equal to 7.
strain, de Hill’s Criterion was used, implemented in soft- For solid elements, the maximum number of iterations is
ware ABAQUSTM [23], provides poor results both in load- equal to 8.

3500 Material Model I (H=1.6) Material Model I (H=1.2)


Material Model II (H=0.4) 3500 Material Model II (H=0.3)
3000 Hill's Criterion Hill's Criterion
3000
Indentation Test Indentation Test
2500
2500

2000
Force [N]

2000
Force [N]

1500 1500

1000 1000

500 500

0 0
0 1 2 3 4 5 0 1 2 3 4 5
displacement [mm] displacement [mm]

Fig. 18. Numerical indentation results for laminate [0/90/0/90/0]s. Fig. 19. Numerical indentation results for laminate [+45/45/+45/0/90]s.
V. Tita et al. / Composite Structures 83 (2008) 413–428 427

5. Conclusions the experimental test results for this work were used to val-
idate and calibrate a composite material failure model
For the experimental approach, it is verified that stack- developed by the authors and this failure model will be
ing sequence and impact energy level can influence on the shown in a future publication.
dynamic response of composite plates. The graphs of For the numerical approach, Material Model I for shell
force–time and energy–time, as well as the images from elements can simulate the indentation test of three stacking
ultrasonic C-scan technique are used in order to compare sequences, if the parameter H is adjusted according to the
the mechanical behavior of the specimens, which is repre- experimental results. However, Material Model I cannot
sented by graph of the absorbed energy versus impact represent the delaminations, because any material degrada-
energy level. Fig. 20 can be divided into three regions: tion law is not activated by this model. Thus, for some
regions of the curve force–displacement, the numerical
• Region 1: the specimens have a quasi-elastic behavior, result does not converge to the experimental result. Mate-
because the fraction of absorbed energy is very low rial Model II for solid elements can simulate the delamina-
(under 35%) as failure mechanisms are not activated; tions, during the indentation test. However, Material
• Region 2: the specimens show some failure mechanisms, Model II does not simulate the non-linear behavior caused
which are matrix crack and delaminations; so, the frac- by the shear stresses with accuracy. Besides, both material
tion of absorbed energy is intermediate between 35% models cannot represent the permanent strain after the
and 75%; final of the unloading phase. In fact, both material models
• Region 3: the specimens show many types of failure can be improved in order to simulate the phenomena with
mechanisms, for example: fiber rupture, matrix crack more accuracy.
and delaminations; so, the fraction of absorbed energy
is very high (over 75%). Acknowledgments

In general, the indentation test can be used to represent The authors would like to thank Dr. Ir. Mieke Lossie
a drop-test when the impact energy level is low and the and technician Paul Van Cauwenbergh (Mechanical Engi-
specimen has a quasi-elastic behavior. Because the indenta- neering Department of Katholieke Universiteit Leuven) for
tion curves do not show the oscillations inherent for the the technical support during the realization of this work.
dynamic response obtained from drop-tests and there are The authors would like to thank Professor Ignaas Verpoest
more failure mechanisms activated during the impact event (Material Engineering Department of Katholieke Universi-
than quasi-static event. Besides, the failure mechanisms teit Leuven (Belgium)) for allowing the realization of this
shown by the impact event are more distributed. With a work at LCPC (Leuven Composites Processing Centre).
quasi-static event they are more concentrated. Thus, the The authors would like to thank FAPESP for the funds
structural global stiffness reduces with more intensity for to realize this work.
drop-test. Finally, it is very important to comment that
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