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1
B.Tech. II (CH), Semester – III L T P C
PRACTICALS:
1. Separation of SO42- from NO3- by BaSO4 precipitation.
2. Determination of total dissolved solids in a given water sample by Conductometric method.
3. Separation of Cu2+ from Ni2+ by Electrodeposition.
4. Spectrophotometric analysis of any two important impurities of water like Ca2+, Mg2+, Fe2+, NO3- ,
NO2-, PO4-3, CO3-2, Cl-, SO4-2
5. Organic spotting of Salicylic acid, Naphthalene, Aniline, Glycerol etc.
6. Electrogravimetric analysis of Cu in Non-ferrous alloys like brass.
7. Estimation of HCl and HAc using Conductometric acid – base titration.
8. Coulometric titration of As2O3 by Internal generation of I2.
9. Separation of Amino acids by Paper Chromatography.
10. To determine the specific rotation of given substance using different concentration of sucrose.
BOOKS RECOMMENDED:
1. Chawla S., “Text Book of Engineering Chemistry”, Dhanpat Rai & Co. Pvt. Ltd., Delhi, 2003.
2. Sharma B. K., “Engineering Chemistry”, Krishna Prakashan Media (P) Ltd, Meerut.,2001
3. Ewing G. W., “Instrumental Methods of Chemical Analysis”, Tata-McGraw Hill., New Delhi, 2001.
4. Khopkar S. M., “Basis Concept of Analytical Chemistry”, New Age International Publishers, 1998.
5. Vogel A. I., “A Text Book of Quantitative Chemical Analysis”, ELBS UK, 5th Edition, 1996.
6. Billmeyer F. W., “A Text Book of Polymer Science”, Wiley Interscience, New York, 3rd ed., 1984.
2
B. Tech. II (CH), Semester - III L T P C
BOOKS RECOMMENDED :
1. Kreyszing E., “Advanced Engineering Mathematics”, John Wiley & Sons, Singapore, Int. Student Ed. 1995.
2. Wiley C. R., “Advanced Engineering Mathematics”, McGraw Hill Inc., New York Ed. 1993.
3. O’Neel Peter., “Advanced Engg. Mathematics”, Thompson, Singapore, Ind. Ed. 2002.
4. Greenbar Michael D., “Advanced Engg. Mathematics”, Pearson, Singapore, Ind. Ed. 2007.
5. Ramana D. V., “Higher Engg. Mathematics”, The MaGraw-Hill Inc., New Delhi, 2007.
3
B. Tech. – II (CH), Semester - III L T P C
PRACTICALS
1. Tension Test on MS and CI specimens
2. Torsion Test on MS Specimen
3. Charpy Impact Test
4. Transverse Test on Wooden beam
5. Spring Test
6. Compression test on CI Columns
7. Shear Strength Test
8. Hardness Test
BOOKS RECOMMENDED:
1. Timoshenko S & Young D H “Elements of Strength of Materials”, Tata Mc Graw Hill, New Delhi, 2006.
2. Ryder G H, “Strength of Material”, English Language Book Society, New Delhi,2006
3. Bhavikatti S S “Strength of Materials”, Vikas Publication House, New Delhi,2007
nd
4. Egar P. Popov & Toader A . Balan “Engineering Mechanics of Solids” 2 Edition, Prentice Hall of India
Pvt Ltd, New Delhi,2002
5. Beer F. P. & Johnston S J, “Strength of Materials” Tata Mc Graw Hill Publication, New Delhi,2004
4
B.Tech. II (CH), Semester – III L T P C
Crystalline and non-crystalline ceramic systems, Glass and porcelain enamels, Cement refractories, Ceramics.
BOOKS RECOMMENDED:
1. ZasterZebski D., “Nature and Properties of Engineering Materials”, John Wiely & Sons, 2nd Edition, 1976.
2. Rumford F., “Chemical Engineering Materials”, Constable and Company Limited, 2nd Edition, 1987.
3. Vlack V., ‘Elements of Material Science & Engineering Structures, Properties and Performance’, Wesley
Publishing Company, 2nd Edition, 1964.
4. Chaudhry H., ‘Chemical Engineering Materials’ Indian Book Distributing Company, 2nd Edition, Delhi, 1982.
5. Lee and Evans, ‘Selecting Engineering Materials for Chemical and Process Plants’, Business Works, 1978.
5
B.Tech. II (CH), Semester-III L T P C
• NITRATION (5 Hours)
Definition & scope of nitration reactions, Nitrating agents, Aromatic Nitration (schimid and Biazz;
nitrators)mixed acid for nitration, D.V.S. value and nitric reaction, Comparison of batch Vs. Cont. nitration,
Mfg. of Nitrobenzene, Dinitrobenzene, O-and P-Chloronitrobenzene.
• HALOGENATION (6 Hours)
Definition and scope of various halogenation reactions, Halogenating agents Industrial halogenation with
types of equipment’s and its materials M/c. MFG. of Chlorobenzene, Benzene hexa-chloride and vinyl
chloride from Ethylene and Acetylene.
