Asc-9800 SM Zesn-2004 e PDF

ZESN-2004
Shimadzu Autosampler for Inductively Coupled Plasma Emission

Spectroscopy
ASC-9800
Service Manual
Read this manual thoroughly before you use the product.
Keep this manual for future reference.
Contents
1. Introduction..................................................................................................................... 2
1.1 Overview ........................................................................................................................................ 2
1.2 Notice ............................................................................................................................................. 2
1.3 Warning Label ................................................................................................................................ 3
1.4 Safety Precautions ......................................................................................................................... 3
2. Installation Procedure ..................................................................................................... 5
2.1 Confirming Installation Site Requirements .................................................................................... 5
2.2 Checking Standard Accessories .................................................................................................... 5
2.3 Installation ...................................................................................................................................... 6
3. Acceptance Inspection Procedure .................................................................................. 7
4. Periodic Inspection ......................................................................................................... 8
4.1 Fuse Replacement ......................................................................................................................... 8
4.2 Spline Bearing Replacement ......................................................................................................... 8
4.3 Operation Check ............................................................................................................................ 8
5. Troubleshooting .............................................................................................................. 9
6. Adjustments for Disassembly and Reassembly ............................................................ 12
6.1 Launching the Adjustment Program ............................................................................................ 12
Tools Required for Adjustments ···············································································12
6.2 Disassembling the Arm Drive Unit and Adjusting the Shaft ........................................................ 14
6.3 Reassembling and Adjusting the Shaft ....................................................................................... 17
6.4 Adjusting Positioning After Reassembly (Using the adjustment program) ................................. 19
-1. Write data to the EEPROM (arm vertical position, arm rotational position, and turntable position).
······················································································································ 19
-2. Automatically register the optimal arm position. ··························································· 19
-3. Attach the plastic cover. ························································································ 19
-4. Attach the arm and turntable.·················································································· 20
-5. Register the arm vertical position ············································································· 21
-6. Confirm that the arm and turntable are attached properly.·············································· 21
-7. Operate the instrument continuously. (Perform this test as necessary.) ····························· 22
-8. Other operations ································································································· 24
7. Disassembling the Main Unit and Part Numbers .......................................................... 25
8. Disassembly and Part Numbers for Each Unit ............................................................. 26
9. Consumable and Maintenance Parts Indicated in the ASC-9800 Instruction Manual ... 29
10. Mounting the Nozzle ..................................................................................................... 30
11. Piping Diagram ............................................................................................................. 30
12. ASC-9800 Total Wiring ................................................................................................. 31
1
1. Introduction
1.1 Overview
The ASC-9800 autosampler is designed to be operated linked to a Shimadzu ICPE-9800 series
multitype ICP emission spectrometer.
1.2 Notice
Specific service training is required to use this service manual properly. We cannot take
responsibility for any problems caused by personnel using this manual without proper service
training.
The manual may include figures or photographs of the ASC-7000, which differ slightly
from the ASC-9800, but they are only intended to explain functionality.
2
1.3 Warning Label
The following label is used on the ASC-9800.
This warning label is attached to the top of the sampler. It cautions the operator to be careful not
to get chemicals on their hands or their hands or fingers pinched if they touch the arm while it is
moving.
1.4 Safety Precautions

1.4.1 Electric Shock
(1) Areas that Remain Powered ON (at Power Supply Voltage) Even When the Power Switch is OFF
 Wiring between the AC inlet and power switch
Always shut off the power supply to the system before touching this area.
Be careful to prevent conductive accessories (such as rings or necklaces) from contacting
high-voltage areas.
(2) Areas with High Voltage When the Power Switch is ON

In addition to the above:
 Wiring from the power switch to the switching power supply
 Components on the switching power supply unit
When checking autosampler actions with the controller cover open and power ON, be sure to
wear electrical gloves to protect from electric shock.
Be careful to prevent conductive accessories (such as rings or necklaces) from contacting
high-voltage areas.
3
(3) Liquids in Flow Lines
Be sure to remove any liquid (reagents and rinse solution) from flow lines and the turntable
before performing maintenance with the cover open. Spilling such liquids may cause a short
circuit.
(4) Safety Inspection After Finishing Operations

