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Int. J. Mach. Tools Manufact. Vol. 38, Nos 5-6, pp. 647 656.

1998

~ Pergamon 1998 Elsevier Science Ltd. All rights reserved


Printed in Great Britain
PII: S0890-6955(97)00113-2 0890-6955/98 $19.00 + 0.00

A S S E S S M E N T O F S T E E L S U R F A C E R O U G H N E S S AND W A V I N E S S
IN R E L A T I O N W I T H P A I N T A P P E A R A N C E

J. SCHEERS, M. VERMEULEN, C. DE MARI~, K. MESEURE


OCAS N. V., the Corporate R&D center of the ARBED - SIDMAR Group
Zelzate, Belgium

Abstract
Paint appearance is an important factor in the overall product quality of steel sheet, especially in the
automotive industry. The present paper deals with the functional behaviour of the surface texture
according to paint appearance. The main results on the improvement of paint appearance of outer car
body panels, obtained with coated and uncoated cold rolled steel, textured with EBT-rolls, is reviewed.
There are different methods to relate steel sheet surface texture to the appearance after painting. From the
literature it is found that waviness has a detrimental effect on the surface appearance after painting.
Different roughness and waviness parameters are compared in order to find a good relation with paint
appearance.
The following surface texture parameters are evaluated in this study: roughness parameters Ra, peak
count Pc, waviness parameters Wca and amplitude between 0.5 - 5mm (Fourier analysis) and envelope
parameters motif W and Ra-macro, measured with a spherical stylus of radius 1.5mm.
Classical parameters such as Ra and Pc are only able to evaluate paint appearance for one single texturing
process, and within very limited range. The ability to predict paint appearance by Ra-macro and Wca also
seems to be limited, because of their dependency on the roll texturing technique. Based on extensive
testing, it is suggested that Fourier analysis might be the best approach to predict the appearance after
painting, and this independently of the texturing process.
The results clearly show the improved appearance of Sibetex textured sheets compared to conventional
textured sheets. This is due to the fact that, with Sibetex sheet, a reduction in waviness can be achieved.
J~ 1998 Elsevier Science Ltd

1. Introduction
The visual appearance of the painted steel sheet when it became obvious that the requirements
surface has always been given close attention for formability and appearance after painting
because it is often experienced as a first were difficult to reconcile. For a non-
expression of the quality of the product towards deterministic roughness, such as the traditional
the end-user, especially in the automotive and shot blast texture, one usually finds that the
consumer appliances industry. higher the roughness, the better the formability,
The two major objectives of the paint but the poorer the appearance after painting.
manufacturer are: first the optimisation of the
chemical and physical properties of the coating
1.1. SurfaceFeatures
to achieve an optimum corrosion resistance and Several studies are published in which the
second, a perfect visual appearance of the influence of the steel sheet surface on the final
painted outer panels. paint appearance is described. From the
Protecting the steel sheet against environmental literature it is found that the surface appearance
influences was also the main challenge for the after painting decreases with increasing
steel manufacturer for many years. More waviness [1, 2, 3, 4, 5, 6].
recently however, sheet steel manufacturers Surface features with short wavelength
have also been focusing their attention on the characteristics ( ~ < O.8mm [1] ) are commonly
visual appearance of painted steel sheet as soon defined as the 'roughness' characteristics of the
as it was clearly established that there was an surface. The 'waviness' characteristics are
influence of steel sheet topography on surface features with spacings larger than the
properties such as orange peel and image roughness features (~. > 0.8ram). Waviness is
clarity. Their interest increased still further measured as the difference between the