• OXIDATION (5 Hours)
Definition and Types, Oxidizing agents, Liquid phase oxidation with oxidizing agents and oxygen. Oxidation
of toluene with MnO2. Mfg. of Acetaldehyde from Acetic acid and mfg. of Acetic acid from Ethanol. Vapor
phase oxidation of Methanol, Benzene and Naphthalene, Apparatus and its M/s. for oxidation reactions.
• HYDROGENATION (5 Hours)
Definition and its scope, properties of hydrogen and sources of hydrogen, gas catalytic hydrogenation and
hydrogenolysis, factors affecting it, Apparatus and M/c., Industrial hydrogenation of fat & oil, Mfg. of
Methanol from CO2 & H2.
• HYDROLYSIS (3 Hours)
Definition and types of hydrolysis, Hydrolyzing agents, equipment’s of hydrolysis, Industrial Hydrolysis of
fat, hydrolysis of carbohydrates, starch to dextrose, Mfg. of ethanol from ethylene (shell process) Mfg. of
phenol from benzene sulfonic.
• POLYMERIZATION (5 Hours)
Introduction & chemistry of polymerization reactions, classifications of polymers methods of polymerization.
(Total contact time : 45 Hours)
BOOKS RECOMMENDED:
1. Groggins P. H., “Unit Processing of Organic Synthesis”, 5th edition, Tata-McGraw Hill, New Delhi, 2001.
2. Gopalarao. M. & Sitting M., “Dryden’s Outlines of Chemical Tech.”, 2nd Ed., East-West Pub., New Delhi,
1997.
3. Austin G. T., “Shreve’s Chemical Process Industries”, 5th Ed. McGraw-Hill Pub., 1994.
4. Felder R.M., Rousseau R.W., "Elementary Principles of Chemical Processes", 3rd ed., John Wiley, New
York, 2000.
5. Kent J.A., “Riggel’s Handbook of Industrial Chemistry”, Van Nostrant Reinhold, 1974.
6
B.Tech. II (CH), Semester – IV L T P C
• SYNCHRONOUS-MACHINE (07Hours)
Construction and basic principals, EMF equation, Synchronous speed, armature reaction, synchronous
reactance, voltage regulation, vector diagram for generating and motoring modes, synchronous motor
starting, Synchronous condensers.
PRACTICALS:
1. Speed control of D.C. shunt motor.
2. Speed –Torque Characteristics of D.C. Shunt motor.
3. D.C. Series motor N.T. characteristics.
4. D.C. Generator Characteristics.
5. Efficiency and regulation of 1 phase Transformer from O.C. and S.C. test .
6. Load test on Induction motor.
7. Circle –diagram.
8. Regulation of an alternator by synchronous impedance method.
9. V and inverted V curve .
10. Calibration of single phase energy meter.
BOOKS RECOMMENDED:
1 Mehta, V.K.,“Principles of Power System” S. Chand & Co., New Delhi, 2005
2 Husain A., “Fundamentals of Electrical Engineering”, Dhanpat Rai & Co., Delhi, 2001
3. Bimbhra P.S., “Electrical machinery” ,Khanna Pub.,Delhi,1998
4. Mukherjee P.K., Chakravorti S. ,“Electrical Machines” Dhanpat Rai & Co., Delhi, 2001
5. Thereja B.L., & Thereja A.K., “A Text Book of Electrical Technology”, S. Chand & Co., New Delhi, 2005
7
B.Tech. II (CH), Semester – IV L T P C
PRACTICALS:
1. Rate determination of chemical reactions.
2. Conductometric rate determination of esterification reaction.
3. Potentiometric estimation of Cu+2 by titration with EDTA.
4. Photometric estimation of Ti.
5. Estimation of Cu+2 by iodimetric titration.
6. Viscosity measurement.
7. Study of Corrosion of Steel at different concentration of Sulfuric Acid OR
Study of effect of inhibitors on corrosion of steel in sulphuric acid.
8. Demo: 1. Effects of removal of DO on corrosion.
9. Demo: 2. Anodic protection of steel in sulphuric acid.
BOOKS RECOMMENDED:
1. Atkins P. & de Paula J., “Physical chemistry”, Oxford University Press, UK, 2002.
2. Chawla S., “Text Book of Engineering Chemistry”, Dhanpat Rai & Co., Delhi, 2003.
3. Dara S. S., “A Text Book of Enginering Chemistry”, S Chand & Sons., New Delhi, 2004.
4. Fontana M. G., “Corrosion Engineering”., Tata-McGraw Hill, New Delhi,1988.
5. Skoog, West & Holler,“Analytical Chemistry: An Introduction”, 6th edition, Saunders College Publishing,
1994.
8
B. Tech. II (CH) Semester-IV L T P C
THEORY OF MACHINES:
• GEARS (05Hours)
Different Types of Motion Transmitting Elements, Advantages and Disadvantages, Types of Gears and
Gear trains, Gear Terminology and classification.
