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Roughness and Paint Appearence
Roughness and Paint Appearence
1998
A S S E S S M E N T O F S T E E L S U R F A C E R O U G H N E S S AND W A V I N E S S
IN R E L A T I O N W I T H P A I N T A P P E A R A N C E
Abstract
Paint appearance is an important factor in the overall product quality of steel sheet, especially in the
automotive industry. The present paper deals with the functional behaviour of the surface texture
according to paint appearance. The main results on the improvement of paint appearance of outer car
body panels, obtained with coated and uncoated cold rolled steel, textured with EBT-rolls, is reviewed.
There are different methods to relate steel sheet surface texture to the appearance after painting. From the
literature it is found that waviness has a detrimental effect on the surface appearance after painting.
Different roughness and waviness parameters are compared in order to find a good relation with paint
appearance.
The following surface texture parameters are evaluated in this study: roughness parameters Ra, peak
count Pc, waviness parameters Wca and amplitude between 0.5 - 5mm (Fourier analysis) and envelope
parameters motif W and Ra-macro, measured with a spherical stylus of radius 1.5mm.
Classical parameters such as Ra and Pc are only able to evaluate paint appearance for one single texturing
process, and within very limited range. The ability to predict paint appearance by Ra-macro and Wca also
seems to be limited, because of their dependency on the roll texturing technique. Based on extensive
testing, it is suggested that Fourier analysis might be the best approach to predict the appearance after
painting, and this independently of the texturing process.
The results clearly show the improved appearance of Sibetex textured sheets compared to conventional
textured sheets. This is due to the fact that, with Sibetex sheet, a reduction in waviness can be achieved.
J~ 1998 Elsevier Science Ltd
1. Introduction
The visual appearance of the painted steel sheet when it became obvious that the requirements
surface has always been given close attention for formability and appearance after painting
because it is often experienced as a first were difficult to reconcile. For a non-
expression of the quality of the product towards deterministic roughness, such as the traditional
the end-user, especially in the automotive and shot blast texture, one usually finds that the
consumer appliances industry. higher the roughness, the better the formability,
The two major objectives of the paint but the poorer the appearance after painting.
manufacturer are: first the optimisation of the
chemical and physical properties of the coating
1.1. SurfaceFeatures
to achieve an optimum corrosion resistance and Several studies are published in which the
second, a perfect visual appearance of the influence of the steel sheet surface on the final
painted outer panels. paint appearance is described. From the
Protecting the steel sheet against environmental literature it is found that the surface appearance
influences was also the main challenge for the after painting decreases with increasing
steel manufacturer for many years. More waviness [1, 2, 3, 4, 5, 6].
recently however, sheet steel manufacturers Surface features with short wavelength
have also been focusing their attention on the characteristics ( ~ < O.8mm [1] ) are commonly
visual appearance of painted steel sheet as soon defined as the 'roughness' characteristics of the
as it was clearly established that there was an surface. The 'waviness' characteristics are
influence of steel sheet topography on surface features with spacings larger than the
properties such as orange peel and image roughness features (~. > 0.8ram). Waviness is
clarity. Their interest increased still further measured as the difference between the
647
648 .I Schcers ~,/ ~t/
unfiltered profile and the filtered roughness painting. A relocation technique was used to
plot. As the cut-off of the filter is decreasing, carefully track the change of the surface profile
the waviness profile follows the unfiltered in function of the application of subsequent
profile more closely (Figure 1). coating layers of an automotive coating system.
Surface Profile The sheet texture in Figure 2 is a combination
of a shot blast texture on the tandem mill and an
j J ~ EBT texture at the temper mill. The waviness
of the substrate can easily be observed. The
_ . . - _ ~ / ' ~ , / ' ~ / ~ ~ t - - . . ~ J ~
cathodic electrocoat, the filler and top coat layer
Waviness Roughness
smoothens out the EBT roughness. The valleys
of the waviness however have been connected
Figure 1." Decomposition of the surface profile in and disturb the appearance of the painted
roughness and waviness surface.
