(19) FEARRMEBRMRP [51] Int. cl. (CO7D 317/34 (2006.01 ) a or 07D 319/04 006,01 ) “se 12] AeA fl iB 2S Ahk ae tone * [21] IRS 200910061436.0 * (81 AFA 200949 119 [11] A9FS CN 1015253294 (22) sik 2009.4.3 (74) enue BEACTR LA Me AURA RS [21] #183 200910061436. 0 co) In] Bina ROLLE RRA fT seit 430074 st aR AL ME ls EAE A 693 & SRIRAM TE IE ATR BH ES (72) SARA EMAL UR Hh ee ABT MS [54] smn 2a EL EH re (57) $538 ARB Bt Fa FD PRE BE DEORE SET i AE Ta TTS FUR A OTE, Sire 4 - FEE - 1, 3 - SR BRIS -¥2HE-1, 3- AACA, Ria SAU BIA TT PARE. RAN LATTE A FAB BRB 4 HD TR oh TL Ea AE BE, HEAR) 79% -95%, CHE 63% -93%, 7 RELBE 99%.200910061436. 0 RAB K FH RAK 1, Sah PARRA MATE, FORMETET: Hn S 30~36wt?s FRR AEE LaA ROPER, MiG BOONE A 47S AAE-1, 3- RA beM 5-7-1, 3-— AAO NIEAD, AR BL Bo i Hah 2, HUEDAIEER 1 PHAM ART, FORME: Aly A LA RR. 3, PUERABER 2AM SRIE, MEET: AURA PR. CR, RMR. ROM, FMUBRA AC1.. H2SO4. HsPO, A/2% H2SO3- 4, AGRA EER 1 2 PRM GRATE, REEF: BRA RMVZE 90°C BI 150°C FHT. 5, ARAAIER 1 BR 2 ARATE, ERE PE Ts rH nh PEL RAR Lh 0.9: LI~1: 0.9. 6. AREAL BOR 1 Bk 2 ARMM AT, HAPEET: ARMA ROEM AE 2 Bs bit.200910061436. 0 ie a1/smt Err gE A BOT BRR KARA RW PRES RITE. BREA PH PREARAMEA EH, AA RET. MRM, wba AM FERPA. SORA E MOE, ZEB pA 5 EVA aS. EShET EtHes 70 FARR FEZ, (Mreck Index) ELSE 25 RAR. HE PARR] Tne, CIRM. ET TAL. AR, PI Pie RET, RENAE TAME, ARMA DM. 1996 ERMA (CPA RED PUR T HN PERE, 2000 FEAR CHE BHD TR T ERE. FRA EAA TERA EPR, BBR AMA, sePiBEO, ACHE EH (1700 TWKg), FAT ARM MSN. RAZ-TRUEAR. SHOU APH FMMALARE TELS ACRHET RHA Bi WAN. APP, TTA, MRAM. BERRA PBA, AP GPRARN AR, BRA AMRE. HARE. BORA. eee ORR SAHARRE MESS OANAREMNEARNRARE. RARSAMNBA BA, AACR BOE RR, TARE RN RAE. PRE AMI BLT, ABT SWART SAREE, WAR ABT SENN RH AEB 7. Blk, Me ARLE, WH SR —RER. EAE SPACE RA, PSE GR, WL EAS Bene TE HARSE Lh, GUTOR SEM WS, FERS SS TR, BORER T BF PAIL RR LE FR CRIES RE AMR: WL SRE NAIL 2 REY ON AR (1D) WSF RE A BUS BRER: H.Hibbert #1 N.M.Carter AZ [J] J.Am.Chem.Soc, 1928, 50: 3120-3127 POTS T Hh PAREN eS RA, A AB LRH. (2) DS REAREA RMA: P.Gimeno AE [P] Span: 475,852, 1979 PPR T HY FAMNA REA, PRR RAE. SRA BUS, ROT AP IA, STE, (BURP200910061436. 