MACHINE DESIGN:
• DESIGN PROCESS, MATERIAL SELECTION, FACTOR OF SAFETY, FAILURES & THEIR CAUSES
(07 Hours)
Introduction, Types of Load, Design Process, Material Selection, Factor of Safety, Failure and Their
Causes, Introduction to Corrosion (Design Aspect).
PRACTICALS:
Design and Drawing of various machine elements using conventional methods and few drawing sheets will
be prepared using CAD software.
BOOKS RECOMMENDED:
1. Rattan, S.S.: Theory of Machines, Tata McGraw-Hill Publishing Co. Ltd., New Delhi, 1984.
2. Rao, J.S., and Dukkipati, R.V.: Mechanism and Machine Theory, Wiley Eastern Ltd., 1992.
3. Green, W.G.: Theory of Machines, 2nd Ed., Balckie, London, 1992.
4. Bhandari, V.B.: Design of Machine Elements, Tata McGraw-Hill Publishing Co. Ltd., 1984.
5. Shigley, J.: Mechanical Engineering Design, McGraw Hill Book Co., 1989.
9
B.Tech. II (CH), Semester-IV L T P C
PRACTICALS
1. Preparation of Boric acid by acidified solution of Borax (Na2B4O7).
2. Preparation of CaCl2 from HCl and lime (CaCO3).
3. Preparation of detergent.
4. Preparation of nitro naphthalene from given chemicals.
5. Preparation of polystyrene from styrene monomer.
6. Preparation of Potash alum from Aluminium Sulphate and Potassium sulphate.
7. Preparation of soap from KOH and coconut oil
8. Determination of the kinematic viscosity of given oil sample using Engler viscometer& Red Wood
Viscometer.
9. Determination of the aniline point of diesel using proper instruments.
10. Determination of the smoke point of kerosene and diesel.
11. Measurement of the softening point of grease sample.
12. Determination of the penetration index using pentrometer.
13. Determination of flash point and fire point of kerosene using Pensky Martin apparatus.
14. ASTM Distillation of gasoline.
BOOKS RECOMMENDED:
1. Austin G. T., “Shreve’s Chemical Process Industries”, 5th Ed. McGraw-Hill Pub., 1994.
2. Gopalarao M. & Sitting M., “Dryden’s Outlines of Chemical Tech.”, 2nd Ed., East-West Pub., New
Delhi,1997
3. Rao B.K.B., “Modern Petroleum Refining Processes”, 4th ed.,Oxford & IBH Publishing Co. Pvt. Ltd., New
Delhi, 2002.
4. Nelson, W.L., “Petroleum Refinry Engineering”, 4th ed. (International student edition), McGraw-Hill
Kogakusha, Ltd., Tokyo, 1958.
5. Mall I.D., “Petrochemicals Process Technology”, Macmillan India Ltd, New Delhi, 2006.
10
B.Tech. II (CH), Semester-IV L T P C
• INTRODUCTION (4 Hours)
Dimension and Units, Fundamental and derived quantities, Mathematical techniques in chemical
engineering.
• BASIC CHEMICAL CALCULATIONS (6 Hours)
Gas laws and phase equilibria, Humidity, saturation and crystallization.
• COMBUSTION (8 Hours)
Combustion and chemical processes.
• MATERIAL BALANCE (9 Hours)
Material balances involving recycle, bypass and purge systems.
• THERMOPHYSICS (8 Hours)
Heat capacity calculations. Enthalpy changes of reactions, dissolution and laws of thermochemistry. Effect
of pressure and temperature on heat of reactions.
• MATERIAL AND ENERGY BALANCE (10 Hours)
Combined material and energy balances for single stage processes. Material and energy balance calculations for
industrial processes.
(Total Contact Hours: 45)
BOOKS RECOMMENDED:
1. Bhatt B.I. & Vora S.M., "Stoichiometry”, 4th Ed., Tata-McGraw-Hill, New Delhi, 2004
2. Hougen O.A., Watson K.M. & Ragatz R.A., “Chemical Process Principals: Part-I”, 2nd Ed., CBS Publishers and
Distributors, New Delhi, 1995.
3. Himmelblau D.M., “Basics Principles and Calculations in Chemical Engineering” 6th Ed., Prentice-Hall India,1996.
4. Whitwell J.C. & Jone R.K., “Conservation of Mass and Energy”, McGraw-Hill, Singapore, 1973.
5. Process Calculation for Chemical Engineering, Second Revised Edition, Chemical Engineering Education
Development Centre, I.I.T., Madras, 1981.
