Professional Documents
Culture Documents
Manhi 931100 01
Manhi 931100 01
Manhi 931100 01
HI 931100 • HI 931101
Waterproof Instruments
for Salinity and Sodium
Content Measurements
www.hannainst.com
1
PRELIMINARY EXAMINATION
Preliminary Examination ...................................... 3 HANNA instruments® has designed these two rugged
General Description ............................................. 3 waterproof salinity and sodium meters for regular use
Functional Description HI931100 ......................... 4 in the lab, as well as in harsh processing
Specifications HI931100 ...................................... 5 environments.
Functional Description HI931101 ......................... 6 HI 931100 is an ion-selective meter that uses a sodium
electrode to read the salt (NaCl) content of a solution.
Specifications HI 931101 ..................................... 7
HI 931100 autoranges (4 scales available) from sample
Operational Guide ................................................ 8 to sample allowing an extremely wide range of
Na Calibration (HI 931101) ................................. 12 measurements without recalibration.
NaCl Calibration (HI 931100) ............................. 15 HI 931101 employs the FC 300B combination
Special Applications & Additional Info ............... 18 sodium electrode to provide sodium readings from 15.0
Temperature Calibration ..................................... 21 mg/L to 60 g/L.
FC 300B Conditioning & Maintenance ............... 23 The calibration is automatic at 2 points, the first is at
Battery Replacement ......................................... 26 2.3 g/L while the second can be either at 0.23 g/L (low
range) or at 23.0 g/L (high range).
Accessories ....................................................... 27
A separate temperature probe, HI 7662, provides tem-
Warranty ............................................................ 29
perature readings from 0 to 80ºC.
CE declaration of conformity ............................. 30
2 3
FUNCTIONAL DESCRIPTION HI 931100 SPECIFICATIONS HI 931100
Range
0.150 to 1.500 / 1.50 to 15.00 / 15.0 to 150.0
150 to 300 g/L NaCl
0.0 to 80.0°C
Resolution
0.001 / 0.01 / 0.1 / 1 g/L NaCl
0.1°C
Accuracy ±5% of reading (NaCl)
(@20°C) ±0.5°C
Typical EMC Deviation
±2% FS (NaCl) / ±0.5°C
Calibration Automatic, 1 or 2 point
at 3.00 g/L (HI 7083) and
0.30 g/L (HI 7085) or 30.0 g/L (HI 7081)
Temperature Compensation
25°C (77°F)
Electrode FC300B sodium electrode
with BNC and 1 m (3.3) cable (not included)
Temperature Probe
HI 7662 (not included)
Input Impedance 1012 Ohm
Battery Type / Life
4 x 1.5V AA / approx. 200 hours of use
Environment 0 to 50°C (32 to 122°F);
RH max 100%
Dimensions 196 x 80 x 60 mm
(7.7 x 3.1 x 2.4")
Weight 500 g (1.1 lb.)
1. Battery compartment
2. BNC connector for electrode
3. Temperature probe socket
4. LCD (Liquid Crystal Display)
5. ON/OFF key, to turn the meter on or off
6. CAL key, to enter/exit calibration mode
7. CFM key, to confirm calibration
8. BUF key, to select calibration buffer value
4 5
FUNCTIONAL DESCRIPTION HI 931101 SPECIFICATIONS HI 931101
6 7
For accurate readings, calibration should be per-
OPERATIONAL GUIDE
formed (or verified) every day if measuring the same
type of samples (e.g. cheese), or every time the
INITIAL PREPARATION sample type is changed (e.g. cheese, meat, sea
water, etc.).
Each meter is supplied com-
plete with four 1.5V AA batter- The recommended working temperature is around
ies. 20-25°C (68-77°F). For greater accuracy, perform
the calibration with standard solutions at a tempera-
Remove the back cover, unwrap
ture as close as possible to the temperature of the
the batteries and install them
sample.
while paying attention to their
polarity.
TAKING SODIUM MEASUREMENTS
Remove the protective cap from the
PROBE CONNECTION FC 300B sodium electrode and, if
possible, rinse it with some of the
Connect the FC 300B sodium FC 300B HI 7662N
SODIUM TEMPERA TURE sample to be measured.
electrode to the BNC socket on ELECTRODE PROBE
the top of the instrument.
Connect the HI 7662 tempera-
ture probe to the RCA socket.
The temperature probe can be
Shift downwards the rubber sleeve
used independently to take tem-
(see picture) to have a properly work-
perature measurements.
ing junction.
