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Journal of Testing and Evaluation

doi:10.1520/JTE20150135 / Vol. 44 / No. 6 / November 2016 / available online at www.astm.org

Xue Luo1 and Robert L. Lytton2

Characterization of Healing of Asphalt Mixtures


Using Creep and Step-Loading Recovery Test

Reference
Luo, X. and Lytton, R. L., “Characterization of Healing of Asphalt Mixtures Using Creep and Step-Loading
Recovery Test,” Journal of Testing and Evaluation, Vol. 44, No. 6, 2016, pp. 2199–2210, http://dx.doi.org/
10.1520/JTE20150135. ISSN 0090-3973

ABSTRACT
Manuscript received March 31, 2015; Healing of asphalt mixtures has been proven to be significant, and different approaches exist
accepted for publication September 23,
to characterize it, such as the phenomenological methods, mechanism-based, and mechanics-
2015; published online December 14,
2015. based methods. To target the actual causal relationship for healing in asphalt mixtures, a new
1 test called the creep and step-loading recovery (CSR) test, along with a new mechanistic
Texas A&M Transportation Inst., Texas
A&M Univ. System, 77843 College method termed the energy-based mechanistic (EBM) approach, was previously developed by
Station, TX (Corresponding author), the authors. This paper aimed at examining the applicability of the CSR test with the EBM
e-mail: xueluo@tamu.edu
approach in characterizing healing of asphalt mixtures. A variety of asphalt mixtures were
2
Zachry Dept. of Civil Engineering, Texas selected and subjected to the CSR test in this study. The internal stress measured by the CSR
A&M Univ., 77843 College Station, TX,
email: r-lytton@civil.tamu.edu test was used in the EBM approach to generate a damage density progression curve, which
directly reflected how the damage developed and healed in the tested material. Based on this
curve, the normalized extent of healing was defined as a direct measure of healing, and the
healing curve (the normalized extent of healing versus the rest time) was defined as a
straightforward tool to qualitatively evaluate the healing ability of asphalt mixtures. To further
achieve a quantitative description of the healing ability, a healing model based on the
Ramberg-Osgood equation was developed to simulate the healing curve. The parameters in
the healing model represent the healing speed at different stages of healing (the initial
healing rate and ultimate healing rate) and the overall ability of the material to heal (the
healing scale). Both the healing curves and healing parameters can discern the difference in
the healing ability caused by the air void content, aging, temperature, and the type of asphalt
binder. In other words, the CSR test, along with the EBM approach, was able to produce a
reasonable and consistent prediction of healing for asphalt mixtures.

Keywords
healing, asphalt mixtures, creep and step-loading recovery test, energy-based mechanistic approach,
healing curve, healing parameters

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2200 Journal of Testing and Evaluation

Nomenclature t0 ¼ the time corresponding to the end of the


creep phase
A ¼ the cross sectional area
Vm ¼ the volume of the asphalt mastic in one
cIh ¼ the initial average crack size before
layer of the asphalt mixture, whose thick-
healing
ness equals to the mean film thickness
cNh ¼ the new average crack size after healing
Dt ¼ the rest time
DSEA ¼ the apparent dissipated strain energy
e_r ¼ the residual strain rate in the recovery
(DSE), which is calculated by integrating
phase
the apparent creep stress and apparent
/fc ¼ the initial damage density before healing
creep strain measured in the creep phase
starts, or equivalently the final damage
DSET ¼ the true DSE, which is calculated by inte-
density at the end of the creep phase
grating the true creep stress and true creep
/i ¼ the damage density at any data point i
strain in the intact material
during the recovery phase
DPSEA ¼ the apparent dissipated pseudo strain
/0 ¼ the initial damage density, which equals
energy (DPSE), which is calculated by
the air void content
integrating the apparent creep stress and
ch ¼ the surface energy for healing
apparent pseudo strain in the creep phase
rA ¼ the apparent creep stress, which is calcu-
DPSET ¼ the true DPSE, which is calculated by inte-
lated by the creep load applied in the
grating the true creep stress and true
creep phase and acts normal to the cross
pseudo strain in the creep phase
section
h ¼ the normalized extent of healing T
^ ¼ the predicted healing based on three pa- r ¼ the true creep stress, which is the stress in
h
the intact material acting normal to the
rameters: h_ 1 , h_ 2 , and hb
_h1 ¼ the initial healing rate, representing the cross section
r1 , r2 , and r3 ¼ the three steps in an increased order in
healing speed of the material at the initial
any of the seven step-loads
stage of healing
ri ¼ the internal stress
h_ 2 ¼ the ultimate healing rate, indicating the heal-
ra , rb , g1 , and g2 ¼ fitting parameters for the internal stress
ing speed of the material after a long time
hb ¼ the healing scale, reflecting the overall
ability of the material to heal
MIh ¼ the number of initial cracks before healing
MNh ¼ the number of new cracks after healing Introduction
RSEA ¼ the apparent recoverable strain energy Healing is a counter process to cracking which alleviates crack-
(RSE), which is calculated by integrating ing damage and restores the strength of a damaged material.
the apparent internal stress and apparent For asphalt pavements, it has been proven that healing is a sub-
residual strain measured in the recovery stantially important issue, and its significance has been demon-
phase strated in both the laboratory and the field. In Ref. [1], the
RSET ¼ the true RSE, which is calculated by inte- flexural beam bending test was used to show that a rest period
grating the true internal stress and true re- of 24 h can increase the fatigue life of a certain type of asphalt
sidual strain mixture by more than 100 %. The same effect of healing with
RPSEA ¼ the apparent recoverable pseudo strain respect to fatigue life was also reported after a number of rest
energy (RPSE), which is calculated by periods were incorporated in the fatigue testing [2]. In Ref. [3],
integrating the apparent internal stress healing was measured by transmitting ultrasonic waves through
and apparent pseudo strain in the recov- an asphalt film after applying a cyclic tensile load. The result
ery phase suggested that considerable healing occurred after each loading
RPSET ¼ the true RPSE, which is calculated by inte- cycle in the asphalt film. In addition to the laboratory evidence,
grating the true internal stress and true there are also numerous facts on the healing of asphalt mixtures
pseudo strain in the recovery phase from field measurements. The data of four in-service asphalt
Sc ¼ the area of all the cracks on the cross pavements indicated that at low loading levels, minor fatigue
section cracks can completely heal so fatigue cracking did not develop
t ¼ the recovery time (any time in the recov- in such conditions [4]. This observation was supported by
ery phase) Ref. [5] from laboratory measurements that the effect of healing

