ASAP 2020 V3.

00 H Unit 1 Serial #: 550 Page 1

Sample: test-CBV600-GS9AC-1.5 two amm wash

Operator:
Submitter:
File: C:\2020\DATA\GOVIND\GS-0175.SMP

Started: 27/09/2013 3:06:31PM Analysis Adsorptive: N2

Completed: 29/09/2013 9:43:04PM Analysis Bath Temp.: -195.780 °C
Report Time: 05/12/2013 10:56:05AM Thermal Correction: Yes
Sample Mass: 0.0475 g Warm Free Space: 21.9895 cm³ Measured
Cold Free Space: 67.8405 cm³ Equilibration Interval: 30 s
Low Pressure Dose: 3.000 cm³/g STP Automatic Degas: Yes

Notes:

Isotherm Tabular Report

Relative Absolute Quantity Elapsed Time Saturation
Pressure (P/Po) Pressure Adsorbed (h:min) Pressure
(mmHg) (cm³/g STP) (mmHg)

00:54 766.74927
0.000003668 0.00281 3.0601 01:48
0.000002247 0.00172 6.1722 02:32
0.000001744 0.00134 9.2856 03:17
0.000001560 0.00120 12.3999 04:02
0.000001449 0.00111 15.5148 04:48
0.000001385 0.00106 18.6295 05:36
0.000001338 0.00102 21.7457 06:25
0.000001286 0.00098 24.8617 07:15
0.000001249 0.00096 27.9775 08:07
0.000001224 0.00094 31.0933 09:00
0.000001224 0.00094 34.2098 09:55
0.000001224 0.00094 37.3267 10:51
0.000001252 0.00096 40.4420 11:48
0.000001293 0.00099 43.5585 12:46
0.000001337 0.00102 46.6741 13:47
0.000001375 0.00105 49.7893 14:48
0.000001472 0.00113 52.9034 15:52
0.000001587 0.00121 56.0166 16:59
0.000001716 0.00131 59.1294 18:07
0.000001851 0.00141 62.2422 19:20
0.000002010 0.00154 65.3525 20:34
0.000002215 0.00169 68.4608 21:46
0.000002439 0.00186 71.5680 23:04
0.000002745 0.00210 74.6725 24:18
0.000003110 0.00237 77.7754 25:33
0.000003522 0.00269 80.8744 26:48
0.000004003 0.00306 83.9702 28:02
0.000004584 0.00350 87.0632 29:18
0.000005264 0.00402 90.1521 30:30
0.000006050 0.00461 93.2363 31:46
0.000006962 0.00531 96.3142 33:01
0.000008028 0.00612 99.3853 34:15
0.000009283 0.00708 102.4496 35:30
0.000011772 0.00897 105.5702 36:10
0.000013572 0.01034 108.6937 36:49
0.000015619 0.01190 111.8162 37:26
0.000017922 0.01366 114.9389 38:02
0.000020584 0.01568 118.0609 38:39
0.000023697 0.01805 121.1810 39:13
0.000027296 0.02079 124.3007 39:45
0.000031451 0.02395 127.4194 40:15
0.000036268
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 ASAP 2020 V3.00 H Unit 1 Serial #: 550 Page 2

Sample: test-CBV600-GS9AC-1.5 two amm wash

Operator:
Submitter:
File: C:\2020\DATA\GOVIND\GS-0175.SMP

Started: 27/09/2013 3:06:31PM Analysis Adsorptive: N2

Completed: 29/09/2013 9:43:04PM Analysis Bath Temp.: -195.780 °C
Report Time: 05/12/2013 10:56:05AM Thermal Correction: Yes
Sample Mass: 0.0475 g Warm Free Space: 21.9895 cm³ Measured
Cold Free Space: 67.8405 cm³ Equilibration Interval: 30 s
Low Pressure Dose: 3.000 cm³/g STP Automatic Degas: Yes

Notes:

Isotherm Tabular Report

Relative Absolute Quantity Elapsed Time Saturation
Pressure (P/Po) Pressure Adsorbed (h:min) Pressure
(mmHg) (cm³/g STP) (mmHg)

0.000041848 0.03187 133.6529 41:10

0.000048288 0.03677 136.7662 41:37
0.000055799 0.04249 139.8763 42:02
0.000064981 0.04947 142.9839 42:23
0.000075435 0.05743 146.0874 42:45
0.000087534 0.06664 149.1883 43:06
0.000101665 0.07739 152.2839 43:26
0.000118332 0.09007 155.3732 43:44
0.000137773 0.10486 158.4553 44:03
0.000161856 0.12319 161.5298 44:23
0.000188729 0.14363 164.5952 44:40
0.000220761 0.16800 167.6491 44:57
0.000258848 0.19698 170.6882 45:14
0.000304279 0.23154 173.7105 45:29
0.000358607 0.27287 176.7133 45:43
0.000423421 0.32218 179.6916 45:58
0.000500968 0.38117 182.6404 46:12
0.000593477 0.45154 185.5537 46:26
0.000703806 0.53546 188.4259 46:39
0.000835519 0.63564 191.2487 46:51
0.001006698 0.76584 194.2731 47:06
0.001211659 0.92173 197.2383 47:20
0.002147521 1.63356 206.1197 47:39
0.002975957 2.26365 211.0570 47:52
0.004057834 3.08646 215.6862 48:05
0.004911257 3.73548 218.5069 48:15
0.005908365 4.49375 221.2353 48:25
48:27 760.56921
0.007538577 5.73313 224.6478 48:35
0.008957333 6.81089 228.3050 48:52
0.009493493 7.21812 229.0686 48:58
0.009908897 7.53348 229.5965 49:04
0.019198433 14.59516 239.9762 49:10
0.031008544 23.57229 247.4339 49:15
0.044825979 34.07470 252.8923 49:19
0.056974849 43.30746 256.2341 49:24
0.060241321 45.78891 257.0052 49:27
0.071219299 54.13091 259.1313 49:31
0.080344319 61.06455 260.6462 49:34
0.090989563 69.15242 262.1943 49:38
0.101675976 77.27090 263.4971 49:42
0.125945038 95.71069 265.9288 49:46
0.150657756
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 ASAP 2020 V3.00 H Unit 1 Serial #: 550 Page 3

Sample: test-CBV600-GS9AC-1.5 two amm wash

Operator:
Submitter:
File: C:\2020\DATA\GOVIND\GS-0175.SMP

Started: 27/09/2013 3:06:31PM Analysis Adsorptive: N2

Completed: 29/09/2013 9:43:04PM Analysis Bath Temp.: -195.780 °C
Report Time: 05/12/2013 10:56:05AM Thermal Correction: Yes
Sample Mass: 0.0475 g Warm Free Space: 21.9895 cm³ Measured
Cold Free Space: 67.8405 cm³ Equilibration Interval: 30 s
Low Pressure Dose: 3.000 cm³/g STP Automatic Degas: Yes

Notes:

Isotherm Tabular Report

Relative Absolute Quantity Elapsed Time Saturation
Pressure (P/Po) Pressure Adsorbed (h:min) Pressure
(mmHg) (cm³/g STP) (mmHg)

