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Fatigue Properties of Ferritebainite Dual-Phase X80 Pipeline Steel Welded Joints
Fatigue Properties of Ferritebainite Dual-Phase X80 Pipeline Steel Welded Joints
Fatigue Properties of Ferritebainite Dual-Phase X80 Pipeline Steel Welded Joints
Z-P. Zhao, G-Y. Qiao, G-P. Li, W-W. Yang, B. Liao & F-R. Xiao
To cite this article: Z-P. Zhao, G-Y. Qiao, G-P. Li, W-W. Yang, B. Liao & F-R. Xiao (2016): Fatigue
properties of ferrite/bainite dual-phase X80 pipeline steel welded joints, Science and
Technology of Welding and Joining, DOI: 10.1080/13621718.2016.1219120
Article views: 59
Download by: [Ryerson University Library] Date: 17 October 2016, At: 07:55
Fatigue properties of ferrite/bainite dual-phase
X80 pipeline steel welded joints
Z-P. Zhao1 , G-Y. Qiao1,2, G-P. Li3, W-W. Yang3, B. Liao1 and F-R. Xiao∗ 1
Fatigue properties are important parameters for the safety design and security evaluation of
pipelines. In this work, fatigue life and fatigue crack propagation of full-thickness X80 pipeline
steel joints compared with the base metal (BM) was investigated. Full-thickness BM specimens
showed superior fatigue life compared with that of welded joints. The fatigue crack initiation of
full-thickness X80 welded joint specimens occurred at the outside weld toe and then grew
inward until a fracture was formed. During fatigue crack growth in the heat-affected zone (HAZ),
crack growth rate linearly increased with increased ΔK in each HAZ subregion. However, the
change rate of fatigue crack growth rate (da/dN ) differed among HAZ subregions. This
difference was related to the variation in crack path and fracture mode because of the possible
microstructural sensitivity of fatigue crack propagation behaviour.
Keywords: X80 steel, HAZ, Fatigue property, Failure mode, Microstructure, Crack propagation
Table 1 Chemical composition (in wt-%) of the X80 steel selected in the present study
C Mn Si P S Mo Ni Cr Cu Nb Ti Al
0.07 1.69 0.21 0.011 0.002 0.003 0.255 0.223 0.129 0.082 0.015 0.035
specimens were used for the investigation. The effects of frequency of 10 Hz were selected in all of the tests. The
stress concentration on fatigue crack initiation were also ana- fatigue crack propagation test was performed using an
lysed. In addition, fatigue crack growth behaviour in HAZ MTS 858 Mini Bionix universal testing machine. The
was examined by means of electron back-scattered diffrac- R-ratio and frequency were set at 0.1 and 10 Hz, respect-
tion (EBSD). This study provided beneficial experimental ively. The tests were initiated with a fatigue precracking
data for safe designs and life prediction of pipelines. process to initiate an initial crack from the sharp notch
of each SENB specimen. The fatigue precracking was
generated by cyclic loading until a crack with the desired
Experimental procedure length was formed. This procedure was conducted follow-
ing the ASTM standard.10 The precrack length of each
In this work, a commercial ferrite/bainite dual-phase X80 SENB specimen was not less than 2.0 mm. Microhard-
pipeline with a thickness of 26.4 mm was used as the base ness tests were performed on the polished specimens
material. The chemical composition of the X80 steel is as across the weld using a Vickers hardness tester (FM-
shown in Table 1. Plates were cut from the commercial ARS 9000) at a load of 500 gf.
longitudinal submerged arc welded (LSAW) pipe with a The analysis of microstructures was performed using
diameter of 1219 mm. The tensile strengths of the BM optical microscopy (OM), scanning electron microscopy
and welded joint are approximately 723 and 702 MPa, (SEM) (S-3400N), EBSD (EDAX) and transmission elec-
respectively. The tensile strength in the welded joint is tron microscopy (TEM) (JOEL 2010).
lower than that in the BM.
