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The National Academies Press: Aggregate Quality Requirements For Pavements
The National Academies Press: Aggregate Quality Requirements For Pavements
The National Academies Press: Aggregate Quality Requirements For Pavements
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GET THIS BOOK Erol Tutumluer, Maziar Moaveni, and Issam I. A. Qamhia; National Cooperative
Highway Research Program; National Cooperative Highway Research Program
Synthesis Program; Synthesis Program; Transportation Research Board; National
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N AT I O N A L C O O P E R AT I V E H I G H W AY R E S E A R C H P R O G R A M
Erol Tutumluer
Maziar Moaveni
Issam I. A. Qamhia
Advanced Transportation Geotechnics Solutions, LLC
Champaign, IL
Subscriber Categories
Highways • Materials • Pavements
Research sponsored by the American Association of State Highway and Transportation Officials
in cooperation with the Federal Highway Administration
2018
The National Academy of Sciences was established in 1863 by an Act of Congress, signed by President Lincoln, as a private, non-
governmental institution to advise the nation on issues related to science and technology. Members are elected by their peers for
outstanding contributions to research. Dr. Marcia McNutt is president.
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practices of engineering to advising the nation. Members are elected by their peers for extraordinary contributions to engineering.
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The Transportation Research Board is one of seven major programs of the National Academies of Sciences, Engineering, and Medicine.
The mission of the Transportation Research Board is to increase the benefits that transportation contributes to society by providing
leadership in transportation innovation and progress through research and information exchange, conducted within a setting that
is objective, interdisciplinary, and multimodal. The Board’s varied committees, task forces, and panels annually engage about 7,000
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interested in the development of transportation.
FOREWORD
Highway administrators, engineers, and researchers often face problems for which information
already exists, either in documented form or as undocumented experience and practice. This infor-
mation may be fragmented, scattered, and unevaluated. As a consequence, full knowledge of what has
been learned about a problem may not be brought to bear on its solution. Costly research findings
may go unused, valuable experience may be overlooked, and due consideration may not be given to
recommended practices for solving or alleviating the problem.
There is information on nearly every subject of concern to highway administrators and engineers.
Much of it derives from research or from the work of practitioners faced with problems in their day-
to-day work. To provide a systematic means for assembling and evaluating such useful information
and to make it available to the entire highway community, the American Association of State High-
way and Transportation Officials—through the mechanism of the National Cooperative Highway
Research Program—authorized the Transportation Research Board to undertake a continuing study.
This study, NCHRP Project 20-05, “Synthesis of Information Related to Highway Problems,” searches
out and synthesizes useful knowledge from all available sources and prepares concise, documented
reports on specific topics. Reports from this endeavor constitute an NCHRP report series, Synthesis
of Highway Practice.
This synthesis series reports on current knowledge and practice, in a compact format, without the
detailed directions usually found in handbooks or design manuals. Each report in the series provides
a compendium of the best knowledge available on those measures found to be the most successful
in resolving specific problems.
PREFACE
By Jo Allen Gause
Staff Officer
Transportation Research Board
Constructing and maintaining pavements requires an abundant and dependable supply of qual-
ity aggregates. Aggregate comes from a wide range of materials, including quarried rock, sand, and
gravel, and materials such as slag, reclaimed asphalt pavement, and recycled concrete aggregate. While
all transportation agencies have specifications for aggregate quality, there is wide variation in what
different agencies consider suitable aggregates for specific applications. This synthesis documents
transportation agency requirements for the quality of aggregates for various pavement types.
Information used in this study was gathered through a literature review and a survey of state
departments of transportation and Canadian provincial transportation agencies.
Erol Tutumluer, Maziar Moaveni, and Issam I. A. Qambia, Advanced Transportation Geotechnics
Solutions, LLC, collected and synthesized the information and wrote the report. The members of
the topic panel are acknowledged on page iv. This synthesis is an immediately useful document that
records the practices that were acceptable with the limitations of the knowledge available at the time
of its preparation. As progress in research and practice continues, new knowledge will be added
to that now at hand.
CONTENTS
1 Summary
3 Chapter 1 Introduction
3 1.1 Introduction and Background
4 1.2 Study Approach
5 1.3 Outline of the Chapters
77 Chapter 6 Conclusions
77 6.1 Objectives and Scope of Synthesis Study
77 6.2 Summary of Key Findings
80 6.3 Conclusions and Gaps in Knowledge
80 6.4 Suggestions for Further Research
81 Bibliography
82 Glossary
85 References
92 Appendices A–D
Note: Photographs, figures, and tables in this report may have been converted from color to grayscale for printing.
The electronic version of the report (posted on the web at www.trb.org) retains the color versions.
Summary
Aggregates encompass a wide range of materials including quarried rock, sand, and gravel in
addition to recycled/artificial/byproduct materials such as reclaimed asphalt pavement (RAP)
and recycled concrete aggregate (RCA), steel furnace slag (SFS), blast furnace slag (BFS), and
quarry byproducts (QB). Aggregate type and quality are important factors for determining use
and placement within different layers of the pavement structure. There are wide variations in
what transportation agencies consider suitable aggregates for specific pavement applications.
This synthesis gathered information and presents information related to aggregate quality
requirements for pavement construction. Both current agency practices as well as state-of-
the-art research findings on sources, locations, standards/provisional testing methods, and
ranges for different types of aggregates used in North America are provided. This includes
quality assurance methods as well as frequency of sampling and testing established. This syn-
thesis also provides information on how aggregate quality has been documented and linked
to both structural and functional pavement performance in the field through agency prac-
tices and experience. Environmental concerns such as leaching and potential risk to ground
or outfall waters are discussed. Finally, knowledge gaps related to characterizations and clas-
sifications of different types of aggregates, including lack of performance-based specifications
and implementation of effective aggregate quality assurance programs, are identified.
The synthesis survey questionnaire (Appendix A) on aggregate quality requirements
for pavements included 34 questions posed to transportation agencies in four categories:
(1) aggregate sources and properties; (2) aggregate sampling, quality control, tests, and
ranges; (3) procedures for approving aggregate sources; and (4) aggregate-related perfor-
mance records. Survey questionnaires were sent out to all 50 U.S. Departments of Transpor-
tation (DOTs) and 12 Canadian provincial agencies. Appendix B is a list of all U.S. DOTs and
Canadian provincial agencies that provided responses. A response rate of 90% was achieved
with U.S. DOTs. In total, 45 U.S. DOTs and eight Canadian provincial agencies (Alberta,
British Columbia, Manitoba, New Brunswick, Ontario, Prince Edward Island, Saskatchewan,
and Yukon) participated in the survey. Twenty-seven U.S. DOTs as well as Ontario and
Yukon provided their approved lists of aggregates. A detailed compilation of the compre-
hensive survey responses provided by participating agencies may be found in Appendix C. In
addition, links to agency-approved lists of aggregates/specifications are provided in Appen-
dix D. The appendices are not printed as part of this report but are available for download
from the TRB website (www.trb.org) by searching for NCHRP Synthesis 524.
Based on the reviews of the survey responses and follow-up communications with agency
contacts, differences exist among transportation agencies when it comes to the methods for
approving aggregate materials and quality assurance programs. Alaska, Illinois, Indiana,
Ohio, Ontario, and Texas were found to have some of the most comprehensive aggregate
1
classification systems with diverse quality classes associated with each aggregate type and
pavement layer application. The findings also indicated that only 44% of the agencies classify
aggregates to meet certain quality requirements for pavements. Furthermore, 32 U.S. DOTs
and seven Canadian provinces indicated that they do not collect information for checking
how the quality of aggregate used may affect pavement end performance. More than 50%
of the surveyed agencies reported that they do not implement pavement materials charac-
terization and performance testing in their specifications to check and control the end per-
formances of different qualities of aggregates. Application of RAP in pavement construction
was found to be more common when compared with uses of RCA, SFS, BFS, and QB. This
was to some extent due to environmental concerns as well as to lack of sufficient knowledge
and research findings related to material characterization and field performance of these
aggregate sources. The outcome of the survey showed that transportation agencies com-
monly blend marginal aggregates and QB with virgin aggregates. Nonetheless, they reported
different procedures to control the quality of those blended aggregate products such as for
controlling the quality of individual components or the entire blend as one product.
Detailed information presented in this synthesis is a compilation of literature review and
survey data intended to inform transportation agencies about the common practices and
specifications being implemented related to effective classifications of aggregate sources
used for pavement construction. Based on the findings of this synthesis, further research
and investigation may need to be directed toward developing a comprehensive, consistent,
and sustainable aggregate quality management system in North America. Related research
activities may focus on establishing implementation strategies for such an aggregate quality
management system to achieve satisfactory pavement performance and at the same time
reduce detrimental environmental impacts.
CHAPTER 1
Introduction
3
Quality Application
granular layers are constructed in both rigid and flexible pavements for primarily drainage and frost
protection purposes. Unbound aggregate base/subbase layers used in rigid pavement structures
primarily provide uniform support conditions to the concrete slabs; the structural contribution
of such layers is often not the primary design aspect. However, in both the asphalt concrete and
Portland cement concrete (PCC) bound layer applications, aggregates play a major role not only in
the volumetric design of these layers but also in their strength, stability, and performance. Coarse
and fine aggregates are the construction building blocks of any pavement layer, unbound or bound,
and are primarily responsible for the load-supporting capacity of a pavement.
This synthesis report will focus on different aspects and quality requirements associated with
the use of different sources of aggregates for pavement construction purposes. As a result, sig-
nificant benefits could be derived from broader application and implementation of major find-
ings from this synthesis. The report should be useful to transportation agencies in their efforts
to identify, appraise, and use available aggregate sources in the most economical ways for the
sustainability of intended roadway applications, especially when the availability of high-quality
natural aggregates is decreasing and posing a challenge to many agencies (ACPA 2009, Langer
2011). Such advances will bring sustainability and offer economic and environment-friendly
alternatives for road construction.
Introduction 5
different aspects of aggregate quality requirements to satisfy desired pavement performance. The
survey questionnaire had separate parts relevant to different aggregate quality requirements and
approval procedures. The questionnaire was purposely designed to be comprehensive and at the
same time brief, in an attempt to increase the survey response rate.
The information was requested to encompass all engineering aspects highlighted in the previ-
ous introduction and background section, primarily in the following categories: (a) aggregate
selection process/guidelines for virgin, marginal, nontraditional as well as recycled, and blended
aggregate sources; (b) the processes that are followed in controlling the quality of different sources
of aggregates for pavement applications, with special focus on material properties and testing
techniques/ranges; (c) current practices, innovations, and provisional standards that may allow
the use of recycled, marginal aggregate sources for construction of pavement layers; (d) aggregate
quality improvement techniques such as stabilization and blending that may allow the use of non-
traditional large size and marginal aggregates; and, finally, (e) aggregate quality-related pavement
distresses as well as environmental and performance concerns related to the use of recycled and
artificial/byproduct aggregate sources.
The synthesis survey questionnaire (see Appendix A) on aggregate quality requirements for
pavements was sent to all 50 U.S. DOTs and 12 Canadian provincial agencies. The survey was not
sent to any U.S. territories such as Guam or Puerto Rico. Figure 1-2 shows a map of the United
States and Canada with all the surveyed states or provinces highlighted. In total, 45 state DOTs in
the United States and eight Canadian provincial agencies (Alberta, British Columbia, Manitoba,
New Brunswick, Ontario, Prince Edward Island, Saskatchewan, and Yukon) responded to the
survey questionnaire (see Appendix B). A detailed compilation of all agency responses to the
questionnaire is provided in Appendix C.
Figure 1-2. Map of the United States and Canada showing all surveyed agencies (AB = Alberta, BC = British
Columbia, MB = Manitoba, NB = New Brunswick, ON = Ontario, PE = Prince Edward Island, SK = Saskatchewan,
and YT = Yukon).
quality perspectives are reviewed. Moreover, material sampling and laboratory testing proce-
dures adopted by agencies, aggregate geology and mineralogy assessment, project acceptance
criteria and performance requirements, prequalification, disqualification, and requalification
techniques are included. Chapter 4 summarizes all the factors and properties that different
transportation agencies consider when it comes to aggregate source approval and certification.
Chapter 5 reports aggregate-related pavement performance records. The content of this chap-
ter is based on findings from an extensive review of published literature, survey responses, and
follow-up communications with the responding agencies. As part of the survey scope, it was
also determined if an agency documents the overall impacts of using nontraditional, blended,
and marginal aggregates. This chapter highlights the effectiveness of aggregate source approval
procedures, certification policies, and performance-based specifications established by trans-
portation agencies to ensure satisfactory field performance. This includes performance trends
of in-service pavements (and experimental test sections) constructed with different aggregate
sources. Techniques used by transportation agencies to measure performance of aggregates
used in different pavement layers are discussed. Survey results regarding potential savings in
cost, energy, and environmental impacts that emerge from using nontraditional and marginal
Introduction 7
aggregate sources are also discussed by presenting performance metrics and case histories from
previous and ongoing projects.
Chapter 6 includes the conclusion and suggestions for future research, as well as knowledge
gaps. This chapter portrays the current state of the practice in aggregate quality requirements for
pavement design and construction through a technical assessment of the facts and information
presented in Chapters 1 to 5. A short summary of the most important findings in each chapter
is presented, and limitations for widespread implementation of promising methods or practices
for classifying aggregate based on quality requirements are discussed.
CHAPTER 2
2.1 Introduction
Both short- and long-term performance of any constructed pavement system largely depends
on the quality of materials used in different layers. To ensure adequate performance of pavements
under traffic loading and environmental conditions, transportation agencies have developed
specifications to check source properties considering aggregate quality. This chapter provides
a brief introduction to different types of aggregate materials available as natural resources and
mined from sand and gravel pits and crushed stone quarry operations throughout the United
States. Furthermore, important aggregate properties with respect to application in a certain
pavement layer, types, sources, tests, and quality aspects used by transportation agencies are
described. Finally, quality-related source properties, provisional testing methods, and restric-
tions put in place for using recycled, artificial/byproduct aggregates as well as blended and sta-
bilized aggregates are presented.