0.176344090 134.00253 269.5269 49:52

0.201779640 153.32439 270.9000 49:56
0.225485165 171.33189 272.0469 49:59
0.250989246 190.70284 273.1525 50:03
0.276890253 210.37593 274.1289 50:06
0.300546821 228.34256 274.9708 50:09
0.326410371 247.98218 275.8263 50:13
0.351503121 267.03458 276.5495 50:17
0.375463904 285.22845 277.2403 50:20
0.401385724 304.90768 277.9270 50:24
0.425439023 323.16931 278.5098 50:27
50:29 759.59778
0.451408272 342.88916 279.0930 50:33
0.476182945 361.70844 279.6554 50:37
0.500844821 380.44196 280.1763 50:40
0.524830403 398.66193 280.7096 50:44
0.550096404 417.85455 281.2237 50:48
0.575722419 437.32056 281.7350 50:51
0.600753874 456.33511 282.2258 50:55
0.625948859 475.47394 282.7126 50:59
0.651191789 494.64923 283.1984 51:03
0.674891997 512.65271 283.6602 51:07
0.701199834 532.63684 284.1149 51:10
0.726044039 551.50940 284.6236 51:14
0.751011599 570.47571 285.1131 51:18
0.775688225 589.22107 285.6312 51:22
0.799867997 607.58887 286.0601 51:25
0.825399675 626.98383 286.6065 51:29
0.850746000 646.23804 287.1212 51:33
0.875928746 665.36804 287.7185 51:37
0.900590921 684.10266 288.4162 51:41
0.925603920 703.10382 289.1733 51:45
0.950492956 722.01086 290.0734 51:49
0.975817978 741.24890 291.1094 51:52
0.990363075 752.29858 291.9922 51:56
0.932273291 708.17407 290.2831 52:03
0.882522182 670.38361 289.2108 52:10
0.831456086 631.59387 288.2282 52:16
0.800845428 608.34265 287.6749 52:23
0.750949501 570.44171 286.8271 52:30
52:32 759.62775
0.700649323 532.23267 285.9349 52:38
0.649732386
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 ASAP 2020 V3.00 H Unit 1 Serial #: 550 Page 4

Sample: test-CBV600-GS9AC-1.5 two amm wash

Operator:
Submitter:
File: C:\2020\DATA\GOVIND\GS-0175.SMP

Started: 27/09/2013 3:06:31PM Analysis Adsorptive: N2

Completed: 29/09/2013 9:43:04PM Analysis Bath Temp.: -195.780 °C
Report Time: 05/12/2013 10:56:05AM Thermal Correction: Yes
Sample Mass: 0.0475 g Warm Free Space: 21.9895 cm³ Measured
Cold Free Space: 67.8405 cm³ Equilibration Interval: 30 s
Low Pressure Dose: 3.000 cm³/g STP Automatic Degas: Yes

Notes:

Isotherm Tabular Report

Relative Absolute Quantity Elapsed Time Saturation
Pressure (P/Po) Pressure Adsorbed (h:min) Pressure
(mmHg) (cm³/g STP) (mmHg)

0.599690850 455.54181 284.1689 52:51

0.550008232 417.80151 283.1889 52:57
0.500054959 379.85562 282.0905 53:03
0.475002412 360.82501 281.2930 53:10
0.449892337 341.75070 280.5440 53:16
0.438421224 333.03693 280.1961 53:22
0.425858814 323.49417 279.8861 53:29
0.413241526 313.90973 279.5656 53:35
0.400596517 304.30423 279.2029 53:42
0.376079456 285.68039 278.5402 53:48
0.351129676 266.72784 277.7940 53:54
0.301039307 228.67781 276.1581 54:01
0.250703976 190.44170 274.1669 54:07
0.199956154 151.89224 271.7015 54:13

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 ASAP 2020 V3.00 H Unit 1 Serial #: 550 Page 5

Sample: test-CBV600-GS9AC-1.5 two amm wash

Operator:
Submitter:
File: C:\2020\DATA\GOVIND\GS-0175.SMP

Started: 27/09/2013 3:06:31PM Analysis Adsorptive: N2

Completed: 29/09/2013 9:43:04PM Analysis Bath Temp.: -195.780 °C
Report Time: 05/12/2013 10:56:05AM Thermal Correction: Yes
Sample Mass: 0.0475 g Warm Free Space: 21.9895 cm³ Measured
Cold Free Space: 67.8405 cm³ Equilibration Interval: 30 s
Low Pressure Dose: 3.000 cm³/g STP Automatic Degas: Yes

Notes:

Isotherm Linear Plot

test-CBV600-GS9AC-1.5 two amm wash - Adsorption
test-CBV600-GS9AC-1.5 two amm wash - Desorption
300

250

200
Quantity Adsorbed (cm³/g STP)

150

100

50

0
0.0 0.1 0.2 0.3 0.4 0.5 0.6 0.7 0.8 0.9 1.0
Relative Pressure (P/Po)

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 ASAP 2020 V3.00 H Unit 1 Serial #: 550 Page 6

Sample: test-CBV600-GS9AC-1.5 two amm wash

Operator:
Submitter:
File: C:\2020\DATA\GOVIND\GS-0175.SMP

Started: 27/09/2013 3:06:31PM Analysis Adsorptive: N2

Completed: 29/09/2013 9:43:04PM Analysis Bath Temp.: -195.780 °C
Report Time: 05/12/2013 10:56:05AM Thermal Correction: Yes
Sample Mass: 0.0475 g Warm Free Space: 21.9895 cm³ Measured
Cold Free Space: 67.8405 cm³ Equilibration Interval: 30 s
Low Pressure Dose: 3.000 cm³/g STP Automatic Degas: Yes

Notes:

Isotherm Log Plot

test-CBV600-GS9AC-1.5 two amm wash - Adsorption
test-CBV600-GS9AC-1.5 two amm wash - Desorption
300

250

200
Quantity Adsorbed (cm³/g STP)

150

100

50

0
-6 -4 -2 0
10 10 10 10
Relative Pressure (P/Po)

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 ASAP 2020 V3.00 H Unit 1 Serial #: 550 Page 7

Sample: test-CBV600-GS9AC-1.5 two amm wash

Operator:
Submitter:
File: C:\2020\DATA\GOVIND\GS-0175.SMP

Started: 27/09/2013 3:06:31PM Analysis Adsorptive: N2

Completed: 29/09/2013 9:43:04PM Analysis Bath Temp.: -195.780 °C
Report Time: 05/12/2013 10:56:05AM Thermal Correction: Yes
Sample Mass: 0.0475 g Warm Free Space: 21.9895 cm³ Measured
Cold Free Space: 67.8405 cm³ Equilibration Interval: 30 s
Low Pressure Dose: 3.000 cm³/g STP Automatic Degas: Yes

Notes:

Horvath-Kawazoe Report
Slit Pore Geometry (Original H-K)
Maximum Pore Volume: 0.407577 cm³/g
at Relative Pressure: 0.101675976
Median Pore Width: 5.841 Å
Relative Pressure Range: 3.668e-06 to 1.017e-01

Diameter of Adsorptive Molecule: 3.000 Å

Diameter of Adsorptive at Zero Interaction Energy: 2.574 Å
Diameter of Sample Atom: 3.040 Å
Diameter of Sample Atom at Zero Interaction Energy: 2.609 Å
Interaction Parameter: 3.49e-43 erg·cm^4

Density Conversion Factor: 0.0015468

Absolute Relative Quantity Pore Width (Å) Cumulative Differential
Pressure Pressure (P/Po) Adsorbed Pore Volume Pore Volume
(mmHg) (cm³/g STP) (cm³/g) (cm³/g·Å)