If the probe is not plugged in,
the secondary display shows gm
NaCl Immerse the tip of the FC300B elec-
"25°C" with the "°C" indicator °C
trode (at least 2.5 cm/1") into the
blinking.
sample to be tested while making
sure that the electrode junction is
completely immersed, and without
To switch the instrument on,
touching the bottom of the beaker.
press and hold the ON/OFF key
for a fraction of a second. Wait for approximately 10 to 15 minutes to allow
for the electrode to adjust and stabilize, i.e. until
These meters have a built-in protection against elec-
no drifting is observed for at least a couple of
tromagnetic interferences and the holding of the
minutes.
keys is to ensure that the commands are not mis-
taken for erroneous signals. During measurement, if possible,
the sample should be gently
In order to take accurate measurements, make
stirred (100 rpm).
sure the instrument is calibrated before use
(see "Calibration" sections for details).
MAGNETIC STIRRER
HI 190M
ON
POWER
OFF MAX
SPEED
8 9
TAKING pNa MEASUREMENTS (HI 931101 only) If the electrode is used rarely (once a month or
less), store it dry. Before using it again, let it
Press the MODE key during measurement to con-
condition overnight in HI 7081 (30.0 g/L NaCl) or HI
vert the value displayed by the HI 931101 to pNa.
7086 (23 g/L Na 1M)
Note that
To avoid very long response time, do not store
pNa = -log aNa
or rinse the electrode with deionized water. Do
where aNa is the activity of ion Na. not rub the electrode.
°C
MODE
TEMPERATURE MEASUREMENTS
Connect the temperature probe to
the meter and turn on.
Dip the HI 7662 temperature probe
into the sample. Allow the reading
to stabilize.
Note: The temperature is always
displayed on the secondary NaCl
gm
LCD. °C
AFTER USE
Turn the meter off by pressing the
ON/OFF key again.
10 11
SINGLE POINT CALIBRATION (OFFSET)
Na CALIBRATION (HI 931101)
• Dip the FC 300B sodium elec-
Calibration can be performed at 1 (offset only) or 2 trode into the HI 7080 (2.3 g/L
points. Na) solution.
For best accuracy, a 2 point procedure is recom-
mended.
PREPARATION
Note: Immerse the electrode
80
70
gm
°C
CAL BUF
12 13
• For exiting the calibration mode Wait for a couple of minutes
and save the single point cali- and then press the CFM key.
bration, press the CAL key. For
CFM
better accuracy however, it is CAL
recommended to perform a 2
• The two point calibration procedure is now com-
point calibration.
pleted and the meter automatically returns to the
normal measurement mode.
TWO POINT CALIBRATION
• After the first point is confirmed,
NaCl CALIBRATION (HI 931100)
immerse the FC 300B electrode
into the second standard solu-
tion: HI 7087 at 0.23 g/L Na or Calibration can be performed at 1 (offset only) or 2
HI 7086 at 23 g/L Na. points.
Note: The electrode should be For best accuracy, a two point procedure is recom-
immersed approximately mended.
2.5 cm (1") into the solu- PREPARATION
tion. • Pour small quantities of
83
70
HI
HI 7083 (3.00 g/L NaCl) solu-
tion and HI 7085 (0.30 g/L) or
• Select the calibration value by HI 7083 HI 7085
14 15
SINGLE POINT CALIBRATION (OFFSET) • To quit the calibration and save
the first point, press the CAL
• Dip the FC 300B sodium elec-
key.
trode into the HI 7083 (3.00 g/L CAL
NaCl) solution.
For better accuracy however, it is recommended
that a two-point calibration is performed.
CAL BUF
°C
• The two point calibration is now
completed and the meter re- CFM
16 17
SPECIAL APPLICATIONS &
ADDITIONAL INFORMATION
MAGNETIC STIRRER
HI 190M
OFF
SPEED
MAX
18 19
TEMPERATURE TEMPERATURE CALIBRATION
The best working temperature is around 20-25°C (for Technical Personnel only)
(68-77°F).
For greatest accuracy, it is recommended to cali- INITIAL PREPARATION
brate the meter with standard solution at a tempera-
ture as close as possible to the temperature of the Prepare a 0°C/32°F bath with ice and water and
sample (± 1°C/±2°F). another one at 50°C/122°F using hot water at a
known temperature. Place insulation material around
Na CONCENTRATION WITH HI 931100 the containers to minimize temperature changes.
Use a Checktemp or another accurate thermometer
It is always possible to determine the Na concentra-
with a resolution of 0.1° as reference.
tion by using the formula:
XNa = XNaCl • (23 / 58.4) °C °C
where
XNa = concentration of Na 0 °C 50 °C
(32 °F) (122 °F)
and
XNaCl = concentration of NaCl
Note: A blinking "°C" indicates
that the temperature probe NaCl
gm
is not connected. °C
PROCEDURE
20 21
• When the input value be-
FC300B CONDITIONING & MAINTENANCE
comes stable, the " " °C
CON
symbol disappears and
"CON" will start blinking. PREPARATION
Press the CFM key to confirm the calibration Remove the protective cap.
value. DO NOT BE ALARMED IF ANY
°C
SODIUM MEASUREMENT
Rinse the sodium electrode tip with
some of the sample to be tested,
then immerse the tip (approx. 2.5
cm /1") in the sample and stir gen-
tly.