Intrusive igneous rocks have a chance to grow large enough minerals to give it a coarse-
grained texture, whereas extrusive igneous rocks cool more rapidly and can be more fine
grained. Igneous rocks often have high amounts of silica. Examples of igneous rocks used in
pavement applications include granite (intrusive), basalt (extrusive), and rhyolite (extrusive).
Granites account for approximately 16% of crushed stone production in the United
States (9% of total aggregate production). Granite is usually classified as excellent crushed
stone, but some granitic type aggregates are weak and brittle due to their poorly bonded
mineral grains. Fine-grained igneous rocks are often “trap rocks,” which are dark-colored,
fine-grained, volcanic rocks, and which make up about 9% of the crushed stone production
(5% of the total aggregate production) (Tutumluer 2013). Examples of trap rock are basalt and
diabase. Trap rocks are classified as excellent crushed stone materials due to their resistance to
chemical reactions and ability to withstand high mechanical stresses (Willett 2011).
Metamorphic Rocks. These rock types are formed by the transformation of existing rocks (may
be sedimentary or igneous) under heat and pressure. Examples of metamorphic rocks
include quartzite, marble, slate, and gneiss. Metamorphic rocks as aggregates can have widely
variable characteristics. Many quartzite and gneiss aggregates can have properties similar to
granite, whereas shale can be slabby and schist can be soft and flaky because of its high mica
content (National Stone, Sand and Gravel Association 2013).
provinces) reported that they do not have any approved lists of aggregates. Additionally, 17%
(seven U.S. DOTs in addition to British Columbia and Saskatchewan provinces) indicated some
other alternatives regarding approved list of aggregate sources. These included (1) an approval
process for aggregates used in HMA and PCC pavements and testing aggregates per project used
in unbound layers; (2) specifications for aggregates to be used for base, subbase, asphalt concrete,
and so forth, considering that an agency owns a number of gravel pits that have been used on
various projects; (3) once a certain aggregate source is approved on a project, using some
aggregates in some cases for other projects for up to a year; or (4) pre-approving the aggregate
producers but still requiring quality testing.
Among the transportation agencies that have an approved list of aggregate types and sources,
93% (26 state DOTs and Ontario province) indicated that they update their list periodically to
include new/other materials into the list of their approved aggregate sources. These transporta-
tion agencies also reported the frequencies when they update their approved list (see Table 2-1).
Only 7% (Washington State DOT and Yukon province) reported that they do not allow new
materials into their approved list of aggregates.
The use of different sources of crushed stone sources was also investigated. The results
are summarized in Figure 2-2, which indicates that the majority of the respondent agencies
use crushed stone aggregates. Half of the participating agencies reported that they use igne-
ous (extrusive) rocks (e.g., basalt or scoria). Note that only Saskatchewan province indicated
that they do not have crushed stone sources. Additionally, New Jersey DOT reported that they
exclude shale, schist, slate, and most sandstones although these sources could be approved if
classified as quartzite and meet physical test requirements.
As discussed in the previous section, the geology and rock origin of natural virgin aggregates is
an important controlling factor of the quality of aggregates. Survey results show that 60% of the
respondents (26 U.S. DOTs and five Canadian provinces) do not receive information regarding
the geologic origins of natural (virgin) aggregates from producers, and 40% (19 U.S. DOTs and
two Canadian provinces) do. Among those agencies that do not receive information regarding the
geologic origins of natural (virgin) aggregates, 71% (19 U.S. DOTs and three Canadian provinces)
indicated that this information is not required/requested by their corresponding agency, while
only 29% (seven U.S. DOTs and two Canadian provinces) reported that geologic origin is identified
in-house by a geologist or petrographer working for the agency.
Information related to different sources of sand and gravel used by participating agencies is
summarized in Figure 2-3. Approximately 71% of the respondent agencies use glacial and fluvial
Number of Responses
0 10 20 30 40 50
Number of Responses
0 10 20 30 40 50
(river) deposits. On the other hand, use of marine, lacustrine (lake), and eolian (windblown)
deposits was found to be less common. Arizona and New Mexico DOTs did not report about
gravel sources, probably because gravel particles can sometimes be found in large sizes and
crushed to be called rock in these states. This is often the case for coarse aggregate materials when
they are referred to as “sand and rock” in the western United States.
In addition to virgin aggregate sources, large quantities of construction and demolition wastes
are produced each year in the United States. The U.S. Environmental Protection Agency (EPA)
estimated that 534 million tons of construction and demolition waste quantities were generated
in the United States in 2014 alone. As shown in Figure 2-4, out of these 534 million tons, 70%
was concrete and 14% was asphalt concrete (EPA 2016).
Number of Responses
0 10 20 30 40 50
Others such as streambed aggregates, drainable
3 6%
stable base 53 survey respondents
Pavement working platforms for subgrade stability
14 26%
applications
Figure 2-5. Pavement layers constructed with specific aggregate quality requirements.
Number of Responses
0 10 20 30 40 50
Figure 2-6. Aggregate types and sources used in pavement layer construction.
As part of the questionnaire, the frequency in utilizing different aggregate sources in pave-
ment construction was investigated. Figure 2-6 summarizes transportation agency responses,
in which 94% indicated the use of RAP and almost 70% indicated the utilization of blended
virgin aggregate sources. Additionally, 15% of the agencies reported the use of marginal
aggregates while 21% of the respondents indicated that they use nontraditional large-sized
aggregates. Also, about half of all responding agencies indicated that they use RCA in pave-
ment applications. Artificial/byproduct and manufactured aggregates, such as SFS, BFS, and
lightweight aggregate (LWA), were reported to be used by 45% of the responding agencies.
The required quality tests for each of these aggregate sources will be further discussed in this
synthesis report.
• For coarse aggregates, AASHTO T 85 or ASTM C127, Standard Method of Test for Specific
Gravity and Absorption of Coarse Aggregate, is used. For example, Oklahoma DOT requires
this test to be conducted on coarse aggregates at the quarries in order to qualify these materials
to be used in construction projects (Oklahoma DOT 2016). Measuring bulk specific gravity
and water absorption of LWA materials is needed, especially for concrete applications to
acquire proper mix proportions (Byard and Schindler 2010, Deshpande and Hiller 2012, Kim
et al. 2012). Bulk specific gravity is also measured for coarse aggregates used in HMA in
order to achieve proper volumetrics.
• For fine aggregates, AASHTO T 84 or ASTM C128, Standard Method of Test for Specific
Gravity and Absorption of Fine Aggregate, is used. This test needs to be conducted on LWA
used in pavement applications (particularly concrete applications) to ensure proper mix pro-
portioning and the additional quantity of water required for the mix (Byard and Schindler
2010, Henkensiefken et al. 2010).
• AASHTO T 19M/T 19 or ASTM C 29/C29M, Standard Test Method for Bulk Density (Unit
Weight) and Voids in Aggregate.
Several AASHTO and ASTM standards are designated to measure the morphological shape
properties of coarse aggregates used in pavement applications. Morphological shape properties
include angularity and flat and elongated ratio. The most common standards are
• ASTM D4791, Standard Test Method for Flat Particles, Elongated Particles, or Flat and Elongated
Particles in Coarse Aggregate. For example, Oklahoma DOT uses this test for open-graded
Portland cement stabilized bases and has a limit of less than 10% (Oklahoma DOT 2009).
• Standards for coarse aggregate angularity include AASHTO TP 61, Standard Method of Test
for Determining the Percentage of Fracture in Coarse Aggregate, and ASTM D5821, Standard
Test Method for Determining the Percentage of Fractured Particles in Coarse Aggregate.
• Fine aggregate angularity (FAA) can be required for some pavement applications, such as
Superpave asphalt concrete mix design (Prowell et al. 2005). Standard test methods include
AASHTO T 304, Standard Method of Test for Uncompacted Void Content of Fine Aggregate,
or ASTM C1252 Method A, Standard Test Methods for Uncompacted Void Content of Fine
Aggregate (as Influenced by Particle Shape, Surface Texture, and Grading).
The following test methods are used to characterize the durability and soundness of aggregate
materials used in pavement applications:
• AASHTO T 210 or ASTM D3744/D 3744M, Standard Method of Test for Aggregate Durabil-
ity Index. For example, Oklahoma DOT requires this test for coarse aggregates at the quarries
for qualifying their materials to be used in Oklahoma DOT construction projects (Oklahoma
DOT 2016).
• AASHTO T 104, Standard Method of Test for Soundness of Aggregate by Use of Sodium
Sulfate or Magnesium Sulfate.
• AASHTO T 103, Standard Method of Test for Soundness of Aggregates by Freezing and
Thawing.
The following test methods are used to characterize the resistance to abrasion and the
toughness of aggregate materials for various pavement applications:
• AASHTO T 327 or ASTM D6928, Standard Method of Test for Resistance of Coarse Aggre-
gate to Degradation by Abrasion in the Micro-Deval Apparatus. For example, Kansas DOT
requires this test as one of the quality tests for their coarse aggregates (Kansas DOT 2017).
• AASHTO T 96 or ASTM C131, Standard Method of Test for Resistance to Degradation of
Small-Size Coarse Aggregate by Abrasion and Impact in the Los Angeles Machine. For example,
Kansas and Oklahoma DOTs require this test as one of the quality tests for coarse aggregates
(Kansas DOT 2017, Oklahoma DOT 2016).
Test methods are used for determining the quality of fines or finer particles (e.g., plasticity
and degradation) and the quantities of deleterious materials in aggregates such as highly reactive
clays, organic matter, and friable particles. These methods include the following:
• The standard test methods for measuring the LL, plastic limit (PL), and PI are AASHTO T 89,
Standard Method of Test for Determining the Liquid Limit of Soils, AASHTO T 90, Standard
Method of Test for Determining the Plastic Limit and Plasticity Index of Soils, and ASTM D4318,
Standard Test Methods for Liquid Limit, Plastic Limit, and Plasticity Index of Soils. Some agen-
cies also use limits on the PI of fine aggregate materials used in certain applications (Prowell
et al. 2005). For example, a PI limit of 6 is specified by Illinois DOT for unbound aggregate base
course materials.
• AASHTO T 21 or ASTMC40/C40M, Standard Test Method for Organic Impurities in Fine
Aggregates for Concrete, is used by Kansas DOT as the standard test procedure when required
by a project or an application (Kansas DOT 2017).
• AASHTO T 176, Standard Method of Test for Plastic Fines in Graded Aggregates and Soils by
Use of the Sand Equivalent Test, or ASTM D2419, Standard Test Method for Sand Equivalent
Value of Soils and Fine Aggregate, also is used for this purpose. Sand equivalent test to deter-
mine the ratio of plastic fines and/or clayey materials is required for Superpave as a standard
test method for fine aggregates used in HMA mixes (Prowell et al. 2005).
• Methylene blue test can be used to determine the amounts of harmful materials in fines,
such as montmorillonite and organic matter (International Slurry Surfacing Associa-
tion 1989). Standard test methods include AASHTO T 330, Standard Method of Test for
the Qualitative Detection of Harmful Clays of the Smectite Group in Aggregates Using
Methylene Blue. ASTM test designation for Methylene blue is ASTM C837, Standard Test
Method for Methylene Blue Index of Clay; or ASTM C1777, Standard Test Method for
Rapid Determination of the Methylene Blue Value for Fine Aggregate or Mineral Filler
Using a Colorimeter, which is required for Superpave mixes (Prowell et al. 2005).
• ASTM C142/C142M, Standard Test Method for Clay Lumps and Friable Particles in
Aggregates, is used by Oklahoma DOT to test aggregates used in bituminous surface treat-
ments (Oklahoma DOT 2009). Indiana DOT also uses AASHTO T 112 for their aggregate
specification and requirements (Indiana DOT 2017a).
• ASTM D7428, Standard Test Method for Resistance of Fine Aggregate to Degradation by
Abrasion in the Micro-Deval Apparatus.
Transportation agencies also identified the quality-related natural (virgin) aggregate properties
that they collect from aggregate producers. The results are shown in Figure 2-7. Specific gravity,
absorption, resistance to degradation, particle shapes, and percent deleterious materials were among
the most common quality properties collected by the respondent agencies. Also, expansion from
hydration reaction, harmful clay content, for example, through the use of Methylene blue test, and
mineralogical composition turned out to be not so common properties collected by producers.
Three transportation agencies reported specific tests or protocols that were required for
determining the aggregate quality properties. These include
• Iowa Pore Index, Iowa Quality Number, X-ray Fluorescence (XRF), X-ray Powder Diffraction
(XRD), and Thermal Gravimetric Analysis (TGA);
• Missouri DOT Test Method TM-14 Water/Alcohol Freeze Test; and
• Alaska Nordic Abrasion test (ASTM 312). The test is performed to measure hardness of coarse
aggregate to be used in surface course HMA. The Alaska Nordic abrasion test is similar to the
micro-deval test but uses a larger drum, with three metal strips in the drum.
Transportation agencies were asked to report if they used natural (virgin) aggregate sources from
other states/provinces. Out of 53 agencies, 83% (41 U.S. DOTs and three Canadian provinces) indi-
cated that they used natural (virgin) aggregates from other sources, while 17% (four U.S. DOTs
Number of Responses
0 10 20 30 40
Other 9 19%
47 survey respondents
Expansion from hydration reaction 6 13%
Alkali Silica Reactivity or Alkali Carbonate Reactivity
(ASR and/or ACR) 23 49%
92%
Specific gravity and absorption 43
Figure 2-7. Quality-related natural (virgin) aggregate properties collected from aggregate producers
by transportation agencies.
and five Canadian provinces) reported that they do not. Those agencies that use aggregates from
other states or provinces were asked to indicate the reasons for this practice. Figure 2-8 presents
the results. Nearly half of the agency respondents indicated that they use natural (virgin) aggregates
from other states or provinces due to budgetary or environmental concerns, while one fourth of
the agency respondents reported the reason as “the need for a better quality aggregate source.” Half
of the agency respondents stated other reasons for using aggregates from other sources. Some of
these reasons are as follows:
• Adding competition to the market, lowering prices, and improving quality.
• Due to request from source near the state border.
• Location of the job site being close to the border of other state.
• Contractor’s decision to use sources in nearby states after meeting the quality requirements
set by the project state.
• Not having any aggregate quarries in the state.
• Producers propose and use out-of-state sources.
