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Holcim Technical Manual English PDF
Holcim Technical Manual English PDF
Holcim Technical Manual English PDF
Technical Manual
Cement & Concrete
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Authors
Publication
Disclaimer
cement plants in south Vietnam at Hon Chong, Hiep Phuoc, Cat Lai,
Thi Vai, to guarantee the best supply security for each project. To
Preface
To develop Vietnam in the 21st century and to meet the requirements of modern society, many high rise
buildings and infrastructure projects, like ports, roads, bridges… are being designed and constructed by
national and international developers, designers and contractors.
These structures are expected to be in service for long time, sometimes for 100 years, with low maintenance
costs. The durability of concrete as building material is a key element for long lasting projects. This Technical
Manual offers an overview of good practices in concrete as well as an overview of relevant Vietnamese and
international standards.
A better understanding of cement/concrete standards can make it easier for designers, consultants and
contractors to choose the type of cement and concrete, suitable for their specific project. With good concrete
practice at the jobsite, the high quality building material “concrete” will be molded and transformed into
long lasting concrete structures, to build Vietnam for future generations.
As the different standards are complex to summarize and the construction industry changes quickly in
Vietnam, it is possible that there are inaccuracies in this Technical Manual. We are looking forward to any
feedback or input for improvement on technical.service-vnm@holcim.com.
Yours sincerely,
Pieter Keppens
Technical Marketing Manager
8
Index
Chapter I
Cement & Concrete 11
A. Components of concrete 11
1. Cement 11
2. Mixing water 12
3. Fine aggregate 13
4. Coarse aggregate 14
5. Admixtures 16
6. Additions 17
Chapter II
Applications with specific requirements 49
A. Infrastructure 49
1. Introduction 49
2. Cement for infrastructure 49
B. Aggressive environments 50
1. Introduction 50
2. Sulfate resistant Portland cement 50
3. Sulfate resistant blended cements 51
C. Massive structure 52
1. Introduction 52
2. Cement for massive structures 52
3. Concrete for massive structures 53
Chapter III
Causes and prevention of concrete defects 62
A. Segregation of concrete 63
B. Cracking 64
1. Plastic settlement cracks 65
2. Plastic shrinkage cracks 66
3. Surface crazing 67
4. Drying shrinkage cracks 67
5. Early thermal cracking 68
E. Chemical attack 72
1. Classification 72
2. Preventive measures 73
G. Fire Resistance 75
1. Concrete in fire 75
2. Preventive measures 75
Chapter IV
Overview of cement & concrete standards 76
A. Cement 77
Vietnamese standards – TCVN 77
American standards – ASTM 83
European standards – EN 86
B. Concrete 89
Vietnamese standards – TCVN 89
American standards – ASTM 91
European standards – EN 93
British standards – BS 95
Reference 98
10
Chapter I: Cement & Concrete 11
A. Components of concrete
General
Mixing water is the total amount of water contained
in fresh concrete. It is the sum of:
• The water added directly to the mix
• The surface moisture of the aggregates
• The water content of the concrete admixtures
and additions, if applicable
(silica fume, pigment in suspension, etc.)
Mixing water has two functions in concrete
technology. It is required for hydration of the
cement, and for the production of a plastic concrete
that can be well compacted.
Maximum Level
(mg/l)
Table I.1 - Limit sulfate and chloride content in mixing water for different purpose
Chapter I: Cement & Concrete A. Components of concrete 13
Grading 90
Passing (%)
7570 : 2006 or ASTM C33 (Standard Specification for 50
= fineness modulus): 20
Other Impurities
Impurities like silt, dust, clay content also have a
disavantage effect on concrete. It should be tested
before use for concrete according to standard TCVN
7572-8 : 2006 (Standard test method for silt, dust,
clay content) or ASTM C117 (Standard Test Method
for Materials Finer than 75-μm).
14 Chapter I: Cement & Concrete A. Components of concrete
Characteristics
4. Coarse aggregate
The most important characteristics of coarse
General aggregates are:
Coarse aggregates form the skeletal structure of the • Specific gravity
concrete and must comply with TCVN 7570 :2006 or
• Bulk density (unit weight) and moisture content
ASTM C33 (Standard Specification for Concrete
• Mineral composition, grain shape, and surface
Aggregates).
texture
• Purity
• Grading (grain size distribution) and aggregate
fractions (range of sizes)
• Soundness
Table I.2
Classification of Aggregate type Specific Gravity (kg/m3) Aggregate Material Application
aggregates by
specific gravity
River or glacial deposits; Reinforced and
Standard aggregate 2700
crushed stone non-reinforced concrete
Fig I.3
The moisture Saturated surface dry
State Ovendry Air dry Damp or wet
state of (SSD)
aggregate
Chapter I: Cement & Concrete A. Components of concrete 15
Fig I.8
6. Additions Polypropylene
Fibers fibers
Polypropylene fibers are organic fibers, used in
concrete to prevent plastic shrinkage cracks. About
0.7kg - 1kg of fibers is required per m3 of concrete
(Fig I.8).
Silica fume
Silica fume (Fig I.11), also known as silica dust or
microsilica, possesses a high pozzolanic activity due
to extreme fineness and very high amorphous silica
content. Silica fume dosages of 5 to 10% by weight
of cement can produce permanent improvement of
concrete characteristics:
Fig I.10
• Reduction of concrete porosity, thus Glass fiber, cut
improvement of durability; increased resistance and bundled
to salts, sulfates, and other aggressive chemicals.
• Carbonation progresses slower, thus
reinforcement is better protected against
corrosion.
• Contributes to concrete strength; allows the
production of high-strength concrete
(80-100MPa)
Fig I.11
Caution Silica fume
Adding silica fume to a concrete mix reduces
the workability and changes the rheologic
characteristics (flow characteristics)! Adequate
workability can be achieved by adding special
superplasticizers.
Fig I.12
Puzzolan
Concrete mixing
In proportioning the constituents of concrete, or Fig I.16 - Influence of the w/c ratio on concrete properties
determining the so-called concrete mix or mix
design, the producer is primarily concerned with The relationships between the w/c ratio and
optimizing concrete's: required characteristics of concrete are well known
• Workability in practice. Thus, the designing engineer usually
• Strength specifies the w/c ratio when he specifies the type of
concrete.
• Production cost
• Durability
Chapter I: Cement & Concrete B. From fresh concrete to hardened concrete 21
Fig I.18
According to EN 206, reinforced concrete with a
Poor filling of
maximum aggregate size of 32mm should normally void spaces, high
contain at least 300kg cement per m3 compacted permeability
concrete. The dosage may be reduced to 250 kg/m3 concrete with
only if the constructed element is permanently only one size of
protected from environmental action and other aggregate
(schematic)
forms of attack.
Example:
Specific Gravity
Component Mass (kg) Unit volume (m3)
(kg/m3)
1) Mixing water = water added + moisture of aggregates. The number through indicate the sequence of the
calculation.
To calculate the actual amount of aggregate Influence of other factors on the workability &
necessary, the water contained as moisture in the strength of concrete
aggregate (generally 4 to 6% for sand and 1 to 3 %
Besides admixtures, many other factors influence
for gravel) must be added for each fraction.
concrete workability. Changing one or more of these
Subtracting the moisture contained in all the
factors changes not only the workability, but also
aggregates from the total mixing water gives the
other characteristics of concrete, for example
necessary amount of water to be dispensed.
strength. Table I.4 shows how various changes in
concrete constituents and mix affect the
The unit volume of entrapped air bubbles (generally
consistence and 28-day compressive strength of
1 to 2 %) as well as the volume of entrained air must
concrete.
also be considered in proportioning the mix by
absolute volume. The example shows a method of
calculating the “dry“ aggregate amount and the
fresh concrete density.
Chapter I: Cement & Concrete B. From fresh concrete to hardened concrete 23
Table I.4
28-day Effect of various
Change Workability compressive factors on
strength
workability and
Smoother grading strength of
concrete
More rounded aggregate
Use of a superplasticizer
a. Slump test :
2. Workability
The slump test is the most well-known and widely
To achieve a high quality concrete structure, the used method to characterize the workability of fresh
method of placing and compaction as well as the concrete. This simple test is used at the job sites to
shape of the concrete element and reinforcement quickly determine whether a concrete batch should
arrangement, should be considered to select the be accepted or rejected.
workability of the concrete.
The slump test measures the ability of concrete to
The concrete workability affects the speed of flow under its own weight, without vibration. This
placement and the degree of compaction of method is suitable for medium to high workability
concrete. Inadequate compaction may result in the concrete with slump ranging from 10 to 210 mm
reduction in both strength and durability of (EN 206).
concrete.