After switching the power ON, use an electrical tester to test exterior metal surfaces (such as the
frame and CPU board communication cable fastening screws) for any voltage (both AC and DC)
relative to ground.
1.4.2 Precautions for Installation

(1) Screw Tips
When lifting the unit, be careful of injury from screw tips protruding from the bottom of the
instrument.
4
2. Installation Procedure
The ASC-9800 is fully inspected before it is shipped from the factory. To ensure the customer can
achieve adequate performance and is satisfied with the instrument, install the instrument according
to the following procedure.
2.1 Confirming Installation Site Requirements

Before installing the ASC-9800 unit, read the "Safety instructions" regarding installation and
operation in the introductory chapter and "3. Installation" in the ASC-9800 Instruction Manual.
Remove the main ASC-9800 unit from the packing carton and the accessories from their bag and
then install the main unit.
(Remove any packing parts.)
2.2 Checking Standard Accessories

To avoid unnecessary problems with the user, refer to "2. Parts" in the ASC-9800 Instruction
Manual to verify, together with the user, that all standard accessory parts are present.
No. Description P/N Q'ty

1 Sampler ASSY S211-87800-41 1
2 Accessories, ASC-9800 --- 1
-1 Cable,RS-232C 9PIN S206-50325-91 1
-2 Bottle, Drilling S206-87284-91 2

-3 Nozzle ASSY, F S206-50290-91 1
-4 Connection tube S211-83697 2
-5 Snap vial, No. 30 S200-93113-05 8
3 Report, Certificate of Compliance ASC-9800 S206-84934-77 1
4 Procedure, Certificate of Compliance S228-30164 1

5 Explanation Document, Certificate of Compliance S465-06072 1
6 IM, ASC-9800 J S305-34215 1

7 IM, ASC-9800 E S305-34216 1
8 Label. Assurance Label 53X34 S037-70238-01 1
5
2.3 Installation
Install the ASC-9800 system according to the following guidelines and by referring to 4.3 to 6.4 in
the ASC-9800 Instruction Manual.
Connecting the Power Supply and Control Cables

1. Connect the power and control cables.
Power switch
ICPE-9800
connector panel
Power switch
Control cable
Note: Type of power cable:

Description P/N Remarks
Cord, UC-975-N01 S071-60821-08 Power cable, 125 VAC/13 A
Cord Set, PHP-206S+PHS-301 2.4M S071-60825-51 Power cable, 250 VAC/10 A
Cord, KP-722+KS-31A 2.4M S071-60827-05 Power cable, 250 VAC/10 A (China)
2. Fill the rinse solution bottle with rinse solution and insert the tip of the rinse solution supply
tube into the rinse solution.
3. Insert the tip of the drain tube into the waste liquid tank.
4. Connect the power cable to the power supply.
5. Switch ON the ASC-9800 power. (The system performs initialization. Refer to 6.3 in the
ASC-9800 Instruction Manual.)
6. Install the nozzle. (Refer to 6.4 in the ASC-9800 Instruction Manual.)
7. Confirm that the autosampler can be controlled properly from the main ICPE-9800 unit.
-1. Launch ICPEsolution and specify the ASC-9800 model in the [Configuration settings]
window. (Refer to 1.3 in the ICPEsolution Instruction Manual.)
-2. Select a suitable method and ignite the plasma. When the autosampler is in the R0 (rinse)
position, the rinse pump switches ON.
-3. In the [Instrument Control] window, set [Auto Sampler] – [Nozzle Destination] to "A1."
Then the autosampler moves to the A1 (auxiliary rinse) position, and the auxiliary rinsing
pump switches ON.
6
-4. Check all flow lines for any leakage.
-5. In the [Instrument Control] window, set [Auto Sampler] – [Nozzle Destination] to "01."
-6. Make sure the nozzle is positioned properly at the test tube in position 01.
8. If the unit functions normally, switch the ASC power OFF.
3. Acceptance Inspection Procedure