Number of Responses
0 10 20 30 40
Figure 2-8. Reasons why one agency may use natural (virgin) aggregate
from other states or provinces.
coating and morphology. Particle size and shape properties, amount of asphalt coating the RAP
particles, and the binder content of the RAP are among the important engineering properties that
control the quality of this material. Since a principal constituent of RAP is its mineral aggregates,
the overall chemical composition of RAP is similar to that of the mineral aggregates. RAP can
be used as a granular base or subbase material in pavement structures (Bennert et al. 2000),
in asphalt mixes (Copeland 2011), and in concrete mixes (Huang et al. 2005). When RAP
is used as an aggregate in an unbound application, the volume of asphalt in the RAP reduces
the specific gravity and the presence of asphalt seals most of the surface area of the particles.
These characteristics result in a lower unit weight and a reduced amount of water needed to
achieve the desired compaction level.
The National Asphalt Pavement Association (NAPA) lists as standard test methods
AASHTO T 308, Standard Method of Test for Determining the Asphalt Binder Content of Hot
Mix Asphalt (HMA) by the Ignition Method, and ASTM D6307, Standard Test Method for
Asphalt Content of Asphalt Mixture by Ignition Method, for recovering aggregates and calculat-
ing the binder content in RAP. These tests are considered quick and easy to perform but require
information about a correction factor for aggregates. Moreover, the asphalt binder content of
the RAP to replace virgin binder in asphalt mixes containing RAP can be determined by using
AASHTO T 164 or ASTM D2172/D2172M, Standard Test Methods for Quantitative Extraction
of Asphalt Binder from Asphalt Mixtures. The use of propyl bromide and other nonhalogenated
solvents is also mentioned by NAPA (National Asphalt Pavement Association 2015).
The theoretical maximum specific gravity of RAP can be determined by using the standard
test method of AASHTO T 209 (R2016), Standard Method of Test for Theoretical Maximum
Specific Gravity (Gmm) and Density of Hot-Mix Asphalt (HMA). For RAP recovery, the standard
specifications used are AASHTO R 59 or ASTM D1856, Standard Specification for Recovery of
Asphalt Binder from Solution by Abson Method. If the viscosity of the extracted binder needs
to be measured, the standard specifications to be followed are AASHTO T 202 or ASTM D2171/
D2171M, Standard Method of Test for Viscosity of Asphalts by Vacuum Capillary Viscometer.
The transportation agencies were asked to indicate if they used RAP materials in the construction
of pavement layers and also to report which quality-related source properties RAP materials were
screened for. The findings are summarized in Figure 2-9. It was also found that most of the agencies
examine the residual asphalt binder content of RAP sources. Moreover, specific gravity, residual
asphalt binder property, and source properties of the aggregates were reported as the common
Number of Responses
0 10 20 30 40 50
Other 13 27%
Freeze-thaw resistance 2 4%
48 survey respondents
quality-related properties that are investigated by respondent agencies. Some agencies mentioned
other quality-related properties associated with utilization of RAP that are listed as follows:
• Effective specific gravity backcalculated from theoretical maximum specific gravity (Rice
method) and asphalt content.
• Decant, PI of fine portion.
Magnesium Sulfate (ACI 2001). However, FHWA Technical Advisory Circular T 5040.37 men-
tions using ASTM C666, Standard Test Method for Resistance of Concrete to Rapid Freezing
and Thawing, for locations where freeze-thaw resistance needs to be checked (FHWA 2007).
Similarly, the AASHTO MP 16 (2015) document lists several tests based on the expected
distresses in the constructed concrete. For example, when D-cracking is a potential distress,
AASHTO MP 16 proposes using AASHTO T 161, Standard Method of Test for Resistance of
Concrete to Rapid Freezing and Thawing, as the test procedure (AASHTO 2015, Reza and
Wilde 2017).
For RCA aggregates where alkali-silica reactions and alkali-carbonate reactions are possible,
AASHTO MP 16 states the uses of AASHTO T 303, Accelerated Detection of Potentially Delete-
rious Expansion of Mortar Bars due to Alkali-Silica Reaction, and ASTM C586, Standard Test
Method for Potential Alkali Reactivity of Carbonate Rocks as Concrete Aggregates (Rock-Cylinder
Method), as standard test methods, respectively (Reza and Wilde 2017). ACI 555R-01 lists plaster,
asphalt, wood, soil, gypsum, plastic, and rubber as some of the contaminants of RCA that can cause
reductions in concrete compressive strength.
Transportation agencies also reported whether they used RCA in pavement layer construction
and also to indicate which quality-related source properties they screen for RCA sources. Figure 2-10
summarizes the results. About 40% of the respondents (15 U.S. DOTs and four Canadian provinces)
reported that they did not use RCA in pavement construction. Moreover, Los Angeles Abrasion
(LAA) loss, percent deleterious/contamination, and specific gravity (bulk)/absorption were found
to be the most common quality properties of RCA that are generally screened by agencies. Only
9% of the agencies stated that they identified ASR for RCA sources. Some agencies also indicated
that they checked the following quality properties related to RCA:
• Aggregate durability index, AASHTO T 210
• Decant, organic impurities
• Florida’s limerock bearing ratio test, similar to continuously reinforced concrete
• Plasticity of fine particles
• Washington State DOT degradation test
Number of Responses
0 10 20 30 40 50
Other 15 32%
Aggregate quarry processes such as blasting, crushing, and screening of coarser grade aggre-
gates produce byproduct mineral fine materials, commonly known as QB or quarry dust. QB
are typically less than 6 mm (0.25 in.) in size and consist of mostly coarse, medium, and fine
sand-sized particles, as well as small fractions of clay and silt-sized particles. Gradation of quarry
fines can vary depending on the rock type quarried. Kalcheff and Machemehl (1980) investigated
average particle size distributions for different types of rocks (flint, trachyte, limestone, diabase,
granite, BFS, and quartzite). They reported similar trends for particle distributions from differ-
ent rock types, with particles passing the No. 200 (0.075 mm) sieve ranging from 6% to 12%.
According to Dumitru et al. (2001), mineralogical tests such as X-ray diffraction analysis should
be conducted to determine the compositions of secondary minerals and to quantify amounts of
harmful content that can be detrimental in some applications of QB. Many standard test meth-
ods conducted on QB are similar to those conducted on fine virgin aggregates discussed above.
NCHRP Synthesis 435: Recycled Materials and Byproducts in Highway Applications: Volume 4:
Mineral and Quarry Byproducts summarizes the common standard tests conducted on mineral
and QB materials (Stroup-Gardiner and Wattenberg-Komas 2013b). See also MIST project report
(Manning 2004).
Lightweight aggregates are used for replacement of normal-weight fine and coarse aggregates
in pavement applications. LWAs can come from different sources and are manufactured from
different materials, including expanded shale, expanded clay, expanded slate, expanded perlite,
expanded slags, and waste fly ash with plastic, among others (Byard and Schindler 2010,
Mallick et al. 2004). They are especially used in concrete applications to reduce internal stresses
from autogenous shrinkage cracking (Byard and Schindler 2010). LWAs are also used for seal
coat and chip seal applications. Kim et al. (2013) compared the performance of chip seal pave-
ments containing different types of LWA or granite aggregates and concluded that pavements
constructed with LWA had a higher initial mean profile depth but a higher drop rate in mean
profile depth with traffic loading. Rahman et al. (2012) reported that the retention rate of LWA
in chip seals was dependent on the source properties and the type of emulsion. According to
the Expanded Shale, Clay and Slate Institute (ESCSI), LWA use in chip seals, compared with
conventional aggregates, results in safer, cheaper, and longer lasting seal coats. This then results
in better skid resistance, with higher skid numbers for LWAs used in chip seal and HMA appli-
cations when compared with the case with limestone aggregates (ESCSI 2017).
Browning et al. (2011) reported that using prewetted vacuum-saturated LWA in concrete
exhibited less shrinkage after 1 year as compared with concretes with normal weight aggregates
without a significant reduction in compressive strength. Higher curing time was also reported
to result in less shrinkage (Browning et al. 2011). Mallick et al. (2004) reported enhancement
for stiffness, rutting resistance, and susceptibility to moisture damage for HMA mixtures with
up to 15% synthetic LWA (made with plastic and waste fly ash) by weight. Mixes with
higher quantities of LWA (20%), on the other hand, were reported to have high absorption
(Mallick et al. 2004). A similar trend for reduction in plastic shrinkage cracking was reported by
Henkensiefken et al. (2010) for fine, manufactured expanded shale, and prewetted LWA volume
replacement up to 33%. Deshpande and Hiller (2012) concluded that helium pycnometry could
estimate the absorption of manufactured LWA more accurately than the standard ASTM C127
test with 24 hours of immersion, due to the higher ability of the helium gas to fill the smaller
voids when compared with water (Deshpande and Hiller 2012). AASHTO M 195 and ASTM
C330 standards cover specifications and procedures for LWA used in structural concrete. Some
of the standards that can be performed for testing LWA, which are also applicable to virgin
aggregates, include ASTM D6928 for micro-deval, ASTM C88 for sodium sulfate soundness,
and ASTM C131 for LAA. Due to the LWA high porosity and the long duration it takes to fill all
the voids when immersed in water, ASTM C127 and ASTM C128 standards for density, specific
gravity, and absorption are not commonly used for LWA.
Information was collected from transportation agencies to determine whether artificial/
byproduct aggregates such as SFS and BFS were used in pavement layer construction and also
which quality-related source properties were examined for these materials. The results are pre-
sented in Figures 2-11 and 2-12. It was found that more than half the survey respondents do not
use SFS or BFS in pavement construction. Agencies that used SFS or BFS reported that specific
Number of Responses
0 10 20 30 40
Mineralogical properties 2 5%
Number of Responses
0 10 20 30 40
Mineralogical properties 2 5%
gravity, freeze-thaw resistance, and expansion properties were the common quality properties
that were tested or screened. Note that expansion properties here refer to general expansion
regardless of use in PCC or HMA. High contents of free calcium and magnesium oxides in SFS
expand when hydrated (Brand and Roesler 2015). Only nine agencies reported that they check
mineralogical properties and chemical compositions of SFS and BFS sources. Alabama DOT
and Texas DOT require both the SFS and BFS materials to undergo all tests that a virgin coarse
aggregate would to be considered for source approval. Furthermore, nine agencies reported
other/additional quality properties associated with SFS and BFS that are listed below:
• SFS: LAA, soundness, wear, specific gravity, and absorption
• BFS: Flat and elongated (F&E) ratio, LAA, wear, soundness, specific gravity, and absorption.
performance in field has been reported. Therefore, some agencies do not consider the degra-
dation requirements based on LAA testing for utilization of BFS [Recycled Materials Resource
Center (RMRC) 2008]. Leachate from BFS poses a potential risk to the environment and remains
an aesthetic concern. Therefore, the odor and discoloration of water need to be checked and the
properties of leachate from BFS such as pH and redox conditions need to be determined (Chesner
et al. 1998).
mixed at various percentages with the DGABC to evaluate whether an optimum mix blend
could be formulated. They reported that RAP, RCA, and DGABC-blended materials obtained
higher resilient modulus values than the currently used virgin aggregates, while RCA mixed
samples resulted in the lowest amount of permanent deformation. Similarly, Arulrajah et al.
(2012) reported that in terms of usage in pavement subbases, RCA and waste rock have geotech-
nical engineering properties equivalent or superior to those of typical quarry granular subbase
materials. Other research has reported similar findings for the use of RAP, RCA, or blends with
virgin aggregates for unbound applications (Arulrajah et al. 2013) and cement-treated applica-
tions (Mohammadinia et al. 2014).
Kazmee and Tutumluer (2015) evaluated the field performance of blended RCA and RAP
test sections, mixed at a ratio of 3:2, respectively, and tested for construction platform and low-
volume road applications using accelerated pavement testing. Laboratory evaluations showed
lower abrasion loss for this blend, compared with other virgin materials inspected. The RCA–RAP
blend exhibited a relatively higher field modulus compared with other constructed test sections
and accumulated the least amount of permanent deformation after a specified number of wheel
passes (Kazmee and Tutumluer 2015).
A recent study by Qamhia et al. (2017a) evaluated construction platforms and subbase
applications of blended materials, QB, and primary crusher run aggregates (PCR), having a
top size of 6 in. to improve stability. To study the packing of the QB with the PCR and deter-
mine the optimum quantities of QB to be mixed, a laboratory study was conducted using a
steel box with dimensions conforming to ASTM recommendations. The large aggregates were
added in one or two equal lifts, and the QB materials were evenly spread on the surface and
then compacted. Preliminary test results from the accelerated pavement testing (a short-term
field test) showed satisfactory performance of the 25% QB blend by weight of the PCR con-
structed in two lifts and 17% QB blend constructed in one lift. Test sections survived 20,000
load repetitions of a 455/55R22.5 super-single tire without accumulating more than 76-mm
or 3-in. rutting, using a wheel load of 10 kips and a tire pressure of 110 psi (Qamhia et al.
2017a, 2017b, 2017c).
Blending of different aggregate sources for Portland cement applications is also a common
practice to achieve the required properties/quality when marginal or recycled aggregates are
used. Reza and Wilde (2017) suggested blending RCA aggregates with high quality conven-
tional aggregates to mitigate the higher likelihood of alkali-silica reactions and issues with
freeze-thaw due to the use of RCA. They proposed using “mechanical interlock blending” or
“belt blending” to ensure the uniformity of mixing for the different aggregate sources. Brand et al.
(2012) evaluated the use of fractionated RAP (FRAP) in concrete mixes, blended with virgin
coarse aggregates in ratios of 0%, 20%, 35%, and 50% by weight of the coarse aggregates. The
FRAP was found to reduce the concrete (compressive, split tension, and flexural) strength,
elastic and dynamic modulus, and the unit weight but increase the workability of the mixes.
Such blending application aims to use the ever-increasing quantities of RAP being produced
due to rehabilitation activities while maintaining the quality of the produced concrete. Results
indicated acceptable paving concrete could be produced for up to 50% FRAP replacement
(Brand et al. 2012).