11
B.TECH.-III (CHEMICAL) 5th SEMESTER SCHEME FOR TEACHING AND EXAMINATION
CS: Core Subject EIS: Elective Interdisciplinary Subject
ES: Elective Subject (from Department) IS: Interdisciplinary Subject
Teaching Scheme Examination Scheme
Sr. Hours per Week Theory Practicals Total
Course Code Credits
No. Sess End Sess End Marks
L Tu Pr Hr Tu
ional Sem ional Sem
1 Chemical Engineering
Thermodynamics-I CH 301 4 3 1 0 2 50 25 50 --- --- 125
(CS-1)
2 Heat Transfer
Operations CH 303 5 3 1 2 2 50 25 50 20 30 175
(CS-2)
3 Mass Transfer
Operations-I CH 305 5 3 1 2 2 50 25 50 20 30 175
(CS-3)
4 Mechanical
Operations CH 307 5 3 1 2 2 50 25 50 20 30 175
(CS-4)
5 EIS-1* 3 3 0 0 2 50 --- 50 --- --- 100
TOTAL 22 15 4 6 250 100 250 60 90 750
Total contact hours per week = 25 Total Credit = 22 Total marks = 750
1
B.Tech.-IV (CHEMICAL) 7th SEMESTER SCHEME FOR TEACHING AND EXAMINATION
CS: Core Subject ES: Elective Subject (from Department)
Teaching
Examination Scheme
Scheme
Sr. Hours per Total
Course Code Credits Theory Practicals
No. Week Marks
Sess End Sess End
L Tu Pr Hr Tu
ional Sem ional Sem
Chemical Reaction
1 Engineering-II CH 401 3 3 0 0 2 50 --- 50 --- --- 100
(CS-1)
2 Instrumentation and
Process Control CH 403 5 3 1 2 2 50 25 50 20 30 175
(CS-2)
3 Process Equipment Design
and Drawing CH 405 5 3 1 2 2 50 25 50 20 30 175
(CS-3)
4 Transport Phenomena
CH 407 4 3 1 0 2 50 25 50 --- --- 125
(CS-4)
5 ES-1** 3 3 0 0 2 50 --- 50 --- --- 100
6 Seminar CH 409 1 0 0 2 --- --- --- --- 20 30 50
7 Project Preliminaries CH 411 2 0 0 4 --- --- --- --- 40 60 100
8 Training CH 413 1 0 0 0 --- --- --- --- --- 50 50
TOTAL 24 15 3 10 250 75 250 100 200 875
Total contact hours per week = 28 Total Credit = 24 Total marks = 875
2
B.Tech. III (CH), Semester-V L T P C
• INTRODUCTION ( 6 Hours)
Conservation of energy and first law of thermodynamics, application to steady state flow process,
enthalpy, internal energy, equilibrium state, phase rule, reversible and irreversible processes, heat capacity
specific heat.
BOOKS RECOMMENDED:
1. Smith J. M., Van Ness H. C., M.M. Abbott, “Introduction to Chemical Engineering Thermodynamics”, 6th
Ed., McGraw-Hill, New York, 2001
2. Dodge B. F., “Chemical Engineering Thermodynamics”, McGraw-Hill Book Co., New York, 1960.
3. Rao Y. V. C., “Chemical Engineering Thermodynamics”, Universities Press Limited, Heydrabad, 1997.
4. Kyle, B.G., "Chemical and Process Thermodynamics”, 2nd Ed., Prentice-Hall of India, New Delhi,1990.
5. Sandler, S.I., "Chemical and Engineering Thermodynamics", 2nd Ed., Wiley, New York, 1989.
3
L T P C
B. Tech. III (CH), Semester – V
3 1 2 5
CH 303: HEAT TRANSFER OPERATIONS
PRACTICALS:
1. Experiment on “Heat transfer through composite wall at different temperature”
2. Experiment on “Thermal conductivity of insulating powder (Asbestos powder)
3. Experiment on “Heat transfer in double pipe heat exchanger in laminar flow”
4. Experiment on “Heat transfer in turbulent flow”
5. Experiment on “Heat transfer by forced convection”
6. Experiment on “Heat transfer coefficient in natural convection”
7. Experiment on “Extended surface heat transfer”
8. Experiment on “Shell and tube heat exchanger”
9. Experiment on “Heat transfer by radiation: Stefan-Boltzmann Law”
BOOKS RECOMMENDED:
1. McCabe W.L., Smith J.C., Harrott P., “Unit Operations of Chemical Engineering”, 6th & 7th Eds. McGraw-
Hill, New York, 2001 & 2005.
2. Kern D. Q., “Process Heat Transfer”, McGraw-Hill, New York, 1950.
3. Hollman J. P., “Heat Transfer – Basic approach”, McGraw-Hill, New York, 1985.
4. Gebhart B. U., “Heat Transfer”, Tata McGraw-Hill, New York, 1961.
5. Coulson J.M., Richardson J.F., Backhurst J. R., Harker J.H. “Chemical Engineering” Vol. 1. 6th Ed.
Elservier, New Delhi, 2004.
4
B. Tech. III (CH), Semester-V L T P C
• INTRODUCTION ( 02 Hours)
Introduction to Mass Transfer Operation: classification & method.
• DIFFUSION AND MASS TRANSFER ( 08 Hours)
Molecular diffusion in fluids, steady state diffusion
(both gases & liquids), diffusivity of liquids & gases.