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LUO AND LYTTON ON HEALING USING CSR TEST 2201

is most profound when cracks are small. In Ref. [6], persuasive The interfacial force of attraction (i.e., surface energy) acting on
field data were reported on healing of asphalt pavements from crack surfaces was regarded as the cause of the growth of the
the surface wave measurements. The stiffness of asphalt pave- contact between crack surfaces. The stress calculated from the
ments were measured before and after traffic loading. The re- interfacial force of attraction and the deformation of the crack
covery of stiffness demonstrated that considerable healing surfaces were used to predict the rate of the growth of the con-
occurred in the pavement that had severe fatigue damage. Since tact area. For asphalt mixtures, the mechanical analysis of the
healing is found to be significant in asphalt pavements, it is healing process becomes more complicated due to: (1) visco-
highly desired to quantify it and incorporate its contribution in elasto-plastic nature of the material; (2) a large number of pre-
the evaluation of performance of asphalt pavements. existing air voids or cracks; and (3) unknown driving forces for
There are currently different approaches available to predict this process. From a mechanical point of view, healing of an
healing in asphalt mixtures. One popular approach is to use the asphalt mixture is the collective behavior of all air voids or
change of a property or an index to quantify the effect of healing. cracks that are driven by certain stresses. In previous studies
The restoration of the property/index of a damaged asphalt mix- [15,16], the authors designed the creep and step-loading recov-
ture during the rest period represents the effect of healing. The ery (CSR) test and developed a mechanics-based method to
change of the property/index is measured using a repeated load address this problem. Since healing usually accompanies the
test with rest periods. The properties/indexes employed include recovery of a material, the authors proposed to study the
modulus [1,2,7] and strain energy [8,9]. This type of approach is mechanics of healing and quantify the amount of healing from
straightforward in describing the effect of healing, but is phe- a recovery process. Investigation of the mechanics of healing
nomenological in nature in characterizing healing. It is not based helps identify the driving forces for healing in asphalt mixtures.
on the actual causes that drive the process of healing, and it does The driving forces are then used in the energy-based mechanis-
not reflect the actual results of healing in the material. tic (EBM) approach to predict healing. The amount of healing
Besides the phenomenological approach, a mechanism- is quantified by the decrease of the cracked area, or damage
based approach has gained attention in the field of asphalt mate- density as the contact between crack surfaces grows. Damage
rials. This approach stems from a study on healing of polymers density is the ratio of the cracked area to the cross sectional
[10]. According to the physical mechanisms involved in the pro- area. As a continuation of this previous work, the damage den-
cess of healing, healing is treated as a combination of two proc- sity determined during healing is utilized to generate a healing
esses: wetting of two crack surfaces (“wetting”) and an increase curve and determine healing parameters in this study. The heal-
of the joint strength of the two crack surfaces (“diffusion”). ing curve and healing parameters are direct measures of the
“Wetting” is a process in which contact and adhesion are gradu- ability of an asphalt mixture to heal. The objectives of this study
ally established between two crack surfaces. When the two crack are to use these healing curves and healing parameters to pre-
surfaces are in complete contact, an increase of the joint strength dict healing, and examine whether the CSR test along with this
occurs through a diffusion process, which involves molecular mechanics-based approach produces a reasonable and consist-
interchange and random entanglement formation. The collective ent prediction of healing for asphalt mixtures.
influence of these two processes on a mechanical property is The paper is organized as follows. A brief review of the
described by a convolution integral function. This theory has CSR test and associated mechanics-based approach is first pre-
been applied to predict healing of asphalt binders [11,12]. sented in the second section. The testing and analysis methods
Recently a micro-damage healing model was developed to are applied to different types of asphalt mixtures to examine
supplement a continuum damage mechanics-based model in their applicability. Details of the tests and materials used in this
predicting fatigue life of asphalt mixtures by considering healing study are given in the third section. Based on the testing results,
[13]. A healing internal state variable was introduced to define the methods to determine healing curves and healing parame-
the density of healed cracks (i.e., healed area of cracks per unit ters are introduced in the fourth section. Then the healing
area of cracks). The change of this variable thus described the parameters of various asphalt mixtures are compared to demon-
progress of healing. A postulated phenomenological-based evo- strate the rationality of the predicted healing. The major find-
lution equation was proposed to predict the rate of the change ings of this study are summarized in the last section.
of the healing internal state variable. It took account of the
major factors that affect healing, including the rest period, tem-
perature, level of damage, and the history of healing. Mechanistic Modeling of Healing
In addition to the aforementioned approaches, mechanics-
based methods have been developed to characterize healing in
Using Internal Stress
viscoelastic and visco-elasto-plastic materials. One of the pre- Healing occurs in rest periods when the load is removed from a
cursory works studied the crack closure and bonding, namely damaged material. For asphalt mixtures, a recovery process also
the direct results of healing, in linear viscoelastic materials [14]. takes place due to the viscoelastic nature of the material. In a

