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Test Procedure
Test Procedure
Scales to measures.
1. For coarse aggregate 2 kg sample is adequate and for fine aggregate 0.5 kg sample is
adequate.
3. Heated very gently on the frying pan or metal plate and stirred with a glass or metallic rod to
maintain uniform distribution of heat, until the sheen disappears from the surface. The fine
aggregates become surface dry when it just starts showing free flowing characteristics.
4. The aggregates is then cooled and reweighed. The surface dry aggregate weight (Wsd) is
noted. The surface moisture is then calculated as follows-
5. Overheating must be avoided, as it will not give the correct surface moisture.
6. If heating is continued either on the fry pan or in the oven till the aggregate is bone
dry aggregate weight is then noted (Wbd) after continuous heating. The absorption (absorbed
water content) is then calculated as follows-
Similarly, if the dry aggregates are received on site and absorption capacity is to be determined then
the aggregates are first soaked in water and then the above methods are deployed to determine the
absorption capacity of aggregates.
The apparatus required for this test is only 250 ml glass measuring cylinder.
1. The glass cylinder is filled with salt-water solution (concentration of the solution will teaspoon
full of common salt for every 570 ml) upto 50 ml mark.
2. Add sand until the level of the sand is upto 100 ml mark.
4. Place the palm on the mouth of the glass cylinder and shake it vigorously.
5. Place the cylinder on hard levelled surface and tap it all round so that sand is leveled.
7. Measure the thickness of the silt layer and the height of the sand. The silt content can be
calculated as follows:
Silt (%) by volume = [(Thickness of silt layer/ Height of sand + Silt) x 100 %]
If silt content by weight exceeds 3% then washing of sand is necessary. After conducting few tests, a
co-relation can be developed for silt layer thicknesses at various intervals of time. The silt content at
10 minutes can be fixed as inspection criteria.
3. BULKING OF SAND
When sand is damp, the water coating on the surface of each sand particle causes separation of
particles from one another due to surface tension. This causes sand to bulk. Bulked sand occupies
more volume and hence if volumetric measuring is done while proportioning it, bulking correction is
necessary.
2. The box is then flooded with water and rodding is done to make the sand settle and
consolidate. Care should be taken that sand does not overflow during the flooding and
compaction.
3. The sand is then leveled in the box and the drop in height is measured (h cm).
Dry sand occupies the same volume as fully saturated sand. The bulking will vary from load to load
and day to day depending on the fineness of sand and its surface moisture content. It is there-fore,
very essential to make bulking corrections by checking the actual bulking of sand proposed to be
used by volumetric batching for mortar or concrete.
2 15
3 20
4 25
5 30
4. SIEVE ANALYSIS
Sieve analysis is done to check the gradation of aggregate. The test is done as follow.
1. Take required amount of aggregate sample (for coarse aggregate take apprx. 2.5 kg and for
fine aggregate take 0.5 kg)
2. Arrange the required no of sieves as per the contract or job requirement in an descending
manner. (i.e. keep the sieve having largest size opening at the top and the smallest size
opening at the bottom)
4. Then measure the weight of aggregate on each sieve and express it as the percentage of
passing.
Now compare these values with the recommended values to know whether it falls within the range or
not. If not falling within the desired gradation then take necessary action.
Grading limit of coarse aggregate and fine aggregate is given below for reference.
Grading Limit of Coarse Aggregate
5. FINENESS MODULUS
Fineness modulus is generally used to get an idea of how coarse or fine the aggregate is. More
fineness modulus value indicates that the aggregate is coarser and small value of fineness modulus
indicates that the aggregate is finer.
1. Sieve the aggregate using the appropriate sieves (80 mm, 40 mm, 20 mm, 10 mm, 4.75 mm,
2.36 mm, 1.18 mm, 600 micron, 300 micron & 150 micron)
5. Add the cumulative weight of aggregate retained and divide the sum by 100. This value is
termed as fineness modulus
Compare the test value with the values given in the following table and you can get an idea about
how coarse or fine the sand is.
Only sand between FM 2.6 to 2.9 is considered suitable for nominal mix proportion.
CONSISTENCY
The basic aim is to find out the water content required to produce a cement paste of
standard consistency as specified by the IS: 4031 (Part 4) – 1988. The principle is that
standard consistency of cement is that consistency at which the Vicat plunger penetrates to
a point 5-7mm from the bottom of Vicat mould.