In-the US the upper limit on waviness is often Numerous contributions can be found in the
taken to be 8mm, but a standard definition of literature to search a correlation between a
waviness has not yet been adopted [ 1]. single 2D-roughness or -waviness parameter
In the European automotive and painting and the appearance after painting [1, 3, 4, 5 ].
industry waviness is sometimes defined to have To obtain a good paint appearance, traditionally
wavelengths 0.5mm < ~, < 5mm. sheet with low average roughness Ra and high
Wavelengths larger than the waviness upper peak count Pc is used [1]. Figure 2 shows that
limit are defined as 'form error' features. [1] waviness rather than roughness disturbs the
The effect of waviness on the appearance of paint appearance. The fact that a low Ra is
painted pans is well-known. Power spectrum needed to improve the paint appearance is only
analysis indicates that only undulations with a due to the relationship between roughness (Ra)
wavelength larger than a certain threshold (500 and waviness (Wca) for random textured sheets.
to 800 lam), are important for the paint quality. Therefor more recent studies are considering
The undulations with smaller wavelength the effect of surface waviness on the final
(called roughness) are covered by the paint. appearance. Waviness parameters often used are
This is not the case for the larger wavelength the average waviness Wca or parameters
undulations, as illustrated in Figure 2. derived from Fourier techniques, examining the
surface profile by means of a spectral
representation of the surface features (e.g.
I/m
waviness features are extracted from the FFY-
amplitude spectrum). Recently envelope
parameters such as the French motif parameter
W and Ra-macro (using a spherical stylus with
Subetrate Cathodic Filler radius 1.5mm) are introduced. Table 1 summa-
Elect rocoat
rizes all the evaluated parameters in this paper.
Figure 2." Evolution of the surface topography
during the paint process Main users and 'accepted' limits for a good
appearance are also indicated (with [*]:
Three dimensional surface measurements were company requirements).
used to study the evolution of the surface during
Table 1: Topography parameters and specifications
Parameter Wavelen[ths Standard Users Limits
Ra < 2.5mm SEP1940 European car industry Ra < 1.5prn [ 1]
Pc < 2.5mm SEP1940 European car industry Pc > 50pks/cm [1]
pSm German car industry pSm < 350~tm [*]
Ra-macro < 2.5mm Scandinavian car ind. Ra-macro < 0.51am [*]
Wca 0.8mm - 8mm = JIS B0610 USA / Japan
W 0.5mm - 5mm = ISO12085 French car industry W < 1.81am[*]
FFT-amplitude 0.5mm - 5mm Paint Industry
Steel surface roughness 649
by means of 3 points and is illustrated with 3 For this type of research, the paint system is
lines: heights Hi and Hi+l and length A (Figure often applied on a glass plate because the initial
4). roughness and waviness are very low. The
disadvantage of this method however is that a
potential influence of the phosphate layer and
the electropaint is not taken into account. For
this reason a high quality paint appearance was
HjI H defined by applying a state-of-the-art high gloss
automotive paint system on polished steel
panels. This reference system was measured
AR, or AW~
and the calculated appearance index reached the
Figure 4: Definition of a Motif level of 92. This value was considered as our
target objective in the development of an
Hj en Hj÷l : motif heights optimum roughness for excellent appearance
T: minimum of Hj / H~j after painting.
AR~:Length of roughness motif All 60 materials, including the polished
AWl: Length of waviness motif samples, are painted using the same tri-cation
phosphate pre-treatment, paint system, applica-
Four successive algorithms try to combine the tion method and layer thickness. For each
motifs to 'stronger', larger motifs (e.g. common substrate all appearance parameters are mea-
peak < two extremes; new T > 2 'old T's; ...). sured on 10 painted samples. The average of the
Difference between roughness and waviness is readings is used to calculate the overall
defined by means of so-called operators: appearance index. Although the same substrate
roughness operator AR = 0.5ram and waviness and paint system may be used, it is well-known
operator A W = 5mm. The length of a motif within the automotive industry, that there can be
always needs to be smaller than the operator a substantial difference in the paint appearance
(e.g. length of waviness motif < 5mm). The on vertical parts in comparison with horizontal
waviness profile is found by combining the parts. Therefor the laboratory paint application
roughness motif heights. Motif parameter W and curing is sometimes carried out on the
calculates the mean height of the waviness panels in both horizontal and vertical
motifs. An assessment length of 30mm is used. orientation.
In this contribution, the mean motif W value of
5 measurements is used.