Agencies can have different requirements for blending. For example, the state of Minnesota’s
standard specification book mentions that if the magnesium sulfate soundness requirement of
<15% loss for coarse aggregates used in Portland cement concrete applications is not met after
five cycles for one aggregate source, then blending of materials from two sources is not permitted
for achieving this requirement (Minnesota DOT 2005). For HMA, Michigan DOT determines
that the aggregate blend used in the mix meet specifications for the content of soft particles and
sand equivalent minimum requirements (Michigan DOT 2014). Kansas DOT, on the other
Number of Responses
0 10 20 30 40
Other 9 22%
41 survey respondents
To utilize quarry byproduct 13 32%
hand, does not allow blending any two aggregate sources for mineral fillers used in HMA mixes
and limits the usage to one mineral filler source per HMA design (Kansas DOT 2015).
Out of the 53 agencies who responded, 77% (35 U.S. DOTs and six Canadian provinces)
blend aggregate from different sources while 23% (10 U.S. DOTs as well as Alberta and Prince
Edward Island provinces) do not. Reasons for blending aggregates are shown in Figure 2-13.
As indicated, most of the agencies blend aggregates to meet either asphalt or concrete mixture
design requirements. Additionally, 63% of the agencies indicated that they blend aggregates to
improve quality. Nearly half of the agencies blend aggregates to use marginal aggregate sources.
Some agencies also reported the following other reasons for blending aggregates:
• Conserving pure silica sand sources for concrete pavement and Surface Aggregate Classifica-
tion “A” for asphalt pavements.
• Supporting batch plants that are not near pit sources.
Information related to different types of materials that are generally used for blending in order to
meet aggregate quality requirements for constructing pavement layers is presented in Figure 2-14.
Most of the transportation agencies blend virgin aggregates with either other virgin materials or
with recycled aggregates, for example, RAP, RCA, or artificial aggregates. In addition, 28% of the
agencies blend virgin aggregates with QB.
Number of Responses
0 10 20 30 40
Figure 2-14. Materials used for blending to meet aggregate quality requirements.
effectively established a stable working platform for pavement construction (Kazmee and
Tutumluer 2015).
Transportation agencies were asked to indicate if they had any special provision for using
nontraditional or marginal aggregate sources such as recycled glass, recycled aggregates, QB,
and large size aggregates for pavement construction. The results are summarized in Figure 2-15,
which shows that only 26 agencies out of 53 survey participants have specifications or provisions
for utilizing alternative materials. Note that out of eight agencies that marked “other,” three
agencies, that is, Arizona and New Brunswick and Yukon provinces, reported that they do not
have any standard for using nontraditional or out-of-specification aggregate sources. The other
five agencies and their considerations are listed in Table 2-3.
Number of Responses
0 10 20
Other 8 31%
26 survey respondents
Filter aggregates, e.g., for pavement interlayers 3 12%
Figure 2-15. Agencies with specifications or special provisions for constructing pavement
layers with nontraditional and/or out-of-specification aggregate sources.
CHAPTER 3
3.1 Introduction
This chapter presents different approaches used by transportation agencies for sampling,
testing, and controlling the quality of aggregates used in pavement construction. QA methods
have been established by many transportation agencies to ensure that the aggregate materials
received on the job site have properties to meet desired criteria for utilizing them in con-
struction of a certain pavement layer. Protocols or specifications used by transportation
agencies to ensure aggregate quality include (1) method specifications, (2) material speci-
fications, and (3) end-result specifications (Dukatz and Marek 1986). Findings from the
survey related to different testing types, frequencies, and procedures performed by agen-
cies on virgin coarse and fine aggregates, RAP, RCA, SFS, and BFS are summarized in this
chapter. Finally, the procedures used to control the quality of blended aggregate products
are discussed.
Participating agencies identified the responsible authority who they put in charge for test-
ing aggregate materials and providing aggregate properties for the design of pavement layers.
Figure 3-1 presents the results.
Figure 3-1 indicates that 81% of the respondents use in-house geotechnical or material labo-
ratories to control the aggregate quality. Additionally, 42% rely on contractor’s laboratory and
testing. And about 30% of the agencies use testing results from producers or external geotechni-
cal laboratories/private consultants for quality assurance purposes. The alternatives included
in Figure 3-1 are considered as the first stage in aggregate quality assurance since in case of a
dispute, private testing laboratories or third parties are often hired to confirm the results. Note
that multiple option selections were made by survey respondents.
29
Number of Responses
0 10 20 30 40 50
Other 9 17%
53 survey respondents
Contractor testing and
22 41%
laboratory
In-house geotechnical/material
43 81%
laboratories
• Through producer’s QC program at the quarry and according to reduced frequency verification
tests mandated by transportation agency; and
• Out-of-state quarries are verified quarterly. However, out-of-country quarries are mandato-
rily tested at redistribution terminals.
Sampling requirements also varied among different agencies. Most agencies specify sampling
techniques for aggregates that comply with a standard, such as AASHTO T 2 (which refers to
ASTM D75), Standard Method of Test for Sampling of Aggregates. For example, Washington
State DOT specifies AASHTO T 2 for sampling requirements for a source approval and requires
limits on aggregate sample cleanliness, sample sizes, and aggregate top sizes based on the aggre-
gate type/application, as indicated in Table 3-1 (Washington State DOT 2017). Similarly, North
Dakota DOT lists AASHTO T 2, AASHTO R 76, and ND T 248 for aggregate sampling and
Number of Responses
0 10 20 30 40 50
Other 21 40%
52 survey respondents
Less than once a year 5 10%
reducing samples of aggregates to testing sizes. Their specification includes standard proce-
dures for sampling aggregates from a roadway, flowing stream, conveyor belt, stockpile, or
truck to ensure representative samples (North Dakota DOT 2015). The State of Alaska also
uses AASHTO T 2 for aggregate sampling (Alaska DOT 2016).
The Illinois DOT manual of test procedures for materials includes detailed procedures for
sampling aggregates from a belt-stream, bin discharge, truck dumps, and stockpile sampling
(Illinois DOT 2015). New Jersey DOT requires obtaining, over a period of several weeks, three
samples from each aggregate size for testing before any source approval (New Jersey DOT 2015).
Idaho DOT requires that the testing of aggregates is performed by an independent laboratory
approved by the agency (Idaho Transportation Department 2014).
North Carolina DOT and North Carolina Aggregates Association (NCAA) jointly published
a comprehensive aggregate QA program that lists procedures and requirements for sampling at
aggregate production and construction sites. The program includes requirements for sampling,
record keeping, sampling checks, verification sampling at the source and job site, and AASHTO or
ASTM tests that are performed on aggregates (North Carolina DOT and NCAA 2017). Additionally,
several agencies provide lists of qualified suppliers/producers, which have been pre-approved
as sources for aggregates in pavement applications. Texas DOT’s aggregate quality monitoring
program, for example, published a list of qualified sources for aggregates for bituminous and
concrete rated applications. Typical source property values are summarized in these catalogs.
Examples of these source qualities include LAA, magnesium sulfate soundness, and micro-deval
(Texas DOT 2007).
Agencies may also require the contractors to perform tests to check the quality of the aggre-
gate materials being constructed. For example, Arizona DOT requires several quality control
test results from contractors, including the sand equivalent test and fractured coarse aggregate
particles for mineral aggregates, as listed in Table 3-2 (Arizona DOT 2008).
Transportation agencies reported how they obtained aggregate samples from project sites to
perform required tests. Figure 3-3 presents the results.
Figure 3-3 shows that 81% of the responding agencies obtain samples and perform quality tests in
their own material laboratories. Moreover, 18 agencies (34%) do the sampling and checking at the
source (quarry) location while 13 agencies (25%) accept samples shipped from aggregate producers
for testing in their agency laboratories. Some agencies assign the sampling to the contractor and then
the quality tests are performed by a consultant/contractor. Finally, there were again multiple option
selections made by survey respondents. This implies that different practices may be taking place
in one agency, depending on what pavement application that aggregate source is used for.
Number of Responses
0 10 20 30 40 50
53 survey respondents
Other 7 13%
Samples checked/inspected
at the source (quarry) 18 34%
location
Figure 3-3. Procedures for obtaining aggregate samples from project sites for
quality tests.
and porosity to also report the testing procedures, for example, ASTM, AASHTO, or agency-
developed specification. The number of agencies at each category for individual tests are
summarized in Table 3-3.
Table 3-3 indicates that 17 agencies do not perform porosity tests on the virgin coarse aggre-
gates and that more than 10 agencies do not run polishing/skid resistance and freeze-thaw tests
on their coarse virgin aggregate sources. Accordingly, 41 agencies follow the AASHTO procedure
to conduct LAA testing, while 22 agencies follow the ASTM test procedure for measuring flat and
elongated ratios of virgin coarse aggregate samples. Moreover, 18 agencies have their own pro-
cedures for determining deleterious materials. Refer to Appendix C for a detailed compilation of
the results given in Table 3-3. Additional tests following other specific test procedures performed
by agencies to determine quality of virgin coarse aggregates are listed in Table 3-4.
Kansas DOT requires some agency specific test procedures for coarse aggregates in order for
an aggregate source to pass their quality requirements. These test procedures are KTMR-21 for
soundness, KT-6 for specific gravity and absorption and, if requested, KTMR-28 for acid insolu-
ble residue. For coarse aggregates used in concrete applications, Kansas DOT also requires addi-
tional tests for durability (KTMR-22) and wetting and drying (KTMR-23) (Kansas DOT 2017).
Alaska DOT runs its own test method (ATM 306) for determining the percentage of flat and
elongated particles in coarse aggregate (Alaska DOT 2016). The state of Arizona conducts its
own test method for fractured coarse aggregate particles, known as ARIZ 212, and ARIZ 251 for
the dry and bulk specific gravity (Arizona DOT 2008). Different quality test ranges, as required
by Arizona DOT in asphaltic concrete are shown in Table 3-5. Different pavement applications
can have different ranges for acceptance by Arizona DOT.
The specifications and ranges for a test vary significantly from one agency to another agency.
A survey by Prowell et al. (2005) indicated different ranges for acceptance of aggregate materials
to be used in Superpave HMA mixtures. As shown in Figure 3-4, most states specify an LAA loss
limit of 40% for HMA mixes, with limits varying from 30% to 55%. Some states also specify LAA
loss limits based on the class of the road, the equivalent single-axle loads, or the type of aggregates
(Prowell et al. 2005).
Furthermore, Kansas DOT requires agency specific test procedures for fine aggregates: KT-6
for specific gravity and absorption, KTMR-26 for mortar strength, and KTMR-28 for acid
insoluble residue, if requested (Kansas DOT 2017).
As noted in the previous section, survey respondents from 42 U.S. DOTs and seven Canadian
provinces reported that they performed at least one test for checking virgin aggregate quality
requirements. These agencies were asked to indicate if they performed the following virgin fine
aggregate quality tests including Na2SO4/MgSO4 soundness, Atterberg limits, deleterious materials,
uncompacted void content, micro-deval for degradation and polishing properties, and sand equiv-
alent. The agencies were asked to report the testing procedures that they followed, and the results
are presented in Table 3-6. Refer to Appendix C for a detailed compilation of the results given in
Table 3-6.
Table 3-6 indicates that 16 agencies do not run micro-deval tests on fine aggregates for measur-
ing degradation and polishing properties and that 29 agencies follow the AASHTO method for
performing sand equivalent test on fine aggregates. Only four agencies use the ASTM procedure.
Moreover, similar to the case for virgin coarse aggregates, 13 agencies have their own procedures
for running deleterious materials test on fine aggregates. Additional tests following other specific
test procedures performed by agencies to determine quality of virgin fine aggregates are listed in
Table 3-7.
Common methods for determining the asphalt content of RAP include ignition method
(AASHTO T 308 or ASTM D6307) and solvent extraction method (AASHTO T 164). Depend-
ing on pavement layer and traffic conditions of the project where RAP is used, additional qual-
ity tests might be required to ensure satisfactory performance. For example, if RAP is used in
a surface mix exposed to high-speed traffic, the polishing or mineralogical composition of the
RAP aggregate might need to be determined.
Deniz et al. (2010) evaluated the expansion properties of RAP aggregates, steel slag RAP, and
virgin aggregates used in Illinois for use as a base or subbase material. ASTM D2940, Standard
Specification for Graded Aggregate Material for Bases or Subbases for Highways or Airports, limits
expansion values to no greater than 0.50% at 7 days when tested in accordance with ASTM D4792,
Standard Test Method for Potential Expansion of Aggregates from Hydration Reactions. Accord-
ing to the findings, stone mastic asphalt RAP, steel slag RAP, surface binder RAP with 60% steel
slag, and surface RAP with 92% steel slag can be safely used as base or subbase materials. However,
porous and nonporous steel slag should not be used without proper curing that satisfies the limita-
tion specified by ASTM D2940 (Deniz et al. 2010).
Transportation agencies were asked about tests they perform for checking RAP quality require-
ments for construction of pavement layers. In total, 28 U.S. DOTs and five Canadian provinces
reported that they perform tests for checking RAP quality requirements. These agencies were
asked to identify if they performed any of the RAP quality tests including residual asphalt binder
content, micro-deval for polishing and degradation properties, deleterious materials, expansion
properties, flat and elongated ratio, and freeze-thaw tests. The agencies were also asked to report
the test procedures, for example, ASTM, AASHTO, and agency-developed test procedure that
they followed. The results are summarized in Table 3-8. Refer to Appendix C for a detailed
compilation of the results given in Table 3-8.
Table 3-8 presents data to indicate that 13 agencies do not evaluate freeze-thaw and expan-
sion properties for their RAP sources, 21 agencies measure residual asphalt content in RAP as a
quality indicator following the AASHTO test procedure, while only three agencies use the ASTM
method. Also, 10 agencies mentioned that they have their own procedures for identifying resid-
ual asphalt content in RAP. Additional tests following other specific test procedures performed
by agencies to determine quality of RAP aggregates are listed in Table 3-9.
recycled coarse and fine aggregates, these limits are 10 kg/m3 for impurities such as plasters, clay
lumps and other impurities of densities less than 1,950 kg/m3, and 2 kg/m3 for asphalt, plastics,
paints, cloth, paper, wood, and similar material particles retained on 1.2 mm sieve, as well as other
impurities of densities less than 1,200 kg/m3 (ACI 2001, Hansen 1986). Illinois DOT considers RAP
as a contaminant for RCA and limits its quantity to 5% for Class C crushed concrete aggregates
used for embankments, subbases, stabilized subbases, bases, gravel roads, and shoulders, and to 2%
for Type B crushed concrete aggregates used for wedge shoulders (Illinois DOT 2017).
