APPENDIX 1: PASS 1 CIP Regime

Pass 1 CIP Regime: Whole Train - 12 Hours

Duration Step
Targets Flows (%) Chemical Sampling
(mins)
Initial Permeate Flush
Permeate Flush Stage 1, < 3000uS/cm based on Target 30 Permeate
Permeate Flush Stage 2, < 3,000uS/cm based on Target 30 Permeate
1% Citric Acid/ 55 gals Sulphonic Acid - Duration = 4 hours
Fill Stage 1 blocks for half hour with New Tank 1
CIP Flow:
30 25-40 Citric/ Sulphonic
0 mins = 25%
15 mins= 40%
Fill Stage 2 blocks for half hour with New Tank 2
CIP Flow:
30 0 mins = 25% 25-40 Citric/ Sulphonic
15 mins= 40%
Drain Stage 1 Blocks during fill
Fill Stage 1 blocks for half hour with New Tank 3
CIP Flow:
30
0 mins = 25%
15 mins= 40%
Fill Stage 2 blocks for half hour with Used Tank 3
CIP Flow:
30
0 mins = 25%
15 mins= 40%
Using New Tank 2, perform block by block rotations every 20
minutes. As follows:
Stage 1 Block 1
Stage 1 Block 2
120 55 Citric/ Sulphonic
Stage 1 Block 3
Stage 1 Block 4
Stage 2 Block 1,2
Stage 2 Block 3,4,5
Permeate flush Stage 1 Blocks
30 based on Target 55
Target: 30 mins
Permeate flush Stage 2 Blocks
30 based on Target 55
Target: 30 mins
1% Citric Acid/ 130gals SMBS - Duration = 3 hours
Fill Stage 1 blocks for half hour with New Tank 1
CIP Flow:
30 25-40 Citric/ SBS
0 mins = 25%
15 mins= 40%
Fill Stage 2 blocks for half hour with New Tank 2
CIP Flow:
30 0 mins = 25% 25-40 Citric/ SBS
15 mins= 40%
Drain Stage 1 Blocks during fill
Using New Tank 3, perform block by block rotations every 20
minutes. As follows:
Stage 1 Block 1
Stage 1 Block 2
120 55 Citric/ SBS
Stage 1 Block 3
Stage 1 Block 4
Stage 2 Block 1,2
Stage 2 Block 3,4,5
Permeate flush Stage 1 Blocks
30 based on Target 55 Permeate
Target: 30 mins
Permeate flush Stage 2 Blocks
30 based on Target 55 Permeate
Target: 30 mins
0.1% HCl - Duration = 1.5 hours
Fill Stage 1 blocks for 45 mins with New Tank 1
CIP Flow:
45 0 mins = 25% 25-40 HCl
30 mins= 40%
45 mins = 55%
Fill Stage 2 blocks for 45 mins with New Tank 2
CIP Flow:
45 0 mins = 25% 25-40 HCl
30 mins= 40%
45 mins = 55%
Leave Soaking during Pass 2 CIP
Permeate flush Stage 1 Blocks
30 < 3000 uS/cm 55 Permeate
Target: Until cond <3,000uS/cm
Permeate flush Stage 2 Blocks
30 < 3000 uS/cm 55 Permeate
Target: Until cond <3,000uS/cm
APPENDIX 2: PASS 2 CIP Regime

DATE ISSUED: 25th August 2020

Duration
Step Targets Flows (%) Chemical Sampling
(mins)
0.5% EDTA + Sulphonic Acid - Total of 4 New Tanks: Duration = 3.5 hours
Conductivity < 2,000 uS/cm
20 Permeate Flush Stage 1 and Stage 2 25 Permeate

30 Fill train with New Tank 1 25 EDTA/Sulphonic

60 Fill train with New Tank 2; ramp up flow to 35% 35 EDTA/Sulphonic

60 Fill train with New Tank 3; ramp up flow to 40% 40 EDTA/Sulphonic

60 Fill train with New Tank 4; ramp up flow to 50% 50 EDTA/Sulphonic

Conductivity = < 2,000 uS/cm
30 Permeate Flush Train 55 Permeate
pH = 7

0.1% HCl - Total of 2 New Tanks: Duration = 3 hours

60 Fill train with New Tank 1 25 HCl

60 Fill train with New Tank 2; ramp up flow to 40% 40 HCl

60 Fill train with New Tank 3; ramp up flow to 50% 50 HCl

Conductivity = < 2,000 uS/cm
20 Permeate Flush Train 55 Permeate
pH = 7
1% Citric Acid + SBS - Total of 2 New Tanks: Duration = 3 hours

60 Fill train with New Tank 1 25 Citric/SBS

60 Fill train with New Tank 2; ramp up flow to 40% 40 Citric/SBS

60 Fill train with New Tank 3; ramp up flow to 50% 50 Citric/SBS

Conductivity = < 2,000 uS/cm
20 Permeate Flush Train 55 Permeate
pH = 7
Sampling
- For Initial Sample on a New Tank, Take sample from tank discharge sample point at the end of the recirculation of the tank contents
- Tank sample from tank dicharge before each switch to the next stage (both during filling and flushing)
- No DOUBLE BATCHES of chemicals to be done - chemicals to be batched 10 bags at a time and monitored to ensure proper mixing