After installing the ASC-9800, check the following items together with the user to make sure they
satisfy the given standards.
Item Pass Criteria

External appearance No scratches, dirty areas, and so on
Contents No missing parts
Flow Line Inspection No leakage
Operation Check Nozzle moves to and stops at specified port
7
4. Periodic Inspection
To ensure safe use of the instrument and maintain instrument performance, perform daily and
periodical inspections according to "7. Maintenance" in the ASC-9800 Instruction Manual. Also
replace periodic replacement parts. Of the parts in the periodic replacement list, only the two types
of peristaltic pumps must be replaced by a service engineer.
Also perform the following, in addition to the above.
4.1 Fuse Replacement

Replace the fuse in the power supply inlet about once every three years, due to deterioration over
time (see section 8 in this manual).
4.2 Spline Bearing Replacement

Replace the spline bearing (P/N 206-50048-03) when wear on the spline bearing increases arm
play (see section 6 in this manual).
4.3 Operation Check

After performing the above inspections, check the unit operation according to sections 2.3.2 to
2.3.8 of this manual.
8
5. Troubleshooting
Note: If the arm or turntable shifts out of position, set it to sample 01 (instrument control) and
adjust the position (fix the arm or turntable position).
If that is unsuccessful, it must be adjusted using the adjustment program.
Symptoms Cause / Details Corrective Measures

The nozzle does not Nozzle is not long enough. Adjust nozzle length.
reach the sample. (Refer to 6.4 in the ASC-9800 Instruction
Manual.)
There is not enough sample. Prepare sufficient quantity of sample.
Nozzle is not inserted Arm fasteners are loose. Tighten arm fastening screws.
properly into (See section 6 in this manual.)
samples. Arm play is excessive. Arm rotation belt tension is too loose.
Arm vertical movement belt tension is too
loose.
(See section 6 in this manual.)
Turntable fastening screws are Tighten the turntable fastening screws.
loose. (See section 6 in this manual.)
Arm position recorded in system Adjust it using the adjustment program.
is poor. (See section 6 in this manual.)
The spline bearing is worn, Replace the spline bearing (206-50048-03).
resulting in excessive play. (See section 6 in this manual.)
The motor is out of The arm vertical movement shaft Readjust the arm vertical movement shaft.
step in vertical arm is out of alignment. (See section 6 in this manual.)
movement. The spline bearing is worn. Replace the spline bearing (206-50048-03).
A part for vertical arm movement Replace the vertical arm movement motor.
has failed. Replace the vertical arm movement belt.
The motor is out of Arm resists rotation. Arm rotation belt tension is too tight.
step in arm rotation. (See section 6 in this manual.)
A part for arm rotation has failed. Replace the arm rotation motor.
Replace the arm rotation belt.
The motor is out of The turntable movement is too Adjust the turntable drive belt tension. (See
step in turntable stiff. section 6 in this manual.)
operation. A part in the turntable drive unit Replace the motor in the turntable drive
has failed. unit.
Replace the belt in the turntable drive unit.
9
The tip of the nozzle Replace the nozzle assembly PTFE tube
assembly PTFE tube for F (S206-50290-91).
for F is dirty or bent.
The fuse blows. Faulty switching power supply Replace the switching power supply
(074-80441-35). (See section 8 in this
manual.)
End of fuse service life Replace the fuse (072-02004-21).
The peristaltic pump End of peristaltic pump tube Replace the peristaltic pump tube
tube ruptured. service life (042-00405-24). (Refer to 7.3 in the
ASC-9800 Instruction Manual.)
If an organic solvent is used as the rinse
solution, then it must be replaced frequently
(daily or at least once a week).
The rinse solution End of peristaltic pump tube Replace the peristaltic pump tube
flowrate decreases service life (042-00405-24).
significantly. (See section 8 in this manual.)
End of peristaltic pump service Replace the peristaltic pump
life (206-77590-92).
Air bubbles are Rinse the flow line.
forming inside the (See section 10 in this manual.)
flow line.
The LED does not Faulty LED Replace the LED (208-94012-92).
illuminate. (See section 8 in this manual.)
The fan does not Faulty fan Replace the fan (206-77621-91) of the unit
rotate. in question.
The fuse blows. Faulty switching power supply Replace the switching power supply
(074-80383-38). (See section 8 in this
manual.)
End of fuse service life Replace the fuse (072-02004-21).
Cannot connect to The ASC-9800 power is not Switch ON the power.
the ASC unit. switched ON.
(Cannot initialize or Faulty controller CPU board Replace the PCB_9K2_ASC board
connect options.) (211-87930-41). (See section 8 in this
manual.)
Faulty ICPE-9800 CPU board Replace the ICPE-9800 CPU board
(211-87900-41).
Faulty RS-232 cable Replace the cable (206-50325-91).
10
Initialization is not EEPROM data is corrupted. Try readjusting using the adjustment
performed. program.
The ASC-9800 is in the boot mode. If the J101 connector on the CPU board
of the unit in question is short-circuited,
correct the circuit so that it is open.
An error has occurred. Try sending the ERR command (for