• DISTILLATION ( 16 Hours)
VLE data, flash, differential and continuous distillation,
McCabe-Thiele and Ponchon-Savarit method, Azeotropic,
Extractive, Reactive, Molecular and Multicomponent distillation,
Equipment for gas-liquid operation
• HUMIDIFICATION ( 06 Hours)
Vapor-gas mixtures, vapor-liquid equilibrium,gas-liquid contact operations,
adiabatic & non-adiabatic operations.
(Total contact time: 45 hours)
PRACTICALS
1. Humidification and dehumidification
2. Mass transfer coefficient
3. Crystallization
4. Azeotropic distillation
5. Diffusion coefficient
6. Latent heat of vaporization
7. Cooling tower
8. Packed distillation
BOOKS RECOMMENDED:
1. Treybal R.E., “Mass-Transfer Operations”, 3rd Ed., McGraw-Hill, New York, 1981.
2. McCabe W.L, Smith J.C., Harriott P., “Unit Operations in Chemical Engineering”, 6th & 7th Eds., McGraw-
Hill, New York,2001 & 2005.
3. Coulson J.M., Richardson J.F., Backhurst J. R., Harker J.H. “Chemical Engineering” Vol. 1. 6th Ed.
Elservier, New Delhi, 2004.
4. Sherwood, T.K., Pigford, R.L., Wilke, C.R., “Mass Transfer”, McGraw-Hill, New York, 1976.
5. Cussler E.L.,“Diffusion: Mass Transfer in Fluid Systems”, 2nd Ed., Cambridge University Press, Cambridge,
1997.
5
B. Tech. III (CH), Semester – V L T P C
• CONVEYERS (03Hours)
Mechanical and Pneumatic conveying, elevators, Bins, silos etc.
(Total contact time: 45 hours)
PRACTICALS:
BOOKS RECOMMENDED:
1. McCabe W.L., Smith J.C., Harriott P., ‘Unit Operations of Chemical Engineering”, 6th & 7th Eds., McGraw-
Hill, New York, 2001 & 2005.
2. Foust A.S., Wenzel L.A., Clump C.W., Maus L., Anderson L.B. “Principles of Unit Operations”, John
Wiley & Sons, New York, 1980.
3. Brown G.G., “Unit Operations”, John Wiley & Sons, New York, 1953.
4. Badger W.L., Banchero J.T., “Introduction to Chemical Engineering”, McGraw Hill, New York, 1997.
5. Coulson J.M., Richardson J.F., “Chemical Engineering”, Vol. 2, 5th Ed., Elservier, New Delhi, 2002.
6
B.Tech. III (CH), Semester-VI L T P C
BOOKS RECOMMENDED:
1. Smith J. M. Van Ness H. C., Abbott M.M., “Introduction to Chemical Engineering Thermodynamics”, 6th &
7th Eds., McGraw-Hill, New York, 2001 & 2005.
2. Dodge B. F., “Chemical Engineering Thermodynamics”, McGraw-Hill, New York, 1960.
3. Rao Y. V. C., “Chemical Engineering Thermodynamics”, Universities Press Limited, Heydrabad, 1997.
4. Sonntag R.E., Van Wylen G.J., “Fundamentals of Statistical Thermodynamics”, John Wiley & Sons,
Singapore, 1991.
5. Sandler, S.I., “Chemical and Engineering Thermodynamics”, 2nd Ed., Wiley, New York, 1989.
7
B. Tech. III (CH), Semester-VI L T P C
CH 304: CHEMICAL REACTION ENGINEERING - I 3 1 2 5
• INTRODUCTION (01 Hour)
Chemical kinetics, Classification of reactions, Variables affecting the rate of reaction, Reaction rate
• KINETICS OF HOMOGENEOUS REACTIONS (06 Hours)
Concentration dependent term and temperature dependent terms of rate equation, Single and multiple
reactions, Elementary and non-elementary reactions, Molecularity and order of reaction, Rate
constant, Representation of reaction rate, Kinetic models, Temperature dependency from Arrhenius’
law, thermodynamics, various theories, Activation energy, Searching for the reaction mechanism
• INTERPRETATION OF BATCH REACTOR DATA (08 Hours)
Constant volume batch reactor, Variable volume batch reactor, Integral method and differential
method of analysis of kinetic data, Temperature and reaction rate
• INTRODUCTION TO REACTOR DESIGN (03 Hours)
Types of reactors, PFR, CSTR etc., Material & energy balances single ideal reactor, Space-time and
space-velocity, Holding time, Introduction of non-ideal flow
• DESIGN FOR SINGLE REACTIONS (08 Hours)
Size comparison of single reactors, General graphical comparison, Multiple reactor system, Recycle
reactor, Autocatalytic reactions
• DESIGN FOR MULTIPLE REACTIONS SYSTEMS (08 Hours)
Reaction in parallel, Reaction in series, Series-parallel reaction and applications
• TEMPERATURE & PRESSURE EFFECTS (04 Hours)
Single & multiple reactions, Heats of reaction from thermodynamics, Product distribution
• INDUSTRIAL APPLICATIONS (04 Hours)
Types of reactors used in industries, Advanced chemical reactors.