Apparatus – Vicat apparatus conforming to IS: 5513 – 1976, Balance, whose permissible
variation at a load of 1000g should be +1.0g, Gauging trowel conforming to IS: 10086 –
1982.
Procedure to determine consistency of cement
i) Weigh approximately 400g of cement and mix it with a weighed quantity of water. The
time of gauging should be between 3 to 5 minutes.
ii) Fill the Vicat mould with paste and level it with a trowel.
iii) Lower the plunger gently till it touches the cement surface.
iv) Release the plunger allowing it to sink into the paste.
v) Note the reading on the gauge.
vi) Repeat the above procedure taking fresh samples of cement and different quantities of
water until the reading on the gauge is 5 to 7mm.
Reporting of Results
Express the amount of water as a percentage of the weight of dry cement to the first place
of decimal.
INITIAL AND FINAL SETTING TIME
We need to calculate the initial and final setting time as per IS: 4031 (Part 5) – 1988. To do
so we need Vicat apparatus conforming to IS: 5513 – 1976, Balance, whose permissible
variation at a load of 1000g should be +1.0g, Gauging trowel conforming to IS: 10086 –
1982.
Procedure to determine initial and final setting time of cement
i) Prepare a cement paste by gauging the cement with 0.85 times the water required to give
a paste of standard consistency.
ii) Start a stop-watch, the moment water is added to the cement.
iii) Fill the Vicat mould completely with the cement paste gauged as above, the mould
resting on a non-porous plate and smooth off the surface of the paste making it level with
the top of the mould. The cement block thus prepared in the mould is the test block.
A) INITIAL SETTING TIME
Place the test block under the rod bearing the needle. Lower the needle gently in order to
make contact with the surface of the cement paste and release quickly, allowing it to
penetrate the test block. Repeat the procedure till the needle fails to pierce the test block to
a point 5.0 ± 0.5mm measured from the bottom of the mould.The time period elapsing
between the time, water is added to the cement and the time, the needle fails to pierce the
test block by 5.0 ± 0.5mm measured from the bottom of the mould, is the initial setting
time.
B) FINAL SETTING TIME
Replace the above needle by the one with an annular attachment. The cement should be
considered as finally set when, upon applying the needle gently to the surface of the test
block, the needle makes an impression therein, while the attachment fails to do so. The
period elapsing between the time, water is added to the cement and the time, the needle
makes an impression on the surface of the test block, while the attachment fails to do so, is
the final setting time.
SOUNDNESS
Soundness of cement is determined by Le-Chatelier method as per IS: 4031 (Part 3) –
1988.
Apparatus – The apparatus for conducting the Le-Chatelier test should conform to IS: 5514
– 1969
Balance, whose permissible variation at a load of 1000g should be +1.0g and Water bath.
The truth of this statement is proved not only by construction delays and cost overruns but
also by catastrophic failures of major structures. Such catastrophies include dam failures,
collapses and foundation breakdowns in multi-storeyed office and apartment structures; and
other failures in stadia, factories, schools, auditoria, public buildings and bridges.
Each construction project determines its own individualized testing needs. A variety of
factors influence the type of testing required. Among these factors are size of the
structures, terrain, type of soil and subsurface conditions at the construction site and other
conditions peculiar to the specific location. The expertise of the construction engineers and
technical personnel working on the project will also have an influence on the testing and
inspection need.
Testing facilities may range from a simple, inexpensive test kit carried in a portable chest to
a fully equipped Central Testing Laboratory.
A small Field Testing Laboratory, which can perform all the required tests can be set up at
any construction site with a small investment of about Rs. 71,300/-. The equipments of the
Laboratory shall be as given below:
17 Hot Plate
1 No. 2,000
With the above equipments, the following testing of construction materials can be
conducted:-
Overview
Specific gravity is defined as the ratio between the weight of a given volume of cement and
weight of an equal volume of water.
Apparatus
Measuring Instruments
NAME CAPACITY / RANGE / SIZE ACCURACY / LEAST COUNT
Lechatelier flask
Balance
Water bath
Other Apparatus
Tray
Le chatelier flask
Environmental Conditions
Temp
Relative humidity
Test Procedure
1. Dry the Le-chatelier flask and fill with kerosene oil or Naptha to a point on the stem between 0
and 1 ml.