canceling the error log during continuous
operation) using the adjustment
program.
11
6. Adjustments for Disassembly and Reassembly
6.1 Launching the Adjustment Program

Tools Required for Adjustments
 Computer (with Japanese version Windows 95/98/NT4/2000/XP/Vista/7 and a serial port)
 Copy the ASC adjustment program ("ASC7061W13.zip") to the computer (same for
ASC-7000/6100/9800 models).
 RS-232C cable (P/N 206-50325-91)
 Power cable (P/N 071-60821-08 or compatible model)
 Turntable cover (P/N 206-50295-01)
 Nozzle assembly for F (P/N 206-50290-91)
 Two rinse solution supply bottles (P/N 206-87284-91)
 Container for recovering rinse solution (P/N 038-00516-06)
 Distilled water (distilled water is preferable, by ion-exchange water is acceptable)
Preparation Before Adjustments

1. Connect the computer to the ASC-9800 using the control cable (RS-232C).
2. Plug the power cable into the ASC-9800 unit and switch the ASC-9800 power switch ON.
The arm moves up and down and the turntable shaft rotates as part of initialization and then
they stop.
3. Launch the adjustment program ("ASC7061W.exe").
Note: The program cannot launch until ASC-9800 initialization is finished.
The following menu is displayed on the computer screen.

============================================================
COM Port No. (1-4)?
============================================================
Note: Normally select "1."
(1) Press the [ENTER] key.
Next, a menu of instrument models is displayed.

============================================================
ASC-7000/6880/9800/6100 Adjustment Program for Windows Ver.1.3
(Press Ctrl+C 2 times and restart it if the program locked up.)
1 ----- ASC-7000/6880 adjustment.

2 ----- ASC-6100 adjustment.
3 ----- ASC-9800 adjustment.
99 ---- Send commands.
Q ----- Quit this program.
-------------------------------------------------------------
Select item?
============================================================
Note: In this case, select "3" to display the following menu.
(3) Press the [ENTER] key.
12
============================================================
ASC-9800 Adjustment Program for Windows Ver.1.3
(Press Ctrl+C 2 times and restart if the program locked up.)
0 ----- Set initial parameters.

1 ----- Automatic positioning about arm rotation.
2 ----- Attach the arm and the turntable.
3 ----- Teach up/down position of arm for FLAME.
4 ----- Position check of the arm and the turntable.
5 ----- Check leakage around pumps.
20 ---- Set serial number.

