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    In2Rpt (7) Formate

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    Nosayba M Alomari
    This document describes an inorganic chemistry laboratory experiment on the preparation of two transition metal complexes - tris(acetylacetonato)iron(III) ([Fe(acac)3]) and bis(acetylacetonato)diaquanickel(II) ([Ni(acac)2(H2O)2]). The experiment involves reacting iron(III) chloride hexahydrate with acetylacetone to produce [Fe(acac)3], and reacting nickel(II) sulfate hexahydrate with acetylacetone to produce [Ni(acac)2(H2O)2]. Percentage yields are calculated for both complexes. Students are asked to record observations, balanced equations,

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    In2Rpt (7) Formate

    Uploaded by

    Nosayba M Alomari
    25 views3 pages
    This document describes an inorganic chemistry laboratory experiment on the preparation of two transition metal complexes - tris(acetylacetonato)iron(III) ([Fe(acac)3]) and bis(acetylacetonato)diaquanickel(II) ([Ni(acac)2(H2O)2]). The experiment involves reacting iron(III) chloride hexahydrate with acetylacetone to produce [Fe(acac)3], and reacting nickel(II) sulfate hexahydrate with acetylacetone to produce [Ni(acac)2(H2O)2]. Percentage yields are calculated for both complexes. Students are asked to record observations, balanced equations,

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    inorganic laboratory sheet

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    In2Rpt[7]formate

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    This document describes an inorganic chemistry laboratory experiment on the preparation of two transition metal complexes - tris(acetylacetonato)iron(III) ([Fe(acac)3]) and bis(acetylacetonato)diaquanickel(II) ([Ni(acac)2(H2O)2]). The experiment involves reacting iron(III) chloride hexahydrate with acetylacetone to produce [Fe(acac)3], and reacting nickel(II) sulfate hexahydrate with acetylacetone to produce [Ni(acac)2(H2O)2]. Percentage yields are calculated for both complexes. Students are asked to record observations, balanced equations,

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    © All Rights Reserved
    Download as DOCX, PDF, TXT or read online from Scribd
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    Download as docx, pdf, or txt
    25 views3 pages

    In2Rpt (7) Formate

    Uploaded by

    Nosayba M Alomari
    This document describes an inorganic chemistry laboratory experiment on the preparation of two transition metal complexes - tris(acetylacetonato)iron(III) ([Fe(acac)3]) and bis(acetylacetonato)diaquanickel(II) ([Ni(acac)2(H2O)2]). The experiment involves reacting iron(III) chloride hexahydrate with acetylacetone to produce [Fe(acac)3], and reacting nickel(II) sulfate hexahydrate with acetylacetone to produce [Ni(acac)2(H2O)2]. Percentage yields are calculated for both complexes. Students are asked to record observations, balanced equations,

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    of 3

    Exp.(7) Preparation of [Fe(acac)3] & Ni(acac)2(H2O)2] Chem.

    323

    Inorganic Chemistry Laboratory (II)

    Experiment Number 7

    Preparation of Tris(acetylacetonato)iron (III); [Fe(acac)3]


    Preparation of Bis(acetylacetonato)diaquanickel (II); [Ni(acac)2(H2O)2]
    _____________________________________________________________________________________________________________________

    Student Name: ………………………..………… Section: ……………………………….……………

    Date of Experiment: …………………….……… Date of Submission: ……………………….…..

    NOTE: Late submission of your report lab will be met with a 10-point deduction for every calendar day it is late.

    A. Preparation of Tris(acetylacetonato)iron (III); [Fe(acac)3]

    Write the balanced equation of reaction:

    Color of yield
    Weight of [Fe(acac)3] ( actual yield (g))
    Number of moles of FeCl3.6H2O

    Number of moles of acetylacetone.

    The Limiting reagent


    Number of moles of [Fe(acac)3]

    Weight of [Fe(acac)3] (Theoretical)

    1 Al Sharif Y & Al Omari N


    Exp.(7) Preparation of [Fe(acac)3] & Ni(acac)2(H2O)2] Chem.323

    Percentage yield of [Fe(acac)3]

    Draw the structure of complex

    Geometry of product
    Symmetry point group of product

    B.Preparation of Bis(acetylacetonato)diaquanickel (II); [Ni(acac)2(H2O)2]

    Write the balanced equation of reaction:

    Color of yield
    Weight of [Ni(acac)2(H2O)2] ( actual yield (g))
    Number of moles of NiSO4.6H2O

    Number of moles of acetylacetone.

    The Limiting reagent


    Number of moles of [Ni(acac)2(H2O)2]

    2 Al Sharif Y & Al Omari N


    Exp.(7) Preparation of [Fe(acac)3] & Ni(acac)2(H2O)2] Chem.323

    Weight of [Ni(acac)2(H2O)2] (Theoretical)

    Percentage yield of [Ni(acac)2(H2O)2]

    Draw the structure of complex

    Geometry of product
    Symmetry point group of product

    Questions:
    Q1. Role of adding the following:
    1. Acetylacetone.

    2. Sodium hydroxide.

    3. Ethanol.

    4. Ammonium hydroxide

    3 Al Sharif Y & Al Omari N

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