647
648 .I Schcers ~,/ ~t/

unfiltered profile and the filtered roughness painting. A relocation technique was used to
plot. As the cut-off of the filter is decreasing, carefully track the change of the surface profile
the waviness profile follows the unfiltered in function of the application of subsequent
profile more closely (Figure 1). coating layers of an automotive coating system.
Surface Profile The sheet texture in Figure 2 is a combination
of a shot blast texture on the tandem mill and an
j J ~ EBT texture at the temper mill. The waviness
of the substrate can easily be observed. The
_ . . - _ ~ / ' ~ , / ' ~ / ~ ~ t - - . . ~ J ~
cathodic electrocoat, the filler and top coat layer
Waviness Roughness
smoothens out the EBT roughness. The valleys
of the waviness however have been connected
Figure 1." Decomposition of the surface profile in and disturb the appearance of the painted
roughness and waviness surface.
In-the US the upper limit on waviness is often Numerous contributions can be found in the
taken to be 8mm, but a standard definition of literature to search a correlation between a
waviness has not yet been adopted [ 1]. single 2D-roughness or -waviness parameter
In the European automotive and painting and the appearance after painting [1, 3, 4, 5 ].
industry waviness is sometimes defined to have To obtain a good paint appearance, traditionally
wavelengths 0.5mm < ~, < 5mm. sheet with low average roughness Ra and high
Wavelengths larger than the waviness upper peak count Pc is used [1]. Figure 2 shows that
limit are defined as 'form error' features. [1] waviness rather than roughness disturbs the
The effect of waviness on the appearance of paint appearance. The fact that a low Ra is
painted pans is well-known. Power spectrum needed to improve the paint appearance is only
analysis indicates that only undulations with a due to the relationship between roughness (Ra)
wavelength larger than a certain threshold (500 and waviness (Wca) for random textured sheets.
to 800 lam), are important for the paint quality. Therefor more recent studies are considering
The undulations with smaller wavelength the effect of surface waviness on the final
(called roughness) are covered by the paint. appearance. Waviness parameters often used are
This is not the case for the larger wavelength the average waviness Wca or parameters
undulations, as illustrated in Figure 2. derived from Fourier techniques, examining the
surface profile by means of a spectral
representation of the surface features (e.g.

I/m
waviness features are extracted from the FFY-
amplitude spectrum). Recently envelope
parameters such as the French motif parameter
W and Ra-macro (using a spherical stylus with
Subetrate Cathodic Filler radius 1.5mm) are introduced. Table 1 summa-
Elect rocoat
rizes all the evaluated parameters in this paper.
Figure 2." Evolution of the surface topography
during the paint process Main users and 'accepted' limits for a good
appearance are also indicated (with [*]:
Three dimensional surface measurements were company requirements).
used to study the evolution of the surface during
Table 1: Topography parameters and specifications
Parameter Wavelen[ths Standard Users Limits
Ra < 2.5mm SEP1940 European car industry Ra < 1.5prn [ 1]
Pc < 2.5mm SEP1940 European car industry Pc > 50pks/cm [1]
pSm German car industry pSm < 350~tm [*]
Ra-macro < 2.5mm Scandinavian car ind. Ra-macro < 0.51am [*]
Wca 0.8mm - 8mm = JIS B0610 USA / Japan
W 0.5mm - 5mm = ISO12085 French car industry W < 1.81am[*]
FFT-amplitude 0.5mm - 5mm Paint Industry
Steel surface roughness 649