The test method is widely standardized throughout
Different test methods for workability are available the world:
including slump, Vebe time, flow table, etc. The • TCVN 3106
choice of the test method depends on the concrete • ASTM C143
workability and its application.
• EN 12350-2
To get reliable results, each test method for The apparatus used in the slump test are: mold,
workability should be applied within its test range tamping rod, measuring equipment (Fig I.20):
(EN206):
Fig I.20
Apparatus to
• Slump ≥ 10 mm and ≤ 210 mm;
determine slump
• Vebe time ≤ 30 sec and > 5 sec;
- In EN and TCVN standards, the slump is the - In ASTM standard, the slump is the vertical
vertical difference between the top of the mould difference between the top of the mould and the
and that of the highest point of the slumped test displaced original center of the top surface of the
specimen. specimen.
Fig I.21 - Determine Slump conform to TCVN and EN Fig I.22 - Determine Slump conform to ASTM standard
standard
True Slump
Fig I.23 - True and shear slump shape
Shear Slump
Depending on the application of concrete, the following slump values are recommended:
Table I.5
Slump range for Slump Range (mm) Application Illustrated photo
different
applications
b. Slump flow: The upright mold (same way as the slump test) is
The slump flow test method is used to determine popularly used in Vietnam. Slump flow is the
workability of very flowable concrete with a very average of the largest diameter of circular spread of
high slump. At this high slump > 200mm, normal the concrete and the circular spread of the concrete
concrete has the tendency to segregate, which at an angle approximately perpendicular to
impacts the concrete quality significantly. To reach a diameter above.
high quality concrete at very high workability, the
mix design needs to be specially developed to avoid Concrete with high workability is used for structure
segregation and achieve the required stability. with dense reinforced steel such as transfer beam,
core walls, pile cap, etc or for the areas that are
Two types of concrete can be distinguished difficult to reach for compaction.
(see Chapter II.E):
- Very flowable concrete (slump flow: 450- 650mm) Fig I.25
- Self Consolidating Concrete (SCC), also known as Structure with
Self Compacting Concrete (slump flow > 650mm). dense reinforce
steel
Fig I.26
Transfer beam
c. VEBE test:
For semi-dry concrete with a low workability, the use
of the Vebe test is recommended. The Vebe time is
the time needed to level and compact fresh concrete
in Vebe consistometer and ranges from 5s to 30s
(EN 206). Some typical applications are:
Fig I.24 - Determine slump flow for fresh concrete - Roller compacted concrete (RCC) for hydraulic
RCC dams
The test method to determine slump flow is ASTM - Base layers of roads, container ports
C1611 or EN 12350-8. In ASTM standard, there are - Precast products: concrete pipes
two ways to measure slump flow of concrete:
- Upright mold
- Inverted mold
26 Chapter I: Cement & Concrete B. From fresh concrete to hardened concrete
The freshly mixed concrete is packed into a similar d. Flow table test:
cone used for the slump test. The cone stands within The flow table test measures the workability of
a special container on a Vebe table, which is vibrated concrete under the impact of compaction energy.
at a standard rate after the cone has been lifted. The Generally, in Viet Nam, EN 12350-5 standard is used
time taken for the concrete to be compacted is to test flow table of fresh concrete.
measured.
Fig I.27
RCC for hydraulic
dams
Rotating Arm
Slump Cone
30mm
Mold
Clip Handle
Bottom 200mm
Plate Top Plate
40mm Hinge
700mm
100x100x100 0.91
Fig I.31 - Cube and cylinder specimens 150 x 150 x 150 1,00
Cube
specimen 200 x 200 x 200 1.05
The below 3 steps are very important to assure the Fig I.36
reliability of the result: Satisfactory
failure of cube
• The sampling of the concrete and the making of specimens
the concrete specimens shall be done properly,
so that the concrete cubes are representative of
Fig I.37
the concrete batch. This procedure is sometimes Unsatisfactory
neglected in some job sites, which may lead to failure of cube
low strength of the concrete specimen. specimens
1 2 3
• The curing in water tanks – specific attention
needs to be given to the transport of concrete
cubes at early age. A careless handling can
4 5 6
impact their final strength.
• Finally, the compressive strength of the concrete
specimen is determined in the laboratory.
Experience shows that the skill of laboratory 7 8 9
Fig I.39
When the specimen shows an unsatisfactory failure, Unsatisfactory
the obtained result will not represent the true failure of
compressive strength of the concrete. cylinder
specimens
A B C D
E F G H
I J K
30 Chapter I: Cement & Concrete B. From fresh concrete to hardened concrete
Method of Foundation: 1set/100m3 Not less than 1 set for each number of set required: First 50m3: 3 set
Sampling Foundation under 115m3 V ≤ 40m3: 1 / 10m3 Then 1 set / 150m3
machinery: 1set/50m3
V ≤ 80m3: 1 / 20m3 Take 2 or more
Frame and thin structure: specimens per set.
1set /20m3 V ≤ 200m3: 1 / 50m3
Testing fmin : lowest strength f’c : the specified fmin: lowest strength Measure
specimen compressive strength. specimen compressive strength
fmed: median strength f’cr : the average fmax: highest strength of the specimens.
specimen compressive strength. specimen fmin: strength of
fmax: highest strength the specimen with
specimen fcm = (fmax + fmin) / 2 lowest strength
fmax: strength of
∆1 = fmax - fmed ; the specimen with
∆2 = fmed - fmin highest strength
fcm = average
strength of all
specimens
• If ∆1 and ∆2 are both • If (fmax – fmin) / fcm > 15% • If (fmax – fmin) /
Compliance less than 15% of fmed, then the sample was fcm > 15% then
checking then invalid. the sample was
favg = (fmin + fmed + fmax)/3 • Otherwise, f = fcm invalid.
Compressive favg ≥ fck The average of 3 favg = average strength of all favg = average
strength consecutive strength tests valid sample. strength of all valid
assessment fmin ≥ 85% x fck shall be equal to or greater For C20 or above samples
than specific strength-f'c Criteria 1 (Rolling average):
First 2 samples: favg ≥ fck +1 Criteria 1 (Rolling
• If f'c ≤ 35 MPa:
average):
individual strength test First 3 samples: favg ≥ fck +2
favg ≥ fck + 4
≥ f‘c - 3.5(MPa)
Any consecutive 4 samples:
• If f'c > 35 MPa: individual favg ≥ fck + 3 Criteria 2 (Individual
strength test ≥ 0.9f 'c Criteria 2 (Individual sample): sample):
When meeting failure case, All valid samples: f ≥ fck - 3 All valid samples:
refer to section 19 ASTM f ≥ fck - 4
C94-2005. For C7.5 to C15
Criteria 1 (Rolling average):
First 2 samples: favg ≥ fck
First 3 samples: favg ≥ fck+1
Any consecutive 4 samples:
favg ≥ fck + 2
Criteria 2 (Individual):
All valid samples: f ≥ fck - 2
32 Chapter I: Cement & Concrete B. From fresh concrete to hardened concrete
d. Comparison of strength between different standard into a different standard. To assure the
standards: compliance to the design, the concrete should be
Every standard has its own system to evaluate the tested according the standard set (TCVN, ASTM, EN,
compliance of the test result to the requirement of BS), used for the design.
the standard.
The following graph provides an indication how
It is very difficult to compare the standards. In TCVN, EN and BS are related in terms of cube
principle, it is not recommended to translate one strength (not to scale).
Table I.10
Comparison of
strength between M300 M350 M400 M450 M500
different standards
in terms of cube
TCVN
sample
b. Air content
4. Special characteristics
Air content of concrete is also an important
a. Concrete density characteristic to indirectly assess the quality of
The density of both fresh and hardened concrete is concrete.
of interest to the engineers for different reasons
including structural design and impact on Fresh concrete always contains a significant amount
compressive strength. of air bubbles. One of the main reasons to compact
the concrete is to remove them. If the concrete is
By choosing suitable aggregates and mix design, the
not well compacted, some air will remain in the
density of concrete can be increased significantly
concrete, reducing the strength significantly.
(heavy concrete) or reduced (light-weight concrete).