Specimens were machined from the BM and welded
joints for tension testing and fatigue testing as shown in
Fig. 1a. Two types of fatigue specimens were machined: Results and discussion
fatigue life specimens and fatigue crack propagation
specimens. In the fatigue life test, full-thickness specimens Microstructure change and microhardness
were used and the steel plate surface and welded joint profile
were not subjected to machining (Fig. 1b). This study Figure 2 depicts typical OM images showing the various
aimed to provide results that could reflect the actual fati- weld zone microstructural regions of LSAW pipe. A
gue life of LSAW pipe. In the fatigue crack propagation macroscopic cross-section of a welded joint is shown at
test, single-edge notched bend (SENB) specimens were the top indicating the various weld regions as BM,
used (Fig. 1c). The location of notch was determined by HAZ and fusion zone (FZ). The BM microstructure con-
the situation of fracture in the fatigue life test. sists of polygonal ferrite (PF) and bainite (BF) (Fig. 2b).
The fatigue life tests were performed by using an MTS The fraction of PF is approximately 54 vol.-%. BF is pre-
servo-hydraulic universal testing machine. A stress ratio dominant granular BF, which consists of fine lath ferrite
(R = σmin/σmax) of 0.1, sinusoidal waveform and a and M/A constituents distributed in the matrix.11
The HAZ contained four different subregions: coarse-
grained (CG), fine-grained (FG), intercritical-grained
(IC) and subcritical-grained (SC). As shown in Fig. 2d,
the CGHAZ microstructure is characterised by BF. The
primary austenite grain boundaries are clearly visible
and the grain sizes gradually decreases with distance from
the fusion line (Fig. 2e). In FGHAZ, the structure is a mix-
ture of BF and ferrite (Fig. 2f ). Meanwhile, in ICHAZ, the
microstructure is unsharp as-rolled mixed one (Fig. 2g).
The SCHAZ microstructure is similar to BM (Fig. 2b and h).
Microhardness values of inside and outside welds are as
shown in Fig. 3. Both of them are consistent in trend with
different regions. The highest hardness value is at FZ and
the hardness gradually declines with distance from the
fusion line. The average hardness in the FGHAZ is
205 HV, which represents the lowest hardness observed.
Compared with BM hardness (around 220 HV), the
FGHAZ hardness decreases significantly, i.e. softening
has occurred in this weld region. According to the descrip-
tion above (Fig. 2), the hardness profile of the welded joint
was corresponding directly to the microstructural change.
1 Schematic illustrations showing the a layout and section- The changes of local microstructure and hardness of the
ing locations of test specimens, b the critical dimensions HAZ influence the overall failure mechanism and fatigue
of the tensile and fatigue test specimens and c SENB crack growth behaviour; these are discussed in succeeding
specimens. All dimensions are in mm sections.
2 OM images of the welded joint microstructures: a welded joint, b BM, c fusion line, d CGHAZ microstructure close to fusion
line, e CGHAZ microstructure far from fusion line, f microstructure of FGHAZ, g microstructure of IGHAZ and h microstructure
of SGHAZ
Fatigue life test stresses of the BM and welded joints are approximately
Fatigue life 350 and 250 MPa, respectively. The safety coefficient of
The S−N curves obtained from the load control fatigue the pipeline strength design is the highest when yield
tests are shown in Fig. 4. The fatigue limits of the BM strength is 80%. For the X80 steel, the minimum yield
and welded joints show nearly identical trend within strength is 550 MPa; hence, the maximum operating
the experimental range, i.e. the fatigue cycles increase stress may reach 440 MPa. Thus, the fatigue limits of
as the maximum stress decreases. The welded joints the BM and welded joints are approximately 4.2 × 105
have a remarkable lower fatigue life than that of the and 1.0 × 105 cycles, respectively, when the maximum
BM at different maximum stresses. The fatigue limit stress is 440 MPa.
Kt = b × [1 + a(t/r)l ] (2)
where α, β and λ are constants whose values are deter-
mined by the geometric shape of welds and the manner
of loading. t and ρ are the thickness of plates and the
notch root radius. For butt-welded joints, the constants
α and λ are usually 1 and 1/2, respectively. The constant
β can be described by β = 0.27 (tan θ)0.25, where θ is the
weld toe angle.