FHWA’s Technical Advisory Circular T5040.37 restricts RCA to have not more than 1% asphalt
and requires 90% of all the aggregates to be “cement paste and aggregate” (FHWA 2007). The
Technical Advisory Circular also requires the RCA to be free from chlorides and reactive materials
unless mitigation measures are taken to prevent recurrence of materials related to distresses in
the new concrete. Chloride content is limited to 0.04 kg chloride ion/m3 (0.06 lb chloride ion/yd3)
for the RCA to be used in new continuously reinforced concrete pavement or jointed reinforced
concrete pavement to slow the corrosion of steel (FHWA 2007). The use of higher chloride con-
tents, however, is permitted for jointed plain concrete pavements with epoxy-coated dowel bars.
AASHTO MP 16-13 (AASHTO 2015) also divides RCA for concrete pavement applications
into three classes based on the maximum allowable quantities of deleterious materials; these
quantities are summarized in Table 3-10 (AASHTO 2015, Reza and Wilde 2017). In Table 3-10,
class designations refer to the weathering exposure categories: Severe (A), Moderate (B), and
Negligible (C).
AASHTO MP 16-13 (2015) lists ranges and levels of different quality tests for RCA used in
concrete applications. These ranges are a maximum LAA loss of 50%; a maximum fines content
[passing sieve No. 200 (0.075 mm) of 1.5%]; a maximum chloride content of 0.6 lb/yd3; and
a maximum sodium sulfate soundness loss of 12% if this test is applicable by local experience
(AASHTO 2015, Reza and Wilde 2017).
In total, 19 U.S. DOTs and British Columbia province indicated that they perform at least
one test for checking RCA quality requirements for construction of pavement layers. Those
20 agencies were asked to identify which of the following RCA quality tests they performed,
including LAA loss, absorption, deleterious materials, ASR, micro-deval for polishing and deg-
radation properties, freeze-thaw, and specific gravity. The agencies were also asked to indicate
which testing procedures they followed. Table 3-11 summarizes the results. Only Pennsylvania
DOT reported that it performs similar tests on both RCA and virgin coarse aggregates, and
five agencies reported they do not run micro-deval, ASR, deleterious, and absorption tests on
their RCA sources. Additionally, 14 agencies perform LAA tests following the AASHTO test
procedure, while two agencies run LAA tests following the ASTM method and three other agen-
cies follow their own specifications. Although the ASR test has been reported in the literature as
an important quality indicator of RCA materials and as one of the predominant deterioration
means of concrete (Thomas et al. 2013), only seven agencies measure this property for RCA
sources using different test methods. Florida DOT reported that they do not perform sound-
ness on RCA because of a possible chemical reaction with the paste. Refer to Appendix C for a
detailed compilation of the results given in Table 3-11.
Blast furnace slag is from the first furnace; steel furnace slag is from the second furnace.
SFS is obtained during the steel-making process. SFS is primarily composed of lime, iron oxide,
and silica. The mechanical properties of SFS such as EAF steel slag satisfy (and normally exceed)
the aggregate requirements for granular aggregate subbase or base for permanent deformation,
stiffness modulus, and fatigue (Pasetto and Baldo 2010). Additionally, Yi et al. (2012) indicated
that using SFS as a coarse aggregate in HMA enhances the mechanical properties and using
SFS in cold in-place recycling mixes improves Marshall stability, resilient modulus, and tensile
strength, and reduces the susceptibility to moisture damage and permanent deformation. Using
SFS in refractory concrete mixes was also found to have comparable mechanical properties to
virgin aggregates when the SFS is heated to a high temperature before use (Yi et al. 2012). BFS
can be considered similar to conventional aggregate for application in pavement construction.
The high stability of BFS aggregates and their ability to lock up can be useful in construction over
weak subgrade. Additionally, the compacted unit weight of BFS aggregates is relatively smaller
than the natural aggregates, and the material characteristics produce the greater volume for the
same weight (Chesner et al. 1998).
In total, 15 U.S. DOTs reported that they perform at least one test for checking SFS or BSF
quality requirements for construction of pavement layers. These agencies were asked which of the
following quality tests they performed for SFS/BFS, including chemical composition, mineralogi-
cal properties, specific gravity, micro-deval for polishing and degradation properties, expansion
properties, and freeze-thaw. Additionally, they were asked to report which testing procedures
they followed. The results are summarized in Tables 3-14 and 3-15. Refer to Appendix C for a
detailed compilation of the results given in Tables 3-14 and 3-15.
The survey findings showed that four agencies do not check expansion properties of SFS and
BFS. Eight agencies perform specific gravity tests on SFS following the AASHTO procedure
and two agencies follow the ASTM method. Additionally, four agencies reported that they have
developed their own procedures for measuring specific gravity of SFS sources. Moreover, seven
agencies perform specific gravity tests on BFS following the AASHTO procedure and only one
agency follows the ASTM method. Additionally, three agencies have developed their own pro-
cedures for measuring specific gravity of BFS. Although mineralogical and chemical properties
need to be considered as important quality indicators for both SFS and BFS aggregate sources
(Lewis 1982), few agencies reported that they check this property. Also, it was found that not
many agencies evaluate the freeze-thaw properties of SFS and BFS aggregates.
Arkansas DOT indicated that the DOT performs LAA testing on SFS and BFS aggregate sources.
Pennsylvania DOT checks the quality of SFS and BFS aggregate sources with similar tests per-
formed on natural coarse aggregates. They have also developed the PMT 130 test procedure for
evaluating expansion characteristics of SFS aggregates.
criteria of Superpave, while the method also ensures good performance (Vavrik et al. 2002). For
Portland cement concrete applications, NCHRP Research Results Digest 281: Aggregate Tests for
Portland Cement Concrete Pavements: Review and Recommendations lists both direct and indirect
tests to be used for aggregate blends in concrete.
Indirect tests are those in which concrete specimens are tested. Tests are also divided into
Level I tests (essential) and Level II tests (optional, based on the outcome of Level I tests). Level
I tests include absorption, gradation, properties of fines passing No. 200 sieve (quantity and
plasticity), shape, angularity and texture, thermal expansion of aggregates, aggregate abrasion,
elastic modulus, polishing, aggregate strength and mineralogy, and ASR as well as freezing and
thawing resistance (D-cracking). Level II tests include Methylene blue test for clays, XRD, XRF,
and TGA for aggregate mineralogy as well as other alternative tests for ASR and D-cracking
(Hanna 2003).
Participating transportation agencies were asked to indicate whether they blend aggregate
to improve quality (e.g., virgin + marginal, virgin + quarry byproduct, etc.). It was found that
36% (13 U.S. DOTs and three Canadian provinces) blend different aggregate types to improve
the quality. Subsequently, those 16 agencies were requested to report if they had certain proce-
dures to control the quality of the blended product. The descriptions of the different procedures
reported by the agencies are listed in Table 3-16.
prediction of product performance within pre-established limits for a desired portion of the out-
put (Indiana DOT 2017b) and proposes two principles included in an aggregate quality control
program: making sure that the correct target quality values are understood and achievable, and
controlling variability within pre-established limits.
Indiana DOT illustrates the process of managing and implementing an aggregate quality con-
trol program into an agency, as shown in Figure 3-5.
EMPLOYEE INPUT
MEASUREMENTS VISUAL
CURRENT PROCESS
OVER TIME OBSERVATIONS
DECISION MAKING
PROCESS
CONTROL
Figure 3-5. Stages for managing and implementing an aggregate quality program in an agency.
CHAPTER 4
4.1 Introduction
This chapter presents information related to the procedures used by transportation agencies to
approve or certify aggregate sources. Agencies often consider various criteria or guidelines to allow a
certain type of aggregate source to be used in construction of a specific pavement layer. Appropriate
classification and use of different aggregate materials—for example, by considering different
aggregate quality classes when building bound and unbound pavement layer applications—
will dictate the end performance under different loading and environmental conditions. The
frequency of aggregate approval and the number of quality classes defined for construction of
individual pavement layers are discussed in this chapter.
44
Number of Responses
0 10 20 30 40 50
specific state quality requirements shall be tested to qualify for the surface course use for gravel
roads (FHWA 2015).
The methods used by transportation agencies to approve aggregates are summarized in
Figure 4-1 above. The results show that 72% of the responding agencies use their own laborato-
ries for approving aggregates, and 30% of the responding agencies do not have an approved list
and test aggregates prior to use on every major construction job. Only Maryland, New Mexico,
and North Dakota state DOTs reported that they use “Pre-approval—Option B,” which is
collecting aggregate source property data from a third party certified aggregate testing lab
on a periodic basis. Furthermore, only eight agencies (15%) mentioned other methods for
approving aggregate sources, as listed in Table 4-1.
Number of Responses
0 10 20 30
Based on producer
6 18%
requests
Those agencies that indicated that they used Preapproval Option A or B or Approval by
Agency Lab (see Figure 4-1) were asked to report how often they performed the approval process.
The results are presented in Figure 4-2. It was found that 47% of the agencies do the approval
once a year, while 18% of the agencies perform the approval based on the producer request.
Only Maryland DOT indicated approval of aggregate sources once every 3 years. Eleven agen-
cies (32%) mentioned other frequencies for approving aggregate sources, as listed in Table 4-2.
Table 4-2. Alternative frequency and conditions for approving aggregate sources.
Table 4-3. Aggregate classes and quality requirements for surface and base virgin aggregates.
are not approved for usage (Indiana DOT 2017a). Indiana DOT has more detailed quality class
designations for coarse aggregates, including Class AP (highest quality aggregates that meet the
specifications for any use), Class AS, and Classes A, B, C, D, and F. Indiana DOT also requires an
absorption value measurement not to exceed 5% for those aggregates to be classified in Classes
AP, AS, A, B, or C (Indiana DOT 2017a). Refer to Appendix D, in which there are links provided
to detailed aggregate specifications as well as material approval lists for different agencies.
Minnesota DOT divides the virgin aggregates used for base and surface applications into seven
quality classes. These are Classes 1, 2, 3, 4, 5, 5Q, and 6. The different quality requirements are
listed in Table 4-3 (Table 3138-1, Minnesota DOT 2016). For recycled materials used in base and
surface applications, Minnesota DOT also defines six quality classes, that is, Classes 1, 3, 4, 5, 5Q,
and 6. The requirements for these classes are listed in Table 4-4 [as defined by Minnesota DOT
2016 (Table 3138-2)].
Michigan DOT has published comprehensive requirements for different aggregate classes
qualified as coarse aggregates, open-graded aggregates, and dense-graded aggregates. Table 4-5
Table 4-4. Aggregate classes and quality requirements for surface and base recycled aggregate
materials, as specified by Minnesota DOT.
Coarse
Aggregates
Dense-
Graded
Aggregates
(1)
Open-Graded
Aggregates
(a)
(b)
(c)
(d)
(e)
(f)
(g)
(h)
(i)
(j)
(k)
(l)
(m)
Aggregate Quality Requirements for Pavements
presents a summary of the different aggregate classes and the physical property and quality
requirements for different aggregate materials. Limits and physical properties are included for
gravel, crushed stone, crushed concrete aggregate, slag materials, and other types of aggregates.
Physical properties include LAA loss, freeze-thaw dilation, percentage crushed materials, and
flat and elongated ratio of particles (Michigan DOT 2009).
In total, 18 agencies indicated that they have established at least one quality class for one
of the following aggregate types: coarse and fine virgin aggregates, RAP, RCA, SFS, and BFS.
Table 4-6 lists the different number of quality classes established for each aggregate type by
the 18 transportation agencies.
Agencies that are not listed in Table 4-6 did not report any defined quality classes for the types
of aggregates mentioned above. For further details related to the number of quality classes listed
in Table 4-6, refer to Appendix D, in which the links to agency specifications are provided.
Table 4-6. Number of quality classes used by transportation agencies for different
aggregate types.
Type of Aggregate
Agency Fine Coarse
RAP RCA SFS BFS
Virgin Virgin
Alaska - Five - - - -
Alberta - Five - - - -
Florida One One One One - -
Illinois Three Four Two Four One Four
Indiana One One One - - -
Kentucky Three Five - - One One
Mississippi Three Three - - - -
Montana One One One One - -
Nevada One One One - - -
New York One One One One One One
New Brunswick Two Two - - - -
Ontario Five Five Two - - -
Oregon One One - - - -
Pennsylvania Five Three One One One One
Tennessee - Fou r - - Four -
Wisconsin One One One One One One
Wyoming Five Five - - - -
Yukon Three Three - - - -
Note: Hyphens indicate zero (0) quality class for certain types of aggregate.
and the geological origin, and the fifth class (Class R) is for recycled concrete aggregates. Qual-
ity requirements for aggregates used in concrete include limits on gradations and quantities of
deleterious materials. Quality tests with which the aggregates must comply include LAA loss
(<40%), freeze-thaw loss after 16 cycles (<12%), and magnesium sulfate soundness loss for the
coarse fractions after five cycles (<15%) (Minnesota DOT 2005, 2016).
For HMA layers, Iowa DOT specifies five different aggregate classes (Types 1–5), mainly based
on frictional characteristics. Aggregates within Type 1 have the best frictional properties and have
the highest hardness values, ranging from 7 to 9 on Mohs scale of hardness. Type 1 includes sev-
eral synthetic aggregates, Type 2 natural aggregates include crushed quartzite, Type 3 is crushed
gravel with >40% igneous and metamorphic rocks, and Types 4 and 5 are crushed dolomite and
limestone, respectively. Iowa DOT accepts the use of any aggregate material of the five types in
their HMA mixes unless otherwise specified in the contract to use a certain class of aggregates
(Iowa DOT 2016). Furthermore, Iowa DOT also divides aggregates for HMA into two broader
types: Type A and Type B. Type A is for higher volume road applications and surface coarse
mixtures (Iowa DOT 2017). Note that some agencies do not allow (or limit) the utilization of
a certain aggregate for construction of a specific pavement layer. For example, Minnesota DOT
specifications do not allow the use of crushed concrete aggregates or RCA in wearing surface
courses (Minnesota DOT 2016).
