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BP10 (A4) PDF
BP10 (A4) PDF
T
HE Gaseous Diffusion Coefficient Apparatus (Model : BP 10) has been designed to allow measurement of
molecular diffusivities to familiarize students with the basic notions of mass transfer theory. The gaseous
diffusivity apparatus involves diffusion with bulk flow.
♦ direct measurement of mass transfer rates in the The diffusion of vapour A from a volatile liquid into another
absence of convective effects gas B can be conveniently studied by confining a small
♦ use of gas laws to calculate concentration differences sample of the liquid in a narrow vertical tube, and
in terms of partial pressures observing its rate of evaporation into a stream of gas B
♦ use of Fick’s Law to measure diffusion coefficients passed across the top of the tube. Normally, for simple
in the presence of a stationary gas instructional purposes, gas B is air and liquid A is an
♦ measurement of the effect of temperature on diffusion organic solvent such as acetone or methyl alcohol.
coefficients
♦ gaining familiarity with the use of laboratory The apparatus consists of a glass capillary tube placed
instruments to achieve accurate measurements of in a transparent thermostatic bath. A horizontal glass tube
data required for industrial process design is fixed to the upper end of the capillary tube and air is
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drawn through this by a small air pump included within c) a travelling microscope
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the unit. This arrangement allows the maintenance of a d)a water bath (thermostatically controlled)
partial pressure difference within the capillary tube e)an experimental manual
between the evaporating liquid surface and the flowing
air stream. A travelling microscope, with sliding vernier Thermostatic bath : capacity 8.0 litres
scale is mounted on a rigid stand alongside the Water heater element : 500 Watts
thermostatic tank and is used to measure the rate of fall Temperature controller : 0 to 100oC, ON/
of the solvent/air meniscus within the capillary. OFF type
Temperature sensor : resistance bulb
The relation between the measured molar mass transfer Vernier range : 0 to 150 x 0.10 resolution
rate (NA, per unit area), the partial pressure gradient and (mm)
the diffusion coefficient D is deduced from the one
dimensional steady state version of Fick’s Law with bulk
flow : REQUIREMENTS
[CA] dy
OVERALL DIMENSIONS
where CA and CB are the molar concentrations of the
vapour A and air B respectively. Height : 0.40 m
Width : 0.45 m
Depth : 0.40 m
SPECIFICATIONS
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Graph of (L-L0) vs. t/(L-L0)
1.400
1.200
1.000
t/(L-L0)
0.800
y = 0.0353x + 0.2886
0.600
0.400
0.200
0.000
0.000 5.000 10.000 15.000 20.000 25.000 30.000
L-L0
1.200
1.000
t/(L - L0) [ks/mm]
0.800
0.600
0.400
0.200
0.000
0.000 5.000 10.000 15.000 20.000 25.000 30.000
(L - L0) [mm]
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