The calculation results of Kf are as shown in Table 2.
The outside weld has the larger fatigue notch stress con-
centration factor. Therefore, crack can easily initiate at
4 S–N curves of the BM and welded joint evaluated at R =
the outside weld during fatigue.
0.1, 10 Hz and room temperature
Apart from the local existence of stress concentration
caused by the weld toe profile, the bulky inclusions at sur-
face of the weld toe can also act as a site of stress concen-
Fracture analysis tration that causes crack initiation during fatigue, as
The fatigue fractures were observed to investigate the fati- shown in Fig. 5b. It was analysed and compared with
gue behaviour of the welded joints. Figure 5 shows the internal fracture surface. The inclusions near the fusion
results of SEM fracture surface of the specimen at a maxi- line were caused by the weld undercut during the welding
mum stress of 400 MPa. The macroscopic fracture indi- process.
cates fatigue fracture processes consisting of crack In summary, stress concentration caused by the weld
initiation, propagation and final fracture (Fig. 5a). The toe profile and bulky inclusions reduce the crack initiation
fatigue crack generally initiates at the surface and propa- life when cracks propagate from the weld toe. This
gates inward (Fig. 5b). Meanwhile, some bulky inclusions phenomenon is one of the reasons why the fatigue life of
exist on the surface and may act as crack sources. The the welded joint specimens is much lower than that of
crack propagation directions can be identified by the BM at different maximum stresses (Fig. 4). To improve
river line patterns (Fig. 5c), and fatigue striations are fatigue life, the formation of weld undercut during weld-
found on the fracture surface (Fig. 5d ). As the crack con- ing should be avoided and the weld toe profile should be
tinues to propagate inward, the fracture surface reveals given the necessary attention at the design and production
the ductile features of flat facets and plenty of clear second stage.
cracks (Fig. 5e). In addition, the spacing of fatigue stria-
tions in this area clearly increases compared with that in Effect of microhardness on fracture path
the early stage (Fig. 5d and f ). With the growth of the fati- The fatigue fracture consists of three different zones: fati-
gue crack, fatigue striation spacing and the size of second gue crack initiation, propagation and the ultimate frac-
crack further increase (Fig. 5g). The final fracture zone ture zone. For the welded joint specimens, fatigue cracks
consists of characteristic dimples (Fig. 5h). initiate at the weld toe and propagate stably inward
under cyclic loading (Fig. 5). Although the direction of
stable propagation is consistently perpendicular to the
Effect of stress concentration on fracture location loading direction for most specimens, the stable propa-
The fatigue life test shows that the initial failure position gation distance of fatigue crack decreases with increased
of the welded joint specimens located at the surface and maximum stress (Fig. 6a). When the effective loading
the crack propagated into the inner part of the specimens area of the cross-section is reduced to a critical value
5 Typical SEM micrographs of the fatigue fracture surface of the welded joints at a maximum stress of 400 MPa. a Overall view
of the fracture surface, b the position of crack initiation, c fracture surface close to CGHAZ, d magnified view of c, e fracture
surface close to FGHAZ, f magnified view of e, g the area close to ultimate fracture region and h ultimate fracture region
6 a Effect of maximum stress on crack propagation distance, b sketch map of fracture path
Different Correlative
subregions m C coefficient
8 Typical OM and TEM micrographs of the fatigue cracks in HAZ. a and c The area in CGHAZ, b and d the area in FGHAZ
9 Crystallographic characteristics of the fatigue cracks in CGHAZ. a Orientation image maps, b image quality maps with grain
boundary misorientation distribution, c image quality maps with CSL boundary distribution and d histogram of CSL boundary
fraction of total number of grain boundaries (%)
are mainly low-Σ (Σ ≤ 29) CSL boundaries. It has been of prior austenite grain it passed through gradually
reported that low-Σ CSL boundaries because of low decreases because of the increasing peak temperatures
boundary energy can play a significant role in the resist- in CGHAZ with distance from the fusion line (Fig.
ance of fatigue crack propagation.16,17 Hence, low-Σ 2e). However, given that the number of different direc-
CSL boundaries forming between bainite laths in differ- tion bainite laths per unit area increases, the fatigue
ent austenite grain boundaries can efficiently arrest and crack propagation resistance also increases. Conse-
deflect the propagation of fatigue microcracks. When quently, the da/dN growth rate decreases with the propa-
the fatigue crack propagates towards FGHAZ, the size gation of cracks.