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2202 Journal of Testing and Evaluation

rest period, the recoverable deformation of an asphalt mixture • Force equilibrium:


gradually restores with time. If the asphalt mixture is not dam-
aged (no crack growth) during loading, the recovery of the bulk rA A ¼ rT ðA  Sc Þ (1)

material is actually the recovery of its intact part. The bulk ma- • Energy balance:
terial refers to a mix of asphalt binder, aggregates, and existing
air voids or cracks; the intact part, which is called the intact DSEA ¼ DSET (2)

material, refers to the combination of asphalt binder and aggre-


DPSEA ¼ DPSET (3)
gates. If the mixture is damaged, there are two simultaneous
processes during the recovery of the bulk material: recovery of
The major steps of using these equations to solve for the
the intact material and healing of cracks. The recovery of the
damage in the creep phase of a damaged asphalt mixture are as
intact material is defined as “true recovery,” and the recovery of
follows:
the damaged bulk material is defined as “apparent recovery.” As
a result, the recovery of undamaged asphalt mixtures is the true 1. Measure apparent material properties of undamaged
recovery; the recovery of damaged mixtures is the apparent asphalt mixtures from the creep phase of nondestructive
recovery, which involves both the true recovery and healing. CSR tests;
The recovery of an asphalt mixture is driven by the internal 2. Determine true material properties of undamaged mix-
stress. Since there is no external load in the recovery phase, the tures by Eq 1 and 2 with apparent material properties;
3. Calculate apparent and true pseudo strains using deter-
force that drives the deformation is provided by the material
mined apparent and true material properties, respectively;
itself, called internal force or internal stress. Note that the inter-
4. Calculate DPSEA of damaged asphalt mixtures from the
nal stress as well as the applied stress in this study is an average
creep phase of destructive CSR tests;
stress, calculated by the force divided by the cross sectional 5. Determine the true creep stress of damaged mixtures by
area. The internal stress that drives the apparent recovery is Eq 3; and
called “apparent internal stress”; the one that drives the true 6. Calculate the damage density by the apparent and true
recovery is called “true internal stress.” The true internal stress creep stresses of damaged mixtures.
and the interfacial force of attraction, or surface energy are the
The calculated damage densities with time form an evolu-
two driving forces for healing of asphalt mixtures [16]. The
tion curve in the creep phase. The damage density at the end of
interfacial force of attraction is usually measured from a surface
the creep phase is the initial damage density in the recovery
energy test. The internal stress is measured by the CSR test that
phase. In other words, it is the starting point for the healing
was designed by the authors in Ref. [15]. A typical CSR test con-
process.
tains two phases: a creep phase under a constant creep load and
In the recovery phase of a CSR test, the energy balance
a recovery phase with several step-loads. The step-load is added
equations are formulated according to the EBM principles:
in the recovery phase to measure the internal stress. More
details of the CSR test are presented in the next section. The RSEA ¼ RSET (4)
true internal stresses are measured from the nondestructive  
2MIh p2 c3Ih 2MNh p2 c3Nh
CSR test, and the apparent internal stresses are obtained from RPSEA Vm ¼ RPSET Vm þ RPSET 
3 3
the destructive CSR test. The nondestructive and destructive 
 ch 2MIh pc2Ih  2MNh pc2Nh
CSR tests are analyzed by the EBM approach to predict healing
(5)
in asphalt mixtures. The EBM approach is a pure mechanical
method based on two basic mechanics principles (force equilib- The major steps of using these equations to solve for the healing
rium and energy balance) [16]. These two principles bridge the of a damaged asphalt mixture in the recovery phase are as
gap between the apparent measurements from the test and the follows:
true responses of the material. By establishing such a connec-
1. Measure the true internal stress from nondestructive CSR
tion, the true responses of the material and the damage infor-
tests and apparent internal stress from destructive CSR
mation, such as the true stress in the intact material and
tests;
damage density, can be obtained by measuring the stress and 2. Determine the true residual strain of damaged asphalt
strain from a test. The step-by-step procedures for applying the mixtures from the recovery phase of destructive CSR tests
EBM approach to the CSR test were elaborated in Ref. [16], so by Eq 4;
they are not repeated herein and only the key equations and 3. Calculate apparent and true pseudo strains in the recov-
major steps are presented below. ery phase;
In the creep phase of a CSR test, a force equilibrium equa- 4. Calculate RPSEA and RPSET using the apparent internal
tion and two energy balance equations are formulated according stress with apparent pseudo strain and true internal stress
to the EBM principles: with true pseudo strain, respectively; and