deterministic steel sheet surface texture has


1.2. Roll Texturing Techniques: from Shot
Blast to EBT been created : SIBETEX ®.

The application of roughness in the production


of steel sheet has a long tradition. At the
beginning of the twentieth century, the 1.3. Basics of Visual Appearance
roughening of mill rolls by shot blasting was Phenomena
introduced. Shot blasting (SB) was found to The visual appearance of a painted surface
remove the directional roughness from the experienced by the end-user is the combination
manual grinding procedures that were used until of many different optical aspects of the paint
then. Steel sheet produced with those roughed layer. The quality of the paint application is
rolls showed better formability and improved always of first and foremost importance. A
appearance after painting. The shot blast total absence of scratches, dust particles or
process was generalised during the fifties. Due other blemish must be achieved. The observer
to the difficulties to obtain a reproducible can be more or less sensitive to the surface
texture, the Electrical Discharge Texture (EDT) texture of the paint which can still be resolved
process was developed which resulted in a very by the human eye. The quality of the virtual
fine stochastic surface roughness [7]. image, whereby the observer does not focus the
Another development started at the early eye on the paint surface itself, is also of prime
eighties. Sidmar in association with the CRM importance. Finally, observers tend to be
and Cockerill Sambre developed the Lasertex sensitive to the intensity of the specular
(LT) process for texturing mill rolls by use of a reflection of the paint layer. From a technical
laser beam. As Lasertex introduced a so-called point of view at least four parameters should be
deterministic roughness, it can be considered as measured in order to assess the quality of a
an important milestone in the evolution of the paint finish on steel substrates.
steel sheet surface textures. Since then this These parameters are :
technology has been applied world-wide and
further developed [8]. • intensity of the specular reflection (Gloss)
Recently, again Sidmar was involved in the • width of the specular reflection (DOI)
development of a fourth mill roll texturing • reflected image distortion (NSIC)
system: the Electron Beam Texturing (EBT). • loss of contrast in the reflected image
The EBT texturing system introduces the fully (NSIC*)
deterministic surface texture, applicable to
tandem and temper mill rolling. A detailed Tests were carried out to determine which of
description of the EBT system can be found in the above measured parameters have a strong
the literature [9]. correlation with the visual perception of the
image clarity of painted steel sheet [4, 6]. From
The four existing roll texturing processes can be the calculated correlation coefficients an
ranked based on the degree of randomness (or Appearance Index (A.I.) was defined as a
determinism) of the obtained surface profiles. weighted average of gloss, distinctness of
Shot Blast Texturing and EDT are strongly image, image distortion (orange peel) and loss
random, EBT is fully deterministic. This means of contrast.
that the texture is build up by a repeating
pattern of peaks and valleys formed by craters A.I. = 0.15 Gloss (20 °) + 0.35 DOI
in such a way that the surface can be described + 0.25 NSIC + 0.25 NSIC*
with a limited number of parameters (e.g. crater
distance, crater diameter, depth, type of This appearance index provides an objective
pattern .... ) [10]. The introduction of EBT also tool for further research. The maximum value
made it possible to use deterministic textured 100 corresponds to a perfect appearance.
rolls at the tandem mill. The use of a Current state-of-the-art automotive paint
deterministic EBT texture at the tandem mill systems, applied on the commercial available
has led to a breakthrough in the development of sheet qualities for outer panels, are commonly
steel sheet roughness. In combination with an accepted as good when the calculated index
EBT texture at the temper mill, the first fully equals 80 or higher [4, 6].
650 ,1. Scheers eta/.

2. Experimental Set-up 2.2.1. Roughness


Average roughness Ra, Peak Count Pc and
2.1. Steel Substrates mean spacing Sm are calculated according to
The steel surfaces used in this study were SEP1940-92 (without pivoting skid). The cut-
selected to cover a wide range of different off ~-c is set to 2.5mm (ISO 2RC), with an
characteristics. Different textures (SB, EDT, assessment length of 12.5mm (standard: 5 * ~).
EBT and SIBETEX), cold rolled (CRS) or Zn- For each parameter the mean value of 4
and ZnFe-coated (Hot dip galvanised GI, measurements is taken. The 2 Pc levels are set
galvannealed GA, Electro-galvanised ELO) to -0.5 and +0.5~tm [11].
were tested. 2.2.2. Waviness
Figure 3 shows a box & whisker plot of the For the calculation of the average waviness
average roughness Ra (as per SEP1940-92) for Wca a digital filtering is recommended to
the different textures (polished, Sibetex, EDT separate the roughness features from the
and Shot Blast). All textured steel sheet waviness features (0.8mm < ~.< 8mm) [1]. Two
materials (Shot blast, EDT and Sibetex) have successive filtering operations to simulate this
about the same Ra-range, with exception of a band pass filter are used at OCAS. A phase
few outliers (with Ra = 3.01am for sanitary corrected Gaussian filter (according to
applications). DIN4777) with cut-off 8mm is used to remove
the form error from the unfiltered profile (this
means wavelengths ~. > 8mm). A 0.8mm cut-off
3.0
Gaussian filter is then used to remove ~. <
0.8mm. After tilt removal of this remaining
2.S
'waviness' profile, the mean height Wca is
2,0 calculated. The final assessment length for Wca
l.S
is 40ram (= 5 * ~ (8ram)). Again, 4
measurements are averaged.
1.0
Fourier analysis is used to examine the surface
O.S features by means of a spectral presentation of
0,0 o
the features. Before Fourier transformation, an
Polished SIbelex EDT Shot Blmet
8mm cut-off (Gaussian) filter is used to remove
the form error from the unfiltered profile with a
Polished S~lex EDT Shot Blur
3.G total measuring length of 100mm. The
1 i amplitude spectrum of the remaining profile
2.G -- :
, i results in 500 spectral points between
o ~T
wavelengths 80mm and 1601am. This spectrum
shows the relative weight of surface features
with various wavelengths. In this study the
= E:3 7s~ mean FFT-amplitude between wavelengths of
__ 2s'~
0.S -- i i ' ul~i|n 500~tm and 5mm (= mean value of amplitudes
0.0 n i J of 144 spectral points) is taken into account,
CRS GI GA ELO CRS GI ELO cgs G[
following the European painting guidelines. The
Figure 3." Ra-range of all tested materials mean amplitude of 5 profile measurements is
computed to obtain a statistical significant
2.2. Surface Characterisation value.
A Rank Taylor Hobson Form Talysurf $5 stylus 2.2.3. Envelope Techniques
profilometer with 120L traverse unit is used to The method of filtering and analysis of the
perform 2D topography measurements. motif parameter W is different and not
Five surface traces, 45 ° with respect to the directly comparable with the other parameters
rolling direction, are recorded for each sample (other parameters are all calculated relative to
over a scan length of 100mm. All parameters the mean line) [12]. A motif is a part of a
are computed from the measured profiles after profile between 2 peaks (so every motif also
appropriate filtering. contains a valley?). This motif is characterised
Steel surface roughness 651

