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Dryers and Cooling Towers 2 PDF
Dryers and Cooling Towers 2 PDF
Moisture Content,
(% Wet Basis) Steam Drum Feed Capacity
Method Pressure. Speed Temp. [Ib product/ Vacuum
Material of Feed Feed Product (Ib/sq in.) (rpm) (“F) (hr)(sqft)] (in. Hg)
Double-drum dryer
Sodium sulfonate trough 53.6 6.4 63 8; 164 7.75
Sodium sulfate trough 76.0 0.06 56 7 150 3.08
Sodium phosphate trough 57.0 0.9 90 9 180 8.23
Sodium acetate trough 39.5 0.44 70 3 205 1.51
Sodium acetate trough 40.5 10.03 67 8 200 5.16
Sodium acetate trough 63.5 9.53 67 8 170 3.26
Single-drum dryer
Chromium sulfate spray film 48.5 5.47 50 5 - 3.69
Chromium sulfate dip 48.0 8.06 50 4 - 1.30
Chromium sulfate pan 59.5 5.26 24 2; 158 1.53
Chromium sulfate splash 59.5 4.93 55 1; 150 2.31
Chromium sulfate splash 59.5 5.35 53 4% 154 3.76
Chromium sulfate dip 59.5 4.57 53 5; 153 3.36
Vegetable glue pan 60-70 10-12 20-30 6-7 - 1-1.6
Calcium arsenate slurry 75-77 0.5-1.0 45-50 3-4 - 2-3
Calcium carbonate slurry 70 0.5 45 2-3 - 1.5-3
Twin-drum dryer
Sodium sulfate dip 76 0.85 55 7 110 3.54
Sodium sulfate top 69 0.14 60 9; 162 4.27
Sodium sulfate top 69 5.47 32 9; 116 3.56
Sodium sulfate splash 71 0.10 60 6 130 4.30
Sodium sulfate splash 71.5 0.17 60 12 140 5.35
Sodium sulfate splash 71.5 0.09 60 10 145 5.33
Sodium phosphate splash 52.5 0.59 58 5; 208 8.69
Sodium phosphate dip 55 0.77 60 5; 200 6.05
Sodium sulfonate top 53.5 8-10 63 a; 172 10.43
Vacuum single-drum dryer
Extract pan 59 7.75 35 8 - 4.76 27.9
Extract pan 59 2.76 35 6 - 1.92 27.9
Extract pan 59 2.09 36 4 - 1.01 atmos.
Extract pan 56.5 1.95 35 7; - 3.19 22.7
Extract Pan 56.5 1.16 50 2; - 0.75 atmos.
Skim milk Pan 65 2-3 10-12 4-5 - 2.5-3.2
Malted milk pan 60 2 30-35 4- 5 - 2.6
Coffee pan 65 2-3 5-10 1-1; - 1.6-2.1
Malt extract spray film 65 3-4 3-5 0.5-1.0 - 1.3-1.6
Tanning extract pan 50-55 8-10 30-35 8-10 - 5.3-6.4
Vegetable glue pan 60-70 10-12 15-30 5-7 - 2-4
(Perrys Chemical Engineers Handbook, McGraw-Hill, 1950 edition).
calculation of residence time when assumptions are made about collecting fines, and a heater and blower for the gaseous drying
terminal temperatures. medium.
Much ingenuity has been applied to the design of fluidized bed
9.9. FLUIDIZED BED DRYERS drying. Many different arrangements of equipment are illustrated
and described in the comprehensive book of Kro11 (1978) for
Free flowing granular materials that require relatively short drying instance. Figure 9.13(a) depicts the basic kind of unit and the other
times are particularly suited to fluidized bed drying. When longer items are a few of the many variants. Tables 9.14 and 9.15 are
drying times are necessary, multistaging, recirculation or batch selected performance data.