• INTRODUCTION TO BIOCHEMICAL REACTION ENGINEERING (03 Hours)
Types of bio-reactors, Design, scale-up, operation and control of bio-reactors, Kinetics of biochemical
reactions
(Total contact time: 45 hours)
PRACTICALS:
1. Integral method of analysis of kinetic data
2. Differential method of analysis of kinetic data
3. Activation energy and frequency factor
4. Half-life method
5. Pseudo first order reaction
6. Study of kinetics of the reaction in presence of DC current
7. Study of membrane reactor
8. Study of spiral coiled reactor
9. Study of annulus flow reactor
10. Study of specific reaction/reactor system
BOOKS RECOMMENDED:
1. Levenspiel O., “Chemical Reaction Engineering”, 3rd Ed., John Wiley & Sons, Singapore, 1998.
2. Fogler H.S., “Elements of Chemical Reaction Engineering”, 4th Ed., Prentice-Hall, NJ, 2006.
3. Smith J. M., “Chemical Engineering Kinetics”, 3rd Ed., McGraw-Hill, New York, 1981.
4. Froment G.F., Bischoff K.B., “Chemical Reactor Analysis and Design”, 2nd Ed., John Wiley & Sons,
Singapore, 1990.
5. Inamdar S.T.A., “Biochemical Engineering – Principles and Concepts”, Prentice-Hall of India, New Delhi,
2007.
6. Shuler M.L., Kargi F., “Bioprocess Engineering – Basic Concepts”, 2nd Ed., Prentice-Hall of India, New
Delhi, 2006.
8
B. Tech. III (CH), Semester –VI L T P C
• INTRODUCTION (4 hours)
Definitions of Unit operations, Basic concepts of fluids and its application area, Properties of fluids,
Unit systems, Standards, Conversion on units, Units and equations, Dimension analysis, Dimension
and units, Dimensional homogeneity, Dimensionless equations, Buckingham π theorem, Common π
groups, examples.
9
PRACTICALS
BOOKS RECOMMENDED
1. McCabe W.L., Smith J.C., Harriott P., “Unit Operations of Chemical Engineering”, 6th & 7th Eds., McGraw-
Hill, New York, 2001 & 2005.
2. Coulson & Richardson’s Chemical Engineering, Vol. 2, 5th Ed., Elesevier, New Delhi, 2005.
3. Coulson & Richardson’s Chemical Engineering, Vol. 4, 2nd Ed., Elesevier, New Delhi, 2001.
4. Coulson & Richardson’s Chemical Engineering, Vol. 6, 4th Ed., Elesevier, New Delhi, 2006.
5. de Nevers N., “Fluid Mechanics for Chemical Engineers”, 2nd Ed., McGraw-Hill, New York, 1991.
10
B. Tech. III (CH), Semester-VI L T P C
• ABSORPTION ( 10 Hours)
Equilibrium, material balance for single component transfer, multi-stage & packed tower
operation, multicomponent system, non-isothermal operation, absorption with chemical
reaction
• DRYING ( 06 Hours)
Equilibrium, batch drying, mechanism, continuous
• LEACHING ( 04 Hours)
Steady state & unsteady state operations, methods of calculation
• CRYSTALLIZATION ( 03 Hours)
Equilibrium, operations and equipment
PRACTICALS
1. Leaching
2. Liquid-liquid extraction
3. Freundlich isotherm
4. Ternary diagram
5. Drying
6. Fluidization apparatus
7. Cooling tower
8. Fluid bed dryer
9. Evaporator
BOOKS RECOMMENDED:
1. Treybal R.E., “Mass-Transfer Operations”, 3rd Ed., McGraw-Hill, Singapore, 1981.
2. McCabe W.L, Smith J.C., Harriott P., “Unit Operations in Chemical Engineering”, 6th &7th Eds.,
McGraw-Hill, New York, 2001 & 2005.
3. Coulson J.M., Richardson J.F., Backhurst J. R., Harker J.H. “Coulson & Richardson's Chemical
Engineering”, Vol. 1, 6th Ed., Elservier, New Delhi, 2004.
4. Chopey N.P., “Handbook of Chemical Engineering Calculations”, 3rd Ed., McGraw-Hill, New
York, 2004.
5. Suryanarayana A., “Mass Transfer Operations”, New Age International, New Delhi, 2002.
11
B. Tech. IV (CH) Semester-VII L T P C
CH 401: CHEMICAL REACTION ENGINEERING - II 3 0 0 3
BOOKS RECOMMENDED:
1. Fogler H.S., “Elements of Chemical Reaction Engineering”, 4th Ed., Prentice Hall, NJ, 2006.
2. Levenspiel O., “Chemical Reaction Engineering”, 3rd Ed., John Wiley & Sons, Singapore, 1998.
3. Smith J. M., “Chemical Engineering Kinetics”, 3rd Edition, McGraw Hill, N Y, 1981.
4. Davis M.E., Davis R.J., “Fundamentals of Chemical Reaction Engineering”, McGraw-Hill, New York,2003.
5. Froment G.F., Bischoff K.B., “Chemical Reactor Analysis and Design”, 2nd Ed., John Wiley & Sons,
Singapore, 1990.