R a - m a c r o is the average roughness (cfr. Ra)
measured with a spherical stylus with radius r =
1.5mm without skid [3]. Ra-macro is calculated 3. Results
in a similar way as the average roughness
according to SEP1940-2 (cut-off ~ is set to 3.1. Texture and Paint Appearance
2.5mm (ISO 2RC), with an assessment length of Figure 5 compares the paint quality of all
12.Smm (standard: 5 * ~ ) , the mean value of 4 materials listed in table 2 using the defined
measurements is taken) [3]. appearance index A.I. by means of Box &
Whisker plots. The left figure shows the range
2.3. Definition of high quality paint of A.I. found for all materials (non coated and
appearance and panel preparation Zn-coated) with the polished reference material
The initial state and nature of the metal and the three different texture types (Sibetex,
substrate contributes to a large extent to the EDT and Shot Blast) on horizontal parts. Effect
appearance of a painted surface. It must of the coating itself (non coated, hot dip
however always be kept in mind that a paint galvanised GI, galvannealed GA or electrolytic
system can, by virtue of its formulation or galvanised ELO) on the paint quality A.I. is
application conditions, also be the cause of shown on the right.
surface roughness and waviness, not related to Figure 3 already showed that all the
the substrate waviness. Therefor a reference investigated textures have about the same
system is needed for further analysis. roughness-range.
652 ,1. Scheers et td.
100 IOO,
Polllhacl Slbetex EDT Shol B l o t
tO o
80
-4
50
4O
3O
PoIllhtd Sbtlz EDT Shot Blair CRS GI GA ELO CRS GI ELO CRS GI
Figure 5." Paint quality of several sheets with different coatings and surface textures
The left figure shows that all the Sibetex Figure 6 shows the appearance index A.I. as a
textured sheets (this means either cold rolled, function of Ra and Pc.
galvanised, galvannealed or electro-galvanised)
have an excellent paint quality, comparable to I ]
• .:,
that of a polished sheet that was used as a
a0 _ ii ~llt II1- . . . . . ~ --
reference. For the same roughness range,
Sibetex significantly improves the appearance • AAi • •
compared to Shot Blast or EDT. Besides, EDT
and Shot Blast show a much larger range in A.I.
comparing to Sibetex. 4o
Galvanised coated sheet (GI) is known to be
less adapted for outer panels. Although the
2000
Sibetex Galvanised sheet is not as good as the R, (pml
other Sibetex sheets (somewhat larger A.I. - 100
'A
3.2. Topography and Paint appearance
m~
In this topic a study is performed to find an i ~ • " ~ T .......
overall correlation between the paint
appearance (A.I.) and some roughness and 4o
Ra-range, the stochastic surfaces (Shot Blast negative skewness. Only a small decrease of the
and EDT) show much lower A.I. values of appearance A.I. with increasing Sm is found.
about 70. Shot Blast and EDT surfaces with Sm-values
Two materials (Shot Blast and EDT) with larger than 1501am already give a poor paint
extreme Ra-level (>3.01am) used in sanitary quality (A.I. < 80). Moreover, a large scatter in
applications are tested as a reference. They both A.I. - values is found for Sm > 2001am for Shot
show the worst appearance (A.I. ~ 40). Blast.
For stochastic textures (EDT, Shot Blast) an
3.2.2. Waviness parameters and Paint
increase of A.I. with the peak count Pc can be
Appearance
found.
As expected, the three investigated roughness
The traditional trend, found with stochastic
parameters (Ra, Pc and Sin) do not show a
textures, that a high peak count value results in
sufficient correlation with the appearance after
a good paint appearance, is no longer valid for
painting. The painting smoothens out the
Sibetex. It seems to be difficult to define a Pc-
roughness of the substrate surface. Features
limit for good paint appearance (as in the case
with longer wavelength undulations (waviness)
of Ra). Sibetex materials with Pc < 50pks/cm
are not filtered out as effectively by the paint
still give an A.I. of about 90.
and remain present on the surface of the paint
A problem arises from the definition of the peak
layer. This is the reason why surface waviness
count. Pc-values are affected by the choice of
has a strong impact on the appearance. The
the bandwidth (in SEP1940-92: _+ 0.51am). The
following investigated parameters (Waviness
polished material has a Pc = 0 pks/cm because
parameters or envelope parameters) are said to
the surface peaks never exceed the 2 reference
have a better correlation with the paint
lines +_ 0.51am. Pc (and Ra too) is a parameter
appearance.
calculated relative to the mean line (this means
sum of profile areas above and below mean line Influence o f waviness p a r a m e t e r Wca on P a i n t
are equal). For Sibetex materials with high Appearance
bearing ratio (negative skewness), this mean Figure 8 shows the paint appearance (A.I.) as a
line is placed closer to the surface. This leads to function of the average waviness Wca in the
a bad peak count with lower Pc-values. range of 0.8mm < ~ < 8mm.