22 23
The sensitive bulb should not touch the bottom of CLEANING PROCEDURE
the beaker. General Soak in Hanna HI 7061 general clean-
The Hanna HI 76405 electrode ing solution for approximately 1 hour.
holder can be used for this Removal of films, dirt or deposits on the membrane/
purpose. junction:
During measurement, the - Protein Soak in Hanna HI 7073 protein clean-
sample should be gently ing solution for 15 minutes.
stirred (approx. 100 rpm). The - Inorganic Soak in Hanna HI 7074 inorganic clean-
Hanna HI 190M stirrer can be MAGNETIC STIRRER
HI 190M
ing solution for 15 minutes.
used for this purpose. POWER
ON
OFF
SPEED
MAX
24 25
BATTERY REPLACEMENT ACCESSORIES
26 27
HI 8061L General cleaning solution, 500 mL FDA
WARRANTY
bottle
HI 7073M Protein cleaning solution, 230 mL bottle
HI 8073M Protein cleaning solution, 230 mL FDA
bottle All Hanna Instruments meters are warranted for
two years against defects in workmanship and mate-
HI 7073L Protein cleaning solution, 500 mL bottle
rials when used for their intended purpose and main-
HI 8073L Protein cleaning solution, 500 mL FDA tained according to instructions.
bottle
Electrodes and probes are warranted for six
HI 7074M Inorganic cleaning solution, 230 mL bottle
months.
HI 7074L Inorganic cleaning solution, 500 mL bottle
This warranty is limited to repair or replacement free of
HI 7077M Oil & Fat cleaning solution, 230 mL bottle
charge.
HI 8077M Oil & Fat cleaning solution, 230 mL
FDA bottle Damages due to accident, misuse, tampering or lack
of prescribed maintenance are not covered.
HI 7077L Oil & Fat cleaning solution, 500 mL bottle
HI 8077L Oil & Fat cleaning solution, 500 mL If service is required, contact the dealer from whom you
FDA bottle purchased the instrument. If under warranty, report the
model number, date of purchase, serial number and
HI 8093 1M KCl + AgCl electrolyte solution, 4 x
the nature of the failure.
50 mL bottle
If the repair is not covered by the warranty, you will be
OTHER ACCESSORIES notified of the charges incurred.
HI 98501 ChecktempC electronic thermometer If the instrument is to be returned to Hanna Instru-
with penetration, stainless steel probe ments, first obtain a Returned Goods Authorization
and 0.1°C resolution (range: -50.0 to Number from the Customer Service department and
150.0°C) then send it with shipment costs prepaid.
FC 300B Sodium electrode, glass body, single When shipping any instrument, make sure it is prop-
junction, refillable, with BNC connec- erly packaged for complete protection.
tor and 1 m (3.3') cable
HI 190M/D Mini-stirrer 230 V (1 liter max stirring
capacity, speed range from 100 to
max 1000 rpm)
HI 190M/U Mini-stirrer 115 V (1 liter max stirring
capacity, speed range from 100 to
max 1000 rpm)
HI 710031 Rugged carrying case
HI 7662 Stainless steel temperature probe with
1 m (3.3') cable
HI 76405 Electrode holder
28 29
CE DECLARATION OF CONFORMITY
30 31
SALES & TECHNICAL SERVICE CONTACTS
Australia:
Tel. (03) 9769.0666 • Fax (03) 9769.0699
China:
Tel. (10) 88570068 • Fax (10) 88570060
Egypt:
Tel. & Fax (02) 2758.683
Germany:
Tel. (07851) 9129-0 • Fax (07851) 9129-99
Greece:
Tel. (210) 823.5192 • Fax (210) 884.0210
Indonesia:
Tel. (21) 4584.2941 • Fax (21) 4584.2942
Japan:
Tel. (03) 3258.9565 • Fax (03) 3258.9567
Korea:
Tel. (02) 2278.5147 • Fax (02) 2264.1729
Malaysia:
Tel. (603) 5638.9940 • Fax (603) 5638.9829
Singapore:
Tel. 6296.7118 • Fax 6291.6906
South Africa:
Tel. (011) 615.6076 • Fax (011) 615.8582
Taiwan:
Tel. 886.2.2739.3014 • Fax 886.2.2739.2983
Thailand:
Tel. 66.2619.0708 • Fax 66.2619.0061
United Kingdom:
Tel. (01525) 850.855 • Fax (01525) 853.668
USA:
Tel. (401) 765.7500 • Fax (401) 765.7575
MANNACLR2 08/05
32