0.00281 0.000003668 3.0601 5.091 0.0047 0.0009

0.00172 0.000002247 6.1722 4.964 0.0095 -0.0380
0.00134 0.000001744 9.2856 4.901 0.0144 -0.0766
0.00120 0.000001560 12.3999 4.874 0.0192 -0.1789
0.00111 0.000001449 15.5148 4.857 0.0240 -0.2767
0.00106 0.000001385 18.6295 4.846 0.0288 -0.4389
0.00102 0.000001338 21.7457 4.838 0.0336 -0.6113
0.00098 0.000001286 24.8617 4.828 0.0385 -0.5099
0.00096 0.000001249 27.9775 4.821 0.0433 -0.6961
0.00094 0.000001224 31.0933 4.817 0.0481 -1.0218
0.00094 0.000001224 34.2098 4.817 0.0529 0.0000
0.00094 0.000001224 37.3267 4.817 0.0577 0.0000
0.00096 0.000001252 40.4420 4.822 0.0626 0.8762
0.00099 0.000001293 43.5585 4.829 0.0674 0.6738
0.00102 0.000001337 46.6741 4.837 0.0722 0.6004
0.00105 0.000001375 49.7893 4.844 0.0770 0.7460
0.00113 0.000001472 52.9034 4.860 0.0818 0.2909
0.00121 0.000001587 56.0166 4.878 0.0866 0.2650
0.00131 0.000001716 59.1294 4.897 0.0915 0.2599
0.00141 0.000001851 62.2422 4.915 0.0963 0.2615
0.00154 0.000002010 65.3525 4.936 0.1011 0.2326
0.00169 0.000002215 68.4608 4.960 0.1059 0.2009
0.00186 0.000002439 71.5680 4.984 0.1107 0.1976
0.00210 0.000002745 74.6725 5.015 0.1155 0.1575
0.00237 0.000003110 77.7754 5.047 0.1203 0.1490
0.00269 0.000003522 80.8744 5.080 0.1251 0.1446
0.00306 0.000004003 83.9702 5.114 0.1299 0.1404
0.00350 0.000004584 87.0632 5.151 0.1347 0.1295
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 ASAP 2020 V3.00 H Unit 1 Serial #: 550 Page 8

Sample: test-CBV600-GS9AC-1.5 two amm wash

Operator:
Submitter:
File: C:\2020\DATA\GOVIND\GS-0175.SMP

Started: 27/09/2013 3:06:31PM Analysis Adsorptive: N2

Completed: 29/09/2013 9:43:04PM Analysis Bath Temp.: -195.780 °C
Report Time: 05/12/2013 10:56:05AM Thermal Correction: Yes
Sample Mass: 0.0475 g Warm Free Space: 21.9895 cm³ Measured
Cold Free Space: 67.8405 cm³ Equilibration Interval: 30 s
Low Pressure Dose: 3.000 cm³/g STP Automatic Degas: Yes

Notes:

Absolute Relative Quantity Pore Width (Å) Cumulative Differential

Pressure Pressure (P/Po) Adsorbed Pore Volume Pore Volume
(mmHg) (cm³/g STP) (cm³/g) (cm³/g·Å)

0.00461 0.000006050 93.2363 5.229 0.1442 0.1208

0.00531 0.000006962 96.3142 5.270 0.1490 0.1173
0.00612 0.000008028 99.3853 5.312 0.1537 0.1121
0.00708 0.000009283 102.4496 5.356 0.1585 0.1087
0.00897 0.000011772 105.5702 5.430 0.1633 0.0653
0.01034 0.000013572 108.6937 5.476 0.1681 0.1056
0.01190 0.000015619 111.8162 5.522 0.1730 0.1050
0.01366 0.000017922 114.9389 5.567 0.1778 0.1064
0.01568 0.000020584 118.0609 5.614 0.1826 0.1020
0.01805 0.000023697 121.1810 5.664 0.1874 0.0978
0.02079 0.000027296 124.3007 5.714 0.1923 0.0956
0.02395 0.000031451 127.4194 5.766 0.1971 0.0934
0.02762 0.000036268 130.5373 5.819 0.2019 0.0898
0.03187 0.000041848 133.6529 5.874 0.2067 0.0877
0.03677 0.000048288 136.7662 5.930 0.2115 0.0857
0.04249 0.000055799 139.8763 5.989 0.2164 0.0825
0.04947 0.000064981 142.9839 6.052 0.2212 0.0761
0.05743 0.000075435 146.0874 6.116 0.2260 0.0754
0.06664 0.000087534 149.1883 6.181 0.2308 0.0738
0.07739 0.000101665 152.2839 6.249 0.2356 0.0702
0.09007 0.000118332 155.3732 6.319 0.2403 0.0677
0.10486 0.000137773 158.4553 6.392 0.2451 0.0653
0.12319 0.000161856 161.5298 6.472 0.2499 0.0600
0.14363 0.000188729 164.5952 6.551 0.2546 0.0601
0.16800 0.000220761 167.6491 6.633 0.2593 0.0573
0.19698 0.000258848 170.6882 6.720 0.2640 0.0540
0.23154 0.000304279 173.7105 6.812 0.2687 0.0510
0.27287 0.000358607 176.7133 6.909 0.2733 0.0476
0.32218 0.000423421 179.6916 7.011 0.2779 0.0454
0.38117 0.000500968 182.6404 7.118 0.2825 0.0428
0.45154 0.000593477 185.5537 7.229 0.2870 0.0403
0.53546 0.000703806 188.4259 7.348 0.2915 0.0373
0.63564 0.000835519 191.2487 7.472 0.2958 0.0353
0.76584 0.001006698 194.2731 7.613 0.3005 0.0332
0.92173 0.001211659 197.2383 7.761 0.3051 0.0310
1.63356 0.002147521 206.1197 8.269 0.3188 0.0271
2.26365 0.002975957 211.0570 8.601 0.3265 0.0230
3.08646 0.004057834 215.6861 8.950 0.3336 0.0205
3.73548 0.004911257 218.5068 9.186 0.3380 0.0185
4.49375 0.005908365 221.2353 9.430 0.3422 0.0173
5.73313 0.007538577 224.6478 9.778 0.3475 0.0152
6.81089 0.008957333 228.3050 10.044 0.3531 0.0212
7.21812 0.009493493 229.0686 10.139 0.3543 0.0125
7.53348 0.009908897 229.5965 10.210 0.3551
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 ASAP 2020 V3.00 H Unit 1 Serial #: 550 Page 9

Sample: test-CBV600-GS9AC-1.5 two amm wash

Operator:
Submitter:
File: C:\2020\DATA\GOVIND\GS-0175.SMP

Started: 27/09/2013 3:06:31PM Analysis Adsorptive: N2

Completed: 29/09/2013 9:43:04PM Analysis Bath Temp.: -195.780 °C
Report Time: 05/12/2013 10:56:05AM Thermal Correction: Yes
Sample Mass: 0.0475 g Warm Free Space: 21.9895 cm³ Measured
Cold Free Space: 67.8405 cm³ Equilibration Interval: 30 s
Low Pressure Dose: 3.000 cm³/g STP Automatic Degas: Yes

Notes:

Absolute Relative Quantity Pore Width (Å) Cumulative Differential

Pressure Pressure (P/Po) Adsorbed Pore Volume Pore Volume
(mmHg) (cm³/g STP) (cm³/g) (cm³/g·Å)

14.59516 0.019198433 239.9762 11.494 0.3712 0.0125

23.57229 0.031008544 247.4339 12.720 0.3827 0.0094
34.07470 0.044825979 252.8923 13.915 0.3912 0.0071
43.30746 0.056974849 256.2341 14.847 0.3963 0.0055
45.78891 0.060241321 257.0052 15.094 0.3975 0.0048
54.13091 0.071219299 259.1313 15.874 0.4008 0.0042
61.06455 0.080344319 260.6462 16.498 0.4032 0.0038
69.15242 0.090989563 262.1943 17.219 0.4056 0.0033
77.27090 0.101675976 263.4971 17.908 0.4076 0.0029