Participating transportation agencies reported the required quality classes for different types
of aggregates used for the construction of asphalt surface course. The results are summarized
in Table 4-7. The number of quality classes established by different agencies have been listed
in Table 4-6.
Table 4-7. Quality classes for aggregates used in asphalt surface course.
Type of Aggregate
Agency
Fine Virgin Coarse Virgin RAP RCA SFS BFS
Alaska - A, B, Superpave - - - -
Designation 1
Alberta - Classes 10,12.5, - - - -
16 mm
Illinois B B B B B B
Indiana - B - - B B
Traffic RAP from
Traffic
Categories A, Category D and
Ontario Categories A, B, - - -
B, C, D, E Category E
C, D, E
mixes
1, 2, 3,
Tennessee 1, 2, 3, 4 - - - -
4
Surface
Aggregate
Texas - Classification A - - - -
or B as indicated
by plans
Paving
Yukon Sand mix Aggregate - - - -
12.5 mm
Note: Hyphens indicate no quality class has been established for certain types of aggregates. Refer to Appendix D,
in which links to agency specifications are provided.
for low-volume and secondary roads (Iowa DOT 2017). Minnesota DOT permits the use of sev-
eral different aggregate classes for plant-mixed asphalt mixtures, including (1) Class A crushed
igneous rocks; (2) Class B crushed rock other than Class A; (3) Class C natural or partially
crushed gravel; (4) Class D crushed natural gravel; (5) Class E mixture of two or more aggregates
from Classes A, B, and D; (6) steel slag in a proportion of 25% or less of the total aggregates mix;
(7) RAP, for which the quality must be checked for the final angularity of the mixture, Los Angeles
Rattler test (Minnesota DOT Procedure 1210) and soundness (Minnesota DOT Procedure
1219), spall materials and lumps (Minnesota DOT Procedure 1219), as well as insoluble residue
test (Minnesota DOT Procedure 1221); and (8) RCA or crushed concrete with a proportion not
exceeding 50% of the total mix (Minnesota DOT 2016).
Participating transportation agencies reported the required quality classes for fine and
coarse virgin aggregates, RAP, RCA, SFS, and BFS used for construction of asphalt base
course. The results are summarized in Table 4-8. Note that the description for each aggre-
gate quality class can be found in the relevant agency specifications with links provided in
Appendix D.
Table 4-8. Quality classes for aggregates used in construction of asphalt base course.
Type of Aggregate
Agency
Fine Virgin Coarse Virgin RAP RCA SFS BFS
Alaska - A, B, Superpave - - - -
Designation 1
Alberta - - - - -
Class 25 mm
Illinois C C C C - C
Indiana - D - - D D
Traffic Traffic
Ontario Categories A, B, Categories A, B, - - - -
C, D, E C, D, E
Fines
Yukon between 3%– Granular "A" - - - -
10%
Note: Hyphens indicate no quality class has been established for certain types of aggregates. Refer to Appendix D,
in which the links to agency specifications are provided.
Table 4-9. Minnesota DOT aggregate quality requirements for aggregates used
in microsurfacing applications.
Participating transportation agencies reported the required quality classes for fine and coarse
virgin aggregates, RAP, RCA, SFS, and BFS used for construction of asphalt surface treatment.
The results are summarized in Table 4-10.
Illinois B B - B B B
Indiana - B - - B B
Gradation Gradation
Ontario - - - -
Classes 2, 4 Classes 1, 2, 3, 4, 5, 6
Surface Aggregate
Texas - Classification A or B as - - - -
indicated by plans
Note: Hyphens indicate no quality class has been established for certain types of aggregates. Refer to Appendix D,
in which links to agency specifications are provided.
Table 4-11. Aggregate classes and aggregate quality requirements for coarse
aggregates used in concrete pavements.
are predominantly chert. Limitations on soundness of such aggregate must be based on service records in the
environment in which they are used.
b Crushed air-cooled, BFS is excluded from the abrasion requirements. The unit mass (by rodding or jigging) of crushed
air-cooled, BFS shall be not less than 1,120 kg/m3 (70 lb/ft3). The grading of slag used in the unit mass test shall
conform to the grading to be used in the concrete. Abrasion loss of gravel, crushed gravel, or crushed stone shall be
determined on the test size or sizes most nearly corresponding to the grading or gradings to be used in the concrete.
When more than one grading is to be used, the limit on abrasion loss shall apply to each.
c The allowable limits for soundness shall be 18% if magnesium sulfate is used. If the salt to be used is not designated,
the aggregate will be acceptable if it meets the indicated limit for either sodium sulfate or magnesium sulfate.
d In the case of crushed aggregates, if the material finer than the 75-µm (No. 200) sieve consists of the dust fraction,
essentially free from clay or shale, this percentage may be increased to 1.5.
deleterious substances for each quality class were previously listed in Table 3-8 (AASHTO 2015).
Similarly, Butler et al. (2013) proposed to divide RCA aggregates into four quality classes, in
which an aggregate material must meet at least three of the four quality property requirements
to be associated with a class, as listed in Table 4-13 (adapted from Butler et al. 2013).
Iowa DOT divides coarse aggregates used in concrete pavements into three classes based on
durability levels as Class 2, Class 3, and Class 3i, in which Class 3i is the most durable one. Dura-
bility of aggregates is determined based on performance monitoring and results of laboratory
testing (Iowa DOT 2016).
Minnesota DOT divides aggregates used in PCC into five classes. Class A includes crushed
aggregates from quarries with rock types such as gneiss (metamorphic rock), quartzite, and
granite. Class B typically covers all non-Class A crushed rocks. Class C includes natural and
partially crushed gravels, while Class D is a mixture of two or more classes of aggregates. Finally,
Class R is for RCA aggregates and requires a concrete engineer to decide on the possibility and
proportioning of these aggregates that can be used in PCC applications (Minnesota DOT 2016).
Participating transportation agencies reported the required quality classes for fine and coarse
virgin aggregates, RAP, RCA, SFS, and BFS used for construction of PCC slabs. The results are
Natural
Coarse Aggregate Property Aggregates RCA-1 RCA-2 RCA-3
summarized in Table 4-14. Note that the description for each aggregate quality class can be
found in the relevant links to agency specifications presented in Appendix D.
Type of Aggregate
Agency
Fine Virgin Coarse Virgin RAP RCA SFS BFS
Illinois A A - A - A
Indiana - AP - - AP AP
Types 1, 2,
Tennessee - Types 1, 2, 3, 4 - - -
3, 4
Note: Hyphens indicate no quality class has been established. Refer to Appendix D, in which links to agency specifications
are provided.
compliance to certain operational criteria, property ranges, and contract compliance for the
sand equivalent, durability index, and R-value tests. Caltrans requires that the durability tests
be conducted on the untreated aggregates for eligibility of use in treated base applications. For
example, the grain size distribution and the quality requirements for a Class 2 aggregate used for
base materials are listed in Table 4-15 (Caltrans 2015).
Similarly, Colorado DOT identifies seven classes for aggregates used in base layers, with
Aggregate Base Course (ABC) Class 6 being the predominant class of aggregates used through-
out the state. According to Colorado DOT, the PI for aggregates used in ABC layer does not
exceed 6. Additionally, the LL values for aggregates used in ABC do not exceed 36 for aggregate
Class 1, 2, and 3 or Class 30 for aggregate Classes 4 through 7 (Locander 2009). Locander (2009)
also proposed that the requirements for RAP used as a base course material had to be similar to
those of Classes 4 through 7, with a PI of less than 6 and an LL lower than 30.
NCHRP Synthesis 598 studied the feasibility of using RAP as a construction material in unbound
layers. Laboratory tests conducted on blends of RAP and other virgin aggregates indicated that
based on toughness, stiffness, and monotonic triaxial testing-based strength characteristics, RAP
was identified as a suitable construction material in unbound aggregate layers for high-volume
roads in nonfreezing conditions. Repeated load triaxial tests indicated the suitability of RAP in
unbound layers for moderate traffic levels in nonfreezing temperatures (Saeed 2008).
Different agencies have different regulations regarding the usage of RAP and its proportioning
in unbound aggregate layers (Hoppe et al. 2015). Hawaii DOT allows use for up to 10% RAP by
weight in base course layers but requires information on the composition of the stockpiled RAP
before usage and limits the maximum quantity of deleterious materials in RAP to 3%. Composi-
tion might be known for previous DOT projects, and when the composition is unknown, samples
are collected to check the gradation and the quantities of deleterious materials. Minnesota DOT
allows a maximum of 3.5% of binder content in aggregate base layers (determined by extraction).
Table 4-15. Aggregate gradation and quality requirements for a Class 2 aggregate
material used as a base course material by California DOT (Caltrans).
Percentage Passing
1-1/2" Maximum 3/4" Maximum
Sieve
Size Operating Contract Operating Contract
Range Compliance Range Compliance
Requirement
Test for Aggregate Quality Operating Range Contract
Compliance
Texas DOT and Washington State DOT allow a maximum of 20% RAP by weight in unbound
aggregate bases. Texas DOT allows up to 50% RAP by weight in cement-treated base layers.
Wisconsin DOT has no limits on the quantity of RAP used in 1¼-in. and 3-in. top size dense-
graded aggregate base layers.
Participating transportation agencies reported the required quality classes for fine and coarse
virgin aggregates, RAP, RCA, SFS, and BFS used for construction of aggregate base course. The
results are summarized in Table 4-16. Note that the description for each aggregate quality class
can be found in the relevant links to agency specifications presented in Appendix D.
Type of Aggregate
Agency
Fine Virgin Coarse Virgin RAP RCA SFS BFS
Alaska - C-1 and D-1 gradations - - - -
Designation 2 Class 20,
Alberta - - - - -
Class 25, and 40 mm
Illinois - D - D - D
Indiana - D - - D D
Ontario - Granular A, M, or O - - - -
Fines not
Yukon more than Granular A - - - -
6%
Note: Hyphens indicate no quality class has been established. Refer to Appendix D, in which links to agency
specifications are provided.
weight deflectometer deflections on top of the drainage layers. These were typically 19 mils for
the unstabilized aggregates and 13 mils for the cement-stabilized open-graded drainage layers
(Kazmierowski et al. 1994).
Michigan DOT allows four classes of granular materials, I through IV, with gradations as
listed in Table 4-18 (adapted from Grove 2004), to be used for porous fill materials.
Participating transportation agencies reported on the required quality classes for fine
and coarse virgin aggregates, RAP, RCA, SFS, and BFS used for construction of permeable
drainage pavement layer. The results are summarized in Table 4-19. Although Michigan
DOT did not report any quality classes, their aggregate specification lists four different
gradation-based classes.
Type of Aggregate
Agency
Fine Virgin Coarse Virgin RAP RCA SFS BFS
Illinois B D - D - D
Indiana - D - - D D
Note: Hyphens indicate no quality class has been established. Refer to Appendix D, in which links to agency
specifications are provided.
CHAPTER 5
5.1 Introduction
This chapter focuses on the aggregate-related pavement performance records and how qual-
ity may be linked to the behavior of individual pavement layers under traffic loading and envi-
ronmental conditions. This includes effects of aggregate quality and source issues on strength,
modulus, permanent deformation, and durability characteristics of bound and unbound layers
in constructed pavement structures. The common aggregate quality-related pavement distresses
reported by transportation agencies will also be presented herein. Finally, environmental
and performance-related concerns experienced by transportation agencies regarding the use of
recycled (e.g., RAP and RCA) and artificial/byproduct aggregates (e.g., SFS, BFS, and quarry
byproducts) will be discussed.
Aggregate quality checks are needed to ensure good performance of aggregates in various pave-
ment layer applications. Source properties affecting the quality of individual aggregate particles
and the ultimate performance of the pavement structure can be related to aggregate’s physical,
chemical, and mechanical properties. In NCHRP Report 598, Saeed (2008) summarized the main
source properties in recycled aggregates that can influence the performance of different layers of
pavement. These properties also apply to virgin aggregate materials used in pavement applications
and are summarized in Table 5-1 (after Saeed 2008). Shear strength of aggregates (mainly recycled
aggregates) was identified as the main quality performance measure when used in structural layers
of flexible and rigid pavements (Saeed 2008). A list of aggregate properties and their influences on
the different pavement layer applications is presented in Table 5-2 (after Saeed 2008).
59
(3) fine aggregate angularity, and (4) sand equivalent (Prowell et al. 2005). Other source
properties tested include abrasion loss by LAA or micro-deval, sulfate soundness, and the
quantities of deleterious materials. The aggregate consensus properties are also determined
for the aggregate blends used in HMA mixes. NCHRP Report 539 states that coarse aggregate
angularity influences the rutting performance of HMA mixes, but it is uncertain if fine
aggregate angularity relates to rutting performance of HMA mixes. The sand equivalent
test relates to the possibility of moisture damage of asphalt mixtures due to poor adhesion
of the binder to the aggregates coated by clay-size particles. The correlation between flat
and elongated ratio and fatigue resistance of asphalt mixtures is controversial as mentioned
in different studies, while the properties of the fine aggregates in HMA can predominantly
control fatigue cracking resistance (Prowell et al. 2005).
Aggregate particle angularity or number/percentage of fractured surfaces has been reported as
one of the most significant factors affecting rutting performance of asphalt pavements (Parker
and Brown 1998). They concluded that mixes with crushed aggregates and highly angular natu-
ral sand showed better rutting performance. Similarly, it was identified through field evaluation
that using rounded coarse aggregates and uncrushed natural aggregates in asphalt mixtures is
one of the main factors contributing to rutting (Button et al. 1990).
A state-of-the-art study by Zaumanis and Mallick (2015) for using high RAP contents (> 40%)
in asphalt plant mixes proposed putting extra efforts into the design and evaluation of RAP,
including proper mixing with the virgin aggregates, the evaluation of the RAP aggregate prop-
erties after binder extraction, and checking the dust content of the RAP, to ensure good field
performance for rutting, fatigue, and longevity (Zaumanis and Mallick 2015). Abdelrahman
et al. (2010) reported a strong relation between the quality of coarse aggregates used in HMA and
performance: aggregate chemical composition can affect moisture susceptibility and bonding to
the asphalt binder; weak bonding between the aggregates and binder in the presence of excessive
deleterious materials such as clay lumps can result in spalling, raveling, and stripping; pavement
aggregate abrasion can be highly correlated to magnesium sulfate soundness and micro-deval
abrasion (Abdelrahman et al. 2010).
