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Journal of Materials Processing Tech.

277 (2020) 116482

Contents lists available at ScienceDirect

Journal of Materials Processing Tech.


journal homepage: www.elsevier.com/locate/jmatprotec

Mechanical behavior of FSW joint welded by a novel designed stationary T


shoulder tool
Sunil Sinhmar*, Dheerendra Kumar Dwivedi
Mechanical & Industrial Engineering Department, Indian Institute of Technology Roorkee, Roorkee 247667, Uttarakhand, India

A R T I C LE I N FO A B S T R A C T

Associate Editor: R Mishra A novel stationary shoulder friction stir welding (SSFSW) tool was developed with provision for automatic
Keywords: removal of plasticized material entering into the shoulder during the welding. Main objective of this tool design
Aluminium was to obtain a symmetrical weld joint with narrow heat affected zone. Mechanical and metallurgical properties
Stationary shoulder of AA2014 aluminium alloy SSFSW joint were compared with the conventional FSW joint. Sound weld joint with
Friction stir welding enhanced mechanical properties were obtained by the stationary shoulder tool. Optical microscopy, FESEM
Heat generation analysis along with EDS, transmission electron microscopy, XRD analysis, microhardness and toughness test
Mechanical properties were performed on both types of weld joint. Weld thermal cycle and heat generation were analyzed for sta-
tionary shoulder and conventional FSW tool and it was found that the SSFSW tool shoulder generates lesser heat
than conventional FSW tool.

1. Introduction and recrystallization is called nugget zone (NZ). Region next to the NZ
which experiences the thermal cycles along with the mechanical force
Friction stir welding was developed in 1991 and it became popular and shows deformed grains is called thermo-mechanical affected zone
among the researchers all over the world. Number of variants has been (TMAZ). Heat affected zone (HAZ) experiences only microstructural
developed for friction stir welding. Most of the variants were related to variation due to heat without any effect of plastic deformation.
the tool design. Recently, a new variant with stationary/non-rotating Stationary shoulder FSW was developed in early 2005 by TWI
shoulder came into picture. Earlier, it was assumed that a rotating (Martin et al., 2011). Initially, stationary shoulder was used for FSW of
shoulder is necessary to produce a sound FSW joint. Development of the Ti alloys to reduce the temperature gradient along the thickness due to
stationary shoulder friction stir welding (SSFSW) tool has changed this low thermal conductivity (Davies et al., 2011). Development of fillet
notion. and corner joints was found to be easier with SSFSW than the con-
Conventional FSW (CFSW) tool uses a rotational shoulder which ventional FSW. Widener et al. (2006) investigated that the fatigue life
produces large amount of heat input, which in turn leads to a wider of AA7075 SSFSW joint enhanced due to higher compressive stress than
heat affected zone (HAZ). Generally, heat affected zone of the alumi- the conventional FSW. Ahmed et al. (2011) found that the stationary
nium alloys (especially heat treatable) shows degradation in the various shoulder tool enhanced the formability of AA6082. Non-rotating
mechanical properties as well as corrosion performance. Rotation of the shoulder reduced the width of the TMAZ and improved the mechanical
shoulder in SSFSW is restricted, which facilitates the welding very low properties of the AA2219 weld joint. Liu et al. (2013) found that the
heat input and narrow HAZ. Moreover, SSFSW tool produces almost non-rotating shoulder reduced the asymmetricity and heterogeneity of
symmetrical weld joint with little or no flash (Ji et al., 2014). Thinning the weld joint. Effect of the rotational and traverse speed was in-
of cross-section of the SSFSW joint was found negligible as compared to vestigated on the stationary shoulder FSW of AA6061. Li et al. (2014)
the conventional FSW joint (Martin, 2013). Stationary shoulder slides observed that the rotational speed was more effective on joint proper-
over the plates during the SSFSW which gives smooth upper surface as ties than the traverse speed. Wu et al. (2015) compared the conven-
compared to the rotating tool (Li et al., 2015). Different zones formed in tional FSW and SSFSW of AA7050 using experimental and simulation
a SSFSW joint are similar to conventional FSW joint. These zones are studies and it was observed that SSFSW required 30% less heat input
more symmetrical and narrower than the conventional FSW joint. Re- than the conventional FSW. Ji et al. (2015) performed vertical com-
gion at the abutting surface which experiences the plastic deformation pensation FSW using interlayer (1–2 mm thickness) of AA2024 in the