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 ASAP 2020 V3.00 H Unit 1 Serial #: 550 Page 10

Sample: test-CBV600-GS9AC-1.5 two amm wash

Operator:
Submitter:
File: C:\2020\DATA\GOVIND\GS-0175.SMP

Started: 27/09/2013 3:06:31PM Analysis Adsorptive: N2

Completed: 29/09/2013 9:43:04PM Analysis Bath Temp.: -195.780 °C
Report Time: 05/12/2013 10:56:05AM Thermal Correction: Yes
Sample Mass: 0.0475 g Warm Free Space: 21.9895 cm³ Measured
Cold Free Space: 67.8405 cm³ Equilibration Interval: 30 s
Low Pressure Dose: 3.000 cm³/g STP Automatic Degas: Yes

Notes:

Horvath-Kawazoe Cumulative Pore Volume Plot

Slit Pore Geometry (Original H-K)
test-CBV600-GS9AC-1.5 two amm wash
0.40

0.35

0.30

0.25
Pore Volume (cm³/g)

0.20

0.15

0.10

0.05

0.00
0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18
Pore Width (Å)

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 ASAP 2020 V3.00 H Unit 1 Serial #: 550 Page 11

Sample: test-CBV600-GS9AC-1.5 two amm wash

Operator:
Submitter:
File: C:\2020\DATA\GOVIND\GS-0175.SMP

Started: 27/09/2013 3:06:31PM Analysis Adsorptive: N2

Completed: 29/09/2013 9:43:04PM Analysis Bath Temp.: -195.780 °C
Report Time: 05/12/2013 10:56:05AM Thermal Correction: Yes
Sample Mass: 0.0475 g Warm Free Space: 21.9895 cm³ Measured
Cold Free Space: 67.8405 cm³ Equilibration Interval: 30 s
Low Pressure Dose: 3.000 cm³/g STP Automatic Degas: Yes

Notes:

Horvath-Kawazoe Differential Pore Volume Plot

Slit Pore Geometry (Original H-K)
test-CBV600-GS9AC-1.5 two amm wash

0.8

0.7

0.6
dV/dw (cm³/g·Å)

0.5

0.4

0.3

0.2

0.1

0.0
0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18
Pore Width (Å)

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 ASAP 2020 V3.00 H Unit 1 Serial #: 550 Page 12

Sample: test-CBV600-GS9AC-1.5 two amm wash

Operator:
Submitter:
File: C:\2020\DATA\GOVIND\GS-0175.SMP

Started: 27/09/2013 3:06:31PM Analysis Adsorptive: N2

Completed: 29/09/2013 9:43:04PM Analysis Bath Temp.: -195.780 °C
Report Time: 05/12/2013 10:56:10AM Thermal Correction: Yes
Sample Mass: 0.0475 g Warm Free Space: 21.9895 cm³ Measured
Cold Free Space: 67.8405 cm³ Equilibration Interval: 30 s
Low Pressure Dose: 3.000 cm³/g STP Automatic Degas: Yes

Notes:

Porosity Distribution by NLDFT

Model: N2 @ 77 on Carbon Slit Pores
Method: Non-negative Regularization; No Smoothing

Volume in Pores < 6.41 Å : 0.14877 cm³/g

Total Volume in Pores <= 999.93 Å : 0.40837 cm³/g
Total Area in Pores >= 6.41 Å : 523.985 m²/g

Pore Size Table

Pore Width Cumulative Incremental Cumulative Incremental
(Å) Volume Volume Area Area
(cm³/g) (cm³/g) (m²/g) (m²/g)

6.41 0.06541 0.06541 204.127 204.127

6.77 0.06669 0.00128 207.906 3.778
6.94 0.06911 0.00242 214.864 6.959
7.30 0.07226 0.00315 223.486 8.622
7.66 0.08005 0.00780 243.851 20.364
8.01 0.09248 0.01243 274.866 31.015
8.37 0.10059 0.00811 294.241 19.375
8.73 0.10059 0.00000 294.241 0.000
9.08 0.10059 0.00000 294.241 0.000
9.62 0.10059 0.00000 294.241 0.000
9.98 0.10059 0.00000 294.241 0.000
10.51 0.12517 0.02458 341.002 46.762
10.87 0.13987 0.01470 368.052 27.049
11.40 0.15900 0.01913 401.603 33.551
11.94 0.17763 0.01864 432.829 31.227
12.47 0.17763 0.00000 432.829 0.000
13.01 0.19904 0.02140 465.734 32.905
13.54 0.20708 0.00804 477.608 11.874
14.26 0.21314 0.00607 486.117 8.508
14.79 0.21710 0.00396 491.466 5.349
15.43 0.22048 0.00338 495.844 4.378
16.29 0.22577 0.00529 502.341 6.498
16.86 0.22925 0.00348 506.471 4.129
17.72 0.23189 0.00264 509.446 2.976
18.57 0.23189 0.00000 509.446 0.000
19.43 0.23548 0.00360 513.151 3.705
20.28 0.23637 0.00088 514.023 0.872
21.14 0.23650 0.00013 514.146 0.123
22.00 0.23680 0.00030 514.423 0.277
23.14 0.23775 0.00095 515.243 0.820
23.99 0.23869 0.00094 516.024 0.781
25.14 0.23988 0.00119 516.973 0.949
26.28 0.24088 0.00099 517.729 0.756
27.42 0.24189 0.00102 518.471 0.742
28.85 0.24242 0.00053 518.838 0.367
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 ASAP 2020 V3.00 H Unit 1 Serial #: 550 Page 13

Sample: test-CBV600-GS9AC-1.5 two amm wash

Operator:
Submitter:
File: C:\2020\DATA\GOVIND\GS-0175.SMP

Started: 27/09/2013 3:06:31PM Analysis Adsorptive: N2

Completed: 29/09/2013 9:43:04PM Analysis Bath Temp.: -195.780 °C
Report Time: 05/12/2013 10:56:10AM Thermal Correction: Yes
Sample Mass: 0.0475 g Warm Free Space: 21.9895 cm³ Measured
Cold Free Space: 67.8405 cm³ Equilibration Interval: 30 s
Low Pressure Dose: 3.000 cm³/g STP Automatic Degas: Yes

Notes:

Pore Size Table

Pore Width Cumulative Incremental Cumulative Incremental
(Å) Volume Volume Area Area
(cm³/g) (cm³/g) (m²/g) (m²/g)