Normally, a typical compacted concrete will have air
percentage varies from 0.5 – 2.5%. Concrete with
For fresh concrete:
high slump usually has lower air content than low
The density plays an important role in controlling
slump concrete. Besides, the plasticizer/super
concrete yield (compared to the mix design) at
plasticizer admixture can increase the air content in
readymix batching plant. Typical readymix concrete
concrete, which may lead to lower strength.
density varies from 2200 – 2500kg/m3 (TCXDVN
374:2006), depending on the aggregate type and
mix design. A rule of thumb
1% excessive air
Based on the density of compacted fresh concrete, reduces the concrete strength by 4-5%.
plant operators are able to check if the mix design is
In some cases, the air content in the concrete is
over- or under yielding: this means that the mix
increased with an air-entraining admixture up to
design gives more or less than 1m3 concrete after
4-6%, to improve the resistance of the concrete
compaction. Fresh concrete density test method
against deterioration caused by freeze-thaw. For the
complies with ASTM C138; EN 12350 – 6; TCVN
tropical climate in southern Vietnam, air entrained
3108:1993.
concrete is normally not used for this purpose.
5000
Final Setting
4000
Penetration Resistance, psi
3000
2000
Fig I.42
Concrete Fig I.44 - Diagram to determine the setting time of concrete
bleeding meter
Chapter I: Cement & Concrete B. From fresh concrete to hardened concrete 35
Fig I.45
3 The test method
to determine the
6 5 water
permeability of
1 2 concrete
4 4 4 4 4 4
4
4
35 B8
40 B10
45 - 50 B12
Fig I.48
5. Production and Transport Homogeneity of
Dosage of the components the mix as a
function of
The production of concrete is closely linked to the
mixing duration
technology and equipment used. The task of dosage
is to dispense the components of the concrete mix –
aggregate, cement, additions, mixing water,
admixtures – in controlled amounts, to produce the
specified mix proportions with great accuracy. Two
systems are used, dosage by volume and dosage by
mass. Dosage by mass gives more accurate results.
Every batching plant must establish sequencing for
adding the material through systematic pretests.
Sequencing is critical for:
• The dispersion
• The mixing effect
• The optimal effect of admixtures
• Plant efficiency
• Mechanical wear Readymix concrete should be brought to the
construction site immediately after production at
Mixing the components the concrete plant and placed without delay in order
The mixer must blend the separate components into to preserve quality. There is a certain danger of
a homogeneous mix. The mixer must also satisfy the segregation during transport, so truck mixers are
following requirements and tasks: used when the concrete is of highly plastic
• High mixing intensity consistence, for long hauls, or when traffic
conditions are poor.
• Short mixing duration
• Dispersion of the cement and the additions
During the trip, concrete must be protected from
• Optimal coating of the aggregates with fines rain, exposure to sun, wind blast, and the like.
mortar (fines paste) Depending on the prevailing weather conditions on
• Fast discharging the day of concreting, suitable measures should be
• Low wear taken (covering the concrete, reducing the
temperature of fresh concrete, etc.).
At ready-mix plants the paddle mixer is the most
common type, used discontinuously for mixing
For delivery by truck mixer, the concrete should be
single batches. Each type of mixer requires a
mixed an additional one to two minutes after arrival
minimum batch size, below which the quality of the
on site and immediately before pouring. Adding
fresh concrete is reduced.
more water should be avoided, because such
additions are uncontrolled and the water cannot be
Mixing duration
mixed in thoroughly. If the delay becomes too long,
The duration of mixing depends on the type of
the concrete may be used only for less critical
mixer (drum or paddle mixer). Mixing duration
applications (fill, lean concrete, etc.).
should be determined by testing.
Definition:
Mixing duration = “Wet-mixing duration”
starts when all components are in the mixer.
Table I.13
Method of Workability of concrete
Method of conveying Structure Picture
conveying (Slump)
Fig I.50
Chapter I: Cement & Concrete B. From fresh concrete to hardened concrete 39
Method of compaction
Selecting the best method of compaction will
depend on the workability of the concrete and the
reinforcement density/rebar spacing of the element.
The most common effective method of compaction
is vibrating. Vibrating is most often done with
internal vibrators (poker-type vibrators) or external
Fig I.53 - Segregate concrete because of too high drop
vibrators (form vibrators or surface finishers with
surface vibrators).
Compaction
Good compaction is the prerequisite for durable
Vibration almost completely overcomes the internal
concrete. The advantages of well-compacted
friction between the aggregates. The separate
concrete are:
particles move closer together, and entrapped air
• Higher density escapes to the surface in the form of air bubbles
• Improved durability (the content of entrapped air after compaction is
• Good compressive strength about 1.5 % by volume). The voids become filled
• Better bond between reinforcement and concrete with fines paste and the fresh concrete is
consolidated under its own weight.
Table I.14
Spacing
Diameter of Effective range Reference values
between
vibrator head diameter for the effective
inserrtion
(mm) (mm) range diameter
points (cm)
and spacing of
< 40 30 25 insertion points
40 bis 60 50 40
> 60 80 70
Rule of thumb
Spacing between insertion points =
8 to 10 times the diameter of the vibrator head
Fig I.57
Spacing between
insertion points,
Right Wrong
insertion point
300-400 mm
depositing “fresh
on fresh“ I II III
I II III
150 mm
Fig I.60
Wetting the forms
Chapter I: Cement & Concrete B. From fresh concrete to hardened concrete 43
8. Pumped concrete
Application Range
The use of pumps is recognized as a modern and
efficient method of transport and placing concrete.
Pumped concrete can be used for practically any
construction task, and is particularly useful when
high performance in placing is required or when the
pouring location is poorly accessible. In general,
there are two types of concrete pumps: stationary
and mobile.
Fig I.62
Casting a large
• Admixtures concrete floor
The rules that apply to using admixtures in concrete slab. Mobile
also apply to pumped concrete. It should be kept in pump fed by a
truck mixer
mind when using air entrainers, that fresh concrete
with an air content greater than 4% can reduce the
delivery capacity of concrete pumps.
• Consistence
Pumped concrete must have a plastic to soft
workability.
• Cement
Practically any standard cement is suitable for use in
pumped concrete. A fresh concrete that can be
efficiently moved through a pipeline should have a
cement content of at least 320 kg/m3.
• Aggregate mix
Experience shows that increasing the fines
(≤ 0.125mm, including cement) to about 400 kg/m3
considerably improves pumpability without
compromising durability of the hardened concrete.
Fig I.63
9. Curing
Purpose and objectives
The purpose of curing is to protect concrete from
water loss and harmful influences during the early
hardening period. Compressive strength alone does
not guarantee durability; the concrete must also be
dense. Especially in the surface layer, hardened
cement paste with high density and low-as-possible
permeability is very important.
Premature drying
Protection against premature moisture loss is
especially important. Protective measures must be
taken immediately after concrete is placed.
Preventive measures
• Leaving forms in place
• Covering with a membrane (Fig I.63)
Fig I.65
• Wrapping with insulating material (Fig I.64)
• Covering with water-retaining fabrics
(burlap, geotextiles)
• Application of a liquid curing compound
(Fig I.65)
• Continuous spraying with water
• Keep under water
• A combination of these measures
46 Chapter I: Cement & Concrete B. From fresh concrete to hardened concrete
Rate of drying Typical effects of these factors are shown in Fig I.66
The rate of drying depends on: and Fig I.67 and Fig I.68 shows the correlations
• air temperature among the factors mentioned. The chart can be used
to estimate the rate of drying.
• concrete temperature
• relative humidity
• wind speed
kept moist 3
30 for 7 days unprotected concrete,
wind speed 10 km/h
20 2
not
kept moist concrete protected
10 1 with a curing compound
0 0
1 3 7 28 90 0 6 12 18 24
Testing age [days] Time [hours]
Fig I.66 - Influence of water retention on strength Fig I.67 - shows the correlations among the factors
development in the surface layer of concrete mentioned. The chart can be used to estimate the rate of
drying.
40 30
25
20 20
15
10
0
10 20 30
rate of drying 6
(kg/m2 hr.)
2
4
1 2
0
Chapter I: Cement & Concrete B. From fresh concrete to hardened concrete 47
Selection of forms
The construction contractor usually selects forms
based on the following criteria: Fig I.70
• Building structure / construction task Peeled-off
concrete skin
• Specified surface quality of the concrete
• Number of potential reuses
• Labor required for erection
• Thermal insulation characteristics
• Price
• Steel, aluminium
Form types
Absorptive forms usually produce a smooth, closed
concrete surface, because they absorb surplus water
and air bubbles. The face of wooden forms should
include only boards which have been used for an
equal number of times, because the absorption Fig I.73
capacity of the wood decreases with each use, which Non-uniform
absorbency of
has an effect on the color of the concrete surface.
wood used in
Raw wooden boards should be coated with cement forms affects the
paste before initial use to remove the wood sugar concrete surface
that disturbs hydration of cement. This coating also
evens out any variations in absorbency of the boards
(Fig I.73).
