Suhu

Tanggal
ruangan

Kode AB Kelembaban

Tanggal Pengujian:
1 2 Rata-rata Alat/Program

1) Warna <1 <1 #DIV/0! #VALUE! MD 100

2) Suhu <1 <1 #DIV/0! #VALUE! MD 100

3) Kekeruhan <1 <1 #DIV/0! #VALUE! MD 100

4) DHL <1 <1 #DIV/0! #VALUE! MD 100
TDS <1 <1 #DIV/0! #VALUE! MD 100

5) pH pH 4,0 pH 7,0 10,0 Alat : Thermoscientific Vstar 93

Standard Paraf Analis

1 2 3 4 5 Rata-rata
Sampel
#DIV/0!
SD #DIV/0!
#DIV/0!
Tanggal
6) Kesadahan Pengujian:

Standarisasi Lar. EDTA

V.CaCO3 (0,01
Duplo M) ml EDTA

1 10 Tanggal Standarisasi :
2 10 M CaCO3 0.01 M
3 10
4 10 M EDTA #DIV/0! M
5 10
6 10
7 10
8 10
9 10
10 10
Rata-rata 10 #DIV/0!

Kesadahan Total
M EDTA
Duplo V. Sampel V. EDTA
1 25 #DIV/0! #DIV/0! mg/L f= 1
2 25
Rata-rata 25 #DIV/0!

Kesadahan Ca
M EDTA
Duplo V. Sampel V. EDTA
1
2
Rata-rata

Pembuatan Standar CaCO3:

Penimbangan Standar CaCO3
Volum Total
 Kadar CaCO3

Kadar standar
spike (A) Contoh uji CaCO3 yg V std Target V akhir
(B) ditambahkan Value (Y)
(Z)
Duplo ml EDTA ml EDTA [ ] CaCO₃ ml CaCO₃ ml (C.U+CaCO₃)
1
2

Rata-rata

Kesadahan (mg/L)=

Catatan : % R = 85 % - 115 %
Tanggal
7) Nitrat Pengujian:
Alat :
Program : %RPD Paraf
Duplo NH4 NH3 N NH4 NH3 N Analis
1
2 #DIV/0!
Rata-rata #DIV/0! #DIV/0! #DIV/0!
x pengencrn #DIV/0! #DIV/0! #DIV/0!
N= #DIV/0! pengenceran 1
NO3= #DIV/0!
Spike Matrix (A) C.U non Spike (B)
Duplo NH4 NH3 N NH4 NH3 N
1
2
Rata-rata
Target Value (G) Kadar Larutan Standar (Z)
Duplo NH4 NH3 N NH4 NH3 N
1
2
Rata-rata
V. Target Value V.Akhir Spike
(Y) Matrix (V)
NH4 NH3 N NH4 NH3 N

Catatan : RPD < 5 %

% R = 85-115 %
Tanggal
8) Ammonia Pengujian:

Alat
Program %RPD Paraf
Duplo NH4 NH3 N NH4 NH3 N Analis
1
2 0 0 0
Rata-rata #DIV/0! #DIV/0! #DIV/0!
pengenceran #DIV/0! #DIV/0! #DIV/0! 1
 Spike Matrik (A) C.U non Spike (B)
Duplo NH4 NH3 N NH4 NH3 N
1
2
Rata-rata
Target Value (G) Kadar Larutan Standar (Z)
Duplo NH4 NH3 N NH4 NH3 N
1
2
Rata-rata
V. Target Value V.Akhir Spike
(Y) Matrix (V)
NH4 NH3 N NH4 NH3 N

Catatan : RPD < 5 %

% R = 85-115 %
Tanggal
9) Nitrit Pengujian:
Alat
Program
Sampel % RPD Paraf Analis
Duplo NO2 N NO2 N
1
2 0 0
Rata-rata #DIV/0! #DIV/0!
pengencrn #DIV/0! #DIV/0! 1
Spike Matrix (E) C.U non Spike (F) Target Value (G) [ ] lar baku (z)
Duplo NO2 N NO2 N NO2 N NO2 N
1
2
Rata-rata
v. lar baku (y) v. akhir spike
matrix (v)
NO2 N NO2 N

Catatan : % RPD = < 5%

% R = 90 - 110%
Tanggal
10) Clorida Pengujian:
Standarisasi AgNO3 :
v. NaCl (V)
Duplo v.t AgNO3 (A) v.t blanko (B) Paraf Analis
0,0141 N
1 25 25.5 0.6 N NaCl 0.0141
2 25 25.5 0.6 N AgNO3 0.0141566265
Rata-rata 25 25.5 0.6
Titrasi Sampel :
Duplo v. sampel v.t AgNO3 (a) v.t blanko (b) %RPD
1 100
2 100 #DIV/0! f= 1 kali
Rata-rata 100 #DIV/0! #DIV/0! Cl (mg/L) = #DIV/0!

Spike Matrix :

Duplo v. spike matrix v.t AgNO3 (c) v.t blanko (d) %RPD
1
2
 Rata-rata
Duplo v. sampel v.t AgNO3 (e) v.t blanko (d) %RPD
1
2
Rata-rata

Catatan : % RPD = < 10%

% R = 90 - 110%

Tanggal
11) Sulfat Pengujian:

Alat
Program
Sampel % RPD
Paraf Analis
Duplo SO₄ SO₄
1
2 #DIV/0!
Rata-rata #DIV/0!
Spike Matrix C.U non Spike Target Value
(E) (F) (G)
Duplo SO₄ SO₄ SO₄
1
2
Rata-rata
Catatan : % RPD = < 10%
% R = 90 - 110%

Tanggal
12) Besi Pengujian:
Alat :
Program :
Sampel % RPD
Paraf Analis
Duplo Fe Fe
1
2 #DIV/0!
Rata-rata
Spike Matrix C.U non Spike Target Value
(E) (F) (G)
Duplo Fe Fe Fe
1
2
Rata-rata
Catatan : % RPD = < 10%
% R = 85 - 115%
Tanggal
13) Mangan Pengujian:
Alat :
Program :
Sampel % RPD
Paraf Analis
Duplo Mn Mn
 1
2 #DIV/0!
Rata-rata #DIV/0!
Spike Matrix C.U non Spike Target Value
(E) (F) (G)
Duplo Mn Mn Mn
1
2
Rata-rata
Catatan : % RPD = < 10%
% R = 90 - 110%

Tanggal
14) TSS Pengujian: 24.05.209

v.contoh uji Cawan + K.Saring Cawan + K.saring +Residu Residu

Penimba-ngan
(ml)
A1 B1 A2 B2 A3 B3
1
2
3
#DIV/0! #DIV/0!
4
Konstan #DIV/0! #DIV/0! #DIV/0! #DIV/0!
#DIV/0! #DIV/0!

#DIV/0!
Kadar TSS (mg/L) = #DIV/0!
Tanggal
15) Minyak & Lemak Pengujian:
Presisi :
Labu kosong Labu + Residu
v.standar (ml) Penimba-ngan
A1 B1 C₁ D₁ A2 B2 C₂
1
2
3
4
Konstan
[ ] standar(Target Value) = 20
mg/L lar. Heksadekana-asam A B C D A B C
stearat
Presisi %R

Catatan : Presisi = 11%, %R = 78-114%

 Sampel :
Labu kosong Labu + Residu
v.sampel (ml) Penimba-ngan
A1 B1 C₁ D₁ A2 B2 C₂
1
2
3
4
Konstan

Paraf Analis
A B C D A B C D

rata-rata

Tanggal
16) COD Pengujian: 28.05.209

Standarisasi Ferro Amonium Sulfat (FAS) :

V.K2Cr2O7 (V) v.t K2Cr2O7
Duplo v.t blanko (B)
0,025 N (A)
1 2 3.98 N K2Cr2O7 0.1
2 2 3.98 N FAS 0.05025

Rata-rata 2 3.98 #DIV/0!

Titrasi Sampel :

V.K2Cr2O7 v.contoh uji

perlakuan (ml) v.t blanko (A) v.t sampel (B) RPD (%)
1 2 3 -
2 2 3 - #DIV/0!
2 3 #DIV/0! #DIV/0! -
pengenceran 1

Recovery :
perlakuan V.K2Cr2O7 v.KHP (ml) v.t blanko (A) v.t KHP (B) %R

1 #DIV/0!
2 #DIV/0! #DIV/0!
#DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0!
Tanggal
17) BOD Pengujian:
Sampel :
v.contoh uji DO 0 Hari DO 5 Hari % Konsumsi
Perlakuan V.Total Faktor P’ceran Oksigen
(ml)
 v.contoh uji % Konsumsi
Perlakuan (ml) V.Total Faktor P’ceran Oksigen

V.Thio DO V.Thio DO
1 #DIV/0! #DIV/0!
2 #DIV/0! #DIV/0!

Blanko 1
2
rt #DIV/0! #DIV/0!
Normalitas (N) Na2S2O3

BOD 1 =(DO 0-DO 5)sampel - (DO 0-DO 5)blanko x Fp #DIV/0!

BOD 2 =(DO 0-DO 5)sampel - (DO 0-DO 5)blanko x Fp #DIV/0!

BOD rata-rata #DIV/0!

#DIV/0!

Larutan Standar :
DO 0 Hari DO 5 Hari
Perlakuan v.lar standar [ ] Lar Standar
V.Thio V.Thio
1
2

Blanko 1
2
rt
Normalitas (N) Na2S2O3

BOD Standar=(DO 0-DO 5)lar standar - (DO 0-DO 5)blanko x Fp

Catatan %RPD = < 30%

[ ] BOD Standar = 198 ± 30,5 mg/L
% Konsumsi Oksigen = 40-70 %
Tanggal
18) Timbal Pengujian:
Alat :
Program :
Sampel % RPD
Paraf Analis
Duplo Pb Pb
1
2 #DIV/0!
Rata-rata #DIV/0!
Spike Matrix C.U non Spike Target Value
(E) (F) (G)
Duplo Pb Pb Pb
1
2
Rata-rata
Catatan : % RPD = < 10%
% R = 90 - 110%
Tanggal
19) Deterjen
Pengujian:
Alat :
 Program :

Target
Spike C.U non
Sampel % RPD Value
Matrix (E) Spike (F) (G)
Duplo
1
2
Rata-rata

20 Posfat Tanggal
Pengujian:
Alat
Program

Target
Spike C.U non Value
P P205 PO4 % RPD
Matrix (E) Spike (F)
(G)
Duplo
1
2
Rata-
rata

21) Zat Organik Tanggal

Pengujian:
Alat :
Program :
Konsentrasi Spike Matrix C.U non Target
Penetapan KMnO4 Sampel (ml) Nilai ZO % RPD
(E) Spike (F) Value (G)
Duplo
1
2
Rata-
rata

Tanggal
22) Seng Pengujian:
Alat :
Program :
 Sampel % RPD
Paraf Analis
Duplo Zn Zn
1
2 #DIV/0!
Rata-rata #DIV/0!
Spike Matrix C.U non Spike Target Value
(E) (F) (G)
Duplo Zn Zn Zn
1
2
Rata-rata
Catatan : % RPD = < 10%
% R = 90 - 110%

Tanggal
23) Tembaga Pengujian:
Alat :
Program :
Sampel % RPD
Paraf Analis
Duplo Cu Cu
1
2 #DIV/0!
Rata-rata #DIV/0!
Spike Matrix C.U non Spike Target Value
(E) (F) (G)
Duplo Zn Zn Zn
1
2
Rata-rata
Catatan : % RPD = < 10%
% R = 90 - 110%

Tanggal
24) Kromium Pengujian:
Alat :
Program :
Sampel % RPD
Paraf Analis
Duplo Cr Cr
1
2 #DIV/0!
Rata-rata #DIV/0!
Spike Matrix C.U non Spike Target Value
(E) (F) (G)
Duplo Cr Cr Cr
 1
2
Rata-rata
Catatan : % RPD = < 10%
% R = 90 - 110%
Tanggal
25) Kadmium Pengujian:
Alat :
Program :
Sampel % RPD
Paraf Analis
Duplo Cd Cd
1
2 #DIV/0!
Rata-rata #DIV/0!
Spike Matrix C.U non Spike Target Value
(E) (F) (G)
Duplo Cd Cd Cd
1
2
Rata-rata
Catatan : % RPD = < 10%
% R = 90 - 110%
Tanggal
26) Nikel Pengujian:
Alat :
Program :
Sampel % RPD
Paraf Analis
Duplo Ni Ni
1
2 #DIV/0!
Rata-rata #DIV/0!
Spike Matrix C.U non Spike Target Value
(E) (F) (G)
Duplo Ni Ni Ni
1
2
Rata-rata
Catatan : % RPD = < 10%
% R = 90 - 110%
Tanggal
27) E.Coli
Pengujian:
Sampel
Paraf Analis
1
2

Total
Koliform

Penyelia

……………….
Paraf
Analis

Paraf
Analis
 Paraf
Analis

+ Residu
D₂

D
+ Residu
D₂

Paraf Analis

Paraf
Analis
245
289

Paraf
Analis
Paraf
Analis
Paraf
Analis

Paraf
Analis

Paraf
Analis