29.99 0.24317 0.00075 519.340 0.501

31.41 0.24383 0.00066 519.758 0.419
32.84 0.24450 0.00067 520.165 0.407
34.27 0.24498 0.00048 520.447 0.282
35.98 0.24543 0.00045 520.697 0.250
37.69 0.24575 0.00031 520.863 0.166
39.12 0.24601 0.00027 521.000 0.137
41.12 0.24637 0.00036 521.173 0.173
42.83 0.24686 0.00049 521.401 0.227
44.83 0.24737 0.00051 521.630 0.229
46.82 0.24737 0.00000 521.630 0.000
48.82 0.24807 0.00070 521.916 0.287
51.10 0.24873 0.00066 522.175 0.259
53.39 0.24873 0.00000 522.175 0.000
55.95 0.24934 0.00060 522.391 0.216
58.52 0.24934 0.00000 522.391 0.000
61.09 0.24934 0.00000 522.391 0.000
63.66 0.25021 0.00087 522.665 0.274
66.80 0.25021 0.00000 522.665 0.000
69.65 0.25096 0.00076 522.882 0.217
72.79 0.25096 0.00000 522.882 0.000
76.22 0.25096 0.00000 522.882 0.000
79.64 0.25096 0.00000 522.882 0.000
83.06 0.25187 0.00090 523.100 0.217
86.77 0.25187 0.00000 523.100 0.000
90.77 0.25187 0.00000 523.100 0.000
94.76 0.25187 0.00000 523.100 0.000
99.04 0.25292 0.00106 523.313 0.213
103.61 0.25292 0.00000 523.313 0.000
108.18 0.25292 0.00000 523.313 0.000
113.03 0.25292 0.00000 523.313 0.000
118.16 0.25292 0.00000 523.313 0.000
123.59 0.25292 0.00000 523.313 0.000
129.29 0.25447 0.00155 523.552 0.239
135.00 0.25465 0.00018 523.579 0.027
140.99 0.25491 0.00026 523.616 0.037
147.27 0.25516 0.00024 523.649 0.033
154.12 0.25531 0.00016 523.670 0.021
160.97 0.25555 0.00023 523.699 0.029
168.10 0.25576 0.00021 523.724 0.025
175.81 0.25590 0.00014 523.740 0.016
183.80 0.25613 0.00023 523.764 0.025
192.07by purchasing
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 ASAP 2020 V3.00 H Unit 1 Serial #: 550 Page 14

Sample: test-CBV600-GS9AC-1.5 two amm wash

Operator:
Submitter:
File: C:\2020\DATA\GOVIND\GS-0175.SMP

Started: 27/09/2013 3:06:31PM Analysis Adsorptive: N2

Completed: 29/09/2013 9:43:04PM Analysis Bath Temp.: -195.780 °C
Report Time: 05/12/2013 10:56:10AM Thermal Correction: Yes
Sample Mass: 0.0475 g Warm Free Space: 21.9895 cm³ Measured
Cold Free Space: 67.8405 cm³ Equilibration Interval: 30 s
Low Pressure Dose: 3.000 cm³/g STP Automatic Degas: Yes

Notes:

Pore Size Table

Pore Width Cumulative Incremental Cumulative Incremental
(Å) Volume Volume Area Area
(cm³/g) (cm³/g) (m²/g) (m²/g)

200.63 0.25650 0.00015 523.802 0.015

209.76 0.25671 0.00021 523.822 0.020
219.18 0.25690 0.00019 523.840 0.018
228.88 0.25702 0.00012 523.850 0.010
239.44 0.25712 0.00011 523.859 0.009
250.00 0.25726 0.00014 523.870 0.011
261.41 0.25739 0.00013 523.880 0.010
273.11 0.25748 0.00009 523.887 0.006
285.38 0.25757 0.00009 523.893 0.006
298.23 0.25770 0.00013 523.902 0.009
311.64 0.25783 0.00013 523.910 0.008
325.62 0.25791 0.00008 523.915 0.005
340.46 0.25800 0.00009 523.920 0.005
355.58 0.25814 0.00014 523.928 0.008
371.85 0.25829 0.00014 523.936 0.008
388.40 0.25838 0.00009 523.941 0.005
406.09 0.25848 0.00010 523.946 0.005
424.35 0.25863 0.00015 523.953 0.007
443.19 0.25876 0.00014 523.959 0.006
463.16 0.25885 0.00009 523.963 0.004
483.99 0.25893 0.00008 523.966 0.003
505.97 0.25902 0.00009 523.970 0.004
528.80 0.25910 0.00008 523.972 0.003
552.48 0.25917 0.00007 523.975 0.003
577.31 0.25924 0.00007 523.977 0.002
603.28 0.25927 0.00004 523.979 0.001
630.38 0.25927 0.00000 523.979 0.000
658.92 0.25927 0.00000 523.979 0.000
688.60 0.25927 0.00000 523.979 0.000
719.42 0.25927 0.00000 523.979 0.000
751.95 0.25927 0.00000 523.979 0.000
785.91 0.25927 0.00000 523.979 0.000
821.01 0.25927 0.00000 523.979 0.000
858.10 0.25927 0.00000 523.979 0.000
896.63 0.25927 0.00000 523.979 0.000
937.15 0.25927 0.00000 523.979 0.000
979.38 0.25927 0.00000 523.979 0.000
999.93 0.25961 0.00033 523.985 0.007

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 ASAP 2020 V3.00 H Unit 1 Serial #: 550 Page 15

Sample: test-CBV600-GS9AC-1.5 two amm wash

Operator:
Submitter:
File: C:\2020\DATA\GOVIND\GS-0175.SMP

Started: 27/09/2013 3:06:31PM Analysis Adsorptive: N2

Completed: 29/09/2013 9:43:04PM Analysis Bath Temp.: -195.780 °C
Report Time: 05/12/2013 10:56:10AM Thermal Correction: Yes
Sample Mass: 0.0475 g Warm Free Space: 21.9895 cm³ Measured
Cold Free Space: 67.8405 cm³ Equilibration Interval: 30 s
Low Pressure Dose: 3.000 cm³/g STP Automatic Degas: Yes

Notes:

Porosity Distribution by NLDFT

Model: N2 @ 77 on Carbon Slit Pores
Method: Non-negative Regularization; No Smoothing

Standard Deviation of Fit: 1.47615, cm³/g STP

Isotherm Table
Relative Experimental Fitted Quantity Absolute Relative
Pressure Quantity Adsorbed Residual Residual
Adsorbed (cm³/g STP) (cm³/g STP)
(cm³/g STP)

0.000003852 62.6006 62.9559 -0.3553 -0.005675

0.000004815 88.1316 88.2590 -0.1274 -0.001445
0.000006019 93.1235 93.3118 -0.1883 -0.002022
0.000007523 97.9775 98.0139 -0.0364 -0.000371
0.000009404 102.6670 102.6282 0.0388 0.000378
0.000011755 105.5417 105.5563 -0.0145 -0.000138
0.000014694 110.4428 111.5807 -1.1379 -0.010303
0.000018367 115.4949 114.3245 1.1704 0.010134
0.000022959 120.4854 121.4045 -0.9191 -0.007628
0.000028699 125.4029 124.2488 1.1542 0.009204
0.000035873 130.3003 129.3403 0.9600 0.007368
0.000044842 135.1541 132.2538 2.9003 0.021459
0.000056052 139.9687 135.2421 4.7266 0.033769
0.000070065 144.5398 138.6378 5.9020 0.040833
0.000087581 149.1994 143.8739 5.3255 0.035694
0.000109476 153.7901 153.0133 0.7768 0.005051
0.000136846 158.3261 162.3328 -4.0067 -0.025307
0.000171057 162.6179 169.2784 -6.6606 -0.040958
0.000213821 167.0379 173.9153 -6.8773 -0.041172
0.000267276 171.2884 177.5758 -6.2874 -0.036706
0.000334096 175.4271 180.7282 -5.3011 -0.030218
0.000417619 179.4492 183.5554 -4.1062 -0.022882
0.000522024 183.3489 186.1556 -2.8068 -0.015308
0.000652530 187.1598 188.5931 -1.4332 -0.007658
0.000815663 190.8597 190.9189 -0.0592 -0.000310
0.001019580 194.4819 193.1873 1.2946 0.006657
0.001274470 197.9875 195.4883 2.4992 0.012623
0.001593090 201.4506 200.4239 1.0267 0.005097
0.001991360 204.9805 205.6083 -0.6279 -0.003063
0.002489210 208.3704 208.4860 -0.1157 -0.000555
0.003111510 211.6855 210.8387 0.8468 0.004000
0.003889380 215.0608 215.9045 -0.8437 -0.003923
0.004861730 218.3589 218.2879 0.0710 0.000325
0.006077160 221.6260 220.4255 1.2005 0.005417
0.007596450 224.7824 225.0827 -0.3003 -0.001336
0.009495570 229.0713 227.3504 1.7209 0.007512
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 ASAP 2020 V3.00 H Unit 1 Serial #: 550 Page 16