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LUO AND LYTTON ON HEALING USING CSR TEST 2203

TABLE 1 Types of asphalt mixtures tested by the CSR test.

Mixture Type Aggregate Asphalt Binder Air Void Content (%) Aging Period (Months) Test Temperature ( C)
AAD, 4 %, 0 Texas limestone AAD 4 0 20
AAD, 4 %, 6 6
AAD, 7 %, 0 7 0
AAD, 7 %, 6 6
AAM, 4 %, 0 AAM 4 0
AAM, 4 %, 6 6
AAM, 7 %, 0 7 0
AAM, 7 %, 6 6
NuStar, 4 %, 0, 10C Hanson limestone NuStar 4 0 10
NuStar, 4 %, 0, 20C 20
NuStar, 4 %, 0, 30C 30
NuStar, 4 %, 6, 10C 6 10
NuStar, 4 %, 6, 20C 20
NuStar, 4 %, 6, 30C 30
Valero, 4 %, 0, 10C Valero 4 0 10
Valero, 4 %, 0, 20C 20
Valero, 4 %, 0, 30C 30
Valero, 4 %, 6, 10C 6 10
Valero, 4 %, 6, 20C 20
Valero, 4 %, 6, 30C 30

5. Calculate the damage density from the recovery phase of kinds of aggregate are the Texas limestone from San Marcos,
destructive CSR tests by Eq 5. TX and Hanson limestone from New Braunfels, TX. The mix-
ture design in this study considers the effects of initial flaws (air
The calculated damage densities with time form a progres-
voids) and environmental conditions (aging and temperature
sion curve in the recovery phase. The starting point of this curve
variation) on the healing ability of asphalt mixtures. The design
is the damage density at the end of the creep phase. The differ-
variables are chosen as two air void contents (4 and 7 %), two
ence between the starting point and an arbitrary point on the
aging periods (0 and 6 months), and three temperatures (10, 20,
progression curve is the amount of the damage that is restored
and 30 C). The purpose of selecting different materials and
due to healing within this rest period.
mixture design variables is to examine whether the CSR test
The content presented above is a general view of the
along with the EBM approach can discriminate the healing abil-
mechanistic-based approach developed in Ref. [16] to analyze
ity of different asphalt mixtures.
the CSR test data. The final product is a continuous damage
The selected materials and mixture design variables are
density curve from the beginning of the creep phase to the end
combined as shown in Table 1. The mixtures with binder AAD/
of the recovery phase, which will be used later to generate heal-
AAM and Texas limestone have two air void contents and two
ing curves and healing parameters. The materials and labora-
aging periods, but tested at one temperature (20 C) due to the
tory tests conducted in this study are first introduced in the
material availability. The mixtures with binder NuStar/Valero
next section.
and Hanson limestone have one air void content (4 %), two
aging periods, and tested at all three temperatures. In Table 1 as
well as all other tables and figures, the number “4” or “7 %” rep-
Materials and Laboratory Tests resents the air void content; the number “0” or “6” represents
Selection of materials considers the variety of material itself and the aging period; and the number “10C”, “20C”, or “30C” repre-
environmental conditions. The laboratory tests include the CSR sents the test temperature. For example, “NuStar, 4 %, 6, 10C”
tests and the surface energy tests. in Table 1 indicates the asphalt binder is NuStar, the air void
The materials selected for testing include four types of content is 4 %, the aging period is 6 months, and the test tem-
asphalt binder and two kinds of aggregate. The four types of perature is 10 C. The twenty kinds of asphalt mixtures listed in
asphalt binder are: the binder AAD and binder AAM from the Table 1 are subjected to the testing procedures introduced next.
Strategic Highway Research Program Materials Reference The CSR test is conducted using the material test system
Library [17]; the binder designated “NuStar” from New Jersey; (MTS). The specimens tested by the MTS are cylindrical, which
and the binder designated “Valero” from California. The two are molded using the superpave gyratory compactor. The