21 ---- Check firmware version.
B/R --- Back up / Recover EEPROM parameters.
--------------------------------------------------------------------
Select item?
============================================================
The above menu switches to the ASC-9800 maintenance menu.
13
6.2 Disassembling the Arm Drive Unit and Adjusting the Shaft
If parts were replaced or the main ASC-9800 unit was disassembled, then adjustments
must be made using the adjustment program.
1. Detach the O-ring on the upper part of the arm, loosen the screws that fasten the arm, and
detach the arm.
2. Remove the turntable by removing the knurled screw from the center of the turntable.
3. Remove the support by loosening the two screws to the side of the support using a hex
wrench.
Enlarged View of Support Support
M2 Hex screw
14
4. Remove the rivets that fasten the autosampler cover. Turn the rivet using a Phillips
screwdriver so that the rivet protrudes slightly, as shown below. Pull out the rivet.
Rivet
A total of six rivets are installed, one on the right side (white), one on the back (black), and
four on the bottom (black).
5. Lift off the autosampler assembly cover.
15
6. Remove the four screws that fasten the shaft drive unit and remove the unit from the frame
with the cables still connected.
(It can be removed by unfastening the cable ties used to bundle the cables.)
7. Remove the retainer plate and loosen the arm rotation motor screws.
Retainer plate screw Arm rotation motor screws
8. Remove the screw that fastens the vertical movement belt to the shaft so that the shaft moves
freely.
The bearing, pulley, spline, belt, and other parts can be replaced by pulling the shaft out.
Bearing
Belt
Pulley
Spline
Bearing
16
6.3 Reassembling and Adjusting the Shaft
1. Gradually tighten the screws of the upper/lower angle assemblies, while checking that the
shaft can slide down under its own weight. Rotate the shaft and check that it moves up and
down at 3 or 4 positions.
Angle assembly screws
2. Fasten the retainer plate in place with screws so that it lightly contacts the pulley assembly,
and check that the arm moves down under its own weight. Then rotate the shaft again to
check it at 3 or 4 positions. (The shaft rotation belt should be loose at this point.)
Retainer plate
3. Adjust the shaft rotation motor position and fasten it in place with screws so that there is no
slack on the shaft rotation belt.
Adjust the motor position so that the shaft can slide up and down as easily as possible in any
position. (If the belt tension is too loose, it will cause a motor step-out error.)
Arm rotation motor screws
17
4. Install the screw that fastens the vertical arm movement belt to the shaft.
5. Reinstall the arm drive unit in the frame.
18
6.4 Adjusting Positioning After Reassembly (Using the adjustment program)
Display the adjustment program menu by referring to "Preparation Before Adjustments" above.
Make adjustments in the follow sequence.

============================================================


--------------------------------------------------------------------
Select item?
-1. Write data to the EEPROM (arm vertical position, arm rotational position, and turntable
position).
"0" (0 ----- Set initial parameters) on the menu
When "Select item?" is displayed, press [0] and [ENTER].
After it writes items WRITE 0 to WRITE 107, the turntable and arm rotate to initialize their origin
positions. Then the menu screen is displayed again.
Note: Skipping this step will cause a slip error. If that occurs, switch ON the power again and do
this step first.
(This step is also required if the control board is replaced in the ASC-9800 unit.)
-2. Automatically register the optimal arm position.

"1" (1 ----- Automatic positioning about arm rotation) on the menu
When "Select item?" is displayed, press [1] and [ENTER].
The arm automatically moves to and registers each position.
After the positions are registered, the menu screen is displayed again.
-3. Attach the plastic cover.

1. Install a fluoropolymer washer on the arm shaft.
2. Attach the plastic cover and fasten it with six rivets.
3. Attach the support. (Leave the two screws loose.)
19
-4. Attach the arm and turntable.
1. "2" ("2 ----- Attach the arm and the turntable.) on the menu
2. Fasten the turntable with the knurled screw. (Orient the turntable with the wavy side upward.)
Fasten the knurled screw with the turntable and support aligned with the dowel pin.
3. When "Select item?" appears, press [2] and [ENTER].
4. When the arm shaft and turntable rotate and the arm moves down to turntable position 1, the
following message is displayed. Follow its instructions. Attach the arm.
===========================================================
Attach the arm and the turntable at sample #1.
After attaching them, hit space bar.
===========================================================
5. Install the arm on the arm shaft.