Sample: test-CBV600-GS9AC-1.5 two amm wash

Operator:
Submitter:
File: C:\2020\DATA\GOVIND\GS-0175.SMP

Started: 27/09/2013 3:06:31PM Analysis Adsorptive: N2

Completed: 29/09/2013 9:43:04PM Analysis Bath Temp.: -195.780 °C
Report Time: 05/12/2013 10:56:10AM Thermal Correction: Yes
Sample Mass: 0.0475 g Warm Free Space: 21.9895 cm³ Measured
Cold Free Space: 67.8405 cm³ Equilibration Interval: 30 s
Low Pressure Dose: 3.000 cm³/g STP Automatic Degas: Yes

Notes:

Isotherm Table
Relative Experimental Fitted Quantity Absolute Relative
Pressure Quantity Adsorbed Residual Residual
Adsorbed (cm³/g STP) (cm³/g STP)
(cm³/g STP)

0.011869500 231.9921 229.3533 2.6388 0.011374

0.014836800 235.4643 235.4493 0.0150 0.000064
0.018546000 239.3601 238.0003 1.3598 0.005681
0.023182500 243.1763 242.3870 0.7893 0.003246
0.028978200 246.5010 246.2805 0.2205 0.000895
0.036222700 249.7145 249.4135 0.3010 0.001206
0.045278400 253.0243 252.2596 0.7647 0.003022
0.056598000 256.1408 255.6863 0.4545 0.001774
0.070747500 259.0484 258.7021 0.3462 0.001337
0.088434400 261.8440 261.4625 0.3816 0.001457
0.110543000 264.4481 264.4908 -0.0427 -0.000161
0.116070000 265.0074 264.9013 0.1060 0.000400
0.121874000 265.5621 265.3223 0.2397 0.000903
0.127967000 266.1049 266.0481 0.0567 0.000213
0.134366000 266.6452 266.5124 0.1328 0.000498
0.141084000 267.1814 267.0879 0.0935 0.000350
0.148138000 267.7053 267.6857 0.0196 0.000073
0.155545000 268.2158 268.2367 -0.0209 -0.000078
0.163322000 268.7318 268.7958 -0.0641 -0.000238
0.171488000 269.2428 269.2332 0.0097 0.000036
0.180063000 269.7368 269.6509 0.0859 0.000318
0.189066000 270.2342 270.0550 0.1793 0.000663
0.198519000 270.7342 270.7100 0.0243 0.000090
0.208445000 271.2323 271.0949 0.1374 0.000507
0.218867000 271.7378 271.7466 -0.0088 -0.000032
0.229811000 272.2444 272.1193 0.1251 0.000459
0.241301000 272.7531 272.8451 -0.0919 -0.000337
0.253366000 273.2457 273.2093 0.0364 0.000133
0.266035000 273.7294 273.5710 0.1584 0.000579
0.279337000 274.2174 274.2294 -0.0119 -0.000044
0.293303000 274.7169 274.5858 0.1311 0.000477
0.307969000 275.2291 275.2618 -0.0327 -0.000119
0.323367000 275.7362 275.6137 0.1224 0.000444
0.339535000 276.2046 276.1370 0.0676 0.000245
0.356512000 276.6939 276.7363 -0.0424 -0.000153
0.374338000 277.2078 277.0850 0.1228 0.000443
0.393055000 277.7155 277.6603 0.0552 0.000199
0.412707000 278.2090 278.2442 -0.0352 -0.000127
0.433343000 278.6878 278.5948 0.0930 0.000334
0.455010000 279.1746 279.1221 0.0525 0.000188
0.477760000 279.6904 279.6497 0.0407 0.000145
0.501648000
Create PDF files without this 280.1938
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 ASAP 2020 V3.00 H Unit 1 Serial #: 550 Page 17

Sample: test-CBV600-GS9AC-1.5 two amm wash

Operator:
Submitter:
File: C:\2020\DATA\GOVIND\GS-0175.SMP

Started: 27/09/2013 3:06:31PM Analysis Adsorptive: N2

Completed: 29/09/2013 9:43:04PM Analysis Bath Temp.: -195.780 °C
Report Time: 05/12/2013 10:56:10AM Thermal Correction: Yes
Sample Mass: 0.0475 g Warm Free Space: 21.9895 cm³ Measured
Cold Free Space: 67.8405 cm³ Equilibration Interval: 30 s
Low Pressure Dose: 3.000 cm³/g STP Automatic Degas: Yes

Notes:

Isotherm Table
Relative Experimental Fitted Quantity Absolute Relative
Pressure Quantity Adsorbed Residual Residual
Adsorbed (cm³/g STP) (cm³/g STP)
(cm³/g STP)

0.526731000 280.7491 280.7046 0.0445 0.000159

0.553067000 281.2832 281.2502 0.0330 0.000117
0.580721000 281.8337 281.7993 0.0344 0.000122
0.609757000 282.4001 282.3451 0.0550 0.000195
0.640244000 282.9878 282.9624 0.0254 0.000090
0.672257000 283.6091 283.5652 0.0439 0.000155
0.705870000 284.2081 284.1583 0.0498 0.000175
0.741163000 284.9196 284.8912 0.0284 0.000100
0.778221000 285.6803 285.6351 0.0452 0.000158
0.817132000 286.4300 286.3970 0.0330 0.000115
0.857989000 287.2786 287.2439 0.0347 0.000121
0.899898000 288.3959 288.3914 0.0046 0.000016
0.903995000 288.5157 288.5112 0.0045 0.000016
0.907932000 288.6316 288.6702 -0.0386 -0.000134
0.911716000 288.7443 288.7016 0.0427 0.000148
0.915352000 288.8540 288.8502 0.0038 0.000013
0.918845000 288.9610 288.9573 0.0037 0.000013
0.922200000 289.0654 289.1003 -0.0349 -0.000121
0.925422000 289.1675 289.1292 0.0383 0.000132
0.928516000 289.2689 289.2658 0.0031 0.000011
0.931486000 289.3706 289.3676 0.0030 0.000010
0.934337000 289.4717 289.5085 -0.0368 -0.000127
0.937074000 289.5712 289.5315 0.0397 0.000137
0.939700000 289.6683 289.6657 0.0026 0.000009
0.942221000 289.7626 289.7602 0.0025 0.000009
0.944638000 289.8536 289.8869 -0.0333 -0.000115
0.946958000 289.9410 289.9053 0.0357 0.000123
0.949183000 290.0245 290.0223 0.0022 0.000008
0.951317000 290.1038 290.1018 0.0020 0.000007
0.953364000 290.1769 290.1750 0.0019 0.000006
0.955327000 290.2448 290.2672 -0.0224 -0.000077
0.957209000 290.3090 290.2847 0.0243 0.000084
0.959013000 290.3706 290.3689 0.0017 0.000006
0.960743000 290.4306 290.4290 0.0016 0.000006
0.962401000 290.4896 290.4881 0.0015 0.000005
0.963991000 290.5483 290.5710 -0.0227 -0.000078
0.965514000 290.6071 290.5829 0.0242 0.000083
0.966974000 290.6661 290.6648 0.0014 0.000005
0.968374000 290.7258 290.7245 0.0013 0.000004
0.969715000 290.7861 290.7849 0.0012 0.000004
0.971000000 290.8470 290.8721 -0.0251 -0.000086
0.972231000
Create PDF files without this 290.9087
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 ASAP 2020 V3.00 H Unit 1 Serial #: 550 Page 18