48 Chapter I: Cement & Concrete B. From fresh concrete to hardened concrete
Form-release agents
Form-release agents make it easier to loosen the
form faces from the concrete surface. At the same
time, they protect and preserve the form material.
They are to be applied thinly and uniformly,
normally before the reinforcement is put in place.
Surplus chemical should be wiped away with a cloth
(Fig I.74). Staining, and irregular gray color of the
concrete surface, can frequently be traced to
improper application of a form-release agent.
Fig I.74
Effect of form-release agents on the concrete surface:
- Left: surplus form-release agent removed with a cloth
- Right: excessive form-release agent used
Applications with
Chapter II:
49
specific requirements
A. Infrastructure
1. Introduction 2. Cement for infrastructure
To support the growth of the economy in Vietnam, In south Vietnam, the cement, used for
both public and private funds invest important infrastructure, is Blended Portland Cement (PCB40),
amounts of capital into infrastructure projects, like compliant to TCVN6260, ASTM C1157 with low
roads, bridges, dams, ports, tunnels, power plants… alkali content (Na2O-eq < 0.60%) to prevent alkali
aggregate reaction.
As this infrastructure is the backbone of the
economy, the design life of these projects is The alkali-aggregate reaction – or “concrete cancer”
significantly longer than normal buildings (houses, in laymen’s terms – is a reaction between
schools). With proper maintenance, a bridge should aggregates, the alkali in the concrete and water to
be used for at least 50 years up to 100 years and form an expansive gel that creates cracks in the
even longer! concrete. This reaction is a very slow process over
years, but can become visible in 5 to 10 years after
To meet this long service life, the concrete for construction.
infrastructure projects requires special attention for
durability, with careful selection of the concrete In case of aggressive environment (presence of
components. chlorides, sulphates, seawater,…), additional
precautions have to be taken (see chapter II.B).
Holcim recommendation
Cement PCB 40 according to TCVN 6260:2009
or ASTM C1157 - GU, with low alkali content
(Na2O-eq M 0.60%)
50
B. Aggressive environments
(sulfate, seawater ...)
1. Introduction 2. Sulfate resistant Portland
To assure the long life of the construction in cement
aggressive environments, special care has to be
Main characteristic of sulfate resistant Portland
taken for the concrete: cement choice, mix design,
cement is a lower C3A content, a specific cement
placing and compacting, and last but not least,
mineral, as this component will react with sulfates
curing.
in the environment to ettringite, that expands in the
concrete pores to create tensions and cracks in the
A key element is the choice of cement, as concrete
concrete.
can be exposed to different aggressions:
• Sulfates in the environment attack the cement The C3A-content of cement can only be measured on
matrix (C3A cement mineral) and create cracks in Ordinary Portland Cement (OPC). For blended
concrete cement, the addition materials will change the
• Chlorides penetrate into the concrete pores and chemistry of cement and the calculated C3A –
can lead to the dangerous pitting corrosion of content (based on the Bogue formula C3A = 2,65
steel reinforcement of the structure Al2O3 – 1,692 Fe2O3) is not valid any more.
• Other aggressive elements (low pH, acids,..) can
attack the cement matrix, by dissolving its This type of cement complies to following standards:
constituents • TCVN 6067
• ASTM C150 – Type II (Medium Sulfate MS) or
For aggressive environments, 2 main types of type V (High Sulfate HS)
cement are generally specified: • BS 4027
• Sulfate resistant portland cement (only for
sulfate attack) The maximum value of C3A depends on the standard
• Sulfate resistant blended portland cement used:
Normal Cement
Attention TCVN
adapted to the aggressive environment Note: According TCVN 6067, OPC type II (comply with ASTM
• Water/cement ratio, C150) does not classify as sulfate resistance cement
to reduce pore space
Fig II.1 - The maximum value of C3A depends on the
• Concrete cover, standard used
to protect steel reinforcement
• Curing of concrete, By limiting the C3A mineral, sulfate resistant
for high quality concrete cover Portland cement offers protection to sulfate attack
from the environment only. It does not offer
additional protection to chloride penetration or
other aggressive elements (low pH, acids…),
compared to a concrete with general use cement
PCB40.
Chapter II: Applications with specific requirements B. Aggressive environments (sulfate, seawater ...) 51
0.3
0.25
0.2
0.15
0.1
0.05
0
7d 14d 21d 28d 56d 91d 105d 112d 180d
Limit of High Sulfate Resistance Holcim Extra Durable (HS) cement Indicative reference values for 35-40MPa concrete:
• Normal cement PCB40 : > 5000 Coulomb (high)
• Sulphate resistant blended cement : 1000 – 1500
Coulomb (low)
Holcim recommendation
For concrete in aggressive environments
(seawater, brackish water, waste water,..),
Fig II.2: Test method to determine the expansion of the Holcim recommends to use a sulfate resistant
mortar bar in sulfate solution blended cement, type TCVN 7711:2007
or ASTM C1157- HS, as it offers several
advantages:
According the EN 197-1:2011 standard, specific
types of blended cement are considered to be • Better protection of steel
sulfate resistance, based on long-term experience reinforcement against corrosion
with these cements. • High sulfate resistance of concrete
• Higher resistance against other
aggressive elements (acids, low pH etc)
52
C. Massive structure
To reduce these risks, specific measures have to be
1. Introduction
taken, for example:
In massive concrete elements, the heat of hydration
• Limit the maximum temperature difference
of cement will increase the concrete temperature at
ΔT < 200C or limit the maximum temperature
the center of the mass element significantly. During
gradient between two points ΔT/m < 500C
the hardening phase, the temperature can rise up to
(TCVN 305:2004)
85 – 100oC for thick elements, with general use
• Limit the maximum temperature in the core Tmax
concrete. When the hardened concrete in the center
< 700C
then cools down, the thermal shortening of the
• Insulation formwork is often used to warm the
concrete creates stresses in the element, which can
concrete surface and reduce temperature
lead to thermal cracking.
difference. It should stay in place for several days
Fig II.4
Heat of until ΔT < 200C. Removing it too soon can cause
the surface to cool quickly and crack.
hydration
development
inside mass These measures should be considered when the
concrete can lead concrete thickness > 1.5m.
to thermal
cracking
For specific concrete structures, these requirements
can be imposed from thickness > 1m, when the
consequence of cracks can lead to significant
damages (example: tunnel elements, gas storage
tanks…)
60 Inside
Surface
40
Form
removal
20
ΔT > 200C
Unprotected surface no cracking Fig II.5
cools fast
0 Timing of
formwork removal
0 1 2 3 4 5 6 7 8
impacts the risk of
Days
thermal cracks
Chapter II: Applications with specific requirements C. Massive structure 53
• Optimize cement content, by using more After execution of the concrete pour, suitable curing
advanced admixtures with insulation material (5cm minimum) is very
• Use larger size aggregates important to reduce the temperature difference
• Compressive strength requirement at 56 days between surface and core. Water curing should not
instead of 28 days. be used as it cools down the surface. For the same
reason, the slab has to be protected from heavy rain,
The fresh concrete temperature should be as low as as this will cool down the surface suddenly and
technically possible. In South Vietnam, maximum increases the risk of thermal cracks.
temperature of 30 – 320C can be obtained using
standard practices: During the hardening phase, the temperature of the
• Cover aggregates to reduce their temperature concrete is measured every two hour for at least 3
days. For this purpose, thermo-couples are placed on
• Sprinkle coarse aggregates regularly
different locations in the concrete element.
• Use of chilled water and ice.
During construction:
• Savings in steel & reduced cost /m column
• Reduced weight and savings on foundation
4000
60%
3000 50%
40%
2000
30%
1000 20%
10%
0 0%
B40 B60 B80 B100
Concrete grade
No vibration
Self compacting 660
required during
concrete – 850mm
casting
Compaction is
Normal concrete <450mm
required
Pavement
Subbase
Soil
Soil
stabilized
by CDM
When aggregates are treated with a small quantity 2. Cement for treated
of cement, the bearing capacity and the stiffness aggregates
(E-modulus) of the layer increases resulting in a
longer service life of the structure. The cement used for the treated aggregate layer
must ensure a high efficiency to develop strength as
For the same bearing capacity, the addition of well as a long workability of the mix. The
cement to aggregates will reduce the required optimization tests in the laboratory will determine
thickness of the aggregate layer, which reduces the the compatibility of the cement and the aggregates.
use of natural resources and expensive aggregates.