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2204 Journal of Testing and Evaluation

cylindrical specimens are 102 mm in diameter and 152 mm in density continues decreasing in the recovery phase. The rate of
height. A pair of steel end-caps are glued to the two ends of the reduction is much larger at the beginning of the recovery phase.
specimen and then connected to the MTS. Three axial linear Based on these damage density progression curves, healing
variable differential transformers (LVDTs) are mounted 120 curves can be generated for each tested material, which is dis-
apart on the middle part of the test specimen, which measure cussed as follows.
the axial deformation of the specimen. The gage length of the
axial LVDT is 90 mm. The average of the three LVDTs is used HEALING CURVE MEASURED FROM CSR TEST
to calculate the average axial strain. The healing curve is defined as the normalized extent of healing
Every asphalt mixture specimen is subjected to two consec- versus the rest time during which healing occurs. It quantifies
utive CSR tests: one is nondestructive and the other is destruc- the amount of healing and indicates the healing ability of the
tive. An example of applied stress and measured strains of a material. The normalized extent of healing is defined in the
CSR test is shown in Fig. 1a. The step-loads are added at differ- following way:
ent locations of the recovery phase in order to measure the in-
/fc  /i
ternal stresses at different stages of recovery. In Fig. 1a, the h¼ ; h 2 ½0; 100% (7)
/fc  /0
internal stresses are measured by the seven step-loads at points
a, b, c, d, e, f, and g. There are three steps in each step-load, The difference between /fc and /i , i.e., /fc  /i , represents the
which cause the change of the strains at the corresponding point amount of healing that occurs from the beginning of the recov-
in time. The strain rate may be in one of the following three ery phase to the data point i. The difference between /fc and
conditions, which indicates the relationship between the step- /0 , i.e., /fc  /0 , is the maximum increase of damage density
load and the internal stress: due to crack growth in the creep phase, which represents the
 e_r < 0 at r1 : r1 < ri maximum amount of healing that could occur in the damaged

 e_r ¼ 0 at r2 : r2 ¼ ri
 e_r > 0 at r3 : r3 > ri FIG. 1 Example of CSR test on a NuStar asphalt mixture.

According to the second condition, the internal stress is meas-


ured by the second step r2 . The internal stresses measured by
the stress and strain in Fig. 1a are a series of discrete points
shown in Fig. 1b. These data points are fitted by an exponential
model (Eq 6) to produce a continuous curve of the internal
stress versus time:
t t
ri ðt Þ ¼ ra eg1 þ rb eg2 (6)

It is worth mentioning that the CSR test shown in Fig. 1 is


destructive; a nondestructive CSR test is similar with a different
number (five) of step-loads in the recovery phase and different
steps (two) in each step-load. More details of the nondestruc-
tive/destructive CSR tests and the methods to determine the
internal stress can be found in Ref. [15].

Determination of Healing Curves


and Healing Parameters
The twenty types of asphalt mixtures listed in Table 1 are sub-
jected to the CSR test procedure introduced above. The test data
is analyzed according to the methods presented in the second
section. The final product of the analysis is a continuous dam-
age density curve for each tested specimen. Some examples are
presented in Fig. 2. As shown in Fig. 2, the damage density
increases with time in the creep phase as the damage accumu-
lates in the material. After removing the creep load, the damage

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LUO AND LYTTON ON HEALING USING CSR TEST 2205

FIG. 2
Progression of damage density of asphalt
mixtures in destructive CSR test.

material. As a result, the ratio of (/fc  /i ) to (/fc  /0 ) /i ¼ /0 , which implies that all of the cracking damage gener-
denotes the proportion of the amount of healing that occurs to ated in the material is healed, or complete healing.
its maximum value that could possibly occur. Such a ratio is Figs. 3–6 present the healing curves of the 20 types of
called the normalized extent of healing. The rest time refers to asphalt mixtures listed in Table 1. Some qualitative observations
the length of the time during which healing occurs, which is are made from these figures:
calculated by: • From Figs. 3 and 4, the slope of the initial tangent line (as
Dt ¼ t  t0 ; t 2 ½t0 ; 1 (8)
illustrated in Fig. 3) of the healing curve decreases when
the air void content changes from 4 to 7 % for all AAD
and AAM asphalt mixtures. In addition, the 4 % mixtures
A healing curve is the relationship between h and Dt. The point have a larger normalized extent of healing; in other
of h ¼ 0 on a healing curve corresponds to /fc ¼ /i , indicating words, they heal more than the 7 % mixtures with the
no healing occurs. The point of h ¼ 100% corresponds to same aging period.

FIG. 3 Healing curves of AAD asphalt mixtures. FIG. 4 Healing curves of AAM asphalt mixtures.