Sample: test-CBV600-GS9AC-1.5 two amm wash

Operator:
Submitter:
File: C:\2020\DATA\GOVIND\GS-0175.SMP

Started: 27/09/2013 3:06:31PM Analysis Adsorptive: N2

Completed: 29/09/2013 9:43:04PM Analysis Bath Temp.: -195.780 °C
Report Time: 05/12/2013 10:56:10AM Thermal Correction: Yes
Sample Mass: 0.0475 g Warm Free Space: 21.9895 cm³ Measured
Cold Free Space: 67.8405 cm³ Equilibration Interval: 30 s
Low Pressure Dose: 3.000 cm³/g STP Automatic Degas: Yes

Notes:

Isotherm Table
Relative Experimental Fitted Quantity Absolute Relative
Pressure Quantity Adsorbed Residual Residual
Adsorbed (cm³/g STP) (cm³/g STP)
(cm³/g STP)

0.973411000 290.9711 290.9700 0.0011 0.000004

0.974541000 291.0341 291.0331 0.0010 0.000004
0.975624000 291.0976 291.0967 0.0010 0.000003
0.976661000 291.1605 291.1856 -0.0251 -0.000086
0.977655000 291.2209 291.1947 0.0262 0.000090
0.978607000 291.2786 291.2778 0.0009 0.000003
0.979519000 291.3340 291.3332 0.0008 0.000003
0.980392000 291.3870 291.3862 0.0008 0.000003
0.981078510 291.4287 291.4415 -0.0128 -0.000044
0.981624530 291.4618 291.4481 0.0137 0.000047
0.982154930 291.4940 291.4933 0.0007 0.000002
0.982670160 291.5253 291.5370 -0.0117 -0.000040
0.983170640 291.5556 291.5431 0.0126 0.000043
0.983656790 291.5851 291.5845 0.0006 0.000002
0.984129010 291.6138 291.6086 0.0053 0.000018
0.984587690 291.6416 291.7992 -0.1576 -0.000540
0.985033210 291.6687 291.8022 -0.1335 -0.000458
0.985465960 291.6950 291.8057 -0.1107 -0.000380
0.985886280 291.7205 291.8085 -0.0880 -0.000302
0.986294530 291.7452 291.8112 -0.0659 -0.000226
0.986691050 291.7693 291.8138 -0.0445 -0.000152
0.987076170 291.7927 291.8164 -0.0237 -0.000081
0.987450220 291.8154 291.8194 -0.0040 -0.000014
0.987813510 291.8374 291.8218 0.0156 0.000053
0.988166350 291.8589 291.8242 0.0347 0.000119
0.988509030 291.8797 291.8264 0.0532 0.000182
0.988841840 291.8999 291.8286 0.0712 0.000244
0.989165070 291.9195 291.8308 0.0887 0.000304
0.989478980 291.9385 291.8328 0.1057 0.000362
0.989783850 291.9570 291.8355 0.1216 0.000416
0.990079930 291.9750 291.8374 0.1376 0.000471

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 ASAP 2020 V3.00 H Unit 1 Serial #: 550 Page 19

Sample: test-CBV600-GS9AC-1.5 two amm wash

Operator:
Submitter:
File: C:\2020\DATA\GOVIND\GS-0175.SMP

Started: 27/09/2013 3:06:31PM Analysis Adsorptive: N2

Completed: 29/09/2013 9:43:04PM Analysis Bath Temp.: -195.780 °C
Report Time: 05/12/2013 10:56:10AM Thermal Correction: Yes
Sample Mass: 0.0475 g Warm Free Space: 21.9895 cm³ Measured
Cold Free Space: 67.8405 cm³ Equilibration Interval: 30 s
Low Pressure Dose: 3.000 cm³/g STP Automatic Degas: Yes

Notes:

Cumulative Surface Area vs. Pore Width

Cumulative Surface Area

500

450
Cumulative Surface Area (m²/g)

400

350

300

250

200
10 50 100 500 1,000
Pore Width (Angstroms)

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 ASAP 2020 V3.00 H Unit 1 Serial #: 550 Page 20

Sample: test-CBV600-GS9AC-1.5 two amm wash

Operator:
Submitter:
File: C:\2020\DATA\GOVIND\GS-0175.SMP

Started: 27/09/2013 3:06:31PM Analysis Adsorptive: N2

Completed: 29/09/2013 9:43:04PM Analysis Bath Temp.: -195.780 °C
Report Time: 05/12/2013 10:56:10AM Thermal Correction: Yes
Sample Mass: 0.0475 g Warm Free Space: 21.9895 cm³ Measured
Cold Free Space: 67.8405 cm³ Equilibration Interval: 30 s
Low Pressure Dose: 3.000 cm³/g STP Automatic Degas: Yes

Notes:

Incremental Surface Area vs. Pore Width

Incremental Surface Area
200

180

160

140
Incremental Surface Area (m²/g)

120

100

80

60

40

20

0
6.5 7.0 7.5 8.0 8.5 9.0 9.5 10 15 20
Pore Width (Angstroms)

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 ASAP 2020 V3.00 H Unit 1 Serial #: 550 Page 21

Sample: test-CBV600-GS9AC-1.5 two amm wash

Operator:
Submitter:
File: C:\2020\DATA\GOVIND\GS-0175.SMP

Started: 27/09/2013 3:06:31PM Analysis Adsorptive: N2

Completed: 29/09/2013 9:43:04PM Analysis Bath Temp.: -195.780 °C
Report Time: 05/12/2013 10:56:10AM Thermal Correction: Yes
Sample Mass: 0.0475 g Warm Free Space: 21.9895 cm³ Measured
Cold Free Space: 67.8405 cm³ Equilibration Interval: 30 s
Low Pressure Dose: 3.000 cm³/g STP Automatic Degas: Yes

Notes:

Differential Surface Area vs. Pore Width

Differential Surface Area

8,000

7,000

6,000
Differential Surface Area (m²/g)

5,000

4,000

3,000

2,000

1,000

0
6.5 7.0 7.5 8.0 8.5 9.0 9.5 10 15 20
Pore Width (Angstroms)

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 ASAP 2020 V3.00 H Unit 1 Serial #: 550 Page 22

Sample: test-CBV600-GS9AC-1.5 two amm wash

Operator:
Submitter:
File: C:\2020\DATA\GOVIND\GS-0175.SMP

Started: 27/09/2013 3:06:31PM Analysis Adsorptive: N2

Completed: 29/09/2013 9:43:04PM Analysis Bath Temp.: -195.780 °C
Report Time: 05/12/2013 10:56:10AM Thermal Correction: Yes
Sample Mass: 0.0475 g Warm Free Space: 21.9895 cm³ Measured
Cold Free Space: 67.8405 cm³ Equilibration Interval: 30 s
Low Pressure Dose: 3.000 cm³/g STP Automatic Degas: Yes

Notes:

Cumulative Pore Volume vs. Pore Width

Cumulative Pore Volume
0.26

0.24

0.22

0.20
Cumulative Pore Volume (cm³/g)

0.18

0.16

0.14

0.12

0.10

0.08

10 50 100 500 1,000

Pore Width (Angstroms)

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 ASAP 2020 V3.00 H Unit 1 Serial #: 550 Page 23

Sample: test-CBV600-GS9AC-1.5 two amm wash

Operator:
Submitter:
File: C:\2020\DATA\GOVIND\GS-0175.SMP

Started: 27/09/2013 3:06:31PM Analysis Adsorptive: N2

Completed: 29/09/2013 9:43:04PM Analysis Bath Temp.: -195.780 °C
Report Time: 05/12/2013 10:56:10AM Thermal Correction: Yes
Sample Mass: 0.0475 g Warm Free Space: 21.9895 cm³ Measured
Cold Free Space: 67.8405 cm³ Equilibration Interval: 30 s
Low Pressure Dose: 3.000 cm³/g STP Automatic Degas: Yes

Notes:

Incremental Pore Volume vs. Pore Width

Incremental Pore Volume

0.06

0.05
Incremental Pore Volume (cm³/g)

0.04

0.03

0.02

0.01

0.00
6.5 7.0 7.5 8.0 8.5 9.0 9.5 10 15 20
Pore Width (Angstroms)

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 ASAP 2020 V3.00 H Unit 1 Serial #: 550 Page 24

Sample: test-CBV600-GS9AC-1.5 two amm wash

Operator:
Submitter:
File: C:\2020\DATA\GOVIND\GS-0175.SMP

Started: 27/09/2013 3:06:31PM Analysis Adsorptive: N2

Completed: 29/09/2013 9:43:04PM Analysis Bath Temp.: -195.780 °C
Report Time: 05/12/2013 10:56:10AM Thermal Correction: Yes
Sample Mass: 0.0475 g Warm Free Space: 21.9895 cm³ Measured
Cold Free Space: 67.8405 cm³ Equilibration Interval: 30 s
Low Pressure Dose: 3.000 cm³/g STP Automatic Degas: Yes

Notes:

Differential Pore Volume vs. Pore Width

Differential Pore Volume

2.5

2.0
Differential Pore Volume (cm³/g)

1.5

1.0

0.5

0.0
10 50 100 500 1,000
Pore Width (Angstroms)

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 ASAP 2020 V3.00 H Unit 1 Serial #: 550 Page 25

Sample: test-CBV600-GS9AC-1.5 two amm wash

Operator:
Submitter:
File: C:\2020\DATA\GOVIND\GS-0175.SMP

Started: 27/09/2013 3:06:31PM Analysis Adsorptive: N2

Completed: 29/09/2013 9:43:04PM Analysis Bath Temp.: -195.780 °C
Report Time: 05/12/2013 10:56:10AM Thermal Correction: Yes
Sample Mass: 0.0475 g Warm Free Space: 21.9895 cm³ Measured
Cold Free Space: 67.8405 cm³ Equilibration Interval: 30 s
Low Pressure Dose: 3.000 cm³/g STP Automatic Degas: Yes

Notes:

Goodness of Fit
300

250

200
Quantity Adsorbed (cm³/g STP)

150

100

50

0
-6 -4 -2 0
10 10 10 10
Relative Pressure (P/Po)

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 ASAP 2020 V3.00 H Unit 1 Serial #: 550 Page 26

Sample: test-CBV600-GS9AC-1.5 two amm wash

Operator:
Submitter:
File: C:\2020\DATA\GOVIND\GS-0175.SMP

Started: 27/09/2013 3:06:31PM Analysis Adsorptive: N2

Completed: 29/09/2013 9:43:04PM Analysis Bath Temp.: -195.780 °C
Report Time: 05/12/2013 10:56:10AM Thermal Correction: Yes
Sample Mass: 0.0475 g Warm Free Space: 21.9895 cm³ Measured
Cold Free Space: 67.8405 cm³ Equilibration Interval: 30 s
Low Pressure Dose: 3.000 cm³/g STP Automatic Degas: Yes

Notes:

Goodness of Fit
300

250

200
Quantity Adsorbed (cm³/g STP)

150

100

50

0
0.0 0.1 0.2 0.3 0.4 0.5 0.6 0.7 0.8 0.9 1.0
Relative Pressure (P/Po)

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 ASAP 2020 V3.00 H Unit 1 Serial #: 550 Page 27

Sample: test-CBV600-GS9AC-1.5 two amm wash

Operator:
Submitter:
File: C:\2020\DATA\GOVIND\GS-0175.SMP

Started: 27/09/2013 3:06:31PM Analysis Adsorptive: N2

Completed: 29/09/2013 9:43:04PM Analysis Bath Temp.: -195.780 °C
Report Time: 05/12/2013 10:56:10AM Thermal Correction: Yes
Sample Mass: 0.0475 g Warm Free Space: 21.9895 cm³ Measured
Cold Free Space: 67.8405 cm³ Equilibration Interval: 30 s
Low Pressure Dose: 3.000 cm³/g STP Automatic Degas: Yes

Notes:

Options Report

Sample Tube
Warm freespace: 1.0000 cm³
Cold freespace: 1.0000 cm³
Non-ideality factor: 0.0000570
Use Isothermal Jacket: Yes
Use Filler Rod: No
Vacuum seal type: Seal Frit
Analysis Conditions
Preparation
Fast evacuation: Yes
Vacuum setpoint: 10 µmHg
Evacuation time: 0.10 h
Leak test: No
Use TransSeal: No
Free Space
Free-space type: Measured
Lower dewar for evacuation: Yes
Evacuation time: 0.10 h
Outgas test: No
Po and Temperature
Po and T type: Measure Po at intervals during analysis. Calculate the
Analysis Bath Temperature from these values.
Measurement interval: 120 min

Dosing
Use first pressure fixed dose: No
Use maximum volume increment: No
Target tolerance: 5.0% or 5.000 mmHg
Low pressure dosing: Yes
Dose amount: 3.0000 cm³/g STP
Minimum equilibration delay: 0.00 h
Maximum equilibration delay: 999.00 h
Equilibration
Equilibration time (P/Po = 0.010000000): 30 s
Equilibration time (P/Po = 0.990000000): 15 s
Equilibration time (P/Po = 0.100000000): 30 s
Minimum equilibration delay at P/Po >= 0.995: 600 s
Sample Backfill
Backfill at start of analysis: No
Backfill at end of analysis: Yes
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 ASAP 2020 V3.00 H Unit 1 Serial #: 550 Page 28

Sample: test-CBV600-GS9AC-1.5 two amm wash

Operator:
Submitter:
File: C:\2020\DATA\GOVIND\GS-0175.SMP

Started: 27/09/2013 3:06:31PM Analysis Adsorptive: N2

Completed: 29/09/2013 9:43:04PM Analysis Bath Temp.: -195.780 °C
Report Time: 05/12/2013 10:56:10AM Thermal Correction: Yes
Sample Mass: 0.0475 g Warm Free Space: 21.9895 cm³ Measured
Cold Free Space: 67.8405 cm³ Equilibration Interval: 30 s
Low Pressure Dose: 3.000 cm³/g STP Automatic Degas: Yes

Notes:

Adsorptive Properties
Adsorptive: Nitrogen
Maximum manifold pressure: 925.00 mmHg
Non-ideality factor: 0.0000580
Density conversion factor: 0.0015468
Therm. tran. hard-sphere diameter: 3.860 Å
Molecular cross-sectional area: 0.162 nm²
Inside diameter of sample tube: 9.53 mm

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