In general, the cement complies to:
• TCVN 6260 : 2009, type PCB40
or
• TCVN 4316 : 2007, type PCBBFS40
2.12
or 2.04
o ASSHTO T180 - ASSHTO T99 2.02
Optimal moisture
2.00
Vary the moisture of mixture (Aggregate + Cement) 5% 6% 7% 8% 9% 10% 11% 12% 13% 14%
Moisture
until the dry density of mixture reach highest value.
The moisture which gives the maximum dry density
Fig II.19 - The correlation between moisture and dry density
would be the optimal moisture (Fig II.18)
Table II.2
Ratio of Length to Strength Correction
Strength
Diameter (L/D) Factor correlation factor
for different
2.0 1.0
sample size
1.75 0.98
1.50 0.96
1.25 0.93
1.00 0.87
1.83
To optimise the cement content, laboratory tests are 2.00
1.19 1.43
required at different dosages e.g: 3%, 5% and 7% 1.50
1.02
(ratio of cement to aggregate on dry weight). 1.00
0.67
Based on project requirements for a targeted 0.00
After compaction of the layer, a suitable curing layer Fig II.23 - Relation between cement dosage and strength
Causes and
Chapter III:
prevention of concrete
defects
• Segregation of concrete
• Attack by fire
A correct identification of the defect and its root cause will allow the user to take
appropriate measures to avoid them in future and improve the quality and durability of
the construction.
A. Segregation of Concrete 63
Various types of segregation can occur when Causes and remedial actions:
concrete is transported, conveyed, poured and The most important causes of concrete segregation
compacted. Segregation impairs the quality and /or (which also point to the remedies) are:
appearance of concrete to varying degrees. • Too high consistency of the fresh concrete
Segregation can occur: • Excessive dosage of a superplasticizer
• between different aggregate fractions • Improper placement or compaction of the
• between aggregate and cement paste concrete (failure to use vertical pipes for
• between fines and water excessive drop heights, concrete deposit points
In practice these types of segregation cannot be spaced too far apart, excessive vibrating)
clearly distinguished. • Unsuitable concrete composition (poor grading,
insufficient cement dosage)
The most important forms of segregation: • Maximum aggregate size too large for section
• Stone pockets, or concentrations of coarse poured
aggregate in the concrete (honey-comb)
• Mixing time too short
• Local concentrations of surplus water with fine
• Leaky forms, allowing cement paste to escape
cement and aggregate particles at vertical
(sieve effect)
surfaces of forms
• Bleeding or surplus mixing water that rises to • Reinforcement too dense (sieve effect)
the surface of the concrete. Bleeding causes
irregular, powdery porous surfaces.
• Micro-segregation or separation of cement and
sand/ fines. This blemishes the appearance of
concrete surfaces
Fig III.1 - Honey comb on concrete Fig III.2 - Stone pockets formed by segregation due to excessive
drop height and/or reinforcement that is too dense
64
B. Cracking
Control of Cracking Cracks Classification
Why control the cracks in concrete? A fundamental There are many types of cracks in a concrete
requirement of any concrete structure is its structure, but they can be classified into 5 main
performance over its intended design life. Concrete types: plastic settlement, plastic shrinkage, early
must be able to withstand wear and deterioration thermal, drying shrinkage, surface crazing (Fig III.3).
given the environment and maintenance regime for
which it was designed. If a concrete structure meets 9 4
its intended design life when exposed to its 4
anticipated environment, then it can be described as 13 2 8 8
being durable. 10
3 6
Plastics Settlement
Plastics Shrinkage
Early thermal
Drying Shrinkage
Fig III.5
Plastic
Settlement cracks
Differential settlement cracks settlement
cracking
direction in
concrete
structure
Reinforcing Large aggregate
bar particles
SECTION A-A SECTION A-A
Differential
A A A settlement A
Settlement cracks
cracks
(a) (b)
66 Chapter III: Causes and prevention of concrete defects B. Cracking
Fig III.6 – Surface cracks caused by plastic shrinkage due to Fig III.7 – Extensive plastic shrinkage cracking in concrete
excessive water loss in the surface layer of the concrete
Chapter III: Causes and prevention of concrete defects B. Cracking 67
Preventive measures
• Avoid mortar-rich concrete mix (lower
sand/aggregate ratio)
• Use coarse sand, avoid very fine sand, if
possible
• Keep setting time of concrete under control
• Cure the concrete as soon as possible.
• Don’t finish concrete while bleed water
exists
• Never sprinkle or trowel dry cement or a
mixture of cement and fine sand to absorb
Fig III.9 – Typical drying-shrinkage cracks in a concrete slab
bleeding water
• Avoid overcompaction of concrete
68 Chapter III: Causes and prevention of concrete defects B. Cracking
Preventive measures
At least for reinforced concrete and larger
concrete sections, there is no way to allow the
concrete to freely shrink – cracking is
unavoidable. But by taking suitable measures,
relatively wide cracks, the damaging cracks,
can be avoided, and in their place numerous,
harmless, barely visible hairline cracks will
form. The preventive measures:
• Proper installation of shrinkage reinforcement
• Installing contraction joints in large
horizontal slabs or long walls at every 6-9m
length according to TCXDVN 313:2004 Fig III.11 - Early thermal cracking on concrete
• Optimize the w/c ratio within the range
0.40 – 0.50
• Reduce the paste volume, use larger size
aggregates Preventive measures
See chapter II.C – Mass Concrete structures
C. Carbonation and corrosion 69
of reinforcement
How does carbonation phenomenon occur?
Carbonation is a chemical reaction between the
carbon dioxide (CO2) from the air with calcium
hydroxide (Ca(OH)2) in the concrete. The process
begins on the surface of concrete and progresses
slowly toward the interior. Carbonation has a
positive influence on the concrete itself, making it
more compact.
ThờiTime
gian (năm)
(years)
Preventive measures
To prevent corrosion of reinforcement by
carbonation, the carbonation front must be
prevented from reaching the reinforcement.
This is achieved by:
Fig III.12 - Carbonation front made visible by a • Sufficient concrete cover all around the
phenolphthalein test on a cut into the concrete. The
reinforcement, generally at least 30 mm.
concrete dyed violet by phenolphthalein has not yet been
carbonated. • Good curing of the concrete, so that after
removal of formwork, the surface concrete
hydrates well and the rate of carbonation is
minimized
70
D. Degradation in seawater
environment
In seawater, concrete can be degraded by two main In presence of chlorides in the concrete, steel
attack mechanisms: reinforcement can corrode locally, even when the
• Chloride-induced corrosion of the steel concrete pH is still high (pH>12). This mechanism is
reinforcement called “pitting corrosion” (Fig III.16), which is very
different from the distributed corrosion, linked to
• Sulphate attack of the cement matrix
carbonation of concrete. This process can be
described according to the reaction:
In general, the degradation from chloride-induced
corrosion advances significantly faster than the Fe2+ + 2Cl- ---> FeCl2
sulphate attack of the cement matrix, and is the
biggest threat for concrete structures in contact The effects of chloride attack are:
with seawater. • Significant and fast reduction of the steel section
For this reason, Ordinary Portland Cement OPC with (locally)
a low C3A-content (sulfate resistant OPC according • Risk for failure of construction
TCVN 6067 or C150 – OPC type V) is not • Does not create significant cracks in concrete, so
recommended for seawater environment, as it has a it is less visible
lower chloride resistance, compared to standard
cement PCB40 (Refer Chapter 4 of ACI 201.2R-01).