Corresponding author.
E-mail addresses: sun25.dme2014@iitr.ac.in, ssinhmar@me.iitr.ac.in (S. Sinhmar).

https://doi.org/10.1016/j.jmatprotec.2019.116482
Received 28 December 2018; Received in revised form 20 September 2019; Accepted 27 October 2019
Available online 04 November 2019
0924-0136/ © 2019 Elsevier B.V. All rights reserved.
S. Sinhmar and D.K. Dwivedi Journal of Materials Processing Tech. 277 (2020) 116482

gap between two plates of AA6061 and it was observed that the SSFSW temperature was measured during the welding at 5 mm and 10 mm
was better than the conventional FSW. Sun et al. (2016) investigated distance away from the center of the weld using K-type thermocouple
the properties of different zones of SSFSW joint (AA6061) and found wires. Holes of 1.5 mm diameter and 3 mm depth were drilled at the
that the HAZ possess lower strength and toughness than the other back side of the plates. Thermocouple wires were inserted and fixed in
zones. Sun et al. (2017) found that the longitudinal residual stress was the drilled hole. A backing plate with special slots was prepared to
lower in SSFSW than the conventional FSW (bead on plate of AA7010) adjust the thermocouples wires during the welding. Data acquisition
and ‘M’ shape residual stress profile was observed in both cases. system (Make – National Instruments, NI 9211) was used for data re-
Despite having number of advantages of SSFSW over conventional cording. Microhardness study was performed on the transverse cross-
FSW, stationary shoulder friction stir welding has not been prominently section of the weld joints using Vicker’s microhardness tester. Load for
used due to the issue related with the extrusion and sticking of the the microhardness testing was kept 100 g for the dwell time of 10 s.
material into the stationary shoulder and overheating during the Distance between two consecutive indentations was kept 0.5 mm.
welding. Due to the limitation of ingress of plasticized material, these Indentations were taken at the mid-thickness of the weld joint. Samples
tools need cleaning and hence, cannot be used continuously for long for the tensile testing were prepared along the transverse direction of
run weld. Current tool design is free from the problem of overheating the weld joint and nugget zone was kept in center. Tensile testing was
and ingress of plasticized material. It can be the best replacement of the performed using universal testing machine (UTM) of ‘Instron USA, M-
earlier used stationary shoulder tool which were facing material ingress 5980’. Capacity of the UTM was 100 kN at room temperature.
problem. Additionally, presented tool design prevents the formation of Crosshead speed rate was kept 0.5 mm/min during the testing.
the wide HAZ and offer improved mechanical properties. Fractured surfaces were analyzed using FESEM. Tensile test samples
were tested in triplicate and prepared according to ASTM E8. Charpy
2. Experimental procedure impact test was performed to study the toughness of the weld joints.
Two samples were prepared for each of NZ and HAZ of the both type of
AA2014 aluminium alloy plate of 6 mm thickness was used for the weld joints. Samples were prepared according to the ASTM E23 and in
friction stir welding. Plate was machined to the dimension of the transverse direction of the weld joint. Nugget zone was kept in the
70 mm x 50 mm x 6 mm. Welding was performed in butt joint config- center of sample to determine the toughness of this region. Similarly,
uration. A vertical milling machine was used for the welding. Both heat affected zone was kept in the center of sample to determine the
plates were cleaned and firmly clamped in the fixture. A non-consum- toughness of this region. V-notch was machined at the center of the
able rotating tool of ‘H13 tool steel’ was used for the conventional FSW. sample and the depth of the notch was kept 2 mm. Length, width and
FSW tool comprises pin and shoulder as its major components. Relative thickness of the toughness samples were kept 55 mm, 10 mm and 5 mm,
size of the pin and shoulder of the FSW tool is the main design aspect respectively. Fractured surface was analyzed using FESEM. All the tests
from heating point of view (Mishra and Ma, 2005). Schematic and were carried out at room temperature.
details of the SSFSW tool are given in next section. Welding process
parameters were kept same for the both type of welding. Process 3. Results
parameters and tool details are shown in Table 1. SSFSW tool was
plunged in the same way as the conventional FSW tool until the sta- 3.1. Development of SSFSW tool
tionary shoulder of the tool touched to the plate to be welded. Dwell
time (it is the time after plunge of the rotating tool before traverse) for An indigenous tool with stationary shoulder was developed for FSW
the conventional FSW was kept 60 s while it was kept 90 s for the with facility of automatic cleaning of the plasticized material entered
SSFSW joint. Sample from the transverse direction of the weld joint was through the gap between rotating shoulder and stationary shoulder
cut for the microstructural analysis. Sample was ground and polished without overheating of tool. Schematic of the SSFSW tool is shown in
upto 2000 grade emery paper. Rough and fine cloth polishing was Fig. 1. Tool has mainly three parts namely stationary shoulder body,
carried out using slurry of magnesium oxide powder to obtain the rotating tool with breaking mechanism for material entered through the
mirror like surface finish. Keller’s etchant was used for 25 s on the gap and stationary shoulder holder. Small rods were fixed (for breaking
polished surface to reveal the grain boundary. Stereo microscope mechanism) at the shank of rotating tool, which were rotating with
(Nikon SMZ 745 T) was used for the macrostructure analysis. ‘Dewinter rotation of the tool. Those rods were capable to break the entered
LT-23B’ microscope was used for the optical microstructural analysis of material, which was moving in upward direction through the gap. Slots
the weld joints. Microstructure of the weld joints was taken from the were produced in the stationary shoulder body to provide the exiting
various regions. Line intercept method and ‘Image J’ software were path to the entered material broken by rods on rotating tool. Dimen-
used for the grain size and precipitate size measurement, respectively. sions of the stationary shoulder tool were kept same as the conventional
Field emission scanning electron microscopy (FESEM) of the po-
lished samples was performed along with the EDS (energy dispersive X-
ray spectroscopy) analysis. EDS was performed for the elemental ana-
lysis of the weld joint. Transmission electron microscopy (TEM) was
performed for high magnification study of fine strengthening pre-
cipitates. Further, X-ray diffraction (XRD) analysis was carried out to
identify the second phase particles using CuKα radiation. Peak