12
B. Tech. IV (CH), Semester – VII L T P C
13
PRACTICALS:
BOOKS RECOMMENDED:
1. Coughanowr D.R., “Process Systems Analysis and Control”, 2nd Ed., McGraw-Hill, New York, 1991.
2. Stephanopoulos G., “Chemical Process Control”, Prentice-Hall of India, New Delhi, 2001.
3. Luben W.L., Luben M.L., “Essentials of Process Control”, McGraw-Hill, New York, 1997.
4. Kopell L.B., Coughanowr D.R., “Process Systems Analysis and Control”, McGraw-Hill, New York, 1986.
5. Eckman D.P., “Industrial Instrumentation”, Dhanpat Rai and Sons, New Delhi, 1999.
6. Morris M. M., Kime C.R., “Logic and Computer Design Fundamentals”, Prentice-all, PLACE2000.
7. Considine D.M., “Process Industrial Instruments and Control Handbook”, McGraw-Hill, New York, 2001.
14
B. Tech. IV (CH) Semester - VII L T P C
CH 405 : PROCESS EQUIPMENT DESIGN & DRAWING 3 1 2 5
15
BOOKS RECOMMENDED:
1. Joshi M.V., Mahajani V.V., “Process Equipment Design”, 3rd Ed., MacMillan, Delhi, 1996.
2. IS Code: 2825 (1969).
3. Bhattacharyya B.C., “Introduction to Chemical Equipment Design: Mechanical Aspects”, 5th Ed., CBS
Publishers, New Delhi, 2008.
4. Soares C., “Process Engineering Equipment Handbook”, McGraw-Hill, New York, 2002.
5. Cheremisinoff N.P., “Handbook of Chemical Processing Equipment”, Butterworth Heinemann, Oxford,
2000.
6. Coulson & Richardson’s Chemical Engineering, Vol. 6, 4th Ed., Elesevier, New Delhi, 2006.
7. Kern D.Q., “Process Heat Transfer”, McGraw-Hill, New York, 1965.
8. Brownell L.E., Young E.H., “Process Equipment Design”, Wiley Eastern, Delhi, 1977.
9. Branan C.R., “Rules of Thumb for Chemical Engineers”, 4th Ed., Elsevier, Oxford, 2005.
16
B. Tech. IV (CH), Semester –VII L T P C
____________________________________________________________________________________
BOOKS RECOMMENDED:
1. Bird R.B., Stewart W.E., Lightfoot E.N., “Transport Phenomena”, 1st & 2nd Eds., John Wiley & Sons,
Singapore, 1960 & 2002.
2. Thomson, W.J., “Introduction to Transport Phenomena” Pearson Education Asia, Singapore, 2000.
3. Brodkey R.S. and Hershey H.C., “Transport Phenomena: A Unified Approach” McGraw-Hill, New York,
1988.
4. Plawsky J.L., “Transport Phenomena Fundamentals”, Marcel Dekker, New York, 2001.
5. Slattery J.C., Sagis L., Oh E-S., “Interfacial Transport Phenomena”, 2nd Ed., Springer, New York, 2007.
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B. Tech. IV (CH), Semester-VIII L T P C
• INTRODUCTION ( 02 Hours)
Basic consideration in chem. Engg. plant design, project identification, preliminary techno-
economic feasibility.
.
• PROCESS DESIGN ASPECTS ( 04 Hours)
Selection of process, factors affecting process selection, types of flow diagrams.
• DEPRECIATION ( 03 Hours)
Types and methods of determination, evaluation.
• PROFITABILITY ( 04 Hours)
Alternative investment & replacement methods for profitability evaluation, economic
consideration in process and equipment design, inventory control.
BOOKS RECOMMENDED:
1. Peters M.S., Timmerhaus, K.D., “Plant Design and Economics for Chemical Engineers”, 4th Ed., McGraw-
Hill, Singapore, 1991.
2. Vilbrant F.C., Dryden, C.E., “Chemical Engineering and Plant Design”, 4th Ed., McGraw-Hill, New York,
1959.
3. Pant J.C. “CPM and PERT with Linear Programming”, Jain Brothers, New Delhi, 1986.
4. Davis, G.S, "Chemical Engineering Economics and Decision Analysis", CENDC, I.I.T., Madras, 1981.
5. Holland, F.A., Watson, F.A and Wilkinson, J.K., "Introduction to Process Economics", Wiley, New
York, 1974.
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B. Tech. IV (CH), Semester – VIII L T P C
• INTRODUCTION (3 hours)
Physical and mathematical modeling, Principles of similarity, Independent variables, Dependent
variables, Parameters and boundary conditions.
BOOKS RECOMMENDED
1. Mickley H. S., Sherwood T. S., Reed C. E., “Application of Mathematical Modeling in Chemical
Engineering”, Tata-McGraw-Hill, New Delhi, 2002.
nd
2. Jensen V.G., Jeffreys G.V., “Mathematical Methods in Chemical Engineering”, 2 Ed.,
Academic Press, London, 1978.