6. Align the arm angle with the sample #1 position on the turntable and then fasten it in place.
Align the arm and turntable so that the nozzle aligns with the midpoint of the #1 position on the
turntable.
Fasten the turntable using the two hex screws on the side.
(Attach the nozzle assembly to make it easier to determine the midpoint position.)
Pressing the space bar displays the menu screen again.
M2 Hex screw
M2 Hex screw
7. Next, align the arm position with sample position 1 and fasten the arm fastening screws.
After installation, pressing the space bar on the computer displays the Menu screen again.
Click [2] and [Enter] again to reconfirm the arm position.
20
-5. Register the arm vertical position
"3" (3 ----- Teach up/down position of arm for FLAME) on the menu
When "Select item?" appears, press [3] and [ENTER].
When the following message appears, follow its instructions.
===========================================================
Set the turntable for flame side and hit space bar.
===========================================================
When the arm moves down to the R1 position on the turntable and the following message appears,
follow its instructions.
===========================================================
Is arm position OK here for flame? (up/down)
Arm
1 --- Move the arm upward.
8m
16mm
2 --- Move the arm downward.
3 --- OK Case
-----------------------------------------
Select item?
===========================================================
Keep adjusting the position up or down until the distance from the bottom of the arm and to the
plastic case (near the arm shaft) is 8 mm.
To do that, either press [1] and [ENTER] or [2] and [ENTER].
When the position is acceptable, press [3] (3 --- OK) and [ENTER].
Confirm that the arm moves to turntable positions #1, #31, and R1, the auxiliary rinse port, and the
rinse port.
The menu screen is displayed.
-6. Confirm that the arm and turntable are attached properly.
"4" (4 ----- Position check of the arm and the turntable.") on the menu
When "Select item?" appears, press [4] and [ENTER].
Confirm that the arm moves back and forth to turntable positions #1, #31, and R1, the auxiliary
rinse port, and the rinse port.
21
The menu screen is displayed.
============================================================


--------------------------------------------------------------------
Select item?
-7. Operate the instrument continuously. (Perform this test as necessary.)

Entering the command described below allows confirmation of the vertical arm movement to each
position. Remove any sample cups and nozzles in advance.
When "Select item?" appears, enter "99" and press [ENTER].

When the following message appears, follow its instructions.
===========================================================
Check Mode
Command= ?
===========================================================
At the "Command=" prompt, enter "TEST" and press [ENTER].

This will cause the instrument to keep repeating the following actions. Switch the power switch
OFF to stop the process.
Arm moves to turntable position R1 and moves up and down.

Arm moves to turntable position #52 and moves up and down.
Arm moves to the auxiliary rinse port and moves up and down.
Arm moves to the rinse port and moves up and down.
Arm moves up and down at the rinse port.
Arm moves to the auxiliary rinse port and moves up and down.
22
Arm moves to turntable position R5 and moves down.
The arm returns to START position (1) and then continues repeating the above cycle.
Once the continuous operation starts, disconnect the RS-232C cable from between the ASC unit
and computer. The system will continue running in the continuous operation mode.
Confirm there are no problems.
If a problem occurs during continuous operation that stops the process (such as the arm rotation
motor step-out), switch the ASC power ON and restart the adjustment and inspection program
again. When the following message appears, follow its instructions.
===========================================================
Arm rotation motor slipped!
Press space bar when you confirm it.
If you cancel the continuous moving error, press E
and input ERR as a command.
===========================================================
Press the [E] key. The following message is displayed.

===========================================================
Check Mode
Command= ?
===========================================================
Enter "ERR" and press [ENTER].

===========================================================
This program will stop within 10 seconds. Restart the program
===========================================================
The ASC unit operates and the menu screen is displayed. Eliminate the cause of the problem and
check the operation again.
23
-8. Other operations
============================================================


--------------------------------------------------------------------
Select item?
============================================================
Entering "20" and pressing [ENTER] (20 ---- Set serial number.) allows confirmation of the serial
number, but it cannot be changed.
Entering "21" and pressing [ENTER] (21 ---- Check firmware version) allows confirmation of the
firmware version number.

