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  • Core Practical 6 Chlorination of 2-Methylpropan-2-Ol With Concentrated Hydrochloric Acid - Lab Book

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    Amal Abu Khalil
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    Core Practical 6 Chlorination of 2-methylpropan-2-ol with concentrated hydrochloric acid_Lab Book

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    106 views3 pages

    Core Practical 6 Chlorination of 2-Methylpropan-2-Ol With Concentrated Hydrochloric Acid - Lab Book

    Uploaded by

    Amal Abu Khalil

    Copyright:

    © All Rights Reserved
    Download as PDF or read online from Scribd
    Flag for inappropriate content
    Download as pdf
    of 3
    URGE e Samii GTM WTa eaiTamn Mateos Vino tar uaa pastor. e a mst 1 Pour 10crm of 2-mettyipropan-20l nd 35cr of encentated © To produce ane purfyasample hydrochioncacdintoa large conical flask Very gery Sil the contents. yrocloncacd intoa age Very gent silt Clee eee eee 2 Pach bug in te mutt ask ey sal apse enove| pment tarp wrten te peau + beret Sekt mg 3 Conia suring ure the bing eed antennae |S senmcntme bn thepesueotowuda0minacsioustelesceowejenmne, | fou re ‘ask. The upper layer isthe crude product ‘© 250m? beaker for quid run « tilanzmf gtr maui rome |* atoms Tetetinie inept Bera srg erg tinePonstetncetnepetncerresteteaaay | temen the separating funnel, and release the carbon dioxide gas produced, at 2-methylpropan-2-ol 8 Run off and discard the lower layer, Ensure none of the aqueous layer /hydrogencarbonate solution ey ees 9 Run off the organic layer into a small conical flask. Add a full spatula calcium chloride (© pperetusfor dsiaton with Soe? pearshepes (or 25cm and 100m? measuring “inde ‘of anhycrous sodium sulfate Place the bung nthe Maskard sl the | @ anhyrous sodium sulfte ‘contents to mix Leave the mixture unl the iui looks completely clear, | « smal conta asks with bungs ‘snirting occasional, © sample tube 10 Decant the organic liguldinta a 0c? pear-shaped (or rounel-bottomed) - be * cosmo? ser tae AL Setup the ask for distilation 12 Gallet the fraction baling between SO%C and 52°C, 13. Place your pure preductinalabelled sample tobe. 14 Cary out the test described inthe Analy’ section of this prota. dist © mold) sodium tyro solution «ute O1motdn=) ni eid Toe conentaed Learning tps hyd as * The groupinon schlean berepace by ahelogen Asweasthe | test tubes method used hereto chlnte a ical, Plane use to make a * spatues

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