by means of 3 points and is illustrated with 3 For this type of research, the paint system is
lines: heights Hi and Hi+l and length A (Figure often applied on a glass plate because the initial
4). roughness and waviness are very low. The
disadvantage of this method however is that a
potential influence of the phosphate layer and
the electropaint is not taken into account. For
this reason a high quality paint appearance was
HjI H defined by applying a state-of-the-art high gloss
automotive paint system on polished steel
panels. This reference system was measured
AR, or AW~
and the calculated appearance index reached the
Figure 4: Definition of a Motif level of 92. This value was considered as our
target objective in the development of an
Hj en Hj÷l : motif heights optimum roughness for excellent appearance
T: minimum of Hj / H~j after painting.
AR~:Length of roughness motif All 60 materials, including the polished
AWl: Length of waviness motif samples, are painted using the same tri-cation
phosphate pre-treatment, paint system, applica-
Four successive algorithms try to combine the tion method and layer thickness. For each
motifs to 'stronger', larger motifs (e.g. common substrate all appearance parameters are mea-
peak < two extremes; new T > 2 'old T's; ...). sured on 10 painted samples. The average of the
Difference between roughness and waviness is readings is used to calculate the overall
defined by means of so-called operators: appearance index. Although the same substrate
roughness operator AR = 0.5ram and waviness and paint system may be used, it is well-known
operator A W = 5mm. The length of a motif within the automotive industry, that there can be
always needs to be smaller than the operator a substantial difference in the paint appearance
(e.g. length of waviness motif < 5mm). The on vertical parts in comparison with horizontal
waviness profile is found by combining the parts. Therefor the laboratory paint application
roughness motif heights. Motif parameter W and curing is sometimes carried out on the
calculates the mean height of the waviness panels in both horizontal and vertical
motifs. An assessment length of 30mm is used. orientation.
In this contribution, the mean motif W value of
5 measurements is used.
R a - m a c r o is the average roughness (cfr. Ra)
measured with a spherical stylus with radius r =
1.5mm without skid [3]. Ra-macro is calculated 3. Results
in a similar way as the average roughness
according to SEP1940-2 (cut-off ~ is set to 3.1. Texture and Paint Appearance
2.5mm (ISO 2RC), with an assessment length of Figure 5 compares the paint quality of all
12.Smm (standard: 5 * ~ ) , the mean value of 4 materials listed in table 2 using the defined
measurements is taken) [3]. appearance index A.I. by means of Box &
Whisker plots. The left figure shows the range
2.3. Definition of high quality paint of A.I. found for all materials (non coated and
appearance and panel preparation Zn-coated) with the polished reference material
The initial state and nature of the metal and the three different texture types (Sibetex,
substrate contributes to a large extent to the EDT and Shot Blast) on horizontal parts. Effect
appearance of a painted surface. It must of the coating itself (non coated, hot dip
however always be kept in mind that a paint galvanised GI, galvannealed GA or electrolytic
system can, by virtue of its formulation or galvanised ELO) on the paint quality A.I. is
application conditions, also be the cause of shown on the right.
surface roughness and waviness, not related to Figure 3 already showed that all the
the substrate waviness. Therefor a reference investigated textures have about the same
system is needed for further analysis. roughness-range.
652 ,1. Scheers et td.