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2206 Journal of Testing and Evaluation

FIG. 5 Healing curves of NuStar asphalt mixtures. FIG. 7 Illustration of healing parameters in the healing prediction model.

• From Figs. 3–6, the AAM asphalt mixture has a larger


slope of the initial tangent line and heals more than the
corresponding AAD mixture with the same air void con-
tent and aging period. The NuStar mixture has a larger
slope of the initial tangent line and heals more than the
• corresponding Valero mixture with the same air void
From Figs. 3–6, the slope of initial tangent line decreases
content and aging period at the same temperature.
when the aging period changes from 0 month to 6
months for all AAD, AAM, NuStar, and Valero asphalt It can be seen that the healing curve is a good measure of
mixtures. Moreover, all of the unaged mixtures heal more the healing ability of asphalt mixtures. It has a promising poten-
than the aged ones with the same air void content and tial to discern the healing ability of different asphalt mixtures.
temperature.
In the following section, a modeling technique is employed
• From Figs. 5 and 6, given the same aging period, the slope
based on the healing curve in order to achieve a quantitative
of the initial tangent line decreases when the test temper-
description of the healing ability of various materials.
ature changes from 30 to 20 C and further to 10 C for all
NuStar and Valero mixtures, and the mixtures at 30 C MODELING OF MEASURED HEALING CURVE
heal most while those at 10 C heal least. It is observed from Figs. 3–6 that there is a rapid increase of the
measured healing in the first approximately 10 s. In other

FIG. 6 Healing curves of valero asphalt mixtures. FIG. 8 Examples of measured and predicted healing of asphalt mixtures.

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LUO AND LYTTON ON HEALING USING CSR TEST 2207

TABLE 2 Values of healing parameters in the healing prediction


model. FIG. 9 Effect of asphalt binder on healing of asphalt mixtures.

Mixture Type h_ 1 h_ 2 hb
10
AAD, 4 %, 0 0.1266 1.27  10 0.3392
AAD, 4 %, 6 0.0271 8.46  1012 0.1174
AAD, 7 %, 0 0.0929 7.21  1014 0.1997
AAD, 7 %, 6 0.0169 7.58  105 0.1022
AAM, 4 %, 0 0.1608 5.13  1010 0.5379
AAM, 4 %, 6 0.0306 7.88  1011 0.2509
AAM, 7 %, 0 0.1178 1.17  1013 0.4339
AAM, 7 %, 6 0.0171 1.03  107 0.1979
NuStar, 4 %, 0, 10C 0.0119 1.97  105 0.0749
NuStar, 4 %, 0, 20C 0.0251 1.54  106 0.0841
NuStar, 4 %, 0, 30C 0.1172 1.39  1013 0.1664
NuStar, 4 %, 6, 10C 0.0072 1.21  104 0.0245
NuStar, 4 %, 6, 20C 0.0246 6.35  1010 0.0459
NuStar, 4 %, 6, 30C 0.0392 2.51  1010 0.1381
Valero, 4 %, 0, 10C 0.0034 4.72  105 0.0307
Valero, 4 %, 0, 20C 0.0093 2.37  1010 0.0351
Valero, 4 %, 0, 30C 0.0226 1.02  107 0.0445
Valero, 4 %, 6, 10C 0.0018 1.06  107 0.0221
Valero, 4 %, 6, 20C 0.0063 4.32  105 0.0306
Valero, 4 %, 6, 30C 0.0143 1.34  10–9 0.0420

words, the healing rate is very large during this period. After
that, the healing rate gradually decreases and the change of the
measured healing is less as the rest time increases. To demon-
strate such characteristics, a model in the form of the Ramberg-
Osgood equation [18] is proposed to simulate the healing curve:
 
h_ 1  h_ 2 Dt FIG. 10 Effect of air void content on healing of asphalt mixtures.
^ ¼ h_ 2 Dt þ
h   (9)
h_ 1  h_ 2 Dt

hb

These three parameters are illustrated in Fig. 7 with the aid of a


measured healing curve. The advantage of using this prediction
model is that the healing ability of the asphalt mixture can be
readily described by these three parameters, so it is convenient
to compare and select a type of asphalt mixture with superior
healing ability.
The healing parameters in Eq 9 are determined using the
software MATLAB [19]. A plot of the measured healing by Eq 7
and the predicted healing by Eq 9 are shown in Fig. 8 for several
example mixtures. The predicted healing (labeled with “p” in
Fig. 8) matches very well with the measured healing (labeled
with “m”). The R-square statistics of the examples in Fig. 8 as
well as the rest in Table 1 are all above 0.98. The determined h_ 1 ,
h_ 2 , and hb are given in Table 2 for each type of mixture. The val-
ues of h_ 2 are much smaller, and most of them are nearly zero.
Therefore, the significant parameters in Eq 9 are h_ 1 and hb .
These two parameters are used to compare the healing ability of
these mixtures and demonstrate the effects of mixture composi-
tion, aging, and temperature, which are elaborated next.