1. Chloride-induced corrosion
of the steel reinforcement
Concrete in contact with sea water or close to the
sea can be damaged by attack by the chloride ions in
sea water (Fig III.15). Chloride ions can also be
introduced into concrete by the mixing water, by
contaminated aggregates (for example: marine Concrete carbonation Chloride corrosion
aggregates) or chloride-based accelerators (which (distributed corrosion) (concentrated pitting corrosion)
Fig III.15
– Corrosion of
steel
reinforcement in
concrete in sea
water
Chapter III: Causes and prevention of concrete defects D. Degradation in seawater environment 71
Chemical Reference
XA1 XA2 XA3
Characteristic test method
Ground water
SO4 -2 (mg/l) EN 196-2 ≥ 200 and ≤ 600 >600 and ≤3000 > 3000 and ≤ 6000
pH ISO 4316 ≤ 6,5 and ≥ 5,5 < 5,5 and ≤ 4,5 < 4,5 and ≥ 4,0
+ ISO 7150-1 or
NH4 (mg/l) > 15 and < 30 > 30 and < 60 > 60 and < 100
ISO 7150-2
> 3000 up to
Mg (mg/l) ISO 7980 ≥ 300 and ≤ 1000 > 1000 and < 3000
saturation
Soil
XA1 : Slightly aggressive chemical environment; XA2 : Moderately aggressive chemical environment
XA3 : Highly aggressive chemical environment
(*) : The 3000mg/kg limit shall be reduced to 2000mg/kg, where there is a risk of accumulation of sulfate ions in the
concrete due to drying and wetting cycles or capillary section
Table III.1 - Limiting value for exposure class for chemical attack from natural soil and ground water
according to standard EN-206 (attack from seawater is discussed separately)
a. Chemical decomposition:
Chemical decomposition of concrete is characterized
by the degrading of one or more constituents of
the hardened cement by external chemicals (Fig
III.17). The decomposed constituent is leached out of
the concrete. The concrete becomes gradually more acid attack
porous, loses strength, and loses protection of the
reinforcement against corrosion. The process always
begins at the interface between concrete and the
aggressive chemical, and progresses (usually slowly)
toward the concrete interior. Fig III.17 - Cement mortar prism attacked by acid
Chapter II: Applications with specific requirements E. Chemical attack 73
Fig III.18
Prefabricated
jacking pipe
elements for
waste water
tunnel
74
F. Alkali – Aggregate Reaction
Alkali-aggregate reaction is a slowly progressing
chemical reaction between certain so-called reactive Preventive measures
aggregate and alkalis that are present in the • Use a cement with low alkali content (%
concrete or that penetrate into the concrete from Na2O eq = % (Na2O + 0.658xK2O) < 0.6%)
the environment. This reaction involves swelling of • Determination of the potential reaction of
the concrete, leading ultimately to heavy cracking these aggregate, through various tests
and significant loss of strength. (chapter I). This should be done extensively
for different layers of the quarry, used at
Alkali-aggregate reaction is known in many the project.
countries. It is difficult to recognize the reaction
with certainty, partially because the processes
involved can extend over a period of time from one
year up to fourty years (Fig III.19)
Fig III.19
Heavy cracking
due to swelling
of concrete
caused by
alkali-aggregate
reaction
G. Fire Resistance 75
1. Concrete in fire
Concrete has a high resistance against fire. Even
when exposed to extremely high temperatures,
concrete emits no smoke or toxic gases. Rather,
concrete prevents fire from spreading. When fire
impacts concrete, the temperature of the concrete
increases slowly. Therefore concrete offers excellent
protection against the spread of fire, without
requiring any fire-resistance treatment. Only after
long and intensive exposure to fire, portions of the
concrete may delaminate or spall off (Fig III.20).
2. Preventive measures
Concrete offers excellent intrinsic protection against
fire and high temperatures.
Critical temperature:
Reinforced and non-reinforced concrete can
withstand temperatures up to 300°C without
damage. This critical temperature of concrete is
reached only very slowly with exposure to fire.
Studies show that it takes one hour for the critical
temperature of 300°C to penetrate 2 cm into the
concrete when the surface is exposed to a flame
temperature of 1000°C (Fig III.21). This temperature
roughly corresponds to that of a blazing wood fire or
gas flame. Under these test conditions, the critical
temperature reaches a depth of 5 cm after 2 hours.
76
Overview of cement
Chapter IV:
As worldwide there are many standards available, this overview only lists the standards that are currently
used in Vietnam.
A. Cement B. Concrete
VIETNAMESE STANDARDS – TCVN VIETNAMESE STANDARDS – TCVN
• Portland Blended Cement – Specifications • TCXDVN 374:2006
TCVN 6260 : 2009
• Portland Cement – Specifications AMERICAN STANDARDS – ASTM
TCVN 2682 : 2009
• ASTM C94
• Portland Blast Furnace Slag Cement
TCVN 4316 : 2007
EUROPEAN STANDARDS – EN
• Sulfate Resistant Portland Cement
TCVN 6067 : 2004 • EN 206-1:2000
VIETNAMESE STANDARD - TCVN
1. Composition 2. Classification
Portland blended cement is produced by Portland blended cement consists of 3 grades:
• Grinding portland clinker with a necessary PCB30, PCB40 and PCB50 with
gypsum content and mineral additives. Grinding • PCB is defined sign of portland blended cement
aid can be used in the grinding process if
• 30, 40 and 50 is the minimum compressive
necessary.
strength of standard mortar sample at 28 days in
MPa, testing method complies with TCVN 6016 :
1995 (ISO 679 : 1989)
3. Physical Specification
Compressive Strength
min 14 18 22
1 - 3 days MPa TCVN 6016:1995
min 30 40 50
- 28 days
Setting time
min 45
2 - Initial set minute TCVN 6017:1995
max 420
- Final set
Fineness
- Retained content on % max 10
3 TCVN 4030:2003
sieve 0.09mm 2800
(cm2/g) min
- Specific surface - Blaine
4. Chemical Specification
- Mineral additives
Content % max 40
2 -
- Filler Content (in % max 20
mineral additives)
1. Composition 2. Classification
Portland cement is produced by grinding portland Portland cement consists of 3 grades: PC30, PC40
clinker with a necessary gypsum content (comply and PC50 with
with TCVN 5438 : 2007). Grinding aid can be used in • PC is defined sign of portland cement
the grinding process if necessary.
• 30, 40 and 50 is the minimum compressive
strength of standard mortar sample at 28 days in
MPa, testing method complies with TCVN 6016 :
1995 (ISO 679 : 1989)
3. Physical Specification
Compressive Strength
min 16 21 25
1 - 3 days MPa TCVN 6016:1995
min 30 40 50
- 28 days
Setting time
min 45
2 - Initial set minute TCVN 6017:1995
max 375
- Final set
Fineness
- Retained content on % max 10
3 TCVN 4030:2003
sieve 0.09mm (cm2/g) min 2800
- Specific surface - Blaine
4. Chemical Specification
1. Composition 2. Classification
Portland blast furnace slag cement is produced by Portland blast furnace slag cement is classified into
• Grinding clinker portland cement with a 2 types:
necessary gypsum content and Blast Furnace • Type I: slag content is from 40 % to 60% - signed
Slag (comply with TCVN 4315 : 2007) PCBBFSI
• Or well mixing ground blast furnace slag with • Type II: slag content is from 60 % to 70% - signed
Portland Cement PCBBFSII
3. Physical Specification
Type I Type II
Test
No Characteristics Unit Requirement PCBBFS PCBBFS PCBBFS PCBBFS PCBBFS PCBBFS
Method
30 40 50 30 40 50
Compressive
Strength min TCVN 14 18 22 12 16 20
1 MPa
- 3 days min 6016:1995 30 40 50 30 40 50
- 28 days
Setting time
min TCVN 45
2 - Initial minute
max 6017:1995 10
- Final
Fineness
TCVN
3 - Specific (cm2/g) min 3300
4030:2003
surface -Blaine
TCVN
4 Soundness mm max 10
6017:1995
4. Chemical Specification
1. Composition 2. Classification
Sulfate resistant portland cement is produced by Portland cement consists of 3 grades: PCSR30, PCSR40
grinding sulfate resistant portland clinker with a and PCSR50 with
necessary gypsum content • PCSR is defined sign of sulfate resistant portland
cement
• 30, 40 and 50 is the minimum compressive
strength of standard mortar sample at 28 days in
MPa (testing method complies with TCVN 6016 :
1995)
3. Physical Specification
Compressive Strength
min 12 16 20
1 - 3 days MPa TCVN 6016:1995
min 30 40 50
- 28 days
Setting time
min 45
2 - Initial set minute TCVN 6017:1995
max 375
- Final set
Fineness
- Retained content on sieve % max 12 10 8
3 TCVN 4030:2003
0.08mm (cm2/g) min 2800 3000 3200
- Specific surface - Blaine
4. Chemical Specification
Alkali content
6 %Na2O eq = %Na2O + % max TCVN 141:2008 0.6
0.658%K2O
7 Residue insoluble % max TCVN 141:2008 1
8 BaO content % max TCVN 141:2008 1.5 – 2.5 (3)
Note 1 : (C3A) = (2.650 x %Al2O3) - (1.692 x %Fe2O3)
Note 2 : (C4AF + 2C3A) = (3.043 x %Fe2O3) + 2C3A
Note:
• Only require (1) or (2)
• (3) only require for sulfate resistant portland cement consist of BaO
Chapter IV: Overview of cement & concrete standards A. Cement/ Vietnamese standard - TCVN 81
1. Composition 2. Classification
Sulfate resistant blended portland cement is Sulfate resistant blended portland cement is
produced by grinding portland cement clinker with a classified into 2 types: PCBMSR30, PCBMSR40, PCBMSR50,
necessary gypsum content and: PCBHSR30, PCBHSR40, PCBHSR50.