2. Dry the inside of the flask above the level of the liquid.
3. Immerse the flask in a constant temp water bath maintained at room temp for sufficient time.
4. Record the level of the kerosene oil in the flask as initial reading.
5. Introduce about 60 g of cement into the flask so that the level of kerosene rises to about say 22
ml mark. Splashing should be avoided and cement should not be allowed to adhere to the sides
of the flask above the liquid.
6. Insert the glass nipple into the flask and roll it gently in an inclined position to free the cement
from air until no further air bubble rises to the surface of the liquid.
7. Keep the flask again in constant temp water bath and note down the new liquid level as final
reading.
Calculation
The difference between the first and final readings represents the volume of liquid displaced by
the mass of cement used in test.
The density is calculated as per the below mentioned formula to the second place of decimal.
Note ::Two tests shall be carried out and the average is reported. If the difference between the
two values differs by more than 0.03, the test shall be repeated.
Precautions
While pouring cement in the Lechatelier flask, care should be taken to avoid splashing and
cement should not adhere to the inside of the flask above the liquid.
Technical Discussions
The test for finding the specific gravity of Portland cement was originally considered to be of
value in detecting adulteration and under burning, but is no longer thought to be of much
importance in view of the fact that other tests lead to more definite conclusions.
Overview
Blaine’s air permeability apparatus consists essentially of a means of drawing a definite quantity
of air through a prepared bed of cement of definite porosity. The fineness is expressed as a total
surface area in square centimeters per gram.
Apparatus
Measuring instruments
Balance 3g 1 mg
Environmental condition
Temperature 27 ± 20 C
Humidity 65 % (max.)
Procedure
Procedure consists of 4 steps
(a)Determination of the density of cement
To determine the density or specific gravity of cement click here.
2. Fill the cell with mercury. Level the mercury to the top of the cell with a glass plate.
4. Remove the top filter paper from the permeability cell and compress a trial quantity of 2.80 g of
cement into the space above filter paper to the gauge line in the cell. Place the other filter paper
above the cement bed.
5. Fill the remaining space in the cell above the filter paper with mercury. Level the mercury to the
top of the cell with a glass plate and remove mercury from the cell and weigh it, M2.
6. Calculate the volume occupied by the cement bed in the cell from the following equation.
V = (M -M )/D,
1 2
Where
7. Average at least two volume determinations that agree to within ±0.005cm3 and record this
value.
i.e. W = (1-e)ρV
or W = 0.500ρV
2. Place the perforated disc on the ledge at the bottom of the cell and place on it a new filter paper
disc. Place the weighed quantity of standard cement, W, in the cell taking care to avoid loss.
3. Tap the cell to level the cement. Place a second new filter paper disc on the leveled cement.
4. Compress the cement with the plunger until the plunger collar is in contact with the top of the
cell. Slowly withdraw the plunger a short distance, rotate 900, repress the cement bed, and then
slowly withdraw.
5. Attach the permeability cell to the manometer tube with an air tight connection and slowly
evacuate the air in the manometer U-tube until the liquid reaches the top mark, then tightly
close the valve.
6. Start the timer when the bottom of the meniscus reaches next to the top mark and stop the
timer when the bottom of the meniscus reaches the bottom mark. Record the time t and temp.
of test.
7. Repeat the whole procedure on two further samples of the same reference cement. Calculate
the average time of the three determinations. Then calculate the apparatus constant using the
formula given below.
Where,
K=Apparatus constant
(d)Determination of fineness
1. Repeat the steps (1 to 6) as done in determination of apparatus constant, but this time using the
cement whose fineness is to be calculated.
Where,
K = Apparatus constant
ρ = Density of cement
t = Time
Technical discussion
Fineness of cement has a great effect on the rate of hydration and hence the rate of gain of
strength.
Finer cement offers a great surface area for hydration and hence faster the development of
strength.
Increase in fineness of cement also increases the drying shrinkage of concrete and hence creates
cracks in structures.
Excessive fine cement requires more water for hydration, resulting reduced strength and
durability.
Fineness of cement affects properties like gypsum requirement, workability of fresh concrete &
long term behavior of structure.
Approximately 95% of cement particles are smaller than 45 micrometers, with the average
particle around 15 micrometers.
In the early 1900s, cement fineness was expressed as the mass of cement per fractional size
(percent weight retained on specific sieve sizes). Now a day’s fineness is usually measured by
the Blaine air-permeability test that indirectly measures the surface area of the cement particles
per unit mass.