100 IOO,
Polllhacl Slbetex EDT Shol B l o t
tO o

80

-4

50

4O

3O
PoIllhtd Sbtlz EDT Shot Blair CRS GI GA ELO CRS GI ELO CRS GI

Figure 5." Paint quality of several sheets with different coatings and surface textures

The left figure shows that all the Sibetex Figure 6 shows the appearance index A.I. as a
textured sheets (this means either cold rolled, function of Ra and Pc.
galvanised, galvannealed or electro-galvanised)
have an excellent paint quality, comparable to I ]
• .:,
that of a polished sheet that was used as a
a0 _ ii ~llt II1- . . . . . ~ --
reference. For the same roughness range,
Sibetex significantly improves the appearance • AAi • •
compared to Shot Blast or EDT. Besides, EDT
and Shot Blast show a much larger range in A.I.
comparing to Sibetex. 4o
Galvanised coated sheet (GI) is known to be
less adapted for outer panels. Although the
2000
Sibetex Galvanised sheet is not as good as the R, (pml
other Sibetex sheets (somewhat larger A.I. - 100

range), the improvement by applying EBT is


most pronounced for this type of coating. 8o

'A
3.2. Topography and Paint appearance
m~
In this topic a study is performed to find an i ~ • " ~ T .......
overall correlation between the paint
appearance (A.I.) and some roughness and 4o

waviness parameters, independent on the ! I


texture or coating. The paint is applied on 2o
~o 40 eo
horizontal parts. Pc(pkg/cm)

Roughness parameters (Ra, Pc, Sm), waviness


Figure 6: Appearance Index A.L versus Ra (top) and
parameters (Wca, FFT amplitude between 0.5
peak count Pc (bottom)
and 5mm) and envelope parameters (motif W
and Ra-macro) are compared to the appearance There is no general correlation between the
index A.I.. paint appearance (A.I.) and Ra. The polished
The aim is to highlight these parameters which material, with the lowest Ra-value gives the
can predict effectively the paint quality. best appearance after painting. Stochastic
textured materials such as Shot Blast and EDT
3.2.1. Roughness parameters and Paint
indeed show a decrease of the paint appearance
Appearance
with increasing Ra. On the contrary, with
Relation between Ra, Pc, Sm and Paint Sibetex, the paint appearance becomes almost
Appearance independent of Ra. A specification limiting Ra
In the literature it is often described that steel < 1.51am to assure good appearance is not valid:
sheet with low Ra and high peak count Pc lead Shot Blast and EDT-materials with Ra between
to a better appearance. In the European car 1 and 1.51am already show A.I. < 80%. Sibetex
industry it is frequently requested to have a with even larger Ra-values between 1.5 and
steel sheet with Ra < 1.51am and Pc > 50pks/cm. 21Jm, still show an A.I. of about 85. With this
Steel surface roughness 653

Ra-range, the stochastic surfaces (Shot Blast negative skewness. Only a small decrease of the
and EDT) show much lower A.I. values of appearance A.I. with increasing Sm is found.
about 70. Shot Blast and EDT surfaces with Sm-values
Two materials (Shot Blast and EDT) with larger than 1501am already give a poor paint
extreme Ra-level (>3.01am) used in sanitary quality (A.I. < 80). Moreover, a large scatter in
applications are tested as a reference. They both A.I. - values is found for Sm > 2001am for Shot
show the worst appearance (A.I. ~ 40). Blast.
For stochastic textures (EDT, Shot Blast) an
3.2.2. Waviness parameters and Paint
increase of A.I. with the peak count Pc can be
Appearance
found.
As expected, the three investigated roughness
The traditional trend, found with stochastic
parameters (Ra, Pc and Sin) do not show a
textures, that a high peak count value results in
sufficient correlation with the appearance after
a good paint appearance, is no longer valid for
painting. The painting smoothens out the
Sibetex. It seems to be difficult to define a Pc-
roughness of the substrate surface. Features
limit for good paint appearance (as in the case
with longer wavelength undulations (waviness)
of Ra). Sibetex materials with Pc < 50pks/cm
are not filtered out as effectively by the paint
still give an A.I. of about 90.
and remain present on the surface of the paint
A problem arises from the definition of the peak
layer. This is the reason why surface waviness
count. Pc-values are affected by the choice of
has a strong impact on the appearance. The
the bandwidth (in SEP1940-92: _+ 0.51am). The
following investigated parameters (Waviness
polished material has a Pc = 0 pks/cm because
parameters or envelope parameters) are said to
the surface peaks never exceed the 2 reference
have a better correlation with the paint
lines +_ 0.51am. Pc (and Ra too) is a parameter
appearance.
calculated relative to the mean line (this means
sum of profile areas above and below mean line Influence o f waviness p a r a m e t e r Wca on P a i n t
are equal). For Sibetex materials with high Appearance
bearing ratio (negative skewness), this mean Figure 8 shows the paint appearance (A.I.) as a
line is placed closer to the surface. This leads to function of the average waviness Wca in the
a bad peak count with lower Pc-values. range of 0.8mm < ~ < 8mm.
It is suggested to use the mean spacing Sm to
eliminate the problem of the bandwidth in the L . , ! I
definition of Pc. Sm is also related to the mean
line but does not need a bandwidth. Sm gives
the mean distance of the peaks relative to the
mean line. -- F .......... T- - i~.-- T ....... ] . . . . . .