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2208 Journal of Testing and Evaluation

FIG. 11 Effect of temperature on healing of asphalt mixtures. FIG. 12 Effect of aging on healing of asphalt mixtures.

COMPARISON OF HEALING BY HEALING PARAMETERS


The initial healing rate and healing scale are first used to exam- Figs. 5 and 6. The shape of the healing curve changes consider-

ine the variation of the healing ability that is caused by different ably from 30 to 20 C and then to 10 C.
types of asphalt binder, as shown in Fig. 9. Comparing AAD It is known that aging also plays an important role in evalu-
and AAM mixtures, which have the same aggregate, both the ating the healing ability of asphalt mixtures. The effect of aging
initial healing rate and healing scale of AAM mixtures are larger is presented in Fig. 12. Both the initial healing rate and healing
than those of the AAD mixtures. Therefore, it concludes that scale decrease as the aging period increases, regardless of the
the AAM mixtures have better healing ability than AAD mix- type of asphalt binder, air void content, and temperature. For
tures. This conclusion is in accord with the findings in the pub- some asphalt mixtures—for example, AAD and AAM
lished literature [20]. Similarly, comparing NuStar and Valero mixtures—there is a substantial reduction of the healing param-
mixtures, which have the same aggregate, the NuStar mixtures eters from the unaged to aged condition. This demonstrates
have better healing ability than Valero mixtures. that these asphalt mixtures are more sensitive to aging in terms
The effect of the air void content on the healing ability is of the healing ability.
examined by comparing the healing parameters of mixtures An application of these findings is that a mixture with a
with 4 % air void content to those with 7 %, which is shown in higher initial healing rate and healing scale should be selected
Fig. 10. It suggests that the asphalt mixtures with 4 % air void for heavy traffic conditions. An additional application is to
content always heal faster and heal more than those with 7 % choose a mixture which has a higher healing scale at elevated
air void content. temperatures or in pavements suffering from a fast aging
The change of the healing ability due to the change of tem- process.
perature is investigated by comparing the healing parameters at
10, 20, and 30 C. The results shown in Fig. 11 indicate that the
temperature has a significant influence on the healing ability of
Conclusions
asphalt mixtures. More specifically, the healing ability is the The paper presents the methods and results of characterizing
highest at 30 C and it decreases rapidly when the temperature healing of various asphalt mixtures using the specially-designed
decreases. Healing of asphalt mixtures at 10 C is much slower CSR test. The primary goal of a CSR test is to measure the inter-
and the amount is less. These facts can also be observed from nal stress during the recovery of a material, which is responsible

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LUO AND LYTTON ON HEALING USING CSR TEST 2209

for the healing process. With the measured internal stress, the [2] Kim, Y. R., Little, D. N. and Lytton, R. L., “Fatigue and
data of the CSR test can be analyzed using the EBM approach Healing Characterization of Asphalt Mixtures,” J. Mater.
to obtain the damage density progression curve. This curve Civil Eng., Vol. 15, No. 1, 2003, pp. 75–83.
[3] Maillard, S., de La Roche, C., Hammoum, F., Gaillet, L.,
directly reflects how the damage develops and heals in an
and Such, C., “Experimental Investigation of Fracture
asphalt mixture subjected to the CSR test. The following points and Healing at Pseudo-Contact of Two Aggregates,”
are emphasized. presented at the Third Euroasphalt and Eurobitume
Congress, Vienna, Austria, May 12–14, 2004, European
• The normalized extent of healing produced by the dam-
Asphalt Pavement Association and Eurobitume, Vienna,
age density progression curve is a direct measure of the Austria.
healing in asphalt mixtures. The relationship between the [4] Nishizawa, T., Shimeno, S., and Sekiguchi, M., “Fatigue
normalized extent of healing and the rest time defines the Analysis of Asphalt Pavements With Thick Asphalt Mix-
healing curve of an asphalt mixture. ture Layer,” Proceeding of the Eighth International Confer-
• By examining healing curves of a variety of asphalt mix- ence on Asphalt Pavements, Seattle, WA, Aug 10–14, 1997,
tures, a healing curve can discern the difference in the ISAP, Lino Lakes, MN, pp. 969–976.
healing ability caused by the air void content, aging, tem- [5] Kim, Y. R., Lee, H., and Little, D. N., “Microdamage Heal-
perature, and the type of asphalt binder. The healing ing in Asphalt and Asphalt Concrete, Vol IV: A Visco-
curve is a straightforward tool to qualitatively evaluate elastic Continuum Damage Fatigue Model of Asphalt
Concrete With Microdamage Healing,” Report No.
the healing ability of asphalt mixtures.
FHWA-RD-98-144, Texas Transportation Institute, College
• A healing model based on the Ramberg-Osgood equation
Station, TX, 2001.
is developed to simulate the healing curve measured from [6] Williams, A. D., Little, D. N., Lytton, R. L., Kim, Y. R., and
the CSR test. The healing model has three parameters to Kim, Y., “Microdamage Healing in Asphalt and Asphalt
represent the healing speed at different stages of healing Concrete, Vol II: Laboratory and Field Testing to Assess
(the initial healing rate and ultimate healing rate) and the and Evaluate Micordamage and Microdamage Healing,”
overall ability of the material to heal (the healing scale). Report No. FHWA-RD-98-142, Texas Transportation Insti-
• Fitting the healing model to the measured healing curves tution, College Station, TX, 2001.
of various asphalt mixtures yields the values of healing [7] Daniel, J. S. and Kim, Y. R., “Laboratory Evaluation of Fa-
parameters. For a CSR test, the significant parameters are tigue Damage and Healing of Asphalt Mixtures,” J. Mater.
the initial healing rate and healing scale. Civil Eng., Vol. 13, No. 6, 2001, pp. 434–440.