• Blast furnace slag (comply with TCVN 4315 : • PCBMSR is defined sign of moderate sulfate
2007) resistant blended portland cement
• Other mineral additives (comply with TCVN 6882 • PCBHSR is defined sign of high sulfate resistant
: 2001) blended portland cement
• 30, 40 and 50 is the minimum compressive
strength of standard mortar sample at 28 days in
MPa (testing method complies with TCVN 6016)
3. Physical Specification
Level
Test
No Characteristics Unit Requirement PCBMSR PCBHSR
Method
30 40 50 30 40 50
Compressive Strength
min TCVN 18 20 22 16 18 20
1 - 3 days MPa
min 6016:1995 30 40 50 30 40 50
- 28 days
Setting time
min TCVN 45
2 - Initial set minute
max 6017:1995 375
- Final set
Fineness
% max
- Retained content on 10
TCVN
3 sieve 0.08mm
4030 :2003
- Specific surface-Blaine cm2/g min 2800
Sulfate durability
(Defined by the
expansion of mortar
bar in sulfate TCVN
4 solution): 7713 :2007
The expansion of
TCVN
5 mortar bar in water % max 0.02
6068 :2004
after 14 days
1. Composition 2. Classification
Low heat blended portland cement is produced by Low heat blended portland cement is classified into
grinding portland clinker with a necessary gypsum 2 types: PCBMH, PCBLH
content and: • PCBMH is defined sign of moderate heat of
• Blast furnace slag hydration blended portland cement, it consists:
(comply with TCVN 4315 : 2007) PCBMH30, PCBMH40
• Other mineral additives • PCBLH is defined sign of Low heat of hydration
(comply with TCVN 6882 : 2001) blended portland cement, it consists: PCBLH30,
PCBLH40
• 30 and 40 is the minimum compressive strength
of standard mortar sample at 28 days in MPa
(testing method complies with TCVN 6016)
3. Physical Specification
Level
30 40 30 40
Heat of hydration
kJ/kg max TCVN 290 (70) 250 (60)
1 - 7 days
(cal/g) max 6070:2005 335 (80) 290 (70)
- 28 days
Compressive strength
min TCVN 18 24 18 24
2 -7 days MPa
min 6016:1995 30 40 30 40
-28 days
Setting time 45
min TCVN
3 - Initial set minute
max 6017:1995 375
- Final set
Fineness
- Retained content on % max 10
TCVN
4 sieve 0.08mm
4030 :2003
- Specific surface-Blaine cm2/g min 2800
1. Composition
Blended hydraulic cement – a hydraulic cement consisting of two or more inorganic ingredients which
contribute to the strength-gaining properties of the cement, which or without other ingredients, processing
additions, and functional additions
2. Classification
No Type of Cement
Hydraulic cement for general construction.
1 Type GU
Use when one or more of the special types are not required
2 Type HE High early strength
3 Type MS Moderate sulfate resistant
4 Type HS High sulfate resistant
5 Type MH Moderate heat of hydration
6 Type LH Low heat of hydration
3. Physical Specification
1. Classification
• Portland cement – a hydraulic cement produced by pulverizing clinker consisting essentially of hydraulic
calcium silicates, usually containing one or more of the forms of calcium sulfate as an inter ground
addition.
• There are five types of portland cement in this specification.
No Type of cement
1 Type I For use when the special properties specified for any other type are not required
When air-entraining is desired, cement type IA, IIA and IIIA are specified
2. Physical specification
- 1 day - - 12 - -
ASTM
4 - 3 days 12 10 24 - 8
C109/C109M
- 7 days 19 17 - 7 15
- 28 days - - - 17 21
- Vicat test
5 ASTM C191
- Time of setting min 45 45 45 45 45
- Time of setting max 375 375 375 375 375
“-” : Not required
Chapter IV: Overview of cement & concrete standards A. Cement/ American standard - ASTM 85
3. Chemical specification
4 - When (C3A) is 8% or less % max ASTM C563 3.0 3.0 3.5 2.3 2.3
5 Loss on ignition % max ASTM C114 3.0 3.0 3.0 2.5 3.0
(C4AF+2(C3A))content or
10 % max ASTM C114 - - - - 25
(C4AF+C2F), as applicable
86 Chapter IV: Overview of cement & concrete standards A. Cement/ European standard - EN
EUROPEAN STANDARD – EN
1. Composition 2. Classification:
Depend on type of cement, which cement comply Standard strength :
with EN standard can consist of different main • There are 3 classes of standard strength at 28
constituents as: days: class 32,5 class 42,5 and class 52,5.
• Portland cement clinker
• Three early strength classes are provided for
• Blast furnace slag
each class of standard strength.
• Pozzolan
- Class with ordinary early strength, indicated by N.
• Fly ash
- Class with high early strength, indicated by R.
• Burnt shale
- Class with low early strength, indicated by L.
• Limestone
• Silica fume
Beside the minor additional constituents can be
used to improve the physical properties of the
cement.
3. Physical Specification
Requirements
Test Cement
No Characteristics Strength class
methods Type (1)
32.5N 32.5R 32.5L* 42.5N 42.5R 42.5L* 52.5N 52.5R 52.5L*
2
- ≥ 10.0 - ≥ 10.0 ≥ 20.0 - ≥ 20.0 ≥ 30.0 ≥ 10.0
Early strength days
(MPa) 7
≥ 16.0 - ≥ 12.0 - - ≥ 16.0 - - -
1 days EN 196-1 All
Soundness /Expansion
3 EN 196-3 All ≤ 10
(mm)
EN 196-8
at 7 days
4 Heat of hydration(J/g) LH ≤ 270
EN 196-9
at 41 h
(1): Types of cement were given below about the composition of each of the 27 products in the family of common cements
(*): Strength class only defined for CEM III cements.
Chapter IV: Overview of cement & concrete standards A. Cement/ European standard - EN 87
4. Chemical Specification
Requirements
Cement
No Characteristics Test reference Strength class
type
32.5N 32.5R 42.5N 42.5R 52.5N 52.5R
Loss on ignition CEM I
1 EN 196-2 ≤ 5%
(% by mass) CEM III
Insoluble residue CEM I
2 EN 196-2 ≤ 5%
(% by mass) CEM III
CEM I
CEM II (1)
Sulfate content ≤ 3.5% ≤ 4.0%
3 EN 196-2 CEM IV
(as %SO3 by mass)
CEM V
CEM III (2) ≤ 4.0%
Chloride content
4 EN 196-2 All (3) ≤ 0.1% (4)
(% by mass)
5 Pozzolanicity EN 196-5 CEM IV Satisfies the test
(1)
Cement type CEM II/B-T may containt up to 4.5 % sulfate for all strength classes.
(2)
Cement type CEM III/C may containt up to 4.5% sulfate.
(3)
Cement type CEM III may containt more than 0.1 % chloride but in that case the maximum chloride content
shall be stated on the packaging and/or the delivery note.
(4)
For pre-stressing applications cements may be produced according to a lower requirement. If so, the value
of 0.1% shall be replaced by this lower value which shall be stated in the delivery note.
88 Chapter IV: Overview of cement & concrete standards A. Cement/ European standard - EN
Main constituents
Minor additional
constituents
(types of common cement) Silica
Main types
Natural
Natural Siliceous Calcareous
calcined
K S DM P Q V W T L LL
Portland
CEM I
Portland-
silicafume CEM II/A-D 90-94 - 6-10 - - - - - - - 0-5
cement
Blast furnace
CEM III/B 20-34 66-80 - - - - - - - - 0-5
cement
CEM III/C 5-19 81-95 - - - - - - - - 0-5
Pozzolanic
cement (c)
CEM IV/B 45-64 - <------------------ 36-55 -----------------> - - - 0-5
Composite
cement (c)
CEM V/B 20-38 31-50 - <---------- 31-49 ----------> - - - - 0-5
(a)
:The values in the table refer to the sum of the main and minor additional constituents.
(b)
:The proportion of silica fume is limited to 10 %
(c)
:In portland-composite cement CEM II/A-M and CEM II/B-M, in pozzolanic cement CEM IV/A and CEM IV/B and in composite cements CEM
V/A and CEM V/B the main constituents other than clinker shall be declared by designation of the cement.
B. Concrete 89
VIETNAMESE STANDARD - TCVN
I. Workability
• Designed Grade: M100, M150, M200, M250, M300, M400, M500, M600 (if higher strength of construction
is required, higher design grade (Ex: M700, M800) is accepted.)
