JOURNAL OF BASIC CHEMICAL PRACTICUM II

FACTORS AFFECTING THE REACTION RATE

BY
NI PUTU AYU SUWARNI
NIM
1913071011

S1 SCIENCE EDUCATION
FACULTY OF MATHEMATIC AND MATURAL SCIENCES
GANESHA UNIVERSITY OF EDUCATION
SINGARAJA
2019
 FACTORS AFFECTING THE REACTION RATE

I. Purpose
Students have the knowledge and skills in conducting experiments on the
effect of concentration, touch surface area, temperature and catalysts on
reaction rates

II. Basic Theory

Students have knowledge and skills in conducting experiments
Chemical reactions can take place at a fast or slow rate. Fast or slow rate
of chemical reactions is influenced by several factors, including the
concentration of reactants, surface area of touch, temperature and catalyst.
In general, the greater the concentration and the surface area of the
reacting substance, the greater the likelihood of collisions occurring, so
that the rate of reaction will also increase. Likewise with temperature.
Increasing the temperature of the system will increase the fraction of
molecules that have more energy than the activation energy so that the
reaction rate will increase.
In addition to the above factors, the reaction rate can also be
increased by adding catalysts. Based on the catalyst phase with the
reaction system, the catalyst can be distinguished from homogeneous
catalysts and heterogeneous catalysts. about the effect of concentration,
touch surface area, temperature and catalyst on the reaction rate.

III. Tools and materials

Tools:
- Glass 50 ml dan 100 ml - Test tube clamp
- Volumetric flask 100 ml - Beaker 400 ml
dan 250 ml - Tube “Y”
- Stopwatch - Stative and clamp
- Balloon - Balance
- Test tube and rack - Tripod
 - Burner - Drop pipette
- Gas conduit

Materials:
- Zinc granules/powder - Soap solution
- HCl 0,5 M, 1M, 1,8M, - KMnO4 0,01 M
3M, 6M - H2SO4 2M
- Na2S2O3 1M - H2C2O4 0,05M
- CaCO3 powder and - H2O2 3%
granules - FeCl3 saturated
- MnO2 powder

IV. Work Procedure

1. Effect of Concentration on Reaction Rate
- The reaction between zinc and hydrochloric acid
a. Put 2 grams of zinc into the balloon, then attach the balloon to
a flask that has been filled with 50 ml of 1M HCl solution
b. Activate the stopwatch just when the balloon can stand. Record
the time required
c. Do the same for 1.8M, 3M and 6M HCl solutions
- The reaction between sodium thiosulfate and hydrochloric acid
a. Provide four 100 ml measuring flasks, successively mark A, B,
C, and D
b. Enter 10 ml of 1M thiosulfate solution into each of the flasks
above
c. To the pumpkin B, C and D add 5 ml, 7.5 ml and 12.5 ml water
respectively and shake the pumpkins to make perfect mixing.
d. To pumpkin A, add 10 ml of 2M HCl solution and shake the
pumpkin. Run the stopwatch just when the HCl solution is
poured and stop the stopwatch just when turbidity occurs
e. Do the same for pumpkin B, C and D
2. Touch Surface Area
a. Weigh 2 types of limestone, CaCO3 which weighs the same (± 0.5
gram) one powder is the other lump
b. Provide 2 "Y" tubes. Fill the first tube with 3 ml of 0.5 M HCl on
one leg of the "Y" tube and CaCO3 powder on the other foot. Fill
the second "Y" tube with 3 ml of 0.5M HCl on one leg and a chunk
of CaCO3 on the other foot.
c. Arrange the tools as shown, in the following way:
- Fill a 400 ml beaker with tap water until it is almost full
- Mark the test tube with a marker or rubber at a distance of ± 3
cm from the bottom of the test tube
- Fill the test tube with tap water until it is full, then put it in the
beaker in an upside down condition so that the mouth of the
tube is submerged in water contained in the beaker. Try the test
tube does not contain air bubbles.
- Pinch the test tube so that it is erect and does not fall
d. The first "Y" tube stopper with a flowing pipe plug. Insert the other
end of the drain pipe into the mouth of the test tube contained in
the beaker.
e. Turn the "Y" tube so that the HCl solution flows from one foot to
the foot containing CaCO3
f. Record the time needed from the reaction to the volume of gas
stored in the test tube right on the markers (markers / rubber)
g. Compare the reaction rates of the two experiments above

3. System Temperature
a. Provide 2 clean test tubes and each filled with 2 ml of 0.05M
H2C2O4 and 1 ml of 1M H2SO4
b. Add 5 drops of 0.01 M KMnO4 to the first tube. Record the time
from the addition of KMnO4 until the color no longer appears
 c. Soak the second test tube in hot water (± 50oC) for 1 minute, then
add 5 drops of 0.01 M KMnO4. Record the time from the addition
of KMnO4 until the color is no longer visible
d. Compare reaction rates in the two experiments above

4. Catalyst
a. Provide 3 test tubes and each filled with 2 ml of 3% H2O2 and 1
ml of soap solution. Shake and observe the gas bubbles that occur
b. Save the first tube for comparison. Add a small spoonful of MnO2
powder to the second tube. Add 5 drops of saturated FeCl3 solution
to the third tube
c. Observe the changes that occur. What conclusions can be obtained
from this experiment?

V. Observation Results
Observation:
1. a. The reaction between Zn and HCl
Consentration HCl Time
1,0 M
1,8 M
3,0 M
6,0 M
Conclusion: …………………………………………………………….
…………………………………………………………………………..
1. b. The reaction between Na2S2O3 with HCl
Flask Time
A
B
C
D
Conclusion: …………………………………………………………….
…………………………………………………………………………..
2. a. Results:
…………………………………………………………………………
…………………………………………………………………………
…………………………………………………………………………
2. b. Results:
…………………………………………………………………………
…………………………………………………………………………
…………………………………………………………………………
Conclusion:
…………………………………………………………………………
…………………………………………………………………………
…………………………………………………………………………

3. Observation Results : Influence of Temperature

Tube Temperature Time
1
2
Conclusion:
…………………………………………………………………………
…………………………………………………………………………
…………………………………………………………………………

4. Observation Results : Influence of Catalyst

Tube Observation
1
2
3
Conclusion:
…………………………………………………………………………
…………………………………………………………………………
…………………………………………………………………………
VI. Question and Discussion
1. Write down the reaction equation for each experiment!
2. What changes can be observed from the above experiments to mark the
speed or slow rate of a reaction?
3. In experiments on the reaction rate between limestone and HCl, what is
the relationship between increasing time and reaction rate? Explain!

VII. Conlusions
………………………………………………………………………………
………………………………………………………………………………
………………………………………………………………………………

VIII. Reference
Book Basic Chemistry Practicum 1 (by Drs. I WayanSubagia, MappSc.,
Ph.D. and Dra. SuheimiSya'ban, M.Pd.).

Singaraja, 17 February 2020

Supporting Lectulers, Practicies,

(Dr. I Nyoman Suardana, M.Si) (Ni Putu Ayu Suwarni)

NIP.196611231993031001 NIM. 1913071011