Cements with finer particles have more surface area in m2 per kg of cement.
Standard specification
Type of cement Indian Standard Reference Finenees Value (mm2/g)
Precautions
The volume of the compacted cement bed should be calculated accurately.
The time taken by the manometer liquid to fall from one mark to the other should be measured
very accurately.
Objective
To determine moisture content and dry density relationship using heavy compaction or modified
compaction method as per IS-2720-Part-8.
Apparatus
• Metal mould (volume = 1000 cm3)
• Balance (capacity = 10 kg, least count = 1g)
• Oven (105 to 1100C)
• Sieve (19 mm)
• Metal rammer (weight = 4.9 kg)
Compaction
Mould and Rammer
Procedure
1. Dry the soil sample by exposing it to air or sun light.
4. Weigh the mould with base plate attached to the nearest 1g. Record this weight as ‘W1’.
6. Compact the moist soil into the mould in five layers of approximately equal mass, each layer
being given 25 blows, with the help of 4.9 kg rammer, dropped from a height of 450 mm above
the soil. The blows must be distributed uniformly over the surface of each layer.
7. After completion of the compaction operation, remove the extension collar and level carefully
the top of the mould by means of straightedge.
8. Weigh the mould with the compacted soil to the nearest 1 g. Record this weight as ‘W2’.
9. After weighing remove the compacted soil from the mould and place it on the mixing tray.
Determine the water content of a representative sample of the specimen. Record the moisture
content as ‘M’.
10. Broken up the remainder of the specimen and repeat step 5 to step 9 by adding suitable
increment of water to the soil. For sandy and gravelly soils the increment in general is 1% to
2%. For cohesive soils the increment in general is 2% to 4%.
11. The total no. of determinations made shall be at least five, and the moisture contents should be
such that the optimum moisture content, at which the maximum dry density occurs, is within
that range.
Calculation
Bulk density, γ in g/cm of each compacted specimen is calculated from the following equation.
b
3
γ = (W -W )/V
b 2 1 m
where,
Dry density, γ in g/cm of each compacted specimen is calculated from the following equation.
d
3
γ = 100 γ /(100+M)
d b
Where,
Graph
The dry densities, γ , obtained in a series of determinations is plotted against the corresponding
d
moisture content ‘M’. A smooth curve is then drawn through the resulting points and the position
of the maximum on this curve is determined, which is called maximum dry density (M.D.D).
And the corresponding moisture content is called optimum moisture content (O.M.C.).
Compaction Curve
Objective
For determination of the relation between the water content and the dry density of soils using
light compaction.
Reference Standard
IS: 2720(Part 7)-1980- Methods of test for soils: Determination of water content-dry density
relation using light compaction.
Sieves [19mm]
Mixing tray
Trowel
Metal container
Preparation sample
Obtain a sufficient quantity (10 kg) of air-dried soil and pulverize it. Take about 5 kg of soil
passing through 19mm sieve in a mixing tray.
Procedure
1. 5 Kg. of soil is taken and the water is added to it to bring its moisture content to about 4 % in
coarse grained soils and 8% in case of fine grained soils with the help of graduated cylinder
2. The mould with base plate attached is weighed to the nearest 1 gm (M1). The extension collar is
to be attached with the mould.
3. Then the moist soil in the mould is compacted in three equal layers, each layer being given 25
blows from the 2.6 Kg rammer dropped from a height of 310 mm. above the soil.
4. The extension is removed and the compacted soil is leveled off carefully to the top of the mould
by means of a straight edge.
5. Then the mould and soil is weighed to the nearest 1 gm. (M2).
6. The soil is removed from the mould and a representative soil sample is obtained water content
determination.
7. Steps 3 to 6 are repeated after adding suitable amount of water to the soil in an increasing
order.
Calculation
Bulk density, g in g/cm at each compacted specimen is calculated from the equation.
m
3
where V = volume of mould in cm
m
3
The dry densities, g obtained in a series of determinations are plotted against the corresponding
d
moisture content. A smooth curve is then drawn through the resulting points and the position of
the maximum on this curve is determined.
Report
The maximum dry density in g/cm is to be reported to the nearest 0.01 and the optimum
3
Adequate period (about 15 minutes for clayey soils and 56 minutes for coarse grained soils) is
allowed after mixing the water and before compacting into the mould.
The blows should be uniformly distributed over the surface of each layer.