"B" + [ENTER]: Saves a backup of currently recorded parameter information.
"R" + [ENTER]: Writes parameter information from a file to the EEPROM.
Parameter information is recorded in the "ASC9800.DAT" file, which is stored in the same
folder as the "ASC7061W.exe" program.
Use this DAT file if the ASC-9800 CPU board is replaced.
Enter "Q" and press [ENTER] (Q ----- Quit this program.) to quit the maintenance program.
24
ZESN-2004
7. Disassembling the Main Unit and Part Numbers
206-50295`COVER
037-02881-03`KNOB
206-50062`TURN_TABLE
020-46148`ZNJ_SA_M4x10
206-50278ÀRM
206-50060`SUPPORTER
026-66206`RING_E
021-04636`ZNJ_SW_M4x10
206-50295`COVER
020-37012-31`SCREW_M4X6
037-51344-02`FASTENER 037-51344-01`FASTENER
211-88568`REAR_PANEL
037-51344-02`FASTENER
037-51344-02`FASTENER
037-51344-02`FASTENER
25
8. Disassembly and Part Numbers for Each Unit
211-88567`PORT_SAMPLER
206-50041-42ÀRM_DRIVE
206-50054-42`TURN_TABLE_DRIVE
037-30031-05`RUBBER
211-88871-41`PUMP_ASC(RINSE)
211-88861-41`FAN_ASC
211-88871-42`PUMP_ASC(AUX)
211-87930-41`PCB_9K2_ASC
064-14543-12`SW_A8L21_15N3 074-80441-35`POWER_SUPPLY_LFA50F-24
072-02004-21_Fuse 075-00138-03`Socket_FN9260
26
026-66206_RETAINING
208-90705_PULLEY
206-77556_WASHER_ARM
SENSOR_208-94013-93 BELT_032-22478-33
ANGLE_ASSY_206-51131
BUSHING_031-40316
PULLEY_208-90704
ASSY_PULLEY_206-50047 208-96126_MOTOR
SLIT_DISK_ARM_206-50049
SPLIN_206-50048-03
206-51110_PLATE
ANGLE_ASSY_206-51131 BUSHING_031-40316
SENSOR_208-94013-92
206-50051_SHAFT_ARM
228-24150-01_MOTOR
206-50041-42ÀRM_DRIVE_ASSY
BEARIMG_031-40232
AXIS_PULLEY_206-50046
PULLEY_S3M_208-90708
ARM_PULLEY_206-51109 BEARIMG_031-40232
BEARING_031-20613
PLATE_GLUED_206-50057 FASTENER_206-50053
BELT_032-21979-31
27
206-50058`SHAFT
211-88869`MOTOR
030-03000`BRG_6000ZZ
032-22472-31`BELT_B100S3M276-G
206-50054-42`TURN_TABLE_DRIVE
030-03000`BRG_6000ZZ
208-90706`PULLEY_S3M60
208-94013-91_SENSOR_WITH_WIRE
206-50059`SLIT_DISK
211-88871-42`PUMP_ASC(AUX) 211-88871-41`PUMP_ASC(RINSE)
211-88567`PORT_SAMPLER
206-50406-42`TUBE_ASSY_AUX 206-50406-41`TUBE_ASSY_RINSE
211-92492-42TUBE_ASSY_AUX 211-92492-41TUBE_ASSY_RINSE
035-65011`HALF_UNION_HZ
206-87284-91_Bottle, Drilling
016-43203`PE_TUBE_4X1.1
038-00516-06_Polyurethane container
28
9. Consumable and Maintenance Parts Indicated in the ASC-9800 Instruction
Manual
Pump tube_S042-00405-24 Pump head_S042-00405-11 Shaft bearing, spline_S206-50048-03
211-88871-41`PUMP_ASC(RINSE) 211-88871-42`PUMP_ASC(AUX) Filter_S211-88565

フィルター
カバー
Test tube, ET-16_S046-00147-04 Snap vial, No. 30_S200-93113-05 Rinse solution bottle_S206-87284-91
Turntable_S206-50062 Turntable cover_S206-50295-01 Nozzle ASSY, F_S206-50290-91
Fuse_S072-02004-21 Test tube,S046-00150-27 Connection tube_S211-83697
Polyurethane container_S038-00516-06 Cable,RS-232C 9PIN_S206-50325-91

Cord Set 2.4M (Europe)_S071-60825-51
Cord Set 2.4M (China)_S071-60827-05
29
10. Mounting the Nozzle
Nozzle fixing Arm

screw
103 Nozzle
11. Piping Diagram
Nozzle Connection tube

Nebulizer
Auxiliary rinsing port

Rinsing ports
To waste liquid container To waste liquid container
Auxiliary rinse solution Rinse solution

supply pump supply pump
Auxiliary rinse Rinse solution

solution
30
ZESN-2004
12. ASC-9800 Total Wiring
Home position sensor

Pump
Arm
Arm Arm
Arm Turntable motor
up/do Turntable
rotati up/down
rotation
on wn
Switching
Power switch power supply
HP Sensor, Arm Up/Down

HP Sensor, Arm Rotation
HP Sensor, Turntable
Arm vertical
Motor, Turntable
Locker ABL-21-15N3
movement
motor
Arm rotation
(Optional)
motor
Motor, Arm Up/Down

(Optional)
Motor, PK243M-01A-C34
(Debugger)
(Debugger)
(Debugger)
Main unit
31

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ZESN-2004

Shimadzu Autosampler for Inductively Coupled Plasma Emission

1.4 Safety Precautions

(2) Areas with High Voltage When the Power Switch is ON

(4) Safety Inspection After Finishing Operations

1.4.2 Precautions for Installation

2.1 Confirming Installation Site Requirements

2.2 Checking Standard Accessories

No. Description P/N Q'ty

-2 Bottle, Drilling S206-87284-91 2

3 Report, Certificate of Compliance ASC-9800 S206-84934-77 1

4 Procedure, Certificate of Compliance S228-30164 1

6 IM, ASC-9800 J S305-34215 1

Connecting the Power Supply and Control Cables

Note: Type of power cable:

3. Acceptance Inspection Procedure

Item Pass Criteria

4.1 Fuse Replacement

4.2 Spline Bearing Replacement

4.3 Operation Check

Symptoms Cause / Details Corrective Measures

An error has occurred. Try sending the ERR command (for

6.1 Launching the Adjustment Program

Preparation Before Adjustments

Note: The program cannot launch until ASC-9800 initialization is finished.

The following menu is displayed on the computer screen.

Next, a menu of instrument models is displayed.

1 ----- ASC-7000/6880 adjustment.

0 ----- Set initial parameters.

20 ---- Set serial number.

The above menu switches to the ASC-9800 maintenance menu.

Enlarged View of Support Support

5. Lift off the autosampler assembly cover.

Retainer plate screw Arm rotation motor screws

Angle assembly screws

Arm rotation motor screws

5. Reinstall the arm drive unit in the frame.

Make adjustments in the follow sequence.

0 ----- Set initial parameters.

20 ---- Set serial number.

-2. Automatically register the optimal arm position.

-3. Attach the plastic cover.

5. Install the arm on the arm shaft.

Pressing the space bar displays the menu screen again.

0 ----- Set initial parameters.

20 ---- Set serial number.

-7. Operate the instrument continuously. (Perform this test as necessary.)

When "Select item?" appears, enter "99" and press [ENTER].

At the "Command=" prompt, enter "TEST" and press [ENTER].

Arm moves to turntable position R1 and moves up and down.

Press the [E] key. The following message is displayed.

Enter "ERR" and press [ENTER].

0 ----- Set initial parameters.

20 ---- Set serial number.

B/R --- Back up / Recover EEPROM parameters.

7. Disassembling the Main Unit and Part Numbers

211-88871-41`PUMP_ASC(RINSE) 211-88871-42`PUMP_ASC(AUX) Filter_S211-88565

Turntable_S206-50062 Turntable cover_S206-50295-01 Nozzle ASSY, F_S206-50290-91

Fuse_S072-02004-21 Test tube,S046-00150-27 Connection tube_S211-83697

Polyurethane container_S038-00516-06 Cable,RS-232C 9PIN_S206-50325-91

Cord Set 2.4M (China)_S071-60827-05

Nozzle fixing Arm