Figure 7 shows the appearance index A.I. versus / i I I /..--~1


the mean spacing Sm.
'°r........... ! ......... ........... .L_OI

eo .....
l.%, 't
i
]
I
,-

I
I

- - V - -
I
I

I
T
i"

i
.

li
I
;
i

i - - * - - ~

~
,!

-- ~
I
I
l

!
--
2.0
t
':!o

.......... ~ ....
!
o!,

& -- E
,!o
W©l ( . m )

--
!

4-
..h ~.b

--
,!,

- I - ~
,.°

....
:

1.2 . . . . . . . . . . . . . . . . . . . . . . . .

2o :
so
i
too 160
i [
200 Ix 300 ~0 ............ 7--- 7.- R-F - t---
Sm tpml ..... 7 - 7 - • . . . . T---
Figure 7: Appearance Index A.I. versus mean
::
spacing Sm °~o" °!, ,!o ,', ,!o ,!, ,!....
R1 ( p l )
In general, a decrease of the paint appearance
with Sm is found. Sibetex materials show a Figure 8." Paint appearance A.I. versus Wca (top)
rather small mean spacing Sm, due to the and Wca versus Ra (bottom)
654 J. Scheers et J/.

In general, the paint appearance A.I. decreases Relation between FFT-amplitude (0.5 a n d 5mm)
with increasing Wca. Although, no overall and Paint Appearance
correlation can be found for all textures and Figure 10 compares the paint appearance (A.I.)
coatings. The polished reference material with with the mean FFT amplitude (between 0.5 and
lowest Wca, gives the best appearance A.I. = 5mm).
92. Stochastic textures (shot blast, EDT) show a
strong decrease of A.I. with increasing waviness
Wca. For Sibetex, this decrease is less
pronounced. Even for Wca larger than 0.51am,
8O
all Sibetex materials show a paint quality A.I. >
80. The use of stochastic surfaces with the same
Wca-level result in a poor paint appearance (A.I 60

<< 80).
An explanation can be found in Figure 8 4O

(bottom) where Wca is plotted versus the


average roughness Ra. In general one can ZO
O0 01 02 03 04
observe that Wca increases together with Ra. FFT-.mpliludl (~lm)

The polished steel panel with low Ra, does not 06

show waviness (Wca <<). For stochastic


surfaces such as EDT and shot blast, a strong
increase of Wca with Ra is found. Due to the
stochasticy of the shot blast and EDT methods,
a wide range of topographic wavelengths is
introduced during texturing. Waviness and ~02
roughness are related in such a case. This is the
only reason why a (relative) good correlation °' • i F - ~- I • sh,,o,o,,I
can be found between roughness (Ra) and paint o°oo oIs i o: i s, ~ o; i
2~, 3 0! 3S
appearance for random surfaces. R I Ipm)