Table 1
Tool dimensions and welding parameters for conventional FSW and SSFSW.
Tool dimensions (mm) Friction stir welding parameters

Shoulder Pin diameter Pin length Rotational Traverse Tilt


diameter speed (rpm) speed (mm/ angle
min) (β)
Top Bottom

16 6 3 5.8 931 13 0°
Fig. 1. Schematic showing SSFSW tool.

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S. Sinhmar and D.K. Dwivedi Journal of Materials Processing Tech. 277 (2020) 116482

Fig. 2. Images of the welded plates using a) conventional FSW, b) SSFSW process, and corresponding macrograph of c) conventional FSW joint, and d) SSFSW joint.

FSW tool (Table 1). Shoulder having 16 mm diameter was rotating in (Fig. 4b and c). Small difference in the grain size was observed in both
case of conventional FSW, whereas same was stationary (just sliding) in the weld joints. Fine grains were observed in the nugget zone of the
case of the SSFSW. Furthermore, current tool was able to produce sound SSFSW joint. Nugget zone and HAZ of the conventional FSW joint
weld joint without overheating. showed coarser grain structure as compared to the SSFSW joint.
High magnification microstructural study and elemental analysis
were performed using FESEM. Images along with EDS analysis of con-
3.2. Macrostructure
ventional FSW and SSFSW are shown in Fig. 5 and 6, respectively.
Second phase particles were identified as Al2Cu precipitates using EDS,
Sound weld joints were produced using conventional FSW and
and further confirmed by using XRD analysis. A peak of the Al2Cu
SSFSW. Welded plates of conventional FSW and SSFSW are shown in
precipitates was observed in the XRD graph (Fig. 7). Nugget zone of the
Fig. 2a and b, respectively. Macrographs of the transverse cross-section
conventional FSW joint (CNZ) is shown in Fig. 5a, which is showing the
of conventional FSW and SSFSW are shown in Fig. 2c and d, respec-
recrystallized grains along with the fine precipitates. Heat affected zone
tively. Large ‘shoulder affected region’ can be observed at the upper
of the conventional FSW shows (Fig. 5b) precipitates along the grain
part of the stir zone in conventional FSW joint. Fig. 2c is also evident of
boundary. Inