CHAPTER 6
INSPECTION
by
Kenneth B. Tator and Kenneth A, Trimber
An analysis of the reaéons for premature coating
failure — deterioration of a coating system resulting in
rusting, pitting, chemical attack or other deterioration —
ln most cases leads to a finding of either improper surtace
preparation or deficient coating application. While there
may be potentially many other reasons for premature
failure such as poorly written specifications, choice of the
wrong coating or paint for a given environment, coating
misinformation, or a service environment more severe than
originally anticipated, it is estimated that approximately
75% to 80% of all premature coating fallures are caused in
whole or in part by deficient surface preparation andlor
coating application.
IWis said that "a painter covers his mistakes." This is
unquestionably true. Unfortunately, after the surtace has
been coated, it is exceedingly difficult to verity the ade-
quacy of surface preparation ~ especially blast cleaning,
Furthermore, without the use of appropriate instruments:
tion, itis impossibie to determine coating thickness or, in
many instances, even the number of coats applied.
However, during the course of application, these items —
as well as many others that: might affect the ultimate
‘coating quality —- can be readily witnessed and easily
verified. Accordingly, formal coating Inspection, following
established guidelines or procedures, is mandatory on
‘many large projects (such as nuclear power plants) and is,
often a requioment on small, critical applications such
as tank lining coating work, Where the consequence of
falluro Is oxpensive, the coated ste! Is inaccessible after
erection or the magnitude of painting great, formal inspec:
tion can often be justified
It must be recognized that any inspection, even the
‘most casual kind, is an expense. Even during the portorm
ance of the work, fundamental inspection requires time. In-
spection, in its simplest form, occurs when a painter stops
after a certain portion of his work is completed and ox
amines it for adequacy. Has he missed any areas? Are
there any runs or sags? Is the blast cleaning pattern
Uniform and the cleanliness adequate — or in the case of
hand or power tool cleaning, are there any loose mill scale
oF rust deposits remaining? Formal inspection is more
costly. Inspection procedures must be written, and the
quality of work witnessed and documented on a periodic
(often daily) basis. The inspector must have access to the
work area, and be allowed sufficient time to complete his,
inspection work. Often this must be done at the expense of
continuing coating operations — and although other tasks
‘can be done duting the inspection period, the net result is.
183
that the more stringent the Inspection requirements, the
longer it takes to complete the coating work. The direct
costs of inspection must be considered because the in.
spectors are specially hired, trained, and equipped with ex:
ensivo instruments in ordar to verify the quality of the
work. Accordingly, inspection Is often considered as an in
surance against the possibility of a highly expensive
premature coating failure.
The purpose of this chapter is to outline the inspec:
tions required to assure quality coating work. In adition,
paint inspection equipment is described and summarized,
including advantages and disadvantages, calibration and
uso, This chaptor is presented in the chronological order of
the inspection sequence beginning with pre-surface
reparation inspections and continuing through final dry
film thickness and hotiday testing. inspection of the paint
itsoll is covered in the two separate chapters on quality
control
1. THE FUNCTION OF THE COATING
INSPECTOR.
‘Throughout this discussion the term “inspector” shall
be used to indicate an individual or a group of individuals
whose job itis to witness and dacument the coating work
in a formal fashion. Whilo informal inspection may be done
by the painter, the painter's foremen, or other persons
directly involved with the coating work, this type of inspec.
tion shall not be considered In the course of this discus-
sion.
The inspector's purpose is to ensure that the re
quirements of the coating specitication are met, His func:
tion fs analogous to that of a policeman: he enforces the
rules (specification) without exception even if he deems
them to be inadequate. The authorization to deviate from
the specification is the responsibility of the “
usually the specification writer, contract administrator, or
‘engineer in charge of the job. The Inspector certainly may.
venture his opinion and give recommendations to the
engineer, but cannot unilaterally deviate from the
‘specifications at the working level
Besides specification enforcement, a thorough
coatings inspector provides a job documentation in-
‘cluding a commentaty on the type and adequacy of equip:
ment at the jobsita, the rate of work progression, informa-
tion regarding ambient conditions and controls, and
verification that the surface preparation, coating applica
tion ‘coating thickness and curing are as required. This issupplemented with any othor information he deoms of con-
sequence to the quality and progress of the work.
‘The amount and type of inspection will vary according
to the slze of the project and the type of application con-
tract. There are @ number of types of contracts, but for
‘simplicity two general categories, “fixed price” and “cost-
plus" will be addressed.
Inspection under a “tixed price” application contract
may be oriented to ensure that the contractor does not
‘out comers” in order to hurry the job. While an evaluation
of the equipment, work procedures, and sequence, etc. is
Important, the equipment and methods by which the con-
tractor accomplishes the job are essentially at his discre-
tion, provided the requirements of the specifications are
mat. When performing inspection services for a “cost-
plus” application contract, a knowledgeable Inspector
‘must be able to evaluate the contractor's equipment for
adequacy and must be able to assess whether the rate of
progress is reasonable,
ll, SAFETY CONSIDERATIONS.
Safety is paramount on any jb. Coating inspectors
should be aware of basic safety requirements. Although
the inspector 1s not expected to be proficlent in all safety
codes and regulations, common sense should certainly
prevail. fighting, scaffolding, or equipment malfunctions
present safety hazards, the appropriate safety personne!
should be notified. Paint application inherently presents
some dangers because the solvents used are flammable,
and becauise many objects to be pairited are relatively high
of inaccessible. To paint these areas requires elaborate
staging oF the use of spiders or swing scaffolding for ac
cossibility. The knowledgeable inspector will assure
hims@ié of the safety of these appurtenances before he
‘beotrnes involved. Other safety concerns are addressed
‘more specifically in SSPC-PA.3, "A Guide to Satety in Paint
Application” and the chapter on Safety in this volume,
Il, INSPECTION SEQUENCE
aspection often begins with a prejob conference at
Which the ground rules are set. The inspector is responsi
bie for witnessing, verifying, inspecting, and documenting
FIGURE 1
‘SLING PSYCHROMETER — used for measuring wot and dry bull
Aemperatures in order to establish relative humidity and dow
paint, The
‘stablization,
trumont fe spun tn the alr to reach temporatu
184
Figune 2
ELECTRIC PSYCHROMETER — utilizes
‘thermometer bulbs, providing the wet and dry bulb temps
readings.
faa to draw air across
tue
the work at various Inspection points. The following points
will be reviewed along with the appropriate instruments
used for each.
1. PreSurface Preparation Inspection
2, Measurement of Ambiont Conditions
3, Evaluation of Compressor (Air Cleanliness) and
Surface Preparation Equipment
4, Determination of Surface Proparation Cleanliness.
and Profile
Inspection of Application Equipment
Witnessing Coating Mixing
Inspecting Coating Application
|. Determination of Wet Film Thickness
Determination of Dry Film Thickness
410, Evaluating Cleanliness Between Coats
11. Pinhole and Holiday Testing
42, Adhesion Testing
19. Evaluating Cure
IV. PRE-SURFACE PREPARATION
INSPECTION
Prior to the commencement of surtace preparation or
other coating activities, It may be necessary to Inspect to
determine if the work is ready to be prepared and painted.
Heavy deposits of grease, soll, dust, dirt, coment splatter
land other contaminants must be removed. Removal of
such large oll and grease deposits prior to blast cleaning
assures that they are not redeposited onto freshly cleaned
‘surfaces. This removal is accomplished by following the
steps outlined In SSPC-SP 1, “Solvent Cleaning”. This is
particularly important when abrasive recycling, blast
‘cleaning methods are used so that the abrasive itself does
not become contaminated, Such contamination would be
deposited onto any steel subsequently cleaned with the
same abrasive
The specification may require that weld splatter be
‘ground or otherwise removed and that sharp edges be
rounded. Laminations in plate steel, if detected prior to
blast cleaning, should be opened. It deep enough, they
may requira-weld filing, and, If sufficiont deterioration
has occurred to the structure, replacement of someFIGURE 3
DIGITAL PSYCHROMETER — gives Instant readout of dry bulb
and wot bulb temperatures.
Courtesy: Atkins Technical inc.
‘structural members, “fish plating" or other repair may be
necessary. Responsibility for such repair should be
‘specified in procurement documents but is not ordinarily,
considered to be part of the coating contract.
‘As @ prelude to most painting operations, taping,
masking and protection of adjoining surfaces not to be
painted must be accomplished.
Inspection of all of the above is done visually, or by
touch. Except perhaps for a radius gage or inspection
mirtor, no readily accepted instruments and standards
are used (although NACE, ASTM, and SSPC are currently
working on standards in these areas)
If the work Involves maintenance painting, a deter-
mination of the percentage of rusting in an area will bo
helpful. t should be made in accordance with SSPC-Vis 2
"Standard Methods of Evaluating Degree of Rusting on
Painted Steel Surlaces". In addition, the coating type
should be ascertained In ordor to assure compatibility with
subsequently applied coats. Although there is no quick
“foo! proof” field method for determining the type of
coating present on a structure, a chemical test series.
developed by the U.S. Naval Civil Engineering Laboratory
|s available for general fold studies. Alternately, and
perhaps best, Is a test patch application of the new
Coating over the old, two weeks or mora in advance of pro-
duction painting. The test patch is then examined for adhe,
sion, signs of.wrinkling, lifting, or other evidence of incom:
patibility. A more conclusive approach is to send coating
‘samples to laboratories for quick, inexpensive determina
tion of generic type (by Infrared spectroscopic analysis).
V. MEASUREMENT OF AMBIENT
CONDITIONS
While this is not specifically an inspection hold-point,
185
1s implicit that surface preparation and coating work be
done only under sultable ambient conditions of
‘temperature, humidity, and dew point. For most catalyzed
coatings, specific minimum temperatures must be met.
Many zinc-rich coatings require certain minimum
humidities as woll. The Inspector should be cognizant of
weather forecasts, particularly it coating work Is to be
done outdoors.
Other ambient conditions that might affect painting
‘operations should be noted such as potential industcial or
chemical airborne contamination, water spray downwind
from a cooling tower, leaking steam or chemical lines, and
contamination from normal plant or adjacent operations,
Olten, a heater or dehumidifier is used to control am:
bient conditions for painting operations. Ideally, a heater
should be indirect fired so it does not contaminate the sur-
face with producte of combustion. Ventilation, if required,
should provide for sufficient air Hlow and adequate ventila-
tion ofall areas where work is being performed, Most
solvents are heavier than alr; thus, the dangers of explo-
sion and flammability are groatost in low.lying areas. Con-
{tol of airborne contaminants such as dust and abrasive
‘must also be effective in order to prevent contamination.
While much of the above is inspected visually with the
acceptance criteria governed by safety requirements and
‘common sense, the ambient conditions of alr temperature,
relative humidity, and dew point are determined using in-
strumentation. This includes psychrometers (Figures 1, 2,
‘and 3} oF Instruments that give direct read-out recording of
humiaify Figure 4) or dew point. Measurements with these
instruments are taken before the work begins each day
‘and periodically throughout the day. A suggested
‘minimum frequency is every four hours, or sooner if
weather conditions appear to be worsening
The psychrometer consists of two identical tube’ thor:
_mometors, one of which is covered with a wick or sock that
FIGURE 4
RECORDING HYGROMETER — ‘lati humidity and
{temperature are recorded on stip charts to provide permanent
dally or weekly records.i
i
i
{
j
7
|
2
FIGURE 5
US. WEATHER BUREAU TABLES — a book of abies for convert-
ing dry bulb and wet bulb temparatures to relative humidity and
dew point.
‘saturated with water. The covered thermometer is called
the “wet bulb" and the other is the “dry bulb”. The dry bulbs
glves tho ambient air temperature while the wet bulb
temperature results from the latent heat loss of water
evaporation from the wetted sock. The faster the rate of
water evaporation, the lower the humidity and dew point,
‘There are generally two types of psychrometers: the
sling psychrometer, shown in Figure 1, and tho fan of
motor-driven psychrometer, shown in Figura 2.
When using the sting peychromoter, the wet bulb sock
is saturated with water, the instrument whirled rapidly tor
approximately 20 seconds, and a reading of the wet bulb
Quickly taken, The cycle Is repeated (spinaingireading
‘without additional wetting) until the wet bulb temperature
FIGURE 6
SURFACE TEMPERATURE THERMOMETER — for establishing
temperatures of substrates during blast cleaning and painting,
186
stabilizes. Stabilization occurs when three consecutive
readings of the wet bulb remain the same. At this time both
the dry and wet bulb temperatures are recorded.
When using the far-operated psychrometer, the wet
bulb sock is saturated with water and the fan is started,
Approximately two minutes are requiced for stabilization,
‘and one need onty observe the wet bulb thermometer and
record both temperatures when the wet bulb temperature
remains unchanged.
a.
oe
FIGURE 7
DIGITAL THERMOMETER — for direct readout of surtaco
temperature,
‘Courtesy: Atkins Technica, ine.
When the instruments are used in air temperatures
less than 32 degrees Fahrenholt, the accuracy of the
readings is quostionabie. The wet bulb thermometer will
drop below the 32 degrees Fahrenhelt temperatura to a
certain point (e.g. 27 degrees Fahrenheit) then “heat up”
rapidly to the 32 degrees Fahrenheit freezing point. Quite
often when using a sling psychrometer, this will take place
during the whiring of the instrument; therotore, a wet bulb
temperature of 32 degrees Fahronhelt may always be ob-
tained, When using the motor-driven peychrometer, ono
can observe the wet bulb temperature drop below freezing,
then rise rapidly to 32°F, However, the low value may sti
be incorrect. Thus if the temperature Is bolow 32°F, the
ambient conditions. will have to be establiched by other
‘means. This could be accomplished by obtaining the
humidity on a direct. read-out. instrument. using
Sophisticated equipment or even inexpensive humidity in-
dicators available for home use. The ambient temperature
will stil be obtained using a standard thermometer. These
two values can then be used to determine the wet bulb and
dow point temperatures by plotting out this information
“in reverse" on the charts or tables described below.
After the dry bulb and wet bulb temperatures are
determined, a psychometric chart or table is used to
determine the relative humidity and dew point
temperatures of the alr. Charts require plotting the dry
bulb and wet bulb temperatures on different lines and in-
{etpolating the relative humidity and dew point trom their
intersection,
The U.S. Department of Commerce Weather Bureau|
i
i
i
Psychometric Tables (Figure 5) consist of individual
tables for relative humidity and dew point. To use the
table, the wet bulb temperature is subtracted from the dry
bulb temperature and the difference found along the top
row of the table, The dry bulb temperature is found down
the loft column and the intersection of the two is either the
humidity or the dew point, depending upon which table is
used. Other tables, such as the U.S. Department of Com-
‘marce, NOAA-WSTA B.0-E (6-72), “Relative Humidity and
Dew Point Tables”, include the relative humidity and dew
point on the same table,
FIGURE 8
{oft to right) Nozzle Orifice Gage measures nozzle orifice ant
Dow Point Is defined as the temperature at which
moisture will condense. Dew point is important in coating
‘work because moisture condensation on the surface will
‘cause freshly blast cleaned steel to rust, ora thin, often in-
visibla flim of moisture trapped between coats may cause
premature coating failure. Accordingly, the industry has
established an arbitrary dow point/surtace temperature
safety factor. Final biast cleaning and coating application
should not take place untess the surface temperature is at
least five degrees Fahrenholt higher than the dew point.
Although, theoretically, a surface temperature just in-
itesimally above the dew point wil! not permit moisture
condensation, the safety factor of five degrees Fahrenheit
has been established to allow for possible instrument in-
accuracies or different locations whore readings are
taken,
Different field instruments are used for determining
‘surface temperature. One of the most common is a surface
temperature thermometer (Figure 6), which consists of a
bimetallic senging element that is shielded from dratte.
The Instrument includes two magnets on the sensing side
{for attachment o forrous substrates. Two or throe minutes
are required {0+ temperature stabilization of this instru-
‘ment. Other field instruments for determining surface
temperature are direct reading thermocouplelthermisters,
(Figure 7). Those instruments havo a sensing probe
touched to the surface, resulting in a direct temperature
readout. Only a few seconds are required for a temperature
FIGURE 9
SWEDISH STANDARDS — approved by SSPC (VS 1) and ASTM
{2g200, are ener ahoogrphe of structural eee four rust
‘fade conditions prior to. surf jon and again after
fend, power tool, and four egress of blast cleaning.
reading to stabilize.
With any of the Instruments used for determining am-
bient conditions and surtace temperatures, the readings
should be taken at the actual locations of the work. For
general readings, however, one should consider the cold-
est polnt on the structure because a surface
temperaturoldew point relationship problem will occur
there first, Air and surface temperature considerations aro
also important to ensure that coatings are not applied out-
side of their tomperature limitations — In areas too cool or
too warm, Accordinaly, readings for this purpose should
‘be made at the coolest or warmest areas.
Typical requirements for ambient painting conditions:
are givon in SSPC-PA 1
187
FIGURE 10
KEANE-TATOR SURFACE PROFILE COMPARATOR ~ consists
of alighted magnifier and reterence disc for visually comparing
the anchor patter of blast cleaned steel, Reference alscs are
avallable for sand, git, oF shot abrasives.
Courtesy: KTATatorFIGURE 11
Koane-Tator Comparator in use 10 moasure surtace proflo
Courtesy: KTATator
VI. EVALUATION OF SURFACE PREPARATION
EQUIPMENT
The air compressor and other equipment used for
blastcleaning and any hand or power tools should be in-
spected. The inspector need not have an extensive
technical background on the equipment, but should be
familiar enough with it to dotermine its suitability. A brit
summary is provided below, but moro detailed information
's available in the chapters on Surface Preparation in this
volume and in the Commentary on Surface Preparation in
Volume 2,
FIGURE 12
‘TESTEX PRESS.O-FILM TAPE — ueod to make a procise reverse
replica of the suriace profile, whichis. measured with a spring
micrometer.
A. AIR COMPRESSOR AND AIR CLEANLINESS
When gin air compressor is used — for blast cleaning,
power tool cleaning, or the operation of spraying equip.
‘ment ~ the compressor should be appropriately sized and
have a suitable volume to maintain the required’ air
Pressures. Equipment suppliers have charts and data
available which are oxcolont aids for determining required.
sizes of compressors, air and abrasive lines, nozzles, and
so forth.
FIQURE 13,
DIAL SURFACE PROFILE GAGE — a depth micrometer that
‘measures the depth of valleys on the steel eurtace aftor bla:
leaning,
Courtesy: Elcomoter, Ine
The compressed air used for blast cleaning, biow-
down, and spray application should be checked for con-
taminants. Adequate moisture and oll traps should be
‘used on all lines to assure that the air is sufficiently dry
and ollfree so it does not Interfere with the quality of the
work. A simple test for dotormining alr cleanliness re-
uites holding a clean white piece of blotter paper approx.
imately 18 inches from the air supply downstream of
moisture and oil separators. The alr is permitted to blow on
the blotter paper for a fow minutes followed by an inspec
tion for signs of detrimental amounts of moisture or oil
contamination on the blotter. Obviously, if there is no
discoloration on ihe blotter, the quailty of the alr is ex-
Coltent, white streams of moisture and oll running down
the sheet indicate unsatisfactory air.
Unfortunately, the point where good air becomes bad
is difficult to determine. However, by use of tho blotter
Paper (or a clean cloth, handkerchief, or paper), one can
make his own judgments as to the air quality. A thorough
inspection of the surface after blast cleaning for signs of
‘molsture of oil contamination should be made and these
rooults correlated with the results of the blotter test. In ad-
ition, the proper functioning of inline moisture and oi!
‘raps can be evaluated on a comparative basis trom the
results of the blotter test. For work requiring that absolute
'y no moisture or oll be permitted in the compressed air,FIGURE 14.
ZAHN CUP — for moasuring tho viscosity of coatings prior to ap.
plication.
oll4ess compressors and sophisticated alr drying equip ~
ment are available.
B. BLAST CLEANING MACHINE
The blast cleaning machine mixes the abrasive with
the alr stream. The abrasive motering valve regulating the
flow of abrasive Into the air stream Is perhaps ane of the
most overlooked but Important considerations affecting
‘the work rate. Generally, too much abrasive is injected into,
the air stream, resulting in both decreased production and
Increased abrasive costs. The machine should be
‘equipped for “dead man” capability so that it can be shut _
down from the nozzle in the event the nozzlo is dropped. It
‘should also be equipped with moisture and oil separators,
‘or extornal separators should be provided. Since the tank
of the blast cleaning machine is a pressure vessel, it
‘should be constructed according to prossuto vossol codes,
FIGURE 18
WET FILM THICKNESS GAGE — m
sures coating thickness
during application by progressively deeper steps marked in mils.
199
C. ABRASIVE
Thera is a great varlety of abrasives available for blast
cleaning, The size, type, and hardness of the abrasive have
a significant impact on the surface profile and speed of
Cleaning, Steal shot and grit, because they can be recy:
‘led, are most commonly used for rotary wheel blast clean-
ing. Where permitted by law, sand is @ very common
abrasive for most field operations. Various slag abrasives,
‘due to lesser hazards from silica, are also widely used, par-
ticularly in tanks, ship holds and other relatively confined
areas. Sand and slag are disposable abrasives and should
not be reeyeled, wheroas most metallic abrasives, such as
Iron and stee! shot and grit, aluminum oxide, and expen:
sive abrasives such as glass boads can be recycled if
fines, paint, rust and mill scale can be adequately
‘separated {fom the abrasive stream. Metallic and non-
metalilc abrasives are reviewed in detail in other chapters
of this volume,
Ht Is most important that all abrasives be clean and
free of moisture. Abrasives should be stored off the
ground, protected from moisture and the elements. Only
sand of slag that has been wasted at the manufacturing
and packaging plant should be used. The washing should
bbe done using frosh water only; if brackish water is used,
chloride contamination of the cleaned surface can result,
with subsequent rust bloom in humid environments,
Although there is no Inspection apparatus for deter-
mining the cleanliness of the abrasive used, a visual
Inspection must be made to assure that It is not damp or
contaminated. When abrasive recycling systems are used,
a simple tost for the presence of oll or grease contamina
tion should be made. Drop some of the abrasive (e.g. a toa-
‘8p00n full) Into a small vial of water (pill bottle size) and
shake vigorously. Inspect the top of the water for a film of
‘grease or oll which will bo prosont if the abrasive is con-
taminated, Dirt and dust in the abrasive can be assessed
in the came manner. Small abrasive "fines" will be held by
surface tension at the meniscus, and a dirty abrasive will
color the water or cause turbidity. Howevar, water-soluble
contaminants such as salt will not be detected using this
test. If water-soluble contaminants are present, a litmus
paper test of the water in the vial wil tell if they are acid or
alkaline:'If noutral, add a drop of 5% silver nitrate solution
to tho water, The formation of a white precipitate will in-
dicate the presence of chlorides. Alternatively, allow the
water to evaporate and look for salt crystals.
D. FORCED AIR AND ABRASIVE HOSES
‘Sharp constrictions or bends in these lines should be
eliminated, and thoy should be kept as short as possible to
avoid friction and loss of pressure. For the same reason,
Internat couplings should be avoided. For safety purposes,
the couplings should be wired together to assure secure
closure, and the blast hoses should be equipped with
static wire grounding,i
i
INTERCHEMICAL WET FILM THICKNESS GAGE
Courtesy: GilbertiCommonweaith, Inc.
MIKROTEST MAGNETIC PUL
E. BLAST CLEANING NOZZLES AND
NOZZLE PRESSURE
A great variaty of nozzle sizes, types, and lengths are
available for cleaning purposes. The specific nozzle
‘chosen will depend upon the specific cleaning Job. Venturi
type noazies provide a higher abrasive velocity than
straight barrel types of the same orifice size. In general,
the fonger the barrel, the larger the orifice and the faster
the cleaning rate. Cracked nozzles and worn nozzles, even
If not cracked, will reduce the rate of blast cleaning, As a
‘ule of thumb, a nozzie that has been worn beyond 25% of
its original inner diameter (L.) should not be used. A noz:
2le orifice gage (Figure 8) is available from equipment sup-
pliers for determining the orifice size after use. The
‘umber etched on the nozzle housing indicates tho size
when new. Nozzles are designated in sixteonths of an inch.
Therefore a Number 8 nozzle is equivalent to % inch.
The amount of air pressure at the blast nozzle is a
determining factor in cleaning rate production. The op:
timum nozzle pressure Is 90 to 100 psig. The blasting air
pressure should be determined at the nozzle rather than at
the gage on the compressor because thore will be prossure
drops in the system due to hose length, bends, restric-
tions, blast pot, and moisture traps. Air pressure at the
blast nozzle can be determined using a hypodermic needle
air pressure gage (Figure 8). The needle of the gage is in-
Sorted through the blast hose as close to the nozzle as is
Practical. The direction of noodle placement should be
toward the nozzle. Pressure readings are taken with the
‘nozzle in operation (abrasive flowing). At the same time, all
‘other pneumatic equipment using the samo compressor
system must be in operation,
F, ROTARY WHEEL BLAST CLEANING
OFF DRY FILM THICKNESS GAGE
sures the thickness of costings applied — EQUIPMENT.
= non-destructivaly
to ferrous subetrat
ELCOMETER INSPECTOR THI
ame principle as the Mi
thickness measurements,
ICKNESS GAGE — oporetes on tho
ikrotest for nondestructive coating
Courtesy: Elcometer
Many fabricating shops and painting sites are
equipped with rotary wheel blastcleaning equipment in
order to tfectively propare a surface for painting. The
‘umber of wheels diractly affects the arca that can bo
‘cleaned, and the type of structural shapes that can ba
‘cleaned. Adjustments can be made to direct the blast pat-
tezn from each wheel to the desired location in order to.
Provide @ uniform cleaning pattern, The rate of speed
through the machine determines the degree of cleaning;
the slower the material goos through the machine, the:
Greater tho degree of cledning. Detalls are given in the
‘chapter on centrifugal blast cleaning in this volume.
Complex. structural shapes are particularly hard to
‘clean using automated equipment. The interior of box
FIGURE 19
ELCOMETER PENCIL PULLOFF GAGE
= Courtesy: Zormea Corp.
190FIGURE 20
BSA TINSLEY GAGE
Courtosy: James G. Biddle Instruments Co.
gliders, enclosed shapes, and shielded members can not
bo cleaned, unloss cleaning is done prior to fabrication. In
many instances, fabricators will employ handheld blast
cleaning equipment in tandem with the automated equip-
ment to reach the inaccessible areas.
G, OTHER METHODS OF SURFACE
PREPARATION
Methods such as vacuum blast cleaning, water
blasting with or without sand injection, wet blast cleaning,
hand and power tool cleaning will not be discussed hore.
Vil. DETERMINATION OF SURFACE
PREPARATION CLEANLINESS AND PROFILE
A. CLEANLINESS
‘All eurfaces should be inspected after surtace
preparation to assure compliance with the specification.
The SSPC Surface Preparation Specifications describe tho
appearance of various types of surface preparation
methods, percentage of the surface area to be cleaned,
type of residues permitted to remain on the surface, and so
forth, Its important thet this inspection be timely, in ordor
to avoid any rusting of cleaned surfaces prior to priming,
‘The written definitions are supplemented by SSPC-Vis
1, the Swedish Standards, which photographically depict
the surface appearance of hand and power tool cleaning
and varlous grades of blast cleaning over four Initial mill
scale and rust conditions of steel (Figure 9). The standards
are visually compared with the prepared surface to deter
mine the degree of cleanliness. Other visual standards for
surface cleanliness ovaluation include the NACE coupons,
and the SNAME Standards. Agreement on the desired ap:
pearance of a cleaned surface using commercially
ries
FIGURE 21
TINSLEY THICKNESS GAGE
‘Courtesy: Dean Bergor
11
available standards is often difticult to achieve because of
shadows and hues caused by the abrasive used, the pat
torn and dogres of prior rusting and numerous other fac
{ofS unique to each project. As a result, jobsite standards
are often developed to reach agreement. Sections of the
structure (or test panels of a similar nature) are prepared
‘and all parties involved ultimately sotect one of the panels
(f areas that Is representative of the desired end result. A
‘complete listing of available standards is provided in the
‘Commentary on Surface Preparation included in Volume 2.
‘COUNTERREIT.
REFERENCE WARK es
SOME.
Figune 22
INSPECTOR THICKNESS GAGE
(Courtesy: GilbertiCommonweath, Ine.
When a cortain surface preparation method is
spocifiod, the intent is that it be employed over 100% of
the area, not just the readily accessible areas.
Cleanliness after surface proparation is also very im-
portant, Residual traces of abrasive must be blown, swept,
‘9r vacuumed from the surface prior to prime coating. It is
also Important to ensure that dust Is removed from the sur
face prior to painting, particularly the “fine film” of dust
like spent abrasive often held to the blast-cleaned surface
by static olectricity.-Any scaffolding, staging or support
steel above the area to be coated must be blown down and
cleaned to prevent abrasive dropping onto the freshly
cleaned surface, or later contaminating the freshly primed
surface. Concurrent blast cleaning and painting should
‘not be permitted unless the blast cleaning is adequately
Isolated to prevent contamination of the freshly painted
surface,
The surface profile should also be measured or
estimated, Note that the profile or roughnoss of a biast-
cleanad substrate Is different than, but closely related to,
eurface cleanliness.FIGURE 23,
Inside of Mikcotest Gage with componente corresponding with
‘those in Figure 22,
Courtesy: Giibort/Commonwealth
B. PROFILE
‘The profile anchor pattem or roughness Is defined as
the maximum average peak to valley depth (or height)
‘caused by the impact of tho abrasive onto the substrate. A
White Metal Blast can have a 1, 2, 3,.0r 4 mil profilo,
likewise, a Commercial Blast can have a 1, 2, 3, or 4 mil
profile. Specifying a certain blast cleanliness says nothing
of the profile requirement. it must be addressed separate.
yy,
Surface profile is important because It Increases the
Surface area to which the coatings can adhore, and pro-
vides a mechanical anchor, resulting in good adhesion. As
@ general rule, thick coatings require a deeper surface pro-
file than thin coatings.
Profile determinations are generally made in the field
‘F shop using one of three instruments: a surface profile
comparator, @ depth micrometer, or a replica tape.
Magnetic measurements of surface profile have been a
tempted with iitle success. More sophisticated laboratory.
methods include a profilometer and a depth moasuring
microscope. SSPC has developed a standard method of
‘moasuring profile using a microscope. This is included in
the SSPC Study “Surface Profile for’ Anti-Corrosion
Paints.” While all methods are worthy of consideration, on-
|y the tleld/shop instruments will be discussed.
The most common comparator is the Keane-Tator Sur
face Profile Comparator (Figures 10 and 11), which con.
sists of a reference disc and a S:power illuminated magni-
fier. The disc is held magnetically against the magnifier,
through which test surface and disc segments can be
viewod. simultaneously. The reference disc has five
Separate leaves or segmonts, each of which is assigned a
number representative of the profile depth of the particular
leat. Each disc is a high purity nickel electroformed copy
of amaster, The master disc was measured microscopical-
ly by the SSPC to establish the profile depth.
The reference disc Is compared with the surface
through the 5-power magnifier. The leaf or leaves which
‘most closely approximate the roughness of the surface are
considered to be the profile of that surface. For example,
the profile might be 2 mils, or perhaps from 2 to 3 mils If
192
the surface roughness appears to tle botwoen the 2 mil and
3 mill leaves.
There are three surface profile discs available, The
fone to use for measurement depends upon the abrasive,
used. Different types of abrasives may result ina different
profile appearance, although the depths might be iden.
tical, For example, shot is round when compared with the
more angular grit. in order to achieve similar profile
depths, the shot by virtue of its shape will generally result,
in greater lateral distances between peaks than will grit,
rosulting inva lower peak count per given area. The optical
effect provides an illusion that the shot-blast-cleaned sur-
face Is deeper than the grit-blast-cleaned surface even
when they are Identical. Therefore, itis essontial that the
correct comparator disc be selected for the abrasive used.
‘The designations for three discs avallable with the in-
strument are for sand, 8; for metalile grt or steel, GIS; and
for steel shot, SH. The numbering aystem on each leaf con-
sists of a number followed by a letter designation, then
another number. The first number represents the protile
depth of that teat, the letter reprosents the abrasive used,
and the final number represents the year that the master
disc was formed, For example, 1S70 indicates that that
feat was prepared to a 1 mil profile using sand as the
abrasive and that the master dise was formed in 1970. The
year that the master disc was formed Is only significant If
It were to be replaced at a later date.
The Ciemtex Coupons are another type of profile
reference standard similar to the compatator discs. They
are stainless stee! coupons individually blast cleaned and.
‘measured for profile depth. SO is also working on a visual
profile comparator.
Another field instrument useful for determining
average profile depths Is a depth micrometer (Figure 13).
The depth micrometer consists of @ conical pin which pro-
jects out from a large flat base approximately the sizo of a
‘nickel. The instrument Is calibrated on a mirror or plate
lass by turning the entire scale ring so that the “zero”
FIGURE 25
PLASTIC SHINS — for calloating dty film thicknoss gages.FIGURE 25,
NATIONAL BUREAU OF STANDARDS CERTIFIED COATING
THICKNESS CALIBRATION STANDARDS for magnetic pull-oft
‘gage calibration,
lines up with the pointer. Theoretically, when the instru:
‘ment is firmly placed on the blast cleaned substrate, the
base will rast on the tops of the “peaks” and the pin will
project into a valley. By taking a number of readings, an
average profile can be obtained. It 1s Important to pick the
instrument up and place it down for each reading, rather
than drag it across the profile; otherwise, the point will
become blunted, yielding erroneous readings.
Surface profile can also bo determined by using
replica tape (Figure 12). The Testex Press-0-Film Replica
‘Tape consiets of an emulsion film of microscopic bubbles
attached to a uniform, 2 mil film of mylar, The tape is
pressed onto the blast-cleaned surface, emulsion side
down, and the mylar rubbed vigorously with a blunt instru:
ment, such as a awizele stick or burnishing tool. The peaks
of the profile will break the bubbles and ultimately touch,
but not alter, the thickness of the mylar, as the mylar is in
‘compressible. The tape is removed and measured using a
light-weight, springtoaded micrometer, which provides a
reading from the upper or outermost surface of the mylar
to the high spots on the emulsion which were not totally
crushed (corresponding with the valleys of the profile). Tho
total micrometer reading is adjusted for the thickness of
the mylar by subtracting 2 mils from the results to provide
a direct reading of the maximum average profile. The tape
{ig available in “coarse” for profile measurements up 102%
mits and “X-coarse” for measurements from 2% to 4%
mits.
The replica tape will allegedly retain the impression
Indefinitely, provided It is stored in a cool area with no
pressure applied. Concelvably, replicas of profiles could
bbe Kept on file permanently for future reference.
It 1s important that the inspector realize that each of
the above methods has Its drawbacks. For example, the
‘comparator is subjective, and persons using it could be
biased by the results of others. The peaks of the profile
may bo too closo together to pormit tho projecting pin of
the Surface Profile Gage (depth micrometer) to reach the
valleys, or the surface might be irregular or wavy, holding
the base of the instrument slightly above the plane of the
profile, giving erroneously high readings. The replica tape
cannot be used for profiles exceeding 4¥4 mits, orf there
is any dirt or dust contamination on the surface, Such con:
tamination wiil be picked up and incorrectly read as add
tional profile depth by the micrometer. Finally, itis impor.
tant to realize that there may not be exact correlation
‘among each of the above methods because each takes in a
different peak count or surface aroa for its measurement.
Therefore, itis advisable that all parties concerned agree
‘on the instrument that will be used to determine the sur
face profile and not deviate from it. Because of the con:
troversy in agreement in surface profile measuring
methods, equipment or technique, manufacturers will oc:
‘casionally supply a profile reference coupon represen-
tative of the roughness necessary for thelr product or alter
natively specify the uso of a spocific instrumont. The SSPC.
‘has prepared a report on profile, tts origin, measurement,
control and effect on coating performance. It is entitled
"Surtace Profile for Anti-Corrosion Paints". The
technology of surface preparation is covered in a serles of
separate chapters in this volume.
Vill. INSPECTION OF APPLICATION
EQUIPMENT
‘The Inspector must also be familiar with the methods.
‘and equipment used for coatings application, A brief sum-
mary is presented here, but more detailed information is
provided in the chapter on paint application of this volume
and in Volume 2,
‘ADJUSTMENT
EXTENSION
REFERENCE
SCALE
waguer
eee Oooo
CZ tems ssi ZA
FIGURE 25
Operating principle of Pencit Plt! or Tinsley Gage.
Courtesy: GilbertiCommensoatth, ine.j
1
i
i
A. SPRAY APPLICATION EQUIPMENT
Spray equipment is classified as either conventional
(air atomized) or airless. With air atomization equipment,
‘the paint ig fed through the fluid tine at relatively low
pressures, and compressed alt is dirocted at the fluid
‘troam through an air cap to atomize it. Adjustment of the
fluid stream and air pressure enables the painter to adjust
the spray pattern. Only the minimum pressures necessary
to adequately atomize the paint should be used. The prop:
oF fluid cap and needle must be chosen, as wall as a cor.
Tesponding air cap size. Bocause the compressed air
‘mixes with the coating, filters should be used to ensure &
clean air supply.
In airless spraying, very high hydraulic pressure
{(1000:3000 psi) is used to atomize the paint through a
precision-ground spray tip, much in the same manner as
Water is dispersed into droplets when passing through a
‘garden hose spray nozzle. in an airless spray gun, genéral-
'y, variations in the spray pattern can be attained only by
changing the spray tip (fluid orifice), although some ad-
justable tips are now available. Consequently, choice of
the appropriate tip, as wll as variation of fluid pressure.
can result in a wide range of spray patterns sultable for
almost any application,
The coating manufacturer's application instructions
usually recommend the appropriate spray tips and caps
for conventional and airless application of thoir material,
This, however, is only a recommendation and under certain
conditions, other tip or cap combinations may be more ap-
Propriate. Care should be taken when cleaning the tip or
‘caps as the orifice can be easily damaged.
Figune 27
ELCOMETER MINITECTOR — a magnetic ux gage utilizing «
battery-operated bridge cireuit to measur coating thicknoss-on
{forrous substrates. Similar modo! algo utlizoe eddy curronts for
‘Measurement of non-conductive coating over nonerraus metal
substrates, 7
Courtesy: Elcometor
104
ES
FIGURE 28
DIGITAL MINITECTOR — same features as the IMINITECTOR ox
cept that thicknesses are shown on digital readout.
The predominant malfunction In spray guns is at-
tributable to lack of cleanliness, both of the spray gun
itself and of fluid lines. Paint chips or agglomerations and.
‘most blasting abrasive particles are of sufficient size to
clog the small diameter orifices, resulting in gun stoppage
oF clogging.
Additionally, cleantiness of mixing pots, spray pots,
spray lines, spray guns or other application equipment is
Important and necessary for good paint application. Dirty
‘equipment can cause new paint to become contaminated
with old. Dislodged particles can clog the spray gun or
‘ven result in the doposition of Incompatible traces of
Previously applied material in the new paint film.
Cleanliness of all spray application equipment should be
verified prior to, oF no later than, the time of mixing of the
aint, Otherwise, resulting clogged paint equipment may
cause the loss of the coating material due to expired pot
life or the presence of contamination.
B. SPRAY POT
The spray pot should be clean and in working order
rior t0 use. Many types of paints, particularly zinc-ich
primers, require the use of an agitated pot (one equipped
with a stiering paddle) in order to keep the paint com-
ponents in suspension. Air and fluid pressure gages
should be available and functional on conventional spray
ots. The pressure release valve should also be operative.
‘The conventional pot should be equipped with diaphragm
pressure regulators, making it possible to contro! both air
‘and fluid pressure to the spray gun from the pot.
C. OTHER MEANS OF COATING
APPLICATIONS
Brushes, rollers, mitts, hopper guns, electrostatic
Spray, squeogees and other tools are used to apply coating:
|
matorials. The proper size, shape, configuration, nap size,
etc. should be chosen for a specific job. The inspector
should be aware of the advantages and disadvantages of
each method.
1X. MIXING OF THE PAINT MATERIAL
‘This is probably one of the most important opera
tlons, as improper mixing or thinning will affect the
Ccoating’s ability to resist the environment. However, mix:
Ing is not always specified as an inspection hold point in
painting operations. Regardless, there should be some
means to assure that all components of a mult
component paint system have beon added, that mixing 1s
thorough and proper and that any required induction times
have been met, Leaking or damaged containers should not
bbe used, particularly with catalyzed paints as some of the
components necessary for complete cure may have leaked
ut and proper proportioning may not be obtainable. Con:
tainers with illegible tabels should not be used. Mixing
should be done until the paint becomes smooth,
homogeneous, and free of surface “swirls” of pigment
lumps or agglomerations. Many paints séttle out upon pro-
longed storage, 50 “boxing” of these paints is beneficial to
censure that all pigment settled on the bottom of the con:
talner is incorporated in the mixed paint.
When adding zinc dust to the vehicle of zinc-rich
primers, Its a usual practice to sift the zine dust through a
Screen into the liquid portion while mixing. This helps to
Teduco a major problem when spraying two-component
zinc+ich primers; that is, gun clogging caused by pigment
agglomerations that are not properly dispersed upon mix.
Ing. For such heavily pigmented coatings, itis also impor.
tant that the spray pot agitator is Kooping the pigment in
suspension.
Preferably, only complete kits of multi-component
paints should’ be mixed. if this cannot be done, the
‘manufacturor must bo consulted to assure that partial mix:
ing of thetr material is permitted. If so, It is imperative that
the components be carefully measured,
Thinners are often required and should be well mixed
Into the paint material. The type and amount of thinner
should be In accordance with the coating manufacturer's
VERIMETER — an
destructive thickne:
substrates.
195
FIGURE 30
tronic magnetic flux thickness gage
{or accurately measuring the dry film thickness of non-magnetic
coatings applied to # ferrous base.
‘CERTOTEST — another
recommendations. The amount of thinner used should be
recorded by the inspector, as any thinner reduces the
volume of solid contents of the mixed paint.
Measurement of viscosity assures that proper thin-
ning ratios are used and that the thinning has not been
‘changed significantly from pot to pot. A common viscosity
‘cup Zahn), as shown in Figure 14, is simply a small cup of
known volume with a precisely sized orifice in the center.
Generally fiv orifice sizes are available and are numbered
1 through 5. The manufacturer can be consulted as to the
orifice size to use for his material, and the time in seconds
for the volume of properly thinned material held by the cup
to pass through the orifice. For example, the manufacturer
might stipulate that the material should be thinned such
that it will pass through a No. 3 Zahn Cup in 20-30 seconds
ata given liquid paint temperature.
The clean cup is fully immersed In tho coating
‘material and withdrawn quickly. A timer is started at the
ppraciso moment that the top of the cup leaves the level of
the liquid. The material wil! flow steadily through the
orifice. When the solid stream breaks at the base of the
cup, the timer is stopped instantly. It is important to hold
the cup one or two Inches above the surface of the liquid
0 that the cup will remain in the solvent atmosphere and
away from all drafts. The amount of thinner is adjusted
accordingly so that volume of paint held by the cup will
flow through the orifice within the stipulated time range.
Viscosity measurements of this type are of value for
quick fleld determinations of thinning and will reveal it
significant changes in the viscosity ocourred from pot to
ot of material. However, the paint applicator himself ts
generally the best judge of proper thinning ratios to assure
that he can apply a smooth wat coat without runs or sags,
Additionally, the viscosity of some high build thixotropic
coatings cannot be measured with the Zahn Cup, but other
viscosimeters can be used. In this case, the manufacturer
should-be contacted for a recommendation.|
|
FIGURE $1
ELCOMETER 101 — a magnetic flux instrument that operates
‘rom the power of a horseshoe magnet only without the need for
an olectrenie power supply
Courtesy: Zormeo Corp.
X. COATING APPLICATION
Besides surface preparation, the actuat coating ap:
plication is the most visible aspect of the coating work
After surtace proparation, it is the most important aspect
as wall, It has been said that “the best coating specifica-
ton is no better than the man behind the spray gun". Ac:
‘cordingly, the coating inspector should be knowledgeable
‘of the various application techniques, These are briefly
reviewed below, but detailed information is avaliable in the
chapter on Paint Application of this volume and in Volume
2
When spraying with conventional (air atomized) equip
‘ment, the epray gun should be held trom sb« to eight inches
{rom the surface and maintained perpendicular to the sur-
face throughout the stroke. For airless application, the
distance should be from 10 to 14 Inches. Atthe end of each
‘pass, the gun trigger should be roleased. Each spray pass
‘should overlap the previous one by 80%, and where post
ble, a oross hatch technique should be used, This requires
4 duplicate series of passes at 90° to the first to ensure
complete and uniform coverage.
{n brush application, the brush should be dipped ap-
proximately two-thirds of its bristle length into-the coating.
‘The bristle tips should be brushed lightly against the side
Of the container to prevent dripping, maintaininig as fully
loaded a brush as possible, Brushing ie more effective
than. spraying’ for working paint into depressed ir
regularities, pits or crevices. However, care should bo
taken to ensure that the coating Is not brushed out too
thin,
‘Other application methods include rolling, using mitts
‘oF pads, dipping, electrostatic spraying, powder coating,
(using fluidized bed or electro-static spray), and, Increas-
ingly, roller coating using automated facilities for flat
sheets. Each has its own specific technique as described
elsewhere in this volume. ;
108
Besides ensuring proper application technique, addi
tional care is necessary when inspecting coating work at
fossil tual power stations, chemical plants, coke plants,
land other areas where atmospheric contamination is pres-
cent. Often water washing between coats or application of
the topcoat within a minimum time interval is necessary.
Otherwise, contaminants often invisible to the unaided eye
may be coated over, leading to premature coating failure,
Deficient and excessive coating thicknesses in multi
coat systems should be observed. In cases where a top-
coat is applied over a generically similar (non-ust in:
hibitive) primer, deficient primer thickness can be “built
up" by additional thickness of the topcoat. However,
Where the primer contains rust Inhibitors or Is a different
generic type, an additional coat of the primor or previously
applied coating must be used before the topcoat can be
applied. Another common practice Is to use coatings of a
different color, orto tint each coat. This is an excallent aid,
to the applicator and inspector to assure that complete
‘coverage is achieved. Upper thickness limits are also
specitied if some cases. When paint thickness exceeds
the specified thickness, the excess should be removed by
grinding, sanding oF blast cleaning as appropriate,
Removal is usually followed by reapplication of a thin coat
to seal irregularities. Excessive or unsightly runs, sags,
drips, streamers, and other film deficlencles should be
brushed out during application or removed after drying.
This again is dono by grinding, sanding, or in extreme
cases, blast cleaning
XL. WET FILM THICKNESS DETERMINATIONS,
Wot film thickness readings are: used to aid the
FIGURE 92
GE THICKNESS GAGE
Courtesy: General Electic|
|
FIGURE 33
Positector for accurate cigltal measurements of coating
Athiokness.
painter and ingpector in determining how much material to
apply in order to achieve the specified dry flim thickness.
Wet film thicknesses on steel and most other metallic
substrates are considered “guideline” thicknesses, with
the dry film thickness being the thickness of record.
However, when coating concrete or nonmetaltic
substrates, the wet film thickness Is often the accepted
value because dry film thickness can be determined only
by destructive means.
The wet film thickness gage is generally a standard
"notch" configuration (Figure 16), although circular dial
‘gages are also used (Figure 16)
‘The notch typo gage consists of two end points on the
same plane with progressively deeper notched steps in
between, Each step is designated by a numbor roprosont.
Ing the distance In mils or microns between the step and
the plane created by tho two end points. The instrument is
pressed firmly into the wet film perpendicular to the
substrate and withdrawn. In every case, the two end points
will be wetted by the coating material, and in addition
‘some of the steps in between. The wat film thickness is,
considered as being between the last wetted step and the
next adjacent higher dry one. For example, if the "a" step
is watted and the "4" step is dry, the wet film thickness Is.
between 3 and 4 mils. fnone of the steps or alof the steps.
in botwoon tho end points are wetted, it is necessary to
turn the gage to a different face, as the wet film thickness.
is outside of that particular rango.
When using this instrument, It is necessary to stay
away from any surface irregularities that could distort the
readings. I determinations are being macle on curved sur-
faces, it Is Important that the gage be used along tho
length of the curve rather than across its width, as the
curve Itself could cause irregular wetting of the stops. The
gauge must also be cleaned thoroughly after each use to
1097
ensure the accuracy of the readings.
‘The Interchemical thickness gage is @ narrow whee!
with two outer rings of the same size and an off-set inner
fing. The instrument ts rolled across the surface and
withdrawn, The wat film thicknoss is that point where the
coating no fonger wets the inner ring.
Wot film thickness gages aro of value only if one
knows how heavy a wet film to apply. The wet film
thicknessidry fllm thickness ratio is based on the percent
solids by volume of the specific material being applied,
The old thoory of doubling the desired dry film thickness to
doterntine the wet film to be applied is only correct if the
solids by volume of the coating material is 50%.
‘The solids by volume of the coating material is infor:
‘mation readily available from the manufacturer and is
commonly included in their product data sheets. The basic
formula is DRY FILM THICKNESS = WET FILM THICK:
NESS X % SOLIDS BY VOLUME. A more workable variation
of the formula showing the required wet film thickness for
the desired dry film thickness Is as follows:
WET FILM THICKNESS
DESIRED ORY FILM THICKNESS
% SOLIDS BY VOLUME
FiguRe 34
ld microprocassor for coating thickness measuroments.
‘Courtesy: Elcometor
Hanai
j
i
}
i
FIGURE 35,
TOOKE SCRATCH GAGE — for determining dy film thickness by
cutting cross section tough tefl and viewing Wunder may
hltication,
The above formula is accurate provided the solids by
volume of the material is accurate. The percentage will
change, however, if any thinner Is added to the coating,
When thinner is added, the total volume of the material is
increased without any corresponding increase in the
amount of solids. Therefore, the thinned material will
result in a lower percentage of solids by volume, Thus,
when comparing thinned versus unthinned material in
‘order to achieve a comparable dry film thickness, a heavier
Wet fllm application of the thinned material will be re.
Guired. The following formula, which incorporates. the
“new'" solids by volume, should be used to determine tho
required wet film thickness when the material Is thinned.
DESIRED DRY FILM THICKNESS
% SOLIDS BY VOLUME
(100% + % THINNER ADDED)
WT =
For example, assume a material contains 78% solids by
volume and is to be applied in one coat to a dry film
thickness of 8 mils, Without thinner added, the required
wat film thickness Is determined as follows:
WET = 10.25 mits
If the coating in the same axample is thinned 20%, the new
required wot films calculated as follows:
See ae
076 ~ (0.68)
12.
WrT = 42.3 mits
This, without thinning, 10.25 wet mils are required to ob-
tain 8 mils dry. After thinning, however, the solids by
volume drops from 78% to 65% and the required wet film
198
thickness Increases nearly 2 mils,
Bocause the use of the wet film thickness gage is
dependent on the solids by volumo, and the solids by
volume is considered as the “in can" parcentage, it is,
essential that wet film thickness readings be taken as
S00n as a film is applied to the surface, Actually, during
‘spray application, between the time the material leaves
the gun and reaches the surface, some of the solvents will
already have evaporated, changing the percent of solids by
volume slightly. But for practical applications, this change
snot too signiticant. Howover, the longer one waits before
‘aking a reading, the less accurate that reading becomes,
For highly pigmented coatings (such as zinc-rich, or very
fast dry coatings, wet film thickness readings may be
unretiab.
Xi. DRY FILM THICKNESS
Ory film thickness readings on steel substrates are
‘commonly taken using magnetic gages. For nonferrous
metallic substrates, eddy current equipment is used,
Calibration of magnetic thicknoss gages should be done in
accordance with SSPC-PA 2, “SSPC Method for Measure-
ment of Dry Paint Thickness with Magnetic Gages".
Although the standard is written for magnetic gages, many
Of tho principles of operation and calibration techniques
apply to the eddy current instruments es veel
Determination of the thickness of each coat in a multi-
‘coat system should be an inspection hold-point. When us-
Ing magnetic gages to measure mult-coat systems, tho
average of the first coat must be determined prior to ap-
plication of the second coat. Readings taken after the sec-
‘ond coat is applied will obviously be the total thickness of
the two coats combined, and the specific thickness of the
‘second coat can only be determined by subtracting the
average thickness obtained from the first coat reading,
‘Tho second coat thickness cannot be determined precise:
'y, however, because it is highly unlikely that specitic
readings taken on the second coat will be over an area of
the first coat that is exactly the first coat average.
Thorotore, with magnetic gages It is nearly impossible to
specifically datermine the thicknesses of coats applied
after the first, and one must rely on averages only.
It Is often a good idea, where practical, to provide a
‘moans to Indicate coating thickness In areas whore it is
celther thin or thick, 60 appropriate repair can be'done by
the coating applicator. Possible methods are brush ap.
plication of a light tinted coat of the same paint, compati-
ble felt tip marking pens, chalk or other material that can
be readily removed or graphic plotting and notation on
charts and records,
Thiokness readings are taken to provide reasonable
assurance that the specified or desired dry film thickness,
hhas been achioved. However, it is not possible to measure
every square inch of the surface. SSPC-PA 2 states that
When using magnetic gages, five separate spot
‘measurements should be made over every 100 square feet
in area, Each spot measuremant consists of an average ofFIGURE 36
three gage readings noxt to one another. The averag of
the five spot measurements must be within the specified
thickness, while single spot measurements aro permitted
to be 80% of the specified thickness. The single gage
readings, however, making up the spot measurement, can
underrun by a greater amount. For example, a specifica
tion calls for 10 to 12 mils, The five spot measurements
(each a cluster of three gage readings) are as follows: Spot
4 (10, 14, 12; average 11); Spot 2 (7, 8, 9 average 8); Spot 3
(12, 12, 12; average 12); Spot 4(7, 12, 11; averago 10}; Spot 5
(12, 13, 115 average 12). This measured area would be a
ceptable because the average of the five spots is 10.6 mils
and within specification. According to SSPC-PA 2, unless
otherwise specified, the & mil spot measurement would be
acceptable because “no single spot measurement ...
shall be loss than 80% of the specified thickness" (@ mils
Is exactly 80%), and the 7 mil reading Is acceptable
because “single gage readings ... may underrun by a
‘greater amount”.
Dry film thickness instruments fall into four basic
catagories: magnetic pulloff, fixed probe, eddy current,
{and destructive, Each of the four categories are addressed
separately.
A, MAGNETIC PULL.OFF
The magnetic pulloff type gages include the
Mikrotest (Figure 17}, the Inspector Thickness Gage
(Figure 18), and the Pencil Pull-Off Figure 19), or Tinsley
type gage (Figures 20 and 21).
Basically, a Mikrotest or Inspector Gage consists of a
lever running through the center of a scale dial which,
houses a helical spring. The scate dial is located at the
fulcrum point of the lover. One ond of tho spring is at-
tached to the lever and the other end to the scale dial. One
199
side of the lever contains a permanent magnet while the
‘opposite end contains a counterbalance (Figures 22 and
23),
To operate, the scale dial is turned clockwise and the
‘magnet brought into direct contact with the metal
Substrate (through the coating or non-magnetic barrier).
‘Then the scale ring is turned counterclockwise, increasing
the spring tension, which applies a pulling force onto the
magnet. Ultimately, the spring tension overcomes the at-
traction of the magnet to the substrate, lifting the magnet
from the surface. The spring tension is callbrated so that
tho point whore the magnet breaks contact with the sur-
face can be equated to the distance of the magnet from
the surface. This distance Is road directly from tho scale
dial In mis (or microns). The calibrated spring tension is an
inverse logarithmic relationship of tho distance botween
‘the magnet and the substrate (e.g. the greater the spring
tension required to remove the magnet, the thinner the
coating).
‘Note that the thickness reading shown on the scale
fing when thé magnet breaks ‘contact with the surface
represents the gap between the magnet and the substrate.
This gap is considered to be the coating thickness.
However, t could also be comprised of voids, rust, embed:
ded contaminates, ote. Therefore, one must include a
thorough visual inspection during the work to ensure that
the coating is applied over a clean surface and does not
become contaminated during drying.
The Mikrotest and Inspector Gage should be
calibrated, or at least calibration verified, prior to, during,
and after each use to assure that they are measuring ac-
curately. Calibration methods are described in SSPC-PA 2,
“Moasurement of Dry Film Thickness with Magnotic
Gages,” which defines the pulloft Instruments as Type 1
gages. It describes two methods of calibration for the in:
struments; non-magnetic shims (generally plastic or mylar)
‘or ealibration test blocks similar to those supplied by the
FIGURE 37
‘A hand:held spring loaded micromater useful for i
thickness of coating chips.FIGURE 38
Pockosized 30x microscope with integral ight source useful for
examining coatings.
National Bureau of Standards, which are chrome and cop-
per plated steel (Figures 24 and 25 respectively). n either
‘case, it is essential that the instrument is calibrated in the
desired thickness range of use. If a coating is being
‘moasured in the thickness range of two to four mils, one
would not use a gage calibrated at 15 to 20 mils,
‘When calibrating using the plastic or non-magnetic
shim method, vorify the shim thickness with a micrometer.
Hold the shim firmly on the bare clean(ed) substrate and
measure it with the thickness instrument. Care must be
taken to assure that the shim does not flex, pushing the
‘magnet from the surface prematurely. If the instrument
does not read the shim thicknoss, Insert the calibration
tool into the slot in the side of the instrument (located at
‘the center of the scale dial), and adjust the scale until the
‘number corresponding with the shim thickness lines up
with the hairline. Check the eatibration by using shims of
lesser and greater thickness to determine the range of ac-
‘curacy. The instrument is now ready for use for measuring
thicknesses within that range over the same substrate and
surface preparation. If a section of the bare substrate is
Unavailable, blast clean small steel test panels (0.0. 4" x
4" x 6") to obtain the same or similar anchor pattern, pro-
tect them from corrosion using a dessicant, VPI Paper, or
other suitable means, and use the panels for calibration,
Calibration using the National Bureau of Standards
plates is somowhat different. First, adjust the instrument
{0 read the thickness stated on the calibration blocks in
7 200
the desired range of use. Next, take a gage reading of the
bare, uncoated substrate after blast cleaning (or other sur-
{ace preparation). The Instrument wit! generally read be-
tween one and two tenths of a mil up to 1 mil or more over,
the bare steel, Therefore, any costing thickness readings,
taken must be corrected by this bare steel base reading in
‘order to determine the coating thickness above the peaks
of the profile. Adjust subsequent thickness readings by
subtracting the magnetic base reading. For examplo, if the
Instrument is calibrated to a 4 mil NBS Standard, and a ¥
‘mil magnetio base reading on bare blast cleaned stee! is,
found, a paint thickness reading of 3¥% mils indicates that,
the true thickness above the peaks is actually only 3 mils,
Wf one chooses not to physically adjust the in.
struments 28 described above, it will be necessary to
develop a calibration correction curve using the Instru-
ment scale as an arbitrary scale. For example, a five on the
‘scale may be equivaient to three mils, a ton equivatont to
seven mils, and s0 on. .
‘Another type of magnetic pull-off gage based on a
similar principle is the pencil pull-off gage (Figure 18) or
Tinsley gage (Figures 20 and 21). Basically, the instrument
housing is similar to @ large pencil with a magnet at one
‘end. An extension spring is attached to the magnet and to
the top of the instrument housing. The Instrument Is held
perpendicular to tho surface and the magnet brought into
Contact with the substrate. As the housing Is lifted, the
magnet remains attached to the substrate until the spring
tension overcomes the attraction of the magnet, popping |
from the surface, The tension on the spring required to lift,
the magnet is read from the scale in mils or microns,
igure 26), This instrument can not be adjusted, although
calibration should be verified. In this case, however, a
Calibration correction curve is necessary ifthe instrument
does not read correctly on the shims. The proferrod
‘method for verifying calibration is the use of calibration
test blocks. Non-magnetic shims (particularly plastic or
mylar) could be used, but great care is necessary to ensure
that flexing doos not cause the magnet to break from tho
substrate prematurely. The pencitstyle gages provide a
‘quick check of coating thicknoss, but considerable judg-
ment is involved in determining the point at whieh the
‘magnet broaks from the surface,
There ate some precautions necessary when using
‘any instrument that has a magnet. First, the magnet Is ox
posed and therefore susceptible to attracting iron filings,
steel shot or grt particles. The magnet must be cleaned of
any contaminants during uso, or the contaminant will in
correctly be read as coating thickness. This Is extremely
important in shop work where grinding is employed. Tho
resulting Iron filings often necessitate that the magnet
and coating surface be cleaned before each thickness
reading. If the instrument Is used on a soft film, allowing
‘the magnet to sink into the surface, a thinner coating
thickness will be recorded. This Is because the coating
itself may be tacky, holding the magnet beyond the point,
where the spring should have lifted it from the surface, orFIGURE 20
‘measurement principle of the Tooke Gage.
the coating under the depression caused by the magnet,
actually will be thinnor. in this case, place a plastic shim
‘on top of the surface to prevent the magnet from deform-
9 the coating and subtract the shim thickness from any
subsequent readings. In addition, If there are any vibra-
tions in the area of instrument use, they could cause the
magnet to be popped from the surface prematurely, giving
‘an erroneously high thickness reading. The instrument
should not be used any closer than 1 inch to an edge of the
surface, In addition, residual magnetism in the structure
‘on which the coating Is measured can have an adverse of-
fect on the readings.
Tho scalo dial type instrumonts have’ an additional
“human error” problem during use. It is easy to continue to
turn the dial beyond the point that tho magnot has lifted
from the surface, giving an incorrect thickness reading. It
is imperative that the dial be stopped as soon as the
magnet lifts from the surface, Advanced versions of the
Mikrotest have addressed this problem by incorporating a
mechanism whieh focks the scale dial in place when the
‘magnet breaks contact with the surface.
B. FIXED PROBE MAGNETIC FLUX GAGES
‘The fixed probe or magnetic flux type gages are
described in SSPC-PA 2 as Type 2.gages. They include the
Minitector (Figures 27 and 28), Verimeter (Figure 29),
Certotest (Figure 30), Elcometer 101 (Figure 31), GE Gage
(Figure 32), Positector (Figure 39), Accuderm, Minitest, Por:
mascope, and others. The Type 2 gages also must bo
calibrated prior to use, but calibration is accomplished us
ing the non-magnetic shim method only. The NBS calibra.
tion plate is not suitable for use with these instruments.
because the calibration plates do not exceed the critical
mass of stee! needed to satisfy the magnetic field of these
instruments. The only exception is the Positector, which
can satisfactorily be calibrated on the NBS calibration
blanks,
Calibration of the electrically operated instruments
{all of the above oxcopt the Positector, which is also elec-
‘wically operated and the Elcometer 101, which is not) is ac-
‘complished by placing the instrument probe directly on the
bare steel substrate (after surface preparation) and ad-
justing the designated knob (ic. "zero") 60 that the meter
reads "0", Next, place the calibration shim of desired
thickness on the steel and adjust the appropriate knob (0.
adjust", “eal", etc.) so that the meter indicates the cor-
rect shim thickness, Repeat this procedure (zero set,
thickness set) until both readings are adjusted correctly,
Once again, check the range of calibration by using other
shims, both of a thinner and heavier thickness, than that
Used in the initial calibration. The instrument is now ready
for use and will correctly record the thickness of the
coating material. Any effect of surface roughness is
calibrated into the instrument because It was adjusted
over the bare steel (or on the NBS plates for the
Posite¢tor, thus eliminating the need for a magnetic base
steading correction factor.
Calibration of the Positestor and Elcometer 101, on
the other hand, requires only that the instrument be ad-
justed to read tho thicknoss of tho shim over bare prepared
steel, rather than an adjustment of the zero reading and
shim reading, Further, (for the Elcometer 101 only), calibra.
tion must be verified for each position of use (2.9. horizon-
tal, vertical, and overhead),
‘The magnetic flux gages experience some of the
‘same problems as the pul-off gages: 1) lower than actual
thickness readings on soft or tacky fllms; 2) necassity of
staying away from the edges during use; and 3) difficulty in
keeping the magnet clean. in addition, because the In-
struments are based on flux principles, they are vulnerable
to the effect of flux leakage from the instrument to nearby
ferrous masses, causing the instrument to be ineffective.
Therefore, it is necessary to stay at least three inches
away from any nearby iron or steel object, oF the instru
FIGURE 40
View through Tooke Gage Meroscope. The intertaco of the
Ccoatingisubstrete is ono division to the itt of .05 on the scale.
Coating thickness Is measured trom this point fo tho ttt ending
Black bench mark at 05.FIGURE «1
TINKER-RASOR LOW VOLTAGE WET SPONGE HOLIDAY DETEC.
TOR ~ used for finding pinholes and holidays in non-conductive
aint films up to 20 mils thick when applied to conductive
Subate
‘ment calibration must be readjusted in these specitic
areas. If used inside @ tank or vessel, théy-should bo
calibrated Inside the vessel to compensate for tlux
leakage. The probe of these instruments must also be kept
Perpendicular to the coated substrate diyring use; other
Wise, incorrect readings will result
C.. MICROPROCESSOR
The computer has now been incorporated into @ dry
film thickness gage. A hand-held microprocessor with
digital thickness display is “available with its physical
operation similar to the magnotio flux gages above (Figure:
34),
D. EDDY CURRENT GAGES
Eddy current instruments measure the thickness of
Ron-conductive coatings on nonferrous motai substrates.
Included with this typo of instrument are the Minitector
(Figures 18 and 18), Minitest, Permascope, and others. The
probe of these instruments is energized by alternating cur:
Font, inducing eddy currents in the motal. The eddy cur-
rents create opposing altemating magnetic fields within
the metal, modifying the electrical characterist
robe coil. The extent of these changes are d
the
shown on @ meter as coating thickness. The eddy current
Instruments are calibrated similarly to the magnetig flux
instruments using the plastic shim method
£, DESTRUCTIVE TEST INSTRUMENTS
Destructive thickness testing includes the use of the
Took Gage (two models are shown in Figures 35 and 36),
Micrometars (Figure 37), or microscopes (Figure 88). The
Tooke Gage consists of a 60X microscope that is used to
ook at slits in the coating made by precision cutting tips
‘Supplied with the instrument, The principle of the Tooke
Gago is basic trigonometry. By making a cut through the
coating at a known angle and viewing perpendicularly to
that cut, the actual coating thickness can be determined,
by measuring the width of the cut from a scale in the
eyepiece of the microscope. The instrument can be used
{for determining the thickness of underlying coats in multi
‘coat systems and oliminates many of the drawbacks of the
‘magnetic instruments caused by magnotle fields, proximi
ty to edgos, irregular surfaces, magnetic effect of the
substrate, profile, and so forth. The instrument can be
‘used on coating thicknesses up to 50 mils provided the
coating Is not too brittie or elastic for a smooth cut to be
made.
Cutting tips of different angles are available. They are
dosignated as either 1X, 2X, oF 10X, The tip used dator
mines the thickness oquivalent for each tine in the
Microscope eyepiece. The number of lines corresponding
with the coating is divided by the number of the tip used.
Therefore, 1 line when using the 1X tip is equivalent to 1/1
(OF 4 mit; line with the 2x tip is ¥% oF 6 mil, and 1 ine with,
‘the 10X tip is 4, or -1 mil. Thus, ifthe coating cross-section
Covers 7 lines and the 2X tip Is used, the thickness is J, or
35 mits (Figures 39 and 40)
Another means of destructively measuring the
coating thickness is the use of either a depth micrometer
0F @ standard micrometer. The dapth micrometer can be
Uused by removing a small soction of the coating down to
tho substrate, permitting the base of the instrumant to rest
‘on the coating while the projecting pin is adjusted to the
Substrate. Altematively, a sample of the coating can be
removed from the substrate and the thickness measured
Using a standard micrometer. The coating chips could also
be returned to a laboratory for micrascaple thickness
determinations. The Tooke gage could also be used for
this purpose. When viewing the edge (cross section) of a
Gisbonded chip, each division of the microscope is
equivalent to 1.0 mil,
Xill, CLEANLINESS BETWEEN COATS
Where more than one coat is to be applied, a proper
Inspection hold point is the determination of tho
leantinass of the surface immodiately prior to application
of tho next coat, In addition to dirt and dust, quite often dry
spray, oF overspray, will cause a problem. All should bo.
removed because the presence of these “contaminants”
‘can result in reduced adhesion between coats and porosi-FIGURE 42
USING A LOW VOLTAGE WET SPONGE DETECTOR — to locate
scontinuites in non-conductive coatings applied to conductive
metal substrates,
Official U.S. Navy Photograph
ty, tendering the coating less resistant to the effects of the
environments. The Surface should also be Inspected for
any adverse contamination {rom the environment (.
residue from chemical facilities, salt, etc)
XIV. PINHOLE AND HOLIDAY DETECTION
After all the coats of paint have been applied, the in-
spector should verify that the appropriate clean-up is done,
and that any abrasions, nicks, or scrapes are repaired as
roquired.
Often holiday, pinhole, or spark testing Is used to find
tho nicks, scrapes, and pinholes in the coating flim, par-
ticularly if the coating Is intended for immersion service.
Holiday testing may be required after application of either
the next to iast, or last coat of paint. Usually when such
testing is specified, it 1s done before final cure of tho
coating has occurred so that any repair material applied
will successfully bond to the underlying coat.
Pinhole and hollday detectors are three general types:
low voltage wet sponge (Figures 41, 42 and 43), DC high
voltage (Figures 44, 45 and 48), and AC electrostatic types.
The low! voltage wet sponge holiday detectors are
used for finding discontinuities In non-conductive
coatings applied to conductive metal bases. The low
voltage detector is sultable for use on coatings up to 20
mils in thickness. The basic unit consists of the detector
itself, a ground cablo, and a sponge electrode. The ground
208
cable Is firmly attached to the bare substrate and the
sponge electrode is saturated with tap water. The elec:
{rode is moved across the entire surface, the water permit
ting @ small current to flow through the pinholes down to
the substrate, Once the current reaches the substrate, the
Circuit is completed to the detector unit and an audibie
signal can be hoard indicating that a pinhole or discon-
tinuity is present. When coatings are in the range of 10 to
20 mils, a non-sudsing wetting agent (such as Eastman
Kodak Photo-Fio) may be added to the water to increase
the wetting properties. Ifthe coating system is found to be.
outside of the 20 mil thickness limits, high voltage holiday
detection equipment should be used.
High voltage detectors basically function on the same
operating principle as the low voltage described above, ex
‘cept that @ sponge Is not used, The instrument consists of
4 testing unit capable of producing various voltage out:
puts, a ground cable, and an electrode made of conductive
materials such as neoprene, brass, or steel. High voltage
units are available up to 20,000 volts and more. High”
voltage detectors are used for non-conductive coatings ap-
plied to conductive substrates. Tha ground wire Is femly
attached to a section of the bare substrate and the elec-
trode is passed over the entire surface. A spark will Jump.
from the electrode through the air gap down to the
substiate at pinholes, holidays, or missed areas,
simultaneousty triggering audible andfor visual signaling
vice in the unit.
For exterior pipeline work: many times the ground
wire of the holiday detector is permitted to drag across the ~
earth provided the pipe itself Is grounded to the earth,
However, tho praferred method of testing is to altach the
‘ground wire directly to the substrate whenever possible
When using high voltage holiday detectors, itis im
FIQURE 43
KD BIRD DOG LOW VOLTAGE WET SPONGE HOLIDAY DETEC:
TOR — ullizes a wetted sponge and ground wire to find pinholes
‘and holidays in dry paint time applied to conductive substrates.FIGURE 48
SPY HIGH VOLTAGE HOLIDAY DETECTOR — for uncovering
flaws in “thick fim systems,
volts DOTA spark jumps trom th
deficient areas.
08 are avaliable up to 22,000
ctrode through the coating at
portant to use only the voltage level recommended by the
coating manufacturer for the coating thickness, Other
wise, damage to “good” coating could eceur. A rule of
thumb is to apply 100 volts per mil of coating for
thicknesses in excess of 20 mils
When testing conductive linings applied over steet
substrates (Le. conductive rubber linings}, the AC Tesla
Coit typé olsctrostatic testers are generally used. The AC
tester has a varlabie voltage output (preferably, the voltage
{is indicated) but does not require the use of a ground wire.
‘Tho unit constantly emits @ corona which Ie blue in color,
>but when a break in the lining is passed over, a white spark
wilt Jump to the substrate at the holiday of imperfection,
Note that surface contaminants or dampness may also
cause @ color change or spark; therefore, itis advisable to
‘lean and retest questionable areas to confirm that a
break in the lining is present.
XV. FIELD ADHESION TESTING
Occasionally, there Is a need to test the adhesion of
the coatings after application. Thore aro different types of
adhesion testing methods used from the simple penknife
to more elaborate testing units. The use of a penknife
Generally requires a subjective evaluation of the coating
adhesion based on some previous experience. Generally,
fone cuts through the coating and probes at it with the
knife blade, trying to lift it from the surface to ascertain
whether or not the adhesion is adequate.
‘A modified version of this type of testing is the cross-
‘out test. The cross-cut test consists of cutting an “X", or a
umber of small “squares or diamonds” through the
Coating down to the substrate. Tape is rubbed vigorously
onto the scribes and-removed: firmly and quickly, The
‘cross-hatch pattem is evaluated according to the percent-
‘age of squares delaminated or remaining intact. The "x"
204
and “cross-cut” tape adhesion tests are described in
ASTM D.2369, "Measuring Adhosion by Tape Test”.
There are also instruments available for testing the
tensile adhesion strength of coatings. They apply a value,
to the adhesion strength in pounds per square inch, thus
eliminating some of the subjectivity of the above tests. An
Instrument for tensile testing is the Elcometor Adhesion
Tester (Figue 47). The Elcometer Adhesion Tester con-
sists of the test unit itself and aluminum test dollies or
lugs, each with @ surface contact area of Ye square Inch,
The dolties are cemented to the coating surface using an
adhesive. After the adhesive has cured, the coating around
the periphery of the dolly is out through down to the
Substrate. The claw of the test instrument is placed under
the lip of the dolly and the unit tightened by hand, using as
uniform a turning speed and motion as possible. The test
Unit applies a pulling force on the head of the dolly,
ultimately breaking it from the surface. The point of the.
break is read from the scale on the instrument in pounds.
per square inch. Not only is the numerical value of impor.
tance when using this Instrument, but also the type of
break. For example, there is a significant difference in the
test results if one finds a clean break to the substrate of
between costs, compared to finding a cohesive break
within a coat. Many times one may experience a fallure of
the adhesive. If this occurs, it establishes that the coating,
tensile adhesion strength is at least as good as that
Pressure that broke the adhesive
{tis generally recommended that the two-component
type epoxy adhesives be used in preference to the single
‘component fast crying cyano-acrylate types, When testing
Zine-tich coatings, for example, it has been found that the
thin cyano-acrylates hava a tendency to penetrate and
bond the zinc particles together, resulting in a much higher
tensilo pull than should bo expected. In other cases, the
adhesive appears to soften and cause premature fallure of
the coating systems,
XVI, EVALUATING CURE
When a coatings to be used in immersion service, the
FIGURE 45
TINKER-RASOR HIGH VOLTAGE HOLIDAY DETECTOR — us
for non-conductive coatings applied fo conductive substrateae
|
{
FIGURE 46
BUCKLEY UVRAL HIGH VOLTAGE HOLIDAY DETECTOR —
‘nother high vollage holiday dotoctor with infinitely variable
‘Voltages tp to 26,000 volts, Used to detect flaws in heavy coating
tyatome and wrapped piping
applled coating film must be allowed to dry cute for a given
Tenath of time prior to being placed into service. This dry
‘cure time Is generally shown on the manufacturer's prod-
uct information, Alternately, forced-heat curing may be
used to reduce the time between curing and service.
Determining the cure of coatings is gonorally difficult,
ASTM D1640 outlines one method, but there are no univer-
sally reliable field tests for such purposes. Solvent rub
tosts can be used, as well as sandpaper tests. When most
coatings are suitably cured, rubbing them with sandpaper
‘will produce a fine dust. I the sandpaper gums up, depend:
ing upon the coating, it may not be cured properly. Cer:
tain phenolcontaining coatings may discolor upon
heating — and the cure of phenolic tank lining coatings is
often dotermined by comparison of their color with color
reference coupons supplied by the coating manufacturer.
Because a coating is “dry” or hard does not
necessarlly maan It Is cured. In fact, for most coatings,
hardness Is not synonymous with cure. The only coating!
types for which this is true ate the solvent deposited
coatings such as the chlorinated rubbers and vinyls. Even
then, residual retained solvents (and moisture in water
‘emulsion coatings), under certain atmospheric conditions
=“
Figure 47
ELCOMETER ADHESION TESTERS. Four tost units shown,
Wrench ls required for 2,000 and 4,000 pound models. Small test
dally is shown In bottom of photograph.
‘of tomparature andor humidity may take a tong time to
‘escape from the paint film, Final attainment of flim proper-
tias will be acquired only upon satisfactory loss of these
entrapped solvents, In some casos this evaporation prok
‘e88 may take as long as two or three weeks or more.
XVI. CONCLUSIONS:
There js a wide variety of inspection instruments,
favaliable for use (0 assure the adequacy of the ambiont
conditions, surface preparation, wet and dry flim
thicknesses, and final coating continuity. The instruments
all have advantages and disadvantages, but the overriding
factor in their successful use Is the knowledge and ability
of the individual using them. It is important that the i
struments be cared tor, calibrated, and used property.
However, instrument inspection is only part of the total in
spection process. It must be combined with a good, com-
‘mon sense visual inspection for detection of misses,
skips, rune, sags, surface contaminants, overspray, dry
spray, and any other defects objectionable for the service
Intended. Proper Instruments, specific knowledge, com-
mon sense and good judgment are required for good
coatings inspection.
Finally, all results of any inspection should be
thoroughly documented in writing to verify that the
specified requirments have beon met. Future
maintenance or the removal and maintenance of a failed
coating system may be dependent on the factual reporting
of every phase of the work.
ACKNOWLEDGEMENT
“The authors and editors gratefully acknowledge the activo
participation of the following In tho roviow procoss for this
Chapter, AI Boltelman, Robert Doyle, Amncld Eickhott, Lewis
Gleekman, Joseph Guddis, Ronald Hamm, John D. Keane, Jay
Leanse, Charle Lowis, Jr, M. Lichtonstadter, Marshall McGee,
‘Stan Moz, Melvin Sandler. M. Sherman, and William Wallace,
The chapter was also presented to the following for advance
eviow: Dean Berger, Paul Campbell, Wiliam Chandier, D. Ws.
hristotforson, Jack Kiewl, Rober MeCielland, Gatewood Nor:
‘man, Bil Pearson, Rober! Richards and Mary Ann Stephens.
205Biocnapaies
Kenneth Tator isthe
wner of KrAator Asso
ston conalting enginoating
tm’ specazing' nt
protetve coatings. "A epi.
fers. prstesiont engine,
far baler fo the Ao
tear Nation! Standards inst
atonal Associaton
land Materials, the Socioty for
Paint “Technology, and the
Steel Structures Painting :
Gouncit Mr. Tatar holds.an MBA from Columbia Univers
yand a
8S, in Chemical Engineering trom Latayetto Golloge, He ie the
author of numerous publications and fas prosented technical
Papers at many association meetings and corporate seminars,
Kennoth Trimbor fe Qual
lly Assurance. Manager’ for
+ figld inspection services at
KTA‘Tator Associates. Mr
Trimber isa coritied Inspactor |
of clear factities, and has
lectured on coatings Inspec:
tion, inspection Instuments
and related topes. In addition,
he has writen a number of |
publications and’ age. histo
Ties. He is a: membor of the
American Sacialy Tor Testing
‘and Materials, tne Institute of
Applied Technology, and the i
Stee! Structures Painting Counell. Mr. Trimbor holds a B.S. in
~ Marketing from Indiana University of Ponnsyhanta.
10.
1"
2,
REFERENCES.
Wiliam F. Gross, Applications Manual for Paint and Protec:
tive Coatings, McGraw-Hill Bock Company, New York, NY,
1970.
aul E. Weaver, Industria Maintonanoe Painting ad Eaition,
‘National Association of Corrosion Engineers, Houston, Pk,
1987,
‘last-OMt", Glemco industries, San Francisco, CA, 1970.
Kenneth 8. Tator, and Kenneth A. Timber, “Coating Inspec-
lion Instruments, Plant Engineering, Sept. 19 and Oct. 3,
1074,
KA, Trimber, and C.A. MeCartney, “Importance of Coat
Application inspection and inetrumerte Available for Use",
presented. at NACE 14th Annual Liberty Bell Corrosion
Course, Sept, 1976,
. Di, Berger, and SE. Moz, “Instrumente for lngpection of
Coatings", Journal of Testing and Evaluation, Vot. 4, NO. 1,
Dp. 26:83, Jan, 1976
Kenneth 6. Talor, and Kenneth A. Trimber: “Goating (Paint)
Inepection instruments, Typos, Uses, and Calibration”
Pagor Number 254, NACE Corrosion 80.
NACE Standard RBO1-78 “Recommended Practice — Design,
Fabrication, and Surface Finieh of Metal Tanks and Vessols
0 Be Lined for Chemical Immersion Service", December,
1977,
NAGE Standard RP-0274 “Recommended Practice — High
Voltage Electrical Inspection of Pipeline Coatinge Prior to fn
tallation”, August, 1974,
SSPO-PA 2 — "Method for Measurament of Ory Paint
Thickness With Magnotic Gages".
NACE — "TPC Publication No.2 — Coatings and Linings for
linmarsion Service”, Chapters 2 and 4, Houston, TX
John D. Keane, Joseph A. Bruno, J, and Raymond EF.
Weaver, Stoo! Structures Paiating Council, “Surface Profile
for Anti. Corrosion Paints”, Piteburgh, PA, 1976.