Deterministic texturing, such as Sibetex,


Figure 10: Appearance Index A.I. vs mean FFT-
permits the optimisation of sheet textures with amplitude between 0.5 and 5ram (top) and
large roughness values for severe deep drawing FFT-amplitude vs Ra (bottom)
applications, without introducing waviness to
preserve a good paint quality. Sibetex shows
small Wca-values (< 0.41am) for Ra's up to A good correlation between the mean FFT
1.51am. Some Sibetex materials with Ra > amplitude (0.5 - 5mm) and the appearance index
1.5Jam show somewhat larger waviness amounts is found. This correlation between the
(0.5 < Wca < 0.61am). This waviness amount is amplitude and A.I., shows only little scatter and
introduced by profile-parts with different is the best among the tested parameters. A
(average) heights. The profile passes correlation coefficient of 0.92 is found. A mean
successively through areas with a 'low' level FFT-amplitude limit of 0.251am can be specified
(EBT crater valleys) and areas with a 'higher' to preserve a good paint quality. However, such
level (in-between the EBT craters). This is an a 'limit value' can only be used with the same
artificial waviness introduced by the filtering paint system and the same application
according to the mean line concept (Figure 9). conditions (horizontal panels).
This contribution of artific ll 'waviness' Materials with low waviness (polished sheet,
features will hardly.effect the paint quality. Sibetex) show the best paint appearance. Shot
blast and EDT with high FFT amplitude result
in a low appearance index. Sibetex always
shows a lower waviness amount compared to
shot blast or EDT for the same roughness Ra
level. Both stochastic surfaces (Shot blast,
EDT) show the same level of waviness for a
Figure 9." Sibetex and waviness given roughness Ra.
Steel surface roughness 655

3.2.3. Envelope Parameters and Paint


Appearance influence the paint quality. Therefor no good
Relation between Motif W (0.5 and 5mm) and correlation between W and A.I. is found.
Paint Appearance Further research on form removals is needed.
Figure 11 shows the appearance index A.I.
Relation between Ra -macro and Paint
versus waviness motif W.
100
Appearance
In the beginning of the nineties, a new
"...~ ; : . . •
measuring method called Ra-macro has been
8...................... !?* ..................................... ...................... presented to find a better correlation with the
AA :

paint appearance and especially with the orange


~ 6O
peel on vertical panels. With Ra-macro a
spherical stylus with a large radius of 1.5ram is
used as a mechanical filter. The mechanical
filter will follow the profile peaks and will not
record valleys with distances smaller than the
radius (1.5mm). These small valleys are not
1 2 3 4 5 s ?

w (~m)
dominating the appearance as they will be filled
Figure 11: Paint appearance (A.I.) versus motif W by the paint. Profile wavelengths smaller than
0.8mm (roughness), which will be covered by
m i u4,vt ~ D o It i
the paint film, are filtered by the stylus.
Wavelengths between 0.8 and 3.5ram
(waviness, important for orange peel) will be
. i ; i
highlighted. Ra-macro is proposed to be a
measure of the peak density and the peak height
variation of the surface profile. Hald6n [3]
found a very good correlation between Ra-
macro and tension (= measure of orange peel).
• .s . . . . . . . . . . . . . . . . . . . . . . . . . . . . ~ ..... ;.............. The Ra-macro concept seems therefor to be a
1, ~
o s to ss 2o
~ ~
2s x
~.o
very promising method. It combines the
advantage of the motif W concept, namely to
Figure 12." Influence of form error removal on W construct an envelope on the top of the profile
(top: LS Line; bottom: 2nd polyn.) peaks, with a filtering to remove the form error.
One can not find a good correlation between Research to evaluate Ra-macro with the OCAS
A.I. and waviness motif W. A motif W-limit of appearance index A.I. need to be done.
1.81am seems to hold only for stochastic
surfaces. Sibetex materials with W up to 41am 4. Conclusions
still show an excellent appearance index A.I.. The paint quality of several materials with Shot
Waviness motif W seems to be strongly Blast, EDT or Sibetex texture has been studied.
dependent on the form error (in this case those Different coatings were taken into account (non
large wavelength undulations with ~, > 5mm). coated, hot dip (GI) and electrogalvanised
This problem can be explained by the fact that (ELO), galvannealed (GA). A high gloss
no upper cut-off limit is specified in the ISO automotive paint system was applied
12085 standard for measuring the motif horizontally on all materials.
parameters. Only a LS-line procedure (tilt Paint quality was characterised by means of a
removal) is recommended. Measurements weighted average of gloss, DOI, orange peel
performed on steel panels with 'large' form and contrast loss: appearance index A.I.. A high
error features (e.g. curved panel) will show quality paint appearance was defined by
large motif W values. This is illustrated in applying the paint system on a polished
Figure 12: the polished sheet panel shows a reference steel panel resulting in a A.I. = 92.
smaller W after removal of the form error by a Different roughness and waviness parameters
2nd order polynomial operation (W = 0.211am are compared with the appearance index A.I. in
compared to W = 0.581am for only LS line order to find a good correlation with the paint
removal). The form error itself will hardly quality.
656 J. Scheers et al.