operation of fluidized beds still may have advantages over other Shallow beds are easier to maintain in stable fluidization and of
modes. course exert a smaller load on the air blower. Pressure drop in the
A fluidized bed is made up of a mass of particles buoyed up out air distributor is approximately l p s i and that through the bed
of permanent contact with each other by a flowing fluid. Turbulent equals the weight of the bed per unit cross section. Some pressure
activity in such a bed promotes high rates of heat and mass transfer drop data are shown in Table 9.14. The cross section is determined
and uniformity of temperature and composition throughout. The by the gas velocity needed for fluidization as will be described. It is
basic system includes a solids feeding device, the fluidizing chamber usual to allow 3-6 ft of clear height between the top of the bed and
with a perforated distributing plate for the gas, an overflow duct for the air exhaust duct. Fines that are entrained are collected in a
removal of the dry product, a cyclone and other equipment for cyclone and blended with the main stream since they are very dry
9.9. FLUIDIZED BED DRYERS 263
TABLE 9.12-(continued)
Moisture
Content Vapor
Pressure Rotation Unit Product Drying
out Absolute S p e Rate
Kind of Dryer,
Kind of Stock
In
(%) (%I (bar) (l/min) (fiJ3r) (kg/m2 hr)
due to their small size. Normally entrainment is 5-10% but can be distribution of residence times can result in nonuniform drying, an
higher if the size distribution is very wide. It is not regarded as effect that is accentuated by the presence of a wide distribution of
feasible to permit high entrainment and recycle back to the drying particle sizes. Multiple beds in series assure more nearly constant
chamber, although this is common practice in the operation of residence time for all particles and consequently more nearly
catalytic cracking equipment. uniform drying. The data of Table 9.14(b) are for multiple zone
Mixing in shallow beds is essentially complete; Figure 9.5(c) dryers. Figures 9.13(c) and (d) have additional zones for cooling the
shows some test data in confirmation. The corresponding wide product before it leaves the equipment. Another way of assuring
Air/Solid
Gas Ratio
Tube Tube Rate Gas Temp ('c) Solid Solid Temp ('c)Moisture (%) (m3/kg) Evaporated
Water
Dia Height (m3/ hr) Rate
Material Location (cm) (m) (NTP) In Out (kg/hr) In Out In Out (NTP) (kg/kg) (kg/hr)
Ammonium
sulphate Japan 18 1 1100 215 76 950 38.5 63 2.75 0.28 1.2 1.5 23.5
Sewage sludge
filter cake U.S.A. - 1200 700 121 2270 15 71 80 10 5.3 7.2 1590
Coal 6 m m U.S.A. - 50,000 371 80 51,000 15 57 9 3 1.o 1.3 4350
Hexamethylene
tetramine Germanv 30 38" 3600 93 50 2500 - 48 6-10 0.08-0.15 1.4 1.9 18.1
Recirculation
Expansion
bellows
t
b l e paddle mixer
H a m m e r mill
B o t t o m bend
-.-.-. .---
Combustion chamber
(a) (b)
1. Fan
2. Ring duct
3. Manifold
4. Inlector
5 . Air outlet
6. F e e d e r
7. Filter
8. H e a t e r
9. Cyclone 7
IO. Disintegrator
II. Bag filter
12. Discharge
Figure 9.12. Examples of pneumatic conveying dryers; corresponding performance data are in Table 9.13. (a) Raymond flash dryer, with a
hammer mill for disintegrating the feed and with partial recycle of product (Raymond Division, Combustion Engineering). (b) Buttner-Rosin
pneumatic dryer with separate recycle and disintegration of large particles (Rosin Engineering Ltd.). (c) Berks ring dryer; the material
circulates through the ring-shaped path, product is withdrawn through the cyclone and bag filter (Penmalt Chemical Co.).
complete drying is a recirculation scheme like that of Figure One way of drying solutions or pastes under fluidizing
9.13(e). In batch operation the time can be made as long as conditions is that of Figure 9.13(g). Here the fluidized mass is of
necessary. auxiliary spheres, commonly of plastic such as polypropylene, into
Stable fluideation requires a distribution of particle sizes, which the solution is sprayed. The feed material deposits uniformly
preferably in the range of a few hundred microns. Normally a size on the spheres, dries there, and then is knocked off automatically as
of 4mm or so is considered an upper limit, but the coal dryers of it leaves the drier and leaves the auxiliary spheres behind. When a
Tables 9.15(a) and (b) accommodate sizes up to 0.5in. Large and mass of dry particles can be provided to start a fluidized bed drying
uniformly sized particles, such as grains, are dried successfully in process, solutions or pastes can be dried after deposition on the
spouted beds [Fig. 9.13(f)]: Here a high velocity gas stream entrains seed material as on the auxiliary spheres. Such a process is
the solid upward at the axis and releases it at the top for flow back employed, for instance, for growing fertilizer granules of desired
through the annulus. Some operations do without the mechanical larger sizes, and has largely replaced rotary dryers for this purpose.
draft tube shown but employ a naturally formed central channel. A few performance data of batch fluid dryers are in Table
266 DRYERS AND COOLING TOWERS
v-
Tl+ T,, and Ti+ Ti.
The procedure will be:
1. Start with known W,, T,, and T;.
g2 2. Specify a moisture content W,.
T2= 85 F 3. Assume a value T2 of the solid temperature.
4. Calculate Ti from the heat balance.
90 F 5. Check the correctness of T, by noting if the times for heat and
-T2, w2 mass transfers in the interval are equal.