0 RoW heaKe HR. KEE. URS ROR, RUS OM. KEE wm EHO, RMNMRK. FATT RRR, ROTMRK. WARP WR, GPA, ARR OO Ba 78 0 PA ES ame. BUA ARR MEERA DRA LAA REAM RL, TEMECULA A, RRR SEPA A SIE oe A ET RE ROT, FERRE ERA: E'S 30~3Owts PREAH BL TERETE FSP AER 4-78 SE L, 3- SU EA SHEL, AAA, PRA AS BUD A EB EE PREGA A ALAR TC, AUR: AR. CR PR. AZ RAV RR @, BTALUUR A: HCI, HySO,, HsPO, Fil/sk HySOs ‘FRSA ALI JRE TE 90°C BI 150°C FEAT. BARS FMRI 0.9: Li~l: 0.9. FRO ALATA ZE 2 BIS NET. SRB LAR AT RE A HA BH TE, CI) 19% -95%) HLH 63% 93%» FARLLLE 99%. FRE AS SEI: owtss AREA MCATH a CREATE RARACEL Le 1) HRA. LL SOW SEM HE Heil, BLY Be ANSE MEY 1Mo, Ze OCR AE RMT RAG S AN, ASTRAL PS EE CAEP FE BEAL, 3ST 60%, S-EME-1, 3-— APPL NEL I 40%), TEE 99.2%. BALI 93.2%. HLA 88.9%, AHEM 95.4%, Whe 190-196°C. SIS: S0wt%e PRAM Hn CHAU ETM AR EG 1: 1.05) RA, DSRBR HEFL FR RSC RAY 1% ZE OCA REM RIM ST, ASB ih TRE GE 1B FBP MEL, 3- SUR UTA 60%, SHEM-1, 3-— AER EH 40%), PH RUAE 99.4% HAGA 94.2%. WLR 89.8%. BEAFHE 95.3%, ha 190-196°C. SEA: 350i REMC H ah (PREAH MEARE 1: 0.95) WBA, LPR HEL, Fl, FBR AE AA 1% 0» FE 150°C Set FAA AY RIS 2 vit, RRA et th CH 4 FRE, 3 FUR RLM 60%, SHRI, 3- RE 40%), PAE 99.0%, BAGH 80.4%. WO 72.7%. HEFEE 90.49%) THAT 190-196C SOND, 33we2s FRSA AR HE CAS ATE HAAR AR UG 1: 0.98) WEE, WARMER ANTHEM Fil, FAB RE BY 1%, $E 120°C A FRA LY 3 A, ARRAS BL a CHOP 4B AME, 3-H 60%, SABE, SPAM 40%), PEAS200910061436. 0 BW Ra/sHE 99.2%. FEAL 95.4%, WL 93.0%, MEFEYE 97.5%) BEAK 190-196°C. SELL: 36wt?s AREAS HI CPR BEAR EG 1: 1) YEE, DA HPO, 9 HEAL, ABA RMB RN 1M, 4 120CKH FARE RN 3 Nit, AEB abe ae CE *P 4 FSHUEL-1, 3-— ER UELI A 60%, SISHE-1, 3-— AREA 40%), PALAU 99.3%, HEIL 91.3%. WOR 86.9%, BEFETE 95.2%, WHAT 190-196°C. SEBIZ\: 30wes AREA H th CREATED MRAR LE 1: 1) TRA, DORAL, AEA RNB RAY 1%, HE 120CKH FARES RM 3 Nt, AGE a PARE CL FA FRIPAE-1, 3-H REL I 60%, S-FEIE-1, 3-— SIREN 40%), FARA 99.4%, FAG 91.1%. WOR 81.4%, BERLE 89.4%, HEA 190-196°C. Seb: 35 wis FREAD ET CP RRAVH MW ABZR EG 1: 1) RA, DZ AEA, FE REY 1%0, FE 120°C AE RBM RE 3 AN, ARR I ih Eh ik PRE CE HH ASE FRAE-1, 3-— IRIEL I 60%, SFEE-L, 3-H LHI 40%), PHL 99.2%. FILA 79.6%. WA 63.1%, WEFELE 79.3%, BBA 190-196°C. SEAL: 36we% RK ERAT Hh CARRERE ABR EG 1: DRA, BURZI, FARA RAB BN 1%, ZE 120°C RRM RW 3 ANT, REUSE ab Eh PERE CHE 5 4 FR AAE-1, 3- SU Mee 60%, S-FBAE-1, 3-— AURAL 40%), 7 ARAEAE 99.1%, FER 79.9%. WHE 73.2%. HEFELE 89.4%, HAR 190-196°C.