Roughness parameters, such as Ra, Pc and Sm 2. M. Sakurai, J.I. Inagaki, M. Yamashita,


give a rather poor overall correlation with the Effects of Surface Texture of Galvannealed
surface appearance after painting. This can be steel sheet on Image Clarity after Painting, in
explained by the fact that the fine roughness Proceedings of the Galvatech '95 Conference,
599, (1995)
features are covered by the paint. Although, for
stochastic surfaces (Shot Blast, EDT) one can 3. M. Hald6n, J.O. Nilsson, L.E. Brattstrom, S.
find that small Ra- and high Pc-values are Holmgren, Characterisation of Steel Sheet
beneficial for the paint appearance. With Surfaces in order to predict Surface
Sibetex, the appearance index A.I. becomes Appearance after Painting, in Proceedings of
the Rolls 2000 Conference, 196-205, (March
nearly independent of Ra, Pc or Sm.
28-29 1996)
Some waviness parameters show an improved
correlation with the appearance index. 4. J. Scheers, C. De Mar& K. Meseure,
Waviness parameter Wca and especially FFT- SIBETEX: Steel's Contribution to an
analysis can be used to predict the paint improved Paint Appearance for Outer Car
Body Panels, Proceedings IBEC'96, 24,
appearance.
(1996)
For stochastic surfaces a strong decrease of A.I.
was found with increasing waviness Wca. For 5. C. Lahaye, An Empirical Method to Predict
these random surfaces Wca is related with the Paint Appearance Starting with Substrate
roughness Ra. High roughness values also result Roughness Data, Proceedings IBEC'96, 24,
(1996)
in an increased waviness amount which reduce
the paint appearance. 6. K. Meseure, J. Scheers, C. De Mar6, Paint
Best overall correlation was found between A.I. Appearance in relation to Surface
and (for all textures and coatings) the mean Topography, Sibetex 3 Seminar, (October 24,
FFl'-amplitude between 500tam and 5ram. The 1996 OCAS Zelzate, Belgium)
appearance index A.I. decreases with increasing 7. D.K. Aspinwall, M.L.H. Wise, K.J.
mean FFT-amplitude. A correlation coefficient Stout,T.H.A. Goh ..... Electrical Discharge
rA2 of 0.92 was found. Texturing, Int. J. Mach. Tools Manufact., 32,
The Motif parameter W gives a rather poor 183-192, (1992)
correlation with the appearance index A.I.. 8. J. Defourny, P. Jodogne, Lasertex: un concept
Motif W also seems to be strongly dependent on de rugosit6: du laminoir/t la tfle rev&ue, La
form error features (i.e. bending) which do not Revue de Mdtallurgie, 439-446, (Mai 1992)
influence the paint quality. 9. A. Hamilius, H. Deroo, L. De Graef, D. De
The best paint quality is obtained with Sibetex Soete, Y. Gadeyne, Gravure des cylindres de
deterministic textures. For the same roughness laminage ~ l'aide d'un faisceau d'61ectrons, La
level Ra, Sibetex always gives the lowest revue de M~tallurgie, 1083-1091, (1992)
waviness amount (Wca or mean FFT-
10. M. Vermeulen, J. Scheers, C. De Mar6,
amplitude). Deterministic texturing is the only Characterisation of EBT surfaces, Sibetex 2
way to avoid waviness. The inherent variability Seminar, (October 20, 1994 OCAS Zelzate,
of the random texturing methods (Shot Blast, Belgium)
EDT) is responsible for introducing a wide
11. Messung des Aritmischen Mittenrauwert Ra
range of topographic wavelengths on the roll
und der Spitzenzahl Pc an Kaltgewalzten
surface. The substrate waviness features can not Flacherzeugnissen aus Stahl, SEP 1940 Stahl
be masked by the paint film and have a Eisen Priifflolatt, Verein Deutscher
detrimental effect on the final paint appearance. Eisenhiittenleute, (January 1992)
12. F. Fritzsche, T. Hartmann, E. Heldt,
5. References Erfahrungen bei der Anwendung der Motif-
1. A. Bastawros, J.G. Speer, G. Zerafa, R. Methode zur Beschreibung Technischer
Krupitzer, Effects of Steel Surface Texture on Oberfl~ichen, Proceedings 9th lnternationales
Appearance after Painting, SAE Technical Oberfliichen-kolloquium, (29-31 Januar 1996,
Paper Series 930032 Chemnitz)

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