EXAMPLE
9.&(continued) 38 I N P U T W l , W Z , T l , A l ! A 1 is th
c inlet air temp T 1 '
decremented value of W,, assume a value of T,, and proceed. The
48 I N P U T T 2 ! T r i a l value
solution is tabulated. 5 8 A2=(2.51*(.391t<T2-Tl}+CWl-W
W T T' e w Z>X(T2-T1+563?>-.2584~*A1+23
.8*~Wl-W2})/(.48bCWl-wz)-.25
0.035 60 450 0 048 >
0.0325 73.04 378.2 0.0402 68 G1=.813+2.82t(Wl-.813>
0.03 75.66 352.2 0.0581
0.025 77.41 31 5.3 0.0872
78 Pl=G1/(.6207+Gl)
0.02 77.23 286.7 0.1133
80 G2=.013+2.31S(W2-.813}
0.015 76.28 261.3 0.1396 90 PZ=G2/(.6287+G2>
0.01 75.15 236.4 0.1687 108 Ql=EXPCl3.7419-5237.9~~Tl+27
0.005 74.67 208.4 0.2067 3 . 2 > j ! vapor pressure
0.003 75.55 192.4 0.2317 1 1 8 Q2=EXPC13.7419-5237.9,(T2+27
0.001 79.00 165.0 0.2841 3.2))
1 2 8 P3=CQl-Pl-Q2+P2?/LOG<CQl-Pl>
When going directly from 0.035 to 0.001, /CQ2-P2)) ! C a P > l m
130 T 3 = ( A l - T l - H 2 + T 2 ? ~ L O C ( ( A 1 - T 1 >
T2= 80.28, /(RZ-T2i> ! taT}lm
T ; = 144.04, 1 4 8 Q=.391tCTZ-T1>+CWl-W2jX<T2-T
1 +563 j
8 = 0.3279 sec. 158 H l = Q / . 4 7 / T 3 ! heatins time
The calculation could be repeated with a smaller air rate in order to 168 W = . 5 S C W 1 + W 2 ~
reduce its exit temperature to nearer 120"C, thus improving thermal 1 7 8 K=EXP(-3.1811-1.7388XLCIG<W>-
efficiency. .2533XLOG<W}*2)
In the vessel with diameter = 0.6 m, the air velocities are 188 H 2 = ( W l - W 2 ) / K / P 3 ! vaporizati
25.0 m/sec at 450°C inlet
on time
198 Z=Hl-H2 ! time difference s h
5.15 m/sec at 165°C outlet ould be zero
288 D I S P Z
20.1 m/sec average. 2 1 4 DISP A 2 , H l
228 GOTO 4 0 ! i f Z is n o t rlear e
The vessel height that will provide the needed residence time is noush to zero.; otherwise the
correct value o f T 2 ha5 bee
H = &e = 20.1(0.2841) = 5.70 m. n found
Very fine particles with zero slip velocity will have the same 2 3 0 END
holdup time as the air. The coarsest with settling velocity of
10 m/sec will have a net forward velocity of
iis = 20.1 - 10 = 10.1m/sec,
which corresponds to a holdup time of
e = s . 7 / i o . i =0.56sec,
Data f o r t h e f i r s t i n t e r v a l
which is desirable since they dry more slowly.
After the assumption of T2, other quantities are evaluated in
the order shown in this program.
1 8 ! Example 9 . 3 . P n e u m a ? ic cor1
verins drrer
28 ! Findins the exit solids ? e
m P T 2 b r trial, then a l l de^
endent quanti t ies
9.14(a). This process is faster and much less labor-intensive than installed). The relatively large power requirements of fluidized bed
tray drying and has largely replaced tray drying in the pharma- dryers are counterbalanced by their greater mechanical simplicity
ceutical industry which deals with small production rates. Drying and lower floor space requirements.
rates of 2-l0lb/(hr)(cuft) are reported in this table, with drying Air rates in Table 9.15 range from 13 to 793 SCFM/sqft, which
times of a fraction of an hour to several hours. In the continuous is hardly a guide to the selection of an air rate for a particular case.
operations of Table 9.15, the residence times are at most a few minutes. A gas velocity twice the minimum fluidization velocity may be taken
Thermal efficiency of fluidized bed dryers is superior to that of as a safe prescription. None of the published correlations of
many other types, generally less than twice the latent heat of the minimum fluidizing velocity is of high accuracy. The equation of
water evaporated being required as heat input. Power requirements Leva (Fluidization,McGraw-Hill, New York, 1959) appears to be
are a major cost factor. The easily dried materials of Table 9.15(a) as good as any of the later ones. It is
show evaporation rates of 58-103 lb/(hr)(HP installed) but the
more difficult materials of Table 9.15(d) show only 5-18 Ib/(hr) (HP (9.20)
268 DRYERS AND COOLING TOWERS
where G,,,, is in lb/(hr)(sqft), pg and ps are densities of the gas and 9.10. SPRAY DRYERS
solid (Ib/cuft), D, is the particle diameter (in.), and p is the gas
viscosity (cP). In view of the wide scatter of the data on which this Suitable feeds to a spray dryer are solutions or pumpable pastes and
correlation is based, shown on Figure 6.14(f), it appears advisable slurries. Such a material is atomized in a nozzle or spray wheel,
to find the fluidization velocity experimentally for the case in hand. contacted with heated air or flue gas and conveyed out of the
Although it is embarrassing again to admit the fact, equipment with a pneumatic or mechanical type of conveyor.