[8] Carpenter, S. H. and Shen, S., “Dissipated Energy
By examining the initial healing rate and healing scale of
Approach to Study Hot-Mix Asphalt Healing in Fatigue,”
different asphalt mixtures, these two parameters can
Transp. Res. Rec., Vol. 2006, 1970, pp. 84–91.
reflect the change of the healing ability with the change of [9] Kim, B. and Roque, R., “Evaluation of Healing Properties
an influential factor, including the type of asphalt binder, of Asphalt Mixtures,” Transp. Res. Rec., Vol. 2006, 1970,
air void content, temperature, and aging. An asphalt mix- pp. 84–91.
ture with better and more asphalt binder at higher tem- [10] Wool, R. P. and O’Connor, K. M., “A Theory of Crack
peratures with less aging possesses superior healing Healing in Polymers,” J. Appl. Phys., Vol. 52, No. 10, 1981,
ability; namely heals faster and heals more. pp. 5953–5963.
• Based on the healing curves and healing parameters, [11] Bommavaram, R. R., Bhasin, A., and Little, D. N.,
which are essentially derived from the damage density “Determining Intrinsic Healing Properties of Asphalt
progression curve, the CSR test along with the EBM Binders,” Transp. Res. Rec., Vol. 2126, 2009, pp. 47–54.
[12] Bhasin, A., Bommavaram, R., Greenfield, M. L., and Little,
approach is able to produce a reasonable and consistent
D. N., “Use of Molecular Dynamics to Investigate Self-
prediction of healing for asphalt mixtures.
healing Mechanisms in Asphalt Binders,” J. Mater. Civil
Eng., Vol. 23, No. 4, 2011, pp. 485–492.
ACKNOWLEDGMENTS
[13] Abu Al-Rub, R. K., Darabi, M. K., Little, D. N., and Masad,
The writers acknowledge the Federal Highway Administration E. A., “A Micro-Damage Healing Model That Improves
(FHWA) for the financial support. Special thanks are to Jeff Prediction of Fatigue Life in Asphalt Mixes,” Int. J. Eng.
Perry and David Zeig from the Texas A&M Transportation Sci., Vol. 48, No. 11, 2010, pp. 966–990.
Institute for their help in laboratory testing and specimen [14] Schapery, R. A., “On the Mechanics of Crack Closing and
Bonding in Linear Viscoelastic Media,” Int. J. Fracture,
preparation.
Vol. 39, No. 1, 1989, pp. 163–189.
[15] Luo, X., Luo, R., and Lytton, R. L., “Characterization of
Recovery Properties of Asphalt Mixtures,” Constr. Build.
References Mater., Vol. 48, 2013, pp. 610–621.
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“Microdamage Healing in Asphalt and Asphalt Concrete, of Healing in Asphalt Mixtures Using Internal Stress,” Int.
Vol I: Microdamage and Microdamage Healing,” Summary J. Solids Struct., Vols. 60–61, 2015, pp. 35–47.
Report FHWA-RD-98-141, Texas Transportation Institution, [17] Jones, D. R., “SHRP Materials Reference Library: Asphalt
College Station, TX, 2001. Cements: A Concise Data Compilation,” Report No. SHRP-

Copyright by ASTM Int'l (all rights reserved); Thu Mar 22 08:14:46 EDT 2018
Downloaded/printed by
Indian Inst of Tech Kharagpur (Indian Inst of Tech Kharagpur) pursuant to License Agreement. No further reproductions authorized.
2210 Journal of Testing and Evaluation

A-645, Strategic Highway Research Program, National [19] The MathWorks Inc., MATLAB Version 8.1.0.604, Math-
Research Council, Washington, D.C., 1993. Works, Inc., Natick, MA, 2013.
[18] Ramberg, W. and Osgood, W. R., “Description of Stress- [20] Si, Z., Little, D. N., and Lytton, R. L., “Characterization of
Strain Curves by Three Parameters,” NACA Tech. Note No. Microdamage and Healing of Asphalt Concrete Mixtures,”
902, NACA, Washington, D.C., 1943. J. Mater. Civil Eng., Vol. 14, No. 6, 2002, pp. 461–470.

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