The quality for aggregates used in HMA was reported to be influenced by the practices and
techniques adopted by the quarries, aggregate plants, asphalt mixing plant operations, and prac-
tices during construction, which ultimately influence the performance (Vazquez et al. 2010).
MS-16: Asphalt in Pavement Preservation and Maintenance related several asphalt pavement dis-
tresses to the quality of aggregates used in HMA mixes: block cracking can result from using
absorptive fine aggregates with low asphalt penetration, corrugations or shoving can result from
using rounded/smooth aggregates, polished aggregates at the surface can result from using soft
aggregates, and aggregate loss from surface treatments can result from using dusty aggregates
(Asphalt Institute 2009). Similarly, Adlinge and Gupta (2013) reported that corrugation, raveling,
and polishing can result from aggregate quality issues in HMA, including the use of smooth-
textured coarse aggregates, loss of adhesion between binder and aggregates, aggregate breakage,
and aggregate wear (Adlinge and Gupta 2013).
Pan (2006) investigated the effect of morphological shape properties (i.e., angularity, flat and
elongated ratio, and surface texture) on the rutting performance of 46 flexible pavement test
sections constructed at the National Center for Asphalt Technology test track. Each of the three
shape properties was individually correlated to the performance of the different test sections.
The University of Illinois Aggregate Image Analyzer (UIAIA) was used to acquire and process
images of aggregate particles to identify imaging-based shape properties. All three morpho-
logical shape properties individually showed good correlation with the rutting performance of
asphalt mixes. Surface texture showed the highest correlation, with coefficient of determination
equal to 0.94 and the lowest p-value for a statistical t-test (see Figure 5-1).
(a) (b)
(c)
Figure 5-1. Aggregate shape properties and rutting performance of National Center for Asphalt
Technology asphalt mixes showing (a) correlation with surface texture index, (b) correlation with flat
and elongated ratio, and (c) correlation with angularity index (Pan 2006).
Moaveni et al. (2014) combined the micro-deval weight loss values with the imaging-based
shape property results of two different imaging systems: Enhanced University of Illinois Aggre-
gate Image Analyzer and a second-generation Aggregate Imaging System (AIMS-II) for the
evaluation of the tendency of aggregates to polishing, breakage, and abrasion. The two systems
similarly classified 11 types of aggregates into four categories according to resistance to breakage
and abrasion (Moaveni et al. 2014).
This tendency to polishing correlates with the frictional properties of the asphalt surface layers
for aggregates used in HMA mixes, as reported by Mahmoud and Perales (2015). Mahmoud and
Ortiz (2014) developed aggregate polishing curves at different time intervals with micro-deval,
which proved that retention characteristics and changes in surface texture characteristics were
dependent on aggregates mineralogy.
In cold regions, if soft aggregate sources are used in the construction of flexible pavements,
depressions would be developed in the wheel paths (wear-induced rutting) due to excessive sur-
face abrasion caused by studded tires. The effect of using hard aggregates to reduce the flexible
pavement wear caused by studded tires has been studied in Alaska, where high-quality aggregates
are not readily available. According to the cost-effectiveness and performance records collected,
pavement performance could be increased by 1.4 to 1.9 times by using harder aggregates con-
forming to the Nordic abrasion specification (Frith et al. 2004).
Participating transportation agencies listed the aggregate quality-related flexible pavement
distresses they have experienced. In total, 29 U.S. DOTs and eight Canadian provinces indicated
at least one aggregate quality-related flexible pavement distress. The most commonly reported
distresses are listed as follows. Refer to Appendix C for a detailed compilation of the individual
distresses reported by each agency.
• Stripping, debonding, raveling, popouts/pickouts or breakdown of coarse aggregate
• Aggregate polishing
• Longitudinal cracking, block cracking, thermal cracking, joint cracking, and fatigue cracking
• Joint problems
• Rutting and shoving
• Aggregate moisture or freeze-thaw damage
• Rapid oxidation caused by using high amount of RAP aggregate
Stripping and polishing in flexible pavements were found to be the most common aggregate-
related distresses reported by agencies.
distresses in PCC pavements. According to Hanna (2003), the quality indicators for aggregates
that can significantly affect the performance of concrete pavements were mainly divided into
five categories: (1) physical properties, (2) mechanical properties, (3) chemical and petrographic
properties, (4) durability properties, and (5) others. The report summarizes common distress
types and the aggregate properties related to each distress type for all concrete pavements, specif-
ically for jointed plain concrete pavements (corner breaks and faulting) and CRCP (punchouts).
The summary of findings is presented in Table 5-5, which lists the aggregate properties that con-
tribute to common distresses or performance parameters and the mechanisms leading to those
distresses or parameters. A summary of the performance parameters and the corresponding
aggregate properties are also presented in Table 5-6. Mineralogy, morphological shape properties,
abrasion resistance, coefficient of thermal expansion, and texture are common aggregate
properties related to the different performance parameters in concrete pavements. In conclusion,
as indicated in Tables 5-5 and 5-6 (both after Hanna 2003), aggregate properties and the quality
significantly influence rigid pavement performance.
As part of the survey questionnaire, information was collected from participating trans-
portation agencies regarding rigid pavement distresses attributed to aggregate quality aspects.
Twenty-seven U.S. DOTs and four Canadian provinces indicated that at least one aggregate
quality aspect contributed to a rigid pavement distress. The commonly reported distresses are
listed as follows. Refer to Appendix C for a detailed compilation of the individual distresses
reported by each agency.
• ASR and resulting cracking issues
• Cracking associated with coefficient of thermal expansion of coarse aggregate
• Sulfate attack
• Carbonate reactivity of both coarse and fine aggregates
• Polishing of fine aggregate
• Durability cracking, freeze-thaw expansion, and staining
• D-cracking and map cracking
• Clay balls/lightweight pieces may affect concrete surface, strength, and durability
• Popouts and corner breaks
• Joint spalling, joint faulting, and scaling
ASR and resulting cracking issues were found to be the common rigid pavement distress
linked to aggregate quality reported by agencies. ASR usually results in random cracking at the
surface of the concrete and is caused by excessive internal expansion. The most reactive aggre-
gate contains opal, chalcedony, and certain forms of chert (opaline and chalcedonic cherts),
volcanic glass, or siliceous impurities. Many igneous rock types that are acidic are potentially
reactive (Thomas et al. 2013).
PCC is unique in the significant degree to which it can be adversely affected by the destructive
forces caused by cycles of freezing and thawing. With respect to the important effects of repeated
freezing and thawing, the colder winter months of the northern states are not necessarily more
unfavorable than the warmer southern winters of the southern regions. While freeze-thaw
related damage may be caused by as few as 2 or 3 cycles of freezing per year (Janssen et al. 1986),
greater numbers of freeze-thaw cycles generally lead to greater damage. Thus, a milder climate
with frequent thaws during the day can be more severe than a colder climate that stays frozen.
This can be especially true at higher elevations that thaw daily but re-freeze at night (Barksdale
1991, Vanderhorst and Janssen 1990). Aggregate-related freeze-thaw damage to concrete pave-
ments is often manifested by D-cracking that occurs at pavement joints and cracks, which results
in the eventual disintegration of the concrete near the joint.
Aggregates with D-cracking potential are often identified by testing with AASHTO T 161
(ASTM C666), though this procedure can take 8 weeks or more to complete. A rapid test
Table 5-5. Concrete pavement performance parameters and the corresponding aggregate properties.
Pavement Performance
Manifestation Mechanisms PCC properties Aggregate properties
type parameter
Table 5-6. Aggregate properties determining quality linked to corresponding concrete pavement
performance parameters.
procedure called the hydraulic fracture test was developed as part of the Strategic Highway
Research Program. This test procedure requires eight working days rather than eight weeks
to complete. Though not considered precise enough to use as an aggregate rejection test, the
procedure does have merit as a screening test (Janssen and Snyder 1994, Snyder et al. 1996).
The identification of some D-cracking aggregates has proved difficult because the aggregates
only appear to produce D-cracking after exposure to deicing salt. Some efforts have been made
to identify these aggregates by pretreating the aggregates with sodium chloride prior to making
AASHTO T 161 concrete specimens (Dubberke and Marks 1985).
Desta et al. (2015) described the redevelopment of the hydraulic fracture test equipment with
major renovations, sample preparation procedures, and analysis of results to produce a reliable
8-day test that predicts the results of the 90-day AASHTO T 161 test with significant accuracy.
Indiana DOT has developed a new testing specification based on the new hydraulic fracture test
(Desta et al. 2015). The new hydraulic fracture test is a simpler, quicker test using equipment that
is less expensive to buy and maintain than equipment used for AASHTO T 161, which can lead
to both cost reduction and cost avoidance. With a quicker test, aggregate quality can be ensured,
especially if the aggregate source needs to be changed during construction or for sources with
highly variable aggregate quality, making these sources a more viable option.
is related to stripping and permanent deformation; (8) micro-deval test is related to potholes,
raveling, and popouts; and (9) magnesium and sulfate soundness are related to potholes, ravel-
ing, and popouts (Kandhal and Parker 1998).
A summary of the aggregate performance tests and correlation values is given in Table 5-8
(Kandhal and Parker 1998). In this table, the correlation coefficient (R) ranges between –1 and 1
and refers to the linear dependence or goodness of fit between a specific test and the performance
of the HMA layer. The significance level (P) refers to the probability of rejecting the null hypoth-
esis when it is true. Higher absolute values of R and lower P values indicate a better correlation
between the prospective test and the performance of the HMA layer.
The research in NCHRP Report 557: Aggregate Tests for Hot-Mix Asphalt Mixtures Used in
Pavements (White et al. 2006) investigated several aggregate performance tests for aggregates
used in asphalt pavements. The study concluded that micro-deval and magnesium sulfate
soundness were important aggregate performance tests for all materials, traffic conditions, and
climates. Accordingly, White et al. (2006) proposed maximum limits of 15% and 20% for micro-
deval and magnesium sulfate soundness tests, respectively.
5.3.2 Mineralogy
Mineral composition of aggregates has a significant effect on the physical and chemical char-
acteristics that ultimately govern the performance of unbound aggregate base or subbase layers
under loading. This is particularly true as far as degradation and polishing due to interparticle
friction is concerned. Calcareous aggregates like limestone and dolomite show significantly lower
resistance to particle degradation and polishing. Therefore, unbound aggregate base or subbase
layers constructed using these aggregates are likely to undergo significant changes in gradation
during compaction and subsequently under traffic loading (Tutumluer 2013).
Furthermore, Pan et al. (2006) studied the effects of particle angularity and surface texture for
21 blends of uncrushed and crushed aggregate sources on the resilient modulus and permanent
deformation behavior of unbound granular materials and concluded that both angularity and
surface texture were closely linked to modulus and deformation.
The effect of aggregate shape, texture, and gradation on the performance of fresh concrete has
also been investigated by Quiroga and Fowler (2004), who observed that aggregate blends with
cubical shape and rounded and smooth particles required less paste at a given slump as opposed
to blends with flat, elongated, angular, and rough-surfaced particles. The effects of shape prop-
erties of aggregates quantified by digital image processing has been studied on the compressive
strength properties of cement concrete (Polat et al. 2013). The study concluded that spherical
particles were desirable for increased compressive strength, unit weight and slump.
The research in NCHRP Synthesis 539 focused on aggregate properties and the performance of
Superpave-designed HMA (Prowell et al. 2005). The study showed that increasing coarse aggregate
fractured faces or angularity increased rutting resistance. Additionally, increased particle index
value or uncompacted voids in coarse aggregates also provided increased rutting resistance. The
latter combines the effect of form (particle shape and often 3-D geometry), angularity, and surface
texture associated with each particle.
The relationship between aggregate surface texture and asphalt pavement skid resistance
was studied by Masad et al. (2007) in Final Report for Highway IDEA Project 114 by using
a second generation of aggregate imaging system (AIMS-II). The findings verified that skid
resistance not only was related to the average aggregate surface texture but also to the texture
distribution within an aggregate sample. Accordingly, aggregate surface texture distribution
could be considered in developing accurate performance models to predict asphalt pavement
skid resistance.
Frictional resistance or skid resistance is an indicator for the performance of asphalt pavements
(Mahmoud and Perales 2015). The frictional resistance is a function of the macrotexture and
microtexture of the pavement surface (Dahir 1979, Mahmoud and Perales 2015). The macro
texture is primarily influenced by the aggregate shape properties of the mix, and the polishing
resistance of aggregates needs to be tested to ensure the quality of the aggregates that are being
used for the surface coarse HMA mixes. Mahmoud and Perales (2015) concluded that surface
texture is a better indicator of aggregates quality to use for ranking aggregate materials for
performance when compared with angularity.
size distribution or decrease in coarse-to-fine fraction ratio (Gatchalian et al. 2006, Lynn et al.
2007, Pintner et al. 1987). It is important to note that, on the one hand, aggregate degrada-
tion can cause abrasion, which results in particles losing their angularity and surface texture or
becoming more rounded and spherical. Aggregate degradation changes the void ratio or packing
properties and ultimately influences the performance. On the other hand, aggregate particles
after breakage possess fresh surfaces that might have sharp edges and rougher surface texture
(Moaveni 2015).
Several studies also focused on comparing LAA wear, micro-deval, and impact and crushing
wear. Brandes and Robinson (2006) reported that micro-deval correlated best with magne-
sium and sodium soundness degradation for aggregates used in HMA when compared with
LAA and another dry test, such as impact and crushing, which showed a lower correlation.
Test results for degradation of coarse aggregates used in the state of Virginia showed less vari-
ability and more repeatability with micro-deval as compared with soundness test. Micro-deval
showed better ability to differentiate the quality of good-performing and poor-performing
aggregates (Hossain et al. 2008a). Another study for the durability of fine aggregates in
Virginia proposed micro-deval over other conventional durability tests due to higher pre-
cision and correlation to performance from 10 aggregate sources (Hossain et al. 2008b).