3. Salariya R. S., “Numerical Methods”, Tata-McGraw Hill, New Delhi, 2002.
4. Lubyen W. L., “Process Modeling, Simulation and Control for Chemical Engineers”, 2nd Ed., McGraw-Hill,
New York, 1989.
5. Pushpavanam S., “Mathematical Methods in Chemical Engineering”, Prentice-Hall of India, New Delhi,
2001.
19
B. Tech. IV (CH), Semester –VIII L T P C
• INTRODUCTION (3 hours)
Introduction to Computer aided design in chemical engineering, Mathematical modeling, Steady state
and dynamic Simulation, Process simulation program (ASPEN PLUS).
PRACTICALS
1. Simulation by ASPEN PLUS for Single distillation column
2. Simulation by ASPEN PLUS for REDFRAC
3. Simulation by ASPEN PLUS for Heat Exchanger
4. Simulation by ASPEN PLUS for Reactors ( CSTR, PFR Etc)
5. Simulation by ASPEN PLUS for Cumin Production system
6. Simulation by ASPEN PLUS for Plant Optimization
7. Simulation by ASPEN PLUS for Property Estimation
8. Simulation by ASPEN PLUS for Methanol- Water System
BOOKS RECOMMENDED
1. Sinnott R. K., “Coulson & Richardson’s Chemical Engineering”, Vol. 6, 4th Ed., Elsevier, 2005.
2. Edgar T. F., Himmelblau D. M., Lasdon L. S., “Optimization of Chemical Processes”, 2nd Ed., McGraw-
Hill, New York, 2001.
3. Smith R., “Chemical Process Design”, McGraw-Hill, New York, 2000.
4. Biegler L. T., Grossmann E. I., Westerberg A. W., “ Systematic Methods of Chemical Process Design”,
Prentice-Hall , New Jersey, 1997.
5. Douglas J., “Conceptual Design of Chemical Processes”, McGraw-Hill, New York, 1989.
20
B. Tech. IV (CH), Semester - VIII L T P C
CH 408: SAFETY AND POLLUTION CONTROL IN CHEMICAL 3 - 2 4
PROCESS INDUSTRIES
• ENVIRONMENTAL AND POLLUTION IN CHEMICAL INDUSTRIES (02 Hours)
Definitions, scope and importance, need for public awareness, sources of pollution
from Chemical industries
• ENVIRONMENTAL LAWS AND STANDARDS (03 Hours)
Laws related to solid, liquid and gases effluents, standards and legislations,
Health and environmental effects, case studies for specific industries like
petrochemicals, fertilizers, desalination, petroleum refining.
• POLLUTION PREVENTION THROUGH PROCESS MODIFICATION (10 Hours)
Recovery of by-products, Energy recovery, Waste utilization and recycle and
reuse and waste generation minimization
• AIR POLLUTION CONTROL (05 Hours)
Air pollution control through mechanical separation, adsorption, etc.
• WATER POLLUTION CONTROL (05 Hours)
Water pollution control by physical, chemical and biochemical methods.
• DESIGN OF CONTROL EQUIPMENT AND SYSTEMS (06 Hours)
Designs to prevent fires and explosions, fire triangles, fault tree analysis, case studies
• SOLID WASTE TREATMENT AND DISPOSAL (04 Hours)
Types of solid waste, generation, onsite handling, storage & processing,
Disposal techniques, recovery of resources, conversion products and energy.
• SAFETY IN CHEMICAL PROCESS INDUSTRIES (10 Hours)
Safety and loss prevention, safety systems, Hazardus properties of chemicals,
characterization of chemical processes, the nature and impact of chemical
plant accidents, occupational safety and industrial hygiene, Toxicology,
toxic release, case studies
(Total contact time: 45 hours)
PRACTICALS
1. Determination of Dissolved Oxygen (DO)
2. Determination of Biochemical Oxygen Demand (BOD)
3. Determination of Chemical Oxygen Demand (COD)
4. Determination of Oil and Grease
5. Determination of Alkalinity
6. Determination of Acidity
7. Determination of Chloride Ion Concentration
8. Determinations of Total Suspended Solids (TSS)
9. Calorific value
10. Sampling Programs
11. Atomic Absorption Spectrophotometer Method
BOOKS RECOMMENDED:
1. Crowl D. A., Louvar J. F., “Chemical Process Safety”, Prantice-Hall, 2nd Ed., New York, 2002.
2. Metcalf & Eddy, “Waste Water Engineering: Treatment, Disposal and Reuse”, Tata-McGraw-Hill, New
Delhi, 2002.
3. MaCarty S., “Chemistry for Environmental Engineering”, Tata-McGraw-Hill, New Delhi, 2004.
4. Rao C.S., Environmental Engineering, Wiley Eastern Limited, New Delhi, 1995.
5. Sanders R E., “Chemical Process Safety”, Butterworth-Heinemann, New Delhi, 2005.
6. Masters G.M., “Introduction to Environmental Engineering and Science”, Prentice-Hall, New Delhi, 1997.
21