It is suggested to use the mean spacing Sm to
eliminate the problem of the bandwidth in the L . , ! I
definition of Pc. Sm is also related to the mean
line but does not need a bandwidth. Sm gives
the mean distance of the peaks relative to the
mean line. -- F .......... T- - i~.-- T ....... ] . . . . . .
eo .....
l.%, 't
i
]
I
,-
I
I
- - V - -
I
I
I
T
i"
i
.
li
I
;
i
i - - * - - ~
~
,!
•
-- ~
I
I
l
!
--
2.0
t
':!o
.......... ~ ....
!
o!,
& -- E
,!o
W©l ( . m )
--
!
4-
..h ~.b
--
,!,
- I - ~
,.°
....
:
1.2 . . . . . . . . . . . . . . . . . . . . . . . .
2o :
so
i
too 160
i [
200 Ix 300 ~0 ............ 7--- 7.- R-F - t---
Sm tpml ..... 7 - 7 - • . . . . T---
Figure 7: Appearance Index A.I. versus mean
::
spacing Sm °~o" °!, ,!o ,', ,!o ,!, ,!....
R1 ( p l )
In general, a decrease of the paint appearance
with Sm is found. Sibetex materials show a Figure 8." Paint appearance A.I. versus Wca (top)
rather small mean spacing Sm, due to the and Wca versus Ra (bottom)
654 J. Scheers et J/.
In general, the paint appearance A.I. decreases Relation between FFT-amplitude (0.5 a n d 5mm)
with increasing Wca. Although, no overall and Paint Appearance
correlation can be found for all textures and Figure 10 compares the paint appearance (A.I.)
coatings. The polished reference material with with the mean FFT amplitude (between 0.5 and
lowest Wca, gives the best appearance A.I. = 5mm).
92. Stochastic textures (shot blast, EDT) show a
strong decrease of A.I. with increasing waviness
Wca. For Sibetex, this decrease is less
pronounced. Even for Wca larger than 0.51am,
8O
all Sibetex materials show a paint quality A.I. >
80. The use of stochastic surfaces with the same
Wca-level result in a poor paint appearance (A.I 60
<< 80).
An explanation can be found in Figure 8 4O
w (~m)
dominating the appearance as they will be filled
Figure 11: Paint appearance (A.I.) versus motif W by the paint. Profile wavelengths smaller than
0.8mm (roughness), which will be covered by
m i u4,vt ~ D o It i
the paint film, are filtered by the stylus.
Wavelengths between 0.8 and 3.5ram
(waviness, important for orange peel) will be
. i ; i
highlighted. Ra-macro is proposed to be a
measure of the peak density and the peak height
variation of the surface profile. Hald6n [3]
found a very good correlation between Ra-
macro and tension (= measure of orange peel).
• .s . . . . . . . . . . . . . . . . . . . . . . . . . . . . ~ ..... ;.............. The Ra-macro concept seems therefor to be a
1, ~
o s to ss 2o
~ ~
2s x
~.o
very promising method. It combines the
advantage of the motif W concept, namely to
Figure 12." Influence of form error removal on W construct an envelope on the top of the profile
(top: LS Line; bottom: 2nd polyn.) peaks, with a filtering to remove the form error.
One can not find a good correlation between Research to evaluate Ra-macro with the OCAS
A.I. and waviness motif W. A motif W-limit of appearance index A.I. need to be done.
1.81am seems to hold only for stochastic
surfaces. Sibetex materials with W up to 41am 4. Conclusions
still show an excellent appearance index A.I.. The paint quality of several materials with Shot
Waviness motif W seems to be strongly Blast, EDT or Sibetex texture has been studied.
dependent on the form error (in this case those Different coatings were taken into account (non
large wavelength undulations with ~, > 5mm). coated, hot dip (GI) and electrogalvanised
This problem can be explained by the fact that (ELO), galvannealed (GA). A high gloss
no upper cut-off limit is specified in the ISO automotive paint system was applied
12085 standard for measuring the motif horizontally on all materials.
parameters. Only a LS-line procedure (tilt Paint quality was characterised by means of a
removal) is recommended. Measurements weighted average of gloss, DOI, orange peel
performed on steel panels with 'large' form and contrast loss: appearance index A.I.. A high
error features (e.g. curved panel) will show quality paint appearance was defined by
large motif W values. This is illustrated in applying the paint system on a polished
Figure 12: the polished sheet panel shows a reference steel panel resulting in a A.I. = 92.
smaller W after removal of the form error by a Different roughness and waviness parameters
2nd order polynomial operation (W = 0.211am are compared with the appearance index A.I. in
compared to W = 0.581am for only LS line order to find a good correlation with the paint
removal). The form error itself will hardly quality.
656 J. Scheers et al.