Similarly, Rangaraju and Edlinski (2008) reported a high correlation between aggregate per-
formance and micro-deval with 18% permissible loss, while sulfate soundness and LAA did
not correlate well with performance given South Carolina DOT’s specifications of 15% and
55% loss, respectively, for these tests. The study also reported higher micro-deval loss for
aggregates with finer gradations (finer micro-deval-C versus micro-deval-B/micro-deval-A
gradations were investigated) (Rangaraju and Edlinski 2008). Similar effect of grain size dis-
tribution on micro-deval loss was also reported for aggregates from 72 sources in the state of
Maine (Nener-Plante 2013).
Erichsen et al. (2011), on the other hand, concluded that a suitable durability test is dependent
on aggregate quality and the method of degradation in the field: LAA test correlates better with
degradation by fragmentation while micro-deval and Nordic abrasion tests correlate better to
degradation by wearing, in which a more poorly graded gradation curve is obtained after the
tests (Erichsen et al. 2011). Similarly, Cooley and James (2003) tested aggregates from 72 sources
in eight states with micro-deval and LAA and reported a poor correlation between micro-deval,
sodium sulfate soundness, and LAA for the same aggregates, indicating that these tests are essen-
tially measuring different properties, depending on the aggregate source. A study for aggregates
used in Alaska concluded better correlation between performance of aggregates in HMA and
micro-deval test when compared with the Washington degradation test that is currently used in
the state (Liu et al. 2017).
Number of Responses
0 10 20
Other 7 33%
Findings from the Transportation Pooled Study TPF-5(129) (Edil et al. 2012) showed that
although RAP materials could show very high resilient modulus values, unbound aggregate
specimens tested in the laboratory and base/subbase layers constructed in the field using 100%
RAP materials often accumulated high permanent deformations. A similar finding was also
reported for using 100% RAP in construction platforms by researchers at the Illinois Center for
Transportation (Kazmee and Tutumluer 2015, Kazmee et al. 2017).
Expansion of RAP is particularly critical when it contains expansive components like steel
slag. Steel slag aggregates are often used in HMA surface courses because of their high fric-
tional characteristics. Therefore, any RAP material obtained from these surface courses with
steel slag aggregates may potentially lead to expansion and resulting pavement heave when used
in unbound aggregate base/subbase courses. Recent experiences with volume changes of up to
10% or more have been attributable to hydration of the calcium and magnesium oxides in the
recycled steel slag aggregate when water was encountered in the pavement base layer (Collins
and Ciesielski 1994). The free lime hydrates rapidly and can cause large volume changes within
a few weeks, while magnesium oxide hydrates more slowly and contributes to long-term expan-
sion that may take years. The potential expansion depends on the origin of the slag, grain size
and gradation, and the age of the stockpile (Rohde et al. 2003).
Deniz et al. (2010) reported that RAP materials had much lower tendencies to expand when
compared with the expansion potentials of virgin steel slag aggregates, likely due to the asphalt
coating around the aggregates that prevents any significant ingress of water into them. Depend-
ing on the level of expansion and the material gradation, dense-graded aggregate base applica-
tions with steel slag may have to be avoided (Deniz et al. 2010).
Ooi et al. (2011) listed the following criteria for using RCA as a base course. The criteria are to
(1) allow only uncrushed concrete that can be visually inspected for use as RCA, (2) accept RCA
only from suppliers that can guarantee the quality, (3) not accept RCA from unknown sources
unless certified by a qualified engineer or scientist as being free from deleterious materials (such
as aluminum), (4) avoid using building demolition RCA, (5) require a paper trail to document
the RCA source, and (6) use a nonferrous metal detector to determine whether aluminum is
present and also to inspect the RCA visually before use.
Reza and Wilde (2017) mentioned some quality concerns regarding the use of RCA in Portland
cement applications. These pertained to concerns over the source of the RCA and possible dis-
tresses in the RCA, exhibited due to material quality, such as D-cracking and ASR. Other con-
cerns included issues with workability and product quality related to the use of RCA in concrete
pavements. High absorption, durability concerns, higher drying shrinkage, and lower modulus
of elasticity are also among the quality concerns related with the use of RCA in PCC (Reza and
Wilde 2017). Several studies also reported leaching to groundwater and high pH levels as issues
with RCA (Engelsen et al. 2012, Reza and Wilde 2017, Sani et al. 2005).
NCHRP Synthesis 435: Volume 5 identified several limitations for using iron and steel slags
in pavement applications including use in HMA and PCC layers, as summarized in Table 5-10,
for BFS, SFS, and other types of slags. Table 5-10 lists slag availability, slag material properties,
and regulations as the most frequent barriers for using combustion byproducts in pavement
applications. Undesirable material properties include high specific gravity, high absorption, and
issues with freeze thaw. One limitation for steel slags is that it can lead to decreased compatibility
and workability and high hauling costs due to its high specific gravity and unit weight (Stroup-
Gardiner and Wattenberg-Komas 2013a).
Due to leaching, expansion, and other past issues experienced by agencies with the use of steel slag,
the 17 agencies that use steel slag aggregates, as listed in NCHRP Synthesis 435: Volume 5, adopted
different criteria for acceptance in applications other than HMA. Some agencies specified an
Question: Comment on barriers to the use of combustion byproducts in highway applications that have been either
overcome or still exist
States with barrier
Barrier category Reasons for classification as barrier
responses
expansion test either by the DOT or by the supplier (Illinois, Indiana, Minnesota, Ohio, South
Carolina, and West Virginia) and some states required moisture curing prior to use. For example,
Ohio requires 1-month moist curing, Missouri requires 3 months, while South Carolina and
West Virginia require 6 months. None of the states listed above permit using steel slag aggregates
in PCC (Washington State DOT 2015). For slag use in concrete pavements, it has been reported
that dissolution of calcium sulfide in air-cooled BFS might lead to paste expansion and cracking,
but the extent is not well known. Concrete toughness, loss of workability, and maintenance
costs (which can be twice as high compared with using natural aggregates from the experience
of Michigan DOT) have been cited as issues for using BFS (Morian et al. 2012).
Leachate from BFS poses a potential risk to the environment and remains an aesthetic concern.
This requires checking the odor and discoloration of water and determining the properties of
leachate from BFS such as pH and redox conditions. The Recycled Materials Resource Center
lists several quality assurance measures to reduce leachate issues, including stockpiling the air-
cooled BFS for a minimum of 1 month before usage and using air-cooled BFS above grade only and
in areas were drainage is not problematic and the BFS is not immersed in water (RMRC 2017). For
example, bucket test for leachate determination can be performed prior to construction, which is
the current practice by Illinois DOT (Illinois DOT 2015, RMRC 2017).
Additionally, the hardness of BFS can be measured by Moh’s scale ranges from 5 to 6, which is
similar to that of durable igneous rock. Nevertheless, BFS is brittle and easy to breakdown when
subjected to impact loading (RMRC 2017). No correlation between LAA test for BFS and its
degradation performance in the field has been reported (Chesner et al. 1998). Therefore, some
of the states do not consider the degradation requirements based on LAA testing for utilization
of BFS. On the other hand, the EPA studied the leachate results of SFS along with the toxicity
characteristic leaching procedure regulatory limits. The results showed that the average values
of metals under consideration did not violate the limits set in toxicity characteristic leaching
procedure regulation levels (Stroup-Gardiner and Wattenberg-Komas 2013a). Therefore, it was
concluded that the use of SFS was safe and did not induce any contamination even in areas where
the groundwater table was shallow.
Participating transportation agencies indicated whether they have any environmental (e.g.,
leaching) or performance (e.g., cracking) concerns regarding the use of recycled aggregate (RAP
and RCA) or artificial/byproduct aggregates (SFS and BFS) in pavement construction. It was
found that 57% (26 U.S. DOTs and three Canadian provinces) have experienced at least one
environmental or performance-related concern. Those 29 agencies described any environmental
or performance issues of their concern, and their concerns are listed in Table 5-11. Using RAP
and RCA in pavement applications was linked to the two most commonly encountered concerns
among different agencies. High percentages of RAP were reported to create premature asphalt
cracking while using RCA involved higher pH and leaching concerns.
Refer to Appendix C for a detailed compilation related to individual responses reported by
each agency.
CHAPTER 6
Conclusions
77
• Uniform practice does not exist among different agencies regarding the use of RAP,
RCA, SFS, and BFS in pavement construction. Furthermore, transportation agencies fol-
low different restrictions considering quality concerns for using recycled and artificial
aggregates.
• Ninety-four percent (94%) of the responding agencies confirmed the use of RAP in pave-
ment applications. Residual asphalt binder property and source properties of RAP aggregates
were reported as the common RAP quality indicators that are investigated by transportation
agencies.
• Forty percent (40%) of the agencies reported that they do not use RCA in pavement
construction.
• Artificial/byproduct and manufactured aggregates, such as SFS, BFS, and LWA, were reported
to be used by 45% of the responding agencies.
• Transportation agencies indicated that they commonly blend marginal aggregates and QB
with virgin aggregates. Out of the 53 agencies, 77% reported that they blend aggregate from
different sources.
• Additionally, 15% of the agencies reported the use of marginal aggregates, while 21% of the
respondents indicated that they use nontraditional large size aggregates.
Conclusions 79
• The use of high percentages of RAP was reported by the survey responding agencies to have
caused premature asphalt cracking. Also, the use of RCA in pavement layer applications was
offered as a possible cause of high pH and leaching issues. Accordingly, the survey results
showed that performance-related concerns have led agencies to limit the increased use of
RAP, while environmental and durability-related concerns are the most prevalent when it
comes to utilizing RCA, SFS, and BFS in pavement construction.
• According to the findings from the reviewed literature, expansion of the RAP material was
particularly a concern when RAP contained expansive components like steel slag.
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81
Glossary
82
Glossary 83
Fluvial In geography and geology, fluvial processes are associated with rivers
and streams and the deposits and landforms created by them.
Glacier A thick, long-lasting mass of ice accumulated on land surfaces.
Leachate Any liquid material that drains from land or stockpiled material and
contains significantly elevated concentrations of undesirable material
derived from the material that it has passed through.
Lightweight Produced from materials such as clay, shale, slate, perlite, and slags.
aggregate The raw material is expanded to about twice the original volume of the
raw material. The expanded material has properties similar to natural
aggregate, but is less dense and therefore yields a lighter product.
Marginal Any aggregate that is not normally usable because it does not have the
aggregate characteristics required by an agency’s specification, however, could be
source used successfully by modifying normal pavement design and construc-
tion procedures through research and investigation.
Mineralogy A subject of geology specializing in the scientific study of chemistry,
crystal structure, and physical (including optical) properties of minerals
and mineralized artifacts.
Morphological Aggregate shape properties including forms such as flatness and elon-
aggregate properties gation or sphericity, angularity, and surface texture.
Nontraditional Aggregate materials with maximum particle sizes up to 8 in. (203 mm)
large size aggregates generally used as rock fills to improve bearing capacity of soft subgrades.
Polishing Polishing relates to the loss of aggregate surface texture, which can affect
pavement’s microtexture and influence its skid resistance.
Porosity Porosity is the dominant pore size and pore size distribution of aggre-
gate particles. Porosity is expressed as the ratio of volume of voids to
the total volume of rock. Porosity of an aggregate particle refers to the
percentage of the particle that is porous by volume. (Absorption % ×
Specific Gravity = Porosity %)
Provisional These are standards that have been adopted on a temporary basis for a cer-
standard tain period. Provisional standards may or may not become a full standard.
p-value In statistical analysis and testing, the p-value or probability value is the
probability for a given statistical model that, when the null hypothesis
is true, the statistical summary (such as the sample mean difference
between two compared groups) would be the same as or of greater mag-
nitude than the actual observed results.
Qualified/Approved Aggregate materials obtained from a specific source such as a quarry
aggregate source that has met the requirements established by an agency for use in a
certain application.
Quality assurance All those planned and systematic actions necessary to provide confi-
dence that a product or facility will perform satisfactorily in service; or
making sure the quality of a product is what it should be.
Quarry byproducts/ Mineral fine materials resulting from different stages in production of
byproduct aggregate aggregates; quarry fines may cover a range of aggregates with maximum
sieve sizes of 0.079 to 0.25 in. (2 to 6.25 mm).
Reclaimed asphalt Removed and/or reprocessed pavement materials containing asphalt
pavement and aggregates.
Recycled aggregate Aggregate source produced by crushing asphalt and/or cement concrete
source to reclaim the aggregate.
Recycled concrete Crushed old concrete particles from sidewalks, pavements, curbing,
aggregate and building slabs. After being compiled, the concrete is processed and
screened, which includes crushing the concrete into smaller pieces.
Rigid pavement Constructed from cement concrete or reinforced concrete slabs.
Soundness Aggregate’s resistance to disintegration by weathering and, in particular,
freeze-thaw cycles.
Statistical t-test A t-test is an analysis of two population means through the use of sta-
tistical examination; a t-test with two samples is commonly used with
small sample sizes and testing the difference between the samples when
the variances of two normal distributions are not known.
Steel furnace slag A byproduct of the steelmaking and steel refining processes. Calcium
oxide and iron oxide are the two major chemical constituents.
Theoretical Theoretical maximum specific gravity is determined by taking a sample
maximum of loose HMA (i.e., not compacted), weighing it, and then determining
specific gravity its volume by calculating the volume of water it displaces. Theoreti-
(Rice method) cal maximum specific gravity is then the sample weight divided by its
volume.
Unbound pavement Layers of a pavement structure consisting of aggregate materials without
layer adding binding agent.
Unsurfaced Gravel or dirt road with no surface material added and constructed
pavement with gravel.
Virgin/natural An aggregate source consists of rock fragments in their natural state
aggregate source that have been subjected to mechanical processing such as crushing,
washing, and sizing.
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Appendices A–D
Appendices A through D are not printed within the report but are available for download from
TRB’s website at www.trb.org by searching for NCHRP Synthesis 524. The appendices include
the following:
Appendix A: Survey Questionnaire
Appendix B: Survey Respondent Information
Appendix C: Compilation of Survey Responses Provided by Agency Respondents
Appendix D: Links to Approved Aggregate Lists and Specifications Published by Agencies
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ISBN 978-0-309-39045-3
9 780309 390453