Code No: R05411001 R05 Set No.

2
IV B.Tech I Semester Examinations,December 2011
ANALYTICAL INSTRUMENTATION
Electronics And Instrumentation Engineering
Time: 3 hours Max Marks: 80
Answer any FIVE Questions
All Questions carry equal marks
?????

1. (a) What instrumentation features do the near Infrared, fundamental infrared and
Far infrared have in common? What differences are there?
(b) Prove that A=2- log %T. where A = absorption coefficient And T = trans-
mission coefficient. [8+8]

2. (a) Describe the constructional details and applications of a proportional counter

with a neat sketch.
(b) Discuss about the dead time of the GM counter.
(c) Write short notes on the Geiger range. [8+4+4]

3. Explain Electrochemical dissolved Oxygen meter. [16]

4. Explain in detail the construction and working principle of single focusing mass
spectrometer. [16]

5. Write short notes on the following in Flame Photometry

(a) Calibration curve method

(b) Standard addition method
(c) Internal standard method
(d) Detectors. [4 × 4]

6. (a) What do you mean by Isothermal operation? Explain

(b) With a neat sketch explain the Katharometer Detector. [4+12]

7. What is the necessity of using an internal standard in spectrometric analysis? De-

scribe one particular system where it is used and show how it helps in analysis of
the sample. [16]

8. Draw and explain Digital pH meters. [16]

?????

1
Code No: R05411001 R05 Set No. 4
IV B.Tech I Semester Examinations,December 2011
ANALYTICAL INSTRUMENTATION
Electronics And Instrumentation Engineering
Time: 3 hours Max Marks: 80
Answer any FIVE Questions
All Questions carry equal marks
?????

1. (a) Describe the constructional details and applications of a proportional counter

with a neat sketch.
(b) Discuss about the dead time of the GM counter.
(c) Write short notes on the Geiger range. [8+4+4]

2. What is the necessity of using an internal standard in spectrometric analysis? De-

scribe one particular system where it is used and show how it helps in analysis of
the sample. [16]

3. (a) What do you mean by Isothermal operation? Explain

(b) With a neat sketch explain the Katharometer Detector. [4+12]

4. Explain in detail the construction and working principle of single focusing mass
spectrometer. [16]

5. Write short notes on the following in Flame Photometry

(a) Calibration curve method

(b) Standard addition method
(c) Internal standard method
(d) Detectors. [4 × 4]

6. Draw and explain Digital pH meters. [16]

7. (a) What instrumentation features do the near Infrared, fundamental infrared and
Far infrared have in common? What differences are there?
(b) Prove that A=2- log %T. where A = absorption coefficient And T = trans-
mission coefficient. [8+8]

8. Explain Electrochemical dissolved Oxygen meter. [16]

?????

2
Code No: R05411001 R05 Set No. 1
IV B.Tech I Semester Examinations,December 2011
ANALYTICAL INSTRUMENTATION
Electronics And Instrumentation Engineering
Time: 3 hours Max Marks: 80
Answer any FIVE Questions
All Questions carry equal marks
?????

1. Explain in detail the construction and working principle of single focusing mass
spectrometer. [16]

2. (a) Describe the constructional details and applications of a proportional counter

with a neat sketch.
(b) Discuss about the dead time of the GM counter.
(c) Write short notes on the Geiger range. [8+4+4]

3. (a) What do you mean by Isothermal operation? Explain

(b) With a neat sketch explain the Katharometer Detector. [4+12]

4. (a) What instrumentation features do the near Infrared, fundamental infrared and
Far infrared have in common? What differences are there?
(b) Prove that A=2- log %T. where A = absorption coefficient And T = trans-
mission coefficient. [8+8]

5. Write short notes on the following in Flame Photometry

(a) Calibration curve method

(b) Standard addition method
(c) Internal standard method
(d) Detectors. [4 × 4]

6. Explain Electrochemical dissolved Oxygen meter. [16]

7. What is the necessity of using an internal standard in spectrometric analysis? De-

scribe one particular system where it is used and show how it helps in analysis of
the sample. [16]

8. Draw and explain Digital pH meters. [16]

?????

3
Code No: R05411001 R05 Set No. 3
IV B.Tech I Semester Examinations,December 2011
ANALYTICAL INSTRUMENTATION
Electronics And Instrumentation Engineering
Time: 3 hours Max Marks: 80
Answer any FIVE Questions
All Questions carry equal marks
?????

1. What is the necessity of using an internal standard in spectrometric analysis? De-

scribe one particular system where it is used and show how it helps in analysis of
the sample. [16]

2. (a) What instrumentation features do the near Infrared, fundamental infrared and
Far infrared have in common? What differences are there?
(b) Prove that A=2- log %T. where A = absorption coefficient And T = trans-
mission coefficient. [8+8]

3. Explain in detail the construction and working principle of single focusing mass
spectrometer. [16]

4. (a) Describe the constructional details and applications of a proportional counter

with a neat sketch.
(b) Discuss about the dead time of the GM counter.
(c) Write short notes on the Geiger range. [8+4+4]

5. Write short notes on the following in Flame Photometry

(a) Calibration curve method

(b) Standard addition method
(c) Internal standard method
(d) Detectors. [4 × 4]

6. (a) What do you mean by Isothermal operation? Explain

(b) With a neat sketch explain the Katharometer Detector. [4+12]

7. Explain Electrochemical dissolved Oxygen meter. [16]

8. Draw and explain Digital pH meters. [16]

?????