065 Oleocorp CPM SKET GmbH

Analysis for glycerin distillation plant

Sampling points / Parameter to be determined / personnel / frequency *

(l = laboratory personnel, o = plant operators)

P.N.1 (P 0843.01) crude glycerin

- parameters for (l) Each parameter once a day and whenever
crude glycerin: start up the plant
see next page

P.N.2 (P 0843.02) dried crude glycerin

Analysis upon special request

P.N.3 (P 0843.14) glycerin / salt mixture to thin film evaporator

- pH-value (o) Once a shift
- Salt amount (visual test) (o) “

P.N.4 (P 0843.04) glycerin distillate I

Analysis upon special request

P.N.5 (W 0843.05) glycerin to bleaching

Analysis upon special request

P.N.6 (W 0843.08) glycerin-distillate II back to K 0843.01

Analysis upon special request

P.N.7 (W 0843.06) pharma grade glycerin

- water content (l) Once a shift
- color (l) “
- odour (l / o) “
- all other parameters for Each parameter once a day
pharma grade glycerin:
see next page (l)

P.N.8 (container under W 0843.04) residue

- glycerin content (l) Upon special request
- MONG content (l) “

P.N.9/1 … P.N.9/4 (F 0843.01A-D) distilled glycerin

- odour (l / o) Once a day
- color (l) “

P.N.10 (W 0843.11) distillate from K 0843.04

Analysis upon special request

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065 Oleocorp CPM SKET GmbH

* This table is for normal plant operation after some month of experience.
(During commissioning the number of analysis may be higher)

It is only for inside the battery limits of CPM-SKET.

Quality management for unloading of crude glycerin and loading of final glycerin as
well as storage is matter of the client.

Methods of analysis

Pharma grade glycerin

- Glycerin content Ph. EUR 2004, page 4487

- Relative density
- Refraktionindex
- Water content
- Color
- Acidity
EN ISO 12185
Ph. EUR 2004, page 4487
Karl Fischer, EN ISO 8534: 1996
(APHA)
Ph. EUR 2004, page 4487

- Ester value Ph. EUR 2004, page 4487

- Sulphate ash Ph. EUR 2004, page 4488
- Chlorides Ph. EUR 2004, page 4488
- Halogene connections Ph. EUR 2004, page 4488
- Heavy metals Ph. EUR 2004, page 4488
- Odour olfactory test

Crude glycerin

- Glycerin content BS 5711-3

- Water content BS 5711-8

- Salt content incineration

- MONG BS 5711-9
- pH-value ISO 10523 modified
- Phosphatides AOCS Ca 20-99 (01) Upon special request
- Methanol content Gas chromatography “

- Free fatty acids (ffa) ISO 660 modified “

- Monoglycerides DGF C-VI 5b modified “

- Proteins (as N) DGF B-II 6 (89) “

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