3. Assessment
• Concrete which is considered to meet the required grade of concrete (M) must satisfy 2 below conditions:
• The mean compressive strength of one set (3 samples) is not less than designed grade of concrete
• Strength of each sample in set is not less than 85% designed grade of concrete
• Concrete which is considered to meet the required class of concrete (B) must satisfy 2 below conditions
at once:
• With the initial period or without standard deviation:
- The mean compressive strength of one set (3 samples) is not less than 1.3 times designed
class of concrete (MPa)
- Strength of each sample in set is not less than 1.1 times designed class of concrete (MPa)
Due to variations in materials, operations, and testing, the average strength necessary to meet these
requirements will be substantially higher than the specified strength. This higher strength amount depends
upon the standard deviation of the test results and the accuracy with which that value can be estimated
from prior data as explained in ACI 318 and ACI 301.
Appendix part of this standard give the guide to calculate the average strength, necessary to meet the
specification:
With:
• f ‘c = the specified compressive strength
• f ‘cr = the required average compressive strength
• s = the standard deviation
(*): Formula to achieve the satisfactory average of three consecutive strength tests.
(**), (***): Formulas for the minimum strength test result of an individual strength test (average of two
cylinders test) result.
92 Chapter IV: Overview of cement & concrete standards B. Concrete/ American standard - ASTM C94
B. When a new mix design or strength level and no standard deviation data is available. Required average
strength for mix design
Bold numbers identify levels of specified strength where the standard deviation should be considered
unusual or inappropriate.
The average of 3 consecutive strength tests shall be equal to or greater than specific strength – f 'c
- If f 'c < 35 MPa: individual strength test ( average of two cylinder tests) ≥ f'c-3.5(MPa)
- If f 'c > 35 MPa: individual strength test (average of two cylinder tests) ≥ 0.9f 'c
Chapter IV: Overview of cement & concrete standards B. Concrete/ European standard - EN 206-1:2000 93
I. Workability
Workability Test methods Requirement
Slump EN 12350-2 ≥ 10 mm and ≤ 210mm
Vebe EN 12350-3 ≤ 30 sec and > 5sec
Degree of compactability EN 12350-4 ≥ 1.04 and < 1.46
Flow table EN 12350-5 > 340mm and ≤ 620mm
Note: the classes of consistence in Tables 1 to 4 are not directly related. In special cases, consistence may also be
specified by target value. For earth moist concrete, i.e concrete with low water content designed to be
compacted in special processes, the consistence is not classified.
Table 4:
Table 1: Table 2: Table 3: Flow diameter in mm
Slump classes Vebe classes Compaction classes Flow diameter
Class
in mm
The consistence may be specified either by reference to a consistence class according to table 1, 2,3 and 4 or,
in special cases, by a target value. For target values, the related tolerances are given in table 5.
The compressive strength is determined on specimens tested at 28 days. For particular uses, it may be
necessary to specify the compressive strength at ages earlier or later than 28 days or after storage under
special conditions.
The characteristic strength of concrete shall be equal to or greater than the minimum characteristic
compressive strength for the specified compressive strength class, see tables below.
• Strength assessment
From December 2003, the standards BS-EN 206-1 and BS 8500 replace the BS 5328 series of standards.
However, some projects in Vietnam still refer to BS 5328, to specify concrete.
I. Workability
• Guidance on the workability appropriate to different uses
Strip footings
Mass concrete foundations
Blinding
Normal reinforced concrete in slabs,
Poker or beam vibration
beam, walls and columns Medium 75
and/ or tamping
Sliding formwork construction
Pumped concrete
Vacuum processed concrete
Domestic general purpose concrete
Trench fill
Self-weight compaction
In situ piling
High 125
Concrete sections containing
Poker
congested reinforcement
Diaphragm walling
self-levelling super plasticized Self-levelling Very high See NOTE 2
concrete
(1) Cohesive mixes may give adequate place ability at lower values of slump than those given here.
NOTE 1. In the "very low" category of workability where strict control is necessary, e.g. pavement quality
concrete placed by "trains", measurement of workability by determination of compacting factor or Vebe
time (see BS 1881:parts 103 and 104) will be more appropriate than slump.
NOTE2. In the "very high" category of workability, measurement and control of workability by
determination of flow is appropriate (see BS 1881: part 105).
96 Chapter IV: Overview of cement & concrete standards B. Concrete/ British standard - BS 5328
C7.5 7.5
C10 10
C15 15
C20 20
C25 25
C30 30
C35 35
C40 40
C45 45
C50 50
C55 55
C60 60
• Strength assessment
Criteria 1 Criteria 2
Average strength of
Specified grade Group of samples Any individual test
samples,
result, f (MPa)
favg (MPa)
First 2 samples
favg ≥ fck + 1 f ≥ fck - 3
First 3 samples
C20 to above favg ≥ fck + 2 f ≥ fck - 3
Any 4 consecutive
favg ≥ fck + 3 f ≥ fck - 3
samples
First 2 samples
favg ≥ fck f ≥ fck - 2
First 3 samples
C7.5 to C15 favg ≥ fck + 1 f ≥ fck - 2
Any 4 consecutive
favg ≥ fck + 2 f ≥ fck - 2
samples
Minimum cement
300 320 340
content (kg/m3)
XS1 - Exposure to airborne salt but not in direct contact with sea water
XS2 - Permanently submerged
XS3 - Tidal, splash and spray zones
Minimum cement
300 320 360
content (kg/m3)
ASTM C115
Fineness TCVN 4030:2003 -
ASTM C204
EN 196-8
Heat of hydration TCVN 6070: 2005 ASTM C186
EN 196-9
Chemical analysis TCVN 141: 2008 ASTM C114 EN 196-2
Water
Specific requirement: TCXDVN 302:2004, ASTM C1602
Admixture
Specific requirement: TCVN 8826:2011, ASTM C494
Aggregate
Specific requirement: TCVN 7570: 2006, ASTM C33
Test methods
Coarse aggregate
Grading TCVN 7572-2:2006 ASTM C136
Specific gravity TCVN 7572-4:2006 ASTM C127
Bulk density and moisture content TCVN 7572-6:2006 ASTM C29
Elongation and flakiness index TCVN 7572-13:2006 -
Cement & Concrete Reference 99
B. Concrete
Specification for ready-mix concrete: TCXDVN 374:2006, ASTM C94, EN 206-1:2000
Test Methods
Fresh concrete
Hardened concrete
ASSHTO T180
Optimal moisture& max dry density 22 TCN 333-06 -
ASSHTO T99
ASTM D1632
Making compressive strength sample 22 TCN 246 -
ASTM D55
E. Source of figures
Figure number Source
Figure: Fig I.1, Fig I.2, Fig I.3, Fig I.5, Fig I.6, Fig I.7, Fig I.9, Fig I.11, Fig I.12, Fig I.13, Holcim Vietnam
Fig I.15, Fig I.16, Fig I.21, Fig I.22, Fig I.23, Fig I.24, Fig I.25, Fig I.26, Fig I.27, Fig I.30,
Fig I.31, Fig I.32, Fig I.33, Fig I.34, Fig I.35, Fig I.36, Fig I.37, Fig I.38, Fig I.39, Fig I.40,
Fig I.41, Fig I.42, Fig I.43,Fig I.44, Fig I.45, Fig I.46, Fig I.47, Fig I.48, Fig I.49, Fig I.50,
Fig I.51, Fig I.52, Fig I.53, Fig I.55, Fig I.56, Fig I.58, Fig I.60, Fig I.61, Fig I.62, Fig II.1,
Fig II.2, Fig II.3, Fig II.4, Fig II.5, Fig II.6, Fig II.7, Fig II.8, Fig II.9, Fig II.10, Fig II.11, Fig II.12,
Fig II.13, Fig II.14, Fig II.15, Fig II.16, Fig II.17, Fig II.18, Fig II.19, Fig II.20, Fig II.21, Fig II.22,
Fig II.23, Fig III.1, Fig III.3, Fig III.4, Fig III.5, Fig III.6, Fig III.7, Fig III.8, Fig III.9, Fig III.10,
Fig III.11, Fig III.14, Fig III.15, Fig III.16, Fig III.18
Fig I.4, Fig I.8, Fig I.10, Fig I.65, Fig III.17 Holcim Swiss
Fig I.14, Fig I.17, Fig I.18, Fig I.19, Fig I.20, Fig I.28, Fig I.29, Fig I.63, Fig I.64, Fig I.66, Fig Holcim Sri Lanka
I.67, Fig I.68, Fig I.69, Fig I.70, Fig I.71, Fig I.72, Fig I.73, Fig I.74, Fig III.2, Fig III.12, Fig
III.13, Fig III.20, Fig III.21
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