unfortunately all aspects of fluidized bed drying must be established Collection of fines with a cyclone separator or filter is a major
with pilot plant tests. The wide ranges of performance parameters aspect of spray dryer operation. Typical equipment arrangements
in Tables 9.14 and 9.15 certainly emphasize this conclusion. A and flow patterns are shown in Figure 9.14.
limited exploration of air rates and equipment size can be made on The action of a high speed spray wheel is represented by Figure
the basis of a drying rate equation and fluidization correlations from 9.14(e); the throw is lateral so that a large diameter vessel is required
the literature. This is done in Example 9.9. A rough approximation with this form of atomization, as shown in Figure 9.14(a). The flow
of a drying rate equation can be based on through circulation drying from nozzles is largely downward so that the dryer is slimmer and
of the granular material on a tray, with gas flow downward. taller. Parallel flow of air and spray downward is the most common
cyclone
inle 1 + DV material
Figure 9.13. Fluidized bed dryers. (a) Basic equipment arrangement (McCabe and Smith, Unit Operations in Chemical
Engineering, McGraw-Hill, New York, 2984). (b) Multiple bed dryer with dualflow distributors; performance data are
in Table 9.14(b) (Romankou, in Dauidson and Harrison, Fluidisation, Academic, New York, 2972). (c) A two-bed
dryer with the lower one used as cooler: (a, b, c) rotary valves; (d) drying bed; (e) cooling bed; (f, g) air distributors;
(h, i) air blowers; (k) air filter; (I) air heater; (m) overflow pipe; (n) product collector (Kroll, 2978). (d) Horizontal
multizone dryer: (a) feeder; (b) air distributor; (c) fluidized bed; (d) partitions; (e) dust guard; (f) solids exit; (8) drying
zone; (h) cooling zone; (i, k) blowers; (1, m) air plenums; (n) air duct; (0)dust collector; (p) exhaust fan (Kroll, 2978).
(e) Circulating fluidized bed used for removal of combined water from aluminum hydroxide: (a) feed; (b) fluidized bed;
(c) solids exit; (d) fuel oil inlet; (e) primary air inlet; ( f ) secondary air inlet; (8) gas exit (Kroll, 2978). ( f ) Spouted bed
with draft tube for drying coarse, uniform-sized granular materials such as grains [Yang and Keairns, AIChE Symp.
Ser. 176, 218 (2978),Fig. I].(g) Fluidized bed dryer for sludges and pastes. The fluidized solids are fine spheres of
materials such as polypropylene. The wet material is sprayed in, deposits on the spheres and dries there. At the outlet
the spheres strike a plate where the dried material is knocked off and leaves the dryer as flakes. The auxiliary spheres
remain in the equipment: (a) feed; (b) distributor; (c) spheres loaded with wet material; (d) returning spheres; (e)
striking plate; (f) hot air inlet; (g) air and solids exit (Kroll, 2978).
9.10. SPRAY DRYERS 269
Gas Out
A
Alternative
Solids feed
i -Solid flow
Gas and Solids Feed --- Gas flow
(e) (R
Figure 9.13-(continued)
arrangement, but the left-hand figure of Figure 9.14(d) is in particles, but may be harmful to thermally sensitive products
counterflow. Figure 9.14(c) has tangential input of cooling air. In because they are exposed to high air temperatures as they leave the
some operations, the heated air is introduced tangentially; then the dryer. The flat bottomed dryer of Figure 9.14(c) contacts the exiting
process is called mixed flow. Most of the entries in Table 9.16(a) are solids with cooling air and is thus adapted to thermally sensitive
parallel flow; but the heavy duty detergent is in counterflow, and materials.
titanium dioxide is either parallel or mixed flow. Counterflow is Two main characteristics of spray drying are the short drying
thermally more efficient, results in less expansion of the product time and the porosity and small, rounded particles of product. Short
270 DRYERS AND COOLING TOWERS
TABLE 9.14. Performance Data of Fluidized Bed Dryers: Batch and Multistage Equipment
Lactose
Ammonium Base Pharmaceutical Liver Weed
Bromide Granules Crystals Residue Killer
Holding capacity (Ib wet product) 100 104 160 280 250
Bulk density, dry (lb/ft3) 75 30 20 30 35
Initial moisture (% w/w basis) 6 10 65 50 20-25
Final moisture (% w/w basis) 1 2 0.4 5.0 1.o
Final drying temperature ("F) 212 158 248 140 140
Drying time (min) 20 90 120 75 210
Fan capacity (ft3/min at 11 in. w.g.) 750 1500 3000 4000 3000
Fan HP 5 10 20 25 20
EvaDoration rate (Ib H,O/hr) 15 5.7 52 100 17
(Courtesy Calmic Engineering Co. Ltd.; Williams-Gardner, 1971).
(b) Multistage Dryers with Dual-flow Distributors [Equipment Sketch in Fig. 9.13(b)]
drying time is a particular advantage with heat sensitive materials. Residence times of air and particles are far from uniform; Figure
Porosity and small size are desirable when the material sub- 9.5(a) and (b) is a sample of such data.
sequently is to be dissolved (as foods or detergents) or dispersed Because of slip and turbulence, the average residence times of
(as pigments, inks, etc.). Table 9.17 has some data on size particles are substantially greater than the mean time of the air,
distributions, bulk density, and power requirements of the several definitely so in the case of countercurrent or mixed flow. Surface
types of atomizers. moisture is removed rapidly, in less than 5 sec as a rule, but falling
The mean residence time of the gas in a spray dryer is the ratio rate drying takes much longer. Nevertheless, the usual drying
of vessel volume to the volumetric flow rate. These statements are operation is completed in 5-30 sec. The residence time distribution
made in the literature regarding residence times for spray drying: of particles is dependent on the mixing behavior and on the size
distribution. The coarsest particles fall most rapidly and take
Source Time (sec) longest for complete drying. If the material is heat-sensitive, very
tall towers in parallel flow must be employed; otherwise,
Heat Exchanger Design Handbook (1983) 5-60 countercurrent or mixed flows with high air temperatures may
McCormick (1979) 20 suffice. In some cases it may be feasible to follow up incomplete
Masters (1976) 20-40 (parallel flow)
spray drying with a pneumatic dryer.
Nonhebel and Moss (1971) <60
Peck (1983) 5-30
Drying must be essentially completed in the straight sided
Wentz and Thygeson (1979) zones of Figures 9.14(a) and (b). The conical section is for gather-
Williams-Gardner (1971) 4-10 (<15ftdia) ing and efficient discharge of the dried product. The lateral throw
10-20 b15ftdia) of spray wheels requires a vessel of large diameter to avoid
9.10. SPRAY DRYERS 271
(Williams-Gardner, 1971).
Silicious Glass
Coal Grit Sand Sand Asphalt
(Williams-Gardner, 1971).
Sodium Weed
Perborate Killer PVC Coal Sand
(Williams-Gardner, 1971).
(5)
the drying time will be
Vapor pressure:
Saturation humidity: where Hs, Hgr and W are final conditions. When the final W is
small, 0.01 in the present numerical example, the single stage drying
time will be prohibitive. In such cases, multistaging, batch drying,
(7) or some other kind of drying equipment must be resorted to.
1 8 ! Example 9 . 3 . F l u i d i z e d Ped
0.36( T4- 100) + 261 d rY e r
T,=350-
RCg 2 8 I N P U T R ! =HfS, r a t i o cat r a t
e 5 l3t f l o w of a i r a n d s o l i d
39 H 3 = . 8 1 5 + 2 9 / R ! =Hs
49 C1=.2434+.225tH3
59 INPUT T 4 ! T r i a l v a l u e o f T s
Procedure: For a specified value of R = A I S , solve Eqs. (6), 68 LOSUB 299
(7),and (8) simultaneously. 78 '{ 1=y
s9 T 4 = 1 . 0 8 9 1 t T 4
99 GOSUB 299
R T, r, H, 4 tl (min) 1 9 8 '{ 2 = y
5 145.14 119.84 0.0730 0.0803 0.662 118 K = . 0 0 0 l t Y l / ( Y Z - Y l ~
6 178.11 119.74 0.0633 0.0800 0.289 128 T4=T4/1.8891-K
8 220.09 119.60 0.0513 0.0797 0.170 139 DISP T4
10 245.72 119.52 0.0440 0.0795 0.136 1 4 9 I F H B S < K . / T 4 j < = . 6 9 8 0 1 THEN 1 6
12 262.98 119.47 0.0392 0.0794 0.120 0
1 5 8 GOTO 68
Take 1 6 0 D I S P USING 1 7 8 j R , T Z , T 4 > H 3 >
H4 T 5#.
1 7 8 IMRGE D D , X I D D U . D , X , D D D . D , X , .
R = 10 Ib air/lb solid, DUD0 > x , .DDDD,>SI . D D D
A = lO(100) = lo00 Ib/hr, 188 E HD
0 = 0.136 min. 298 ! SR f o r T 4
2 1 8 P = .E..X P ( 1 1 . 9 1 7 6 - 7 1 7 3 . 9 . ( T 4 + J S 9
. J > *'
Cross section: 228 H 4 = 1 8 S P y 2 9 / < 1 - P > ! = H.3
258 T 3 = T 4 + 9 8 8 % ( H 4 - H 3 > / C l ! = T 4
A/G, = 1000/34.34 = 29.12 sqft, 6.09 ft dia. E48 Y = - T 3 + 3 5 9 - ( . 3 6 t ( T 4 - 1 0 8 ) + 2 6 1 )
/ R. ./ e - 1
-
Avg density: 2'59 T 5 = . 2 9 i { H 4 - H 3 > / 6 9 ! = time
268 RETURN
$(1/20.96 + 1/19.03) = 0.0501 Ib/cuft. 279 EtJD
Linear velocity:
u=-- Gf - 34.34
= 24.62 fpm
ps(60) 0.0501(0.464)(60) T. H I1 Time
Bed depth:
-+
R
Ts A S -
5 1 4 5 . 1 1 1 3 . 8 4 ,97338 ,61883 662
L = U B = 24.62(0.136) = 3.35 ft.
6 1 7 8 . 1 1 1 9 . 7 4 .8633 .8888 ,289
8 2213.1 1 1 9 . 6 1 , 4 5 1 3 ,8797 ,178
la 2 4 5 . 7 1 1 9 . 5 3 , 9 4 4 8 .879rJ ,136
Note: In a completely mixed fluidized bed, the drying time is 1 2 2 6 3 . 8 1 1 9 . 4 7 .a392 ,8794 ,128
determined by the final moisture contents of the air and solid. 15 2 8 8 . 4 1 1 9 . 4 2 , 8 3 4 3 .8792 ,188
274 DRYERS AND COOLING TOWERS
A i r diffuser
Exhaust o ~ r
plates
AIR 230
FjED
I 6o I
,Feed
rj
+c--
productto
collectw
Sweeper air
Figure 9.14. Spray dryer arrangements and behavior. (a) Spray dryer equipped with spray wheel; straight section LID = 0.5-1.0 (Proctor and
Schwartz Znc.). (b) Spray dryer equipped with spray nozzle; straight section LID = 4-5 (Nonhebel and Moss, 1971). (c) Spray dryer for very
heat sensitive products; flat bottom, side air ports and air sweeper to cool leaving particles. (d) Distribution of air temperatures in parallel
and countercurrent flows (Musters, 1976,p . 18, Fig. 1.5).(e) Droplet-forming action of a spray wheel (Stork-Bowen Engineering Co.).
9.10. SPRAY DRYERS 275
Moisture Air
Content Temperature
spry Flow
Kind of Stock In(%) Out(%) Device Pattern In (“C) Out (“C)
(b) Performance of a Dryer 18ft Dia by 18ft High with a Spray Wheel and a Fan Capacity of 11,000cfm at the
Outleta
APPLICATIONS
For direct drying of liquids, slurries, and pastes, drum dryers are
the only competition for spray dryers, although fluidized bed dryers
sometimes can be adapted to the purpose. Spray dryers are capable
of large evaporation rates, 12,000-15,000Ib/hr or so, whereas a
300sqft drum dryer for instance may have a capacity of only
3000 Ib/hr. The spherelike sprayed particles often are preferable to
drum dryer flakes. Dust control is intrinsic to spray dryer
0
100
d
200
I
A
300
-
400
I I
500
I
600
construction but will be an extra for drum dryers. The completely
enclosed operation of spray dryers also is an advantage when toxic
or noxious materials are handled.
A i r inlet, OC
THERMAL EFFICIENCY
'The full lines are against temperature, the dashed ones against Exit air usually is maintained far from saturated with moisture and
concentration: (a) sodium silicate; (b) coffee extract, 22%; (c) water at a high temperature in order to prevent recondensation of moisture
dispersible dye, 19.5%; (d) gelatin. in parallel current operation, with a consequent lowering of thermal
[Data of Duffie and Marshall, Chem. Eng. Prog. 49, 417 480 (195311.
efficiency. With steam heating of air the overall efficiency is about
40%. Direct fired dryers may have efficiencies of 8 0 4 5 % with inlet
temperatures of 500-550°C and outlet of 65-70°C. Steam
accumulation of wet material on the walls; length to diameter ratios consumption of spray dryers may be 1.2-1.8 Ib steam/lb evapor-
of 0.5-1.0 are used in such cases. The downward throw of nozzles ated, but the small unit of Table 9.19(b) is naturally less efficient. A
permits small diameters but greater depths for a given residence 10% heat loss through the walls of the dryer often is taken for
time; LID ratios of 4-5 or more are used. design purposes. Pressure drop in a dryer is 15-50in. of water,
depending on duct sizes and the kind of separation equipment used.
ATOMIZATION DESIGN
Proper atomization of feed is the key to successful spray drying. The design of spray dryers is based on experience and pilot plant
The three devices of commercial value are pressure nozzles, determinations of residence time, air conditions, and air flow rate.
pneumatic nozzles, and rotating wheels of various designs. Usual Example 9.10 utilizes such data for the sizing of a commercial scale
pressures employed in nozzles range from 300 to 4000psi, and spray dryer.
9.11. THEORY OF AIR-WATER INTERACTION IN PACKED TOWERS 277
aThis factor will only occur if a critical value of the variable is exceeded.
Not for suspensions.
(Nonhebel and Moss, 1971).
The smallest pilot unit supplied by Bowen Engineering has a Analysis of the interaction of air and water involves the making
diameter of 30 in. and straight side of 29 in., employs parallel flow, of material and enthalpy balances. These are made over a
up to 25ACFM, 150-1000”F, particle sizes 30-40pm average, differential section of the tower shown on Figure 9.15(a) and are
either pneumatic nozzle or spray wheel. The performance of this subsequently integrated to establish the size of equipment for a
unit is given in Table 9.19. The magnitude of the “product number” given performance. In terms of empirical heat, k,, and mass, k,,
is arrived at by pilot plant work and experience; it increases with transfer coefficients, these balances are
increased difficulty of drying or thermal sensitivity or both.
Although much useful information can be obtained on this small Gdh = LC, dT = L dT (9.21)
scale, Williams-Gardner (1971) states that data on at least a 7 ft dia = k,(hs- h ) dz (9.22)
dryer be obtained for final design of large capacity units. = kh(T - T,) dz. (9.23)
9.1 1. THEORY OF AIR-WATER INTERACTION IN PACKED In Eq. (9.21) the heat capacity of water has been taken as unity.
TOWERS The approximations that are involved in making an enthalpy
difference a driving force are discussed for example by Foust et al.
The key properties of mixtures of air and water vapor are described (1980). Rearrangement and integration leads to the results
in Section 9.1. Here the interactions of air and water in packed
towers under steady flow conditions will be analyzed. The primary
objectives of such operations may be to humidify or dehumidify the (9.24)
L
air as needed for particular drying processes or other processes, or
to cool process water used for heat transfer elsewhere in the plant. dT
Humidification-dehumidification usually is accomplished in spray (9.25)
towers, whereas cooling towers almost invariably are filled with
some type of packing of open structure to improve contacting but _- (9.26)
with minimum pressure drop of air.
278 DRYERS AND COOLING TOWERS
TABLE 9.19. Product Numbers and Performance of a 30 x Both forms of the integral are employed in the literature to define
29 in. Pilot Plant Spray Dryer the number of transfer units. The relation between them is
(a) Product Numbers of Selected Materials
k,Z/G = (L/G)(NTU). (9.27)
Material Product nunher The height of a transfer unit is
Make the straight side four times the diameter and the cone
100 F 60":
(a)
Equilibrium p
c
'
c
c-
balance
I h = f (T)
Figure 9.15. Relations in a packed continuous flow air-water contactor. (a) Sketch of the tower
with differential zone over which the enthalpy and material balances are made. (b) Showing
equilibrium and operating lines from which the integrand l/(h3 - h) can be found as a function
of liquid temperature T. (c) Showing interfacial conditions as determined by the coefficient
ratio k,/k, ; when this value is large, interfacial and saturation temperatures are identical.
EXAMPLE 9.11 or
Sizing of a Cooling Tower: Number of Transfer Units and
Height of Packing HTU = 5.51(L/G)0.59.
Water is to be cooled from 110 to 75°F by contact with air that
enters countercurrently at 90°F with a dewpoint of 60°F. The data of Tower height:
London et al. (1940) of Figure 9.16 for height of transfer unit are
applicable. Calculations will be made for two values of the Z = (HTU)(NTU).
coefficient ratio k,/k,, namely, 25 and m Btu/("F) (Ib dry air), of
Eq. (9.31). The effect of the ratio of liquid to gas rates, L/G, will For several values of L/G:
be explored.
Ll G 0.6 1 1.4 1.7
HTU (ft) 4.08 5.51 6.72 7.54
T, = 110 F
Evaluation of interfacial temp and the NTU for L/G = 1 with
k,/k, = 25:
T h T. l/(k-h)
78.5 30.5 78.099 0.0864
89 41 88.517 0.0709
96 48 95.400 0.0575
106.5 58.5 105.581 0.0385
0.2533
h = 27 + (L/G)( T - 75),
h, = h + 25(T - 75),
T h L/G=O.6 1 1.4 1.7
h, =0.24T + (18/29)(0.457 + 1100)</(1 -e),
< = exp[11.9176- 7173.9/(T, + 389.5))
78.5
89
30.5
41
0.0725
0.0494
0.0807
0.0683
0.90
0.1 107
0.1006
0.2070
96 48 0.0376 0.0549 0.1 020 0.2854
When k,/k,+m, T, in Eq. (9.33) is replaced by T.
