G.

Line Work

10 ml n - butanol

1. Insert in to a measuring flask

2. Added 1 grain of boiling stone
3. Added little by little 3 drops of
concentrated sulfuric acid
4. Added 30 ml of glacial acetic acid in the
fuem hood

Mixed solution
5. Mounted refux cooler
6. Hetated mixture solution at 90℃ - 100 ℃ for
3 hours
7. Insert into the sparating funnel
8. Added 30 mL of water and shake it strong
9. Separated

Up l ayer Low layer

10. Added 25 ml of water

11. Added 7 ml NaHCO3 saturated
12. Shake it
13. Sparated by a sparating funnel

filtrate Residu

14. Added 2,5 gram MgSO4 anhidrate that

have been heated before
15. Shake it with spatula
16. Sparated

filtrate Residu

17. counted

mass