11 Crystallographic characteristics of the fatigue cracks in FGHAZ. a Orientation image maps, b image quality maps with grain
boundary misorientation distribution, c image quality maps with CSL boundary distribution and d histogram of CSL bound-
ary fraction of total number of grain boundaries (%)
Besides low-Σ CSL boundaries, M/A constituents in maximum stress decreases to the maximum operating
granular BF also play a role that cannot be ignored for stress (440 MPa), the fatigue limits of BM and welded
fatigue crack growth behaviour. As shown in Fig. 10, joint specimens are approximately 4.2 × 105 and 1 ×
thin film-like and rodlike M/A constituents exist between 105 cycles, respectively.
the parallel BF laths. According to a previous report, an (ii) The fatigue crack initiation of the full-thickness X80
M/A film structure is an effective barrier to dislocation welded joint specimens occurs at the outside weld toe
motion and crack propagation, despite the small misor- because of stress concentration resulting from the
ientation between neighbouring grains.18 In addition, inclusions and weld toe profile; the fatigue crack
our previous study on BM indicates that rodlike M/A grows inward until the ultimate fracture forms. The
can strongly inhibit dislocation movement in crack tip stable propagation distance of fatigue crack decreases
and can arrest crack propagation.3 Thus, the M/A con- with increased maximum stress, and the direction of
stituents between BF laths can lead to strongly deflected ultimate fracture tends to the low hardness zone.
fatigue crack trajectories. This observation is consistent (iii) During fatigue crack propagation in HAZ, the crack
with that in our study. growth rate linearly increases with ΔK in every HAZ sub-
Compared with that in CGHAZ, the crack path in region. According to the Paris model, the m values of
FCHAZ is more tortuous and shows some branches CGHAZ, FGHAZ and ICHAZ are approximately 6.86,
during the main crack propagation process (Fig. 8b and 1.83 and 3.75, respectively. FGHAZ has the least value
d). Based on the above discussion, these results indicate because it has more low-Σ CSL boundaries that directly
that the crack propagation in the FGHAZ is much harder reduce the local driving force for crack propagation and
than that in CGHAZ; this deduction is in accordance increase the total length of crack path. Furthermore,
with the conclusion of m value (Table 3). The microstruc- film-like and rodlike M/A constituents can act as effective
ture in FCHAZ is dominated by a mixture of fine and barriers to the crack propagation in CGHAZ.
homogeneous BF and ferrite, significantly contributing
to the increase in the number of high-angle boundaries
(Fig. 11a and b). A considerable amount of ferrite–ferrite Acknowledgements
and ferrite–BF boundaries leads to the significant differ- This work was financially supported by the Natural
ence of direction and crack length between the two sides Science Foundation of China [Grant No. 51171162] and
of the grain boundary because it has low-Σ CSL bound- the Natural Science Foundation – Steel and Iron Foun-
aries (Fig. 11c). Thus, the direction of crack changes dation of Hebei Province [Grant No. E2015203234].
obviously after crossing low-Σ CSL boundaries. However,
the fraction of low-Σ CSL boundaries in CGHAZ and
FCHAZ are 10.7 and 16.9%, respectively (Fig. 9d and ORCiD
Fig. 11d ). Hence, the crack path in FCHAZ is more tor-
tuous than that in CGHAZ, and the crack growth rate in Z-P. Zhao http://orcid.org/0000-0001-5790-3356
FGHAZ is reduced accordingly because of the crack path
deflection that decreases the local driving force for crack
propagation. References
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