106.5 106.5 0.0248 0.0361 0.0663 0.1778
The four temperatures at which the integrands are evaluated
for the Chebyshev integration are found with Eq. (9.34) and 0.1844 0.2400 0.3700 0.7708
tabulated in the calculation summary following. NTU-, 1.613 2.100 3.238 6.745
Equations (9.30) and (9.31) are solved simultaneously for h and Z+ 6.58 11.57 21.76 50.86
h, with the aid of the Newton-Raphson method as used in the
computer program; the integrands are evaluated and the integration
are completed with Eq. (9.35).
The number of transfer units is sensitive to the value of L / G ,
but the effect of k,/k, is more modest, at least over the high range
used; data for this ratio do not appear to be prominently recorded.
Figure 9.16 shows a wide range of heights of transfer units for the
different kinds of packings, here characterized by the surface ad
(sqft/cuft) and substantial variation with L/G. The last line of the
calculation summary shows variation of the tower height with L/G.
Data of London et al. (1940) of Figure 9.16:
(G/L)(HTU) = 5.51(G/L)0.41
282 DRYERS AND COOLING TOWERS
*
the top converts some kinetic energy into pressure energy which
assists in dispelling the exit humid air into the atmosphere.
The ratio of base diameter to height is 0.75-0.85, the ratio
of throat and base diameters is 0.55-0.65, and the ratio of
vertical depth of air opening to base diameter is 0.1-0.12. Air
VERTICAL SPACINO 24" IVERTICAL
I
SPACING 2 4 " velocity through the tower is 3-6ft/sec, water flow rates range
DECK I DECK J from 600 to 1800Ib/(hr)(sqft). Two towers each 375ft high are
I/2 "I I " ~7/8"17/8~ able to service a 500 MW power plant. Natural draft towers are
uneconomical below heights of 70 ft. The upper limit is imposed
principally by environmental visual considerations; towers 500 ft
high are in existence. A cost comparison is made with item d.
c. Hyperbolic fan assisted towers can have as much as three times
V E R T I C A L S P A C I N GI - l24"
/e" the capacity of the same size natural draft towers. The fans
VERTICAL SPACINQ 2 4 " provide greater control than the natural draft systems; for
example, they may be turned on only at peak loads. Rules of
Factors in Eq. 9.38 for the Number of Decks thumb cited by Cheremisinoff and Cheremisinoff (1981) for
Deck Type a b
relative sizing is that fan assisted hyperbolic towers may have
diameters 2/3 and heights 1/2 those of purely natural draft designs.
A 0.060 0.62 d. Countercurrent-induced draft construction is the most widely
B 0.070 0.62 used type in process industries. Mechanical draft is capable of a
C 0.092 0.60
greater degree of control than natural draft and such towers are
D 0.119 0.58
able in some cases to cool the water within 2°F of the wet bulb
E 0.110 0.46
F 0.100 0.51 temperature of the air. The elevated fan location introduces
G 0.104 0.57 some structural and noise problems. The flow of air is quite
H 0.127 0.47 uniform across the cross section and its discharge is positive and
I 0.135 0.57 at high velocity so that there is little backflow of humid air into
J 0.103 0.54 the tower. A cost comparison (dated 1978) with hyperbolic
Figure 9.17. Kinds of fill made of redwood slats for cooling towers, towers is made by Singham (1983, Sec. 3.12.4.1). The case is for
and factors for determining the required number of decks with inlet a water rate of 6.1 m3/sec, cooling range of 8.S'C, approach of
water at 120°F (Cherembinof and Cheremisinof, 1981). lWC, and wet bulb of 17°C. The cost of the natural draft tower
9.12. COOLING TOWERS 283
AIR OUTLET
t
I
(a)
Figure 9.18. Main types of cooling towers. (a) Atmospheric, dependent on wind velocity. (b) Hyperbolic stack natural draft. (c) Hyperbolic
assisted with forced draft fans. (d) Counterflow-induced draft. (e) Crossflow-induced draft. ( f ) Forced draft. ( 9 ) Induced draft with surface
precooler for very hot water; also called wet/dry tower. [ ( b ) - ( e )from Cherernisinof and Cheremisiinof, 1981).
- 95 - I I I I I
- ~-
U
90% WATER FLOW ,
60 65 70 75 BO 60 65 70 75 80
AIR WET-BULB TEMPERATURE (OF) AIR WET -BULB TEMPERATURE (OF) AIR WET-BULB TEMPERATURE ( O F 1
F i r e 9.19. Typical cooling tower performance curves (Cheremisinoff and Cheremisinoff, 1981).