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    Chromatogram BDE 047S

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    Fabricio Amorim
    1) The document reports on the analysis of a sample containing 2,2,3,3-tetrabromodiphenyl ether in isooctane using gas chromatography-mass spectrometry (GCMS). 2) A peak was observed at 13.900 minutes, which corresponds to 2,2',4,4'-tetrabromodiphenyl ether. 3) The sample was run with an oven program of 80C, increasing to 340C at 17C/min and holding for 8 minutes using a DB-5MS column.

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    Chromatogram BDE 047S

    Uploaded by

    Fabricio Amorim
    22 views1 page
    1) The document reports on the analysis of a sample containing 2,2,3,3-tetrabromodiphenyl ether in isooctane using gas chromatography-mass spectrometry (GCMS). 2) A peak was observed at 13.900 minutes, which corresponds to 2,2',4,4'-tetrabromodiphenyl ether. 3) The sample was run with an oven program of 80C, increasing to 340C at 17C/min and holding for 8 minutes using a DB-5MS column.

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    Chromatogram-BDE-047S

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    1) The document reports on the analysis of a sample containing 2,2,3,3-tetrabromodiphenyl ether in isooctane using gas chromatography-mass spectrometry (GCMS). 2) A peak was observed at 13.900 minutes, which corresponds to 2,2',4,4'-tetrabromodiphenyl ether. 3) The sample was run with an oven program of 80C, increasing to 340C at 17C/min and holding for 8 minutes using a DB-5MS column.

    Copyright:

    © All Rights Reserved
    Download as PDF, TXT or read online from Scribd
    Flag for inappropriate content
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    22 views1 page

    Chromatogram BDE 047S

    Uploaded by

    Fabricio Amorim
    1) The document reports on the analysis of a sample containing 2,2,3,3-tetrabromodiphenyl ether in isooctane using gas chromatography-mass spectrometry (GCMS). 2) A peak was observed at 13.900 minutes, which corresponds to 2,2',4,4'-tetrabromodiphenyl ether. 3) The sample was run with an oven program of 80C, increasing to 340C at 17C/min and holding for 8 minutes using a DB-5MS column.

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    © All Rights Reserved
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    of 1

    File :B:\QC Data\GCMS-06 Minimal\DATA\071819\10-.

    D
    Operator : ZA
    Acquired : 18 Jul 2019 17:51 using AcqMethod CHICK_2019.M
    Instrument : GCMS 6 Column: DB-5MS, 30m, 0.25 ID, 0.25 um
    Sample Name: BDE-047S Oven Program: 80c, 17c/min to 340c, 8min
    Misc Info : 2,2,3,3-TETRABROMODIPHENYL ETHER IN ISOOCTANE GC Parameters: Cons. Split, 12psi constant flow
    Vial Number: 56 Split 20:1, 1uL inj.; GC/MS; INJ 270c

    Abundance TIC: 10-D\data.ms

    600000

    2,2',4,4'-Tetrabromodiphenyl ether
    500000

    13.900
    400000

    300000

    200000

    100000

    Time--> 13.20 13.30 13.40 13.50 13.60 13.70 13.80 13.90 14.00 14.10 14.20 14.30 14.40 14.50 14.60 14.70 14.80 14.90 15.00 15.10 15.20 15.30 15.40
    Abundance Scan 2885 (13.901 min): 10-219071290.D\data.ms
    25000 325.9 485.8

    20000

    63.1

    15000

    10000

    40.0 138.1 162.9 222.8

    5000
    207.0 245.9 405.8
    108.4
    86.9 281.0
    123.9 192.9 296.8 376.8
    176.8 266.8 354.9 428.7
    0
    m/z--> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 220 230 240 250 260 270 280 290 300 310 320 330 340 350 360 370 380 390 400 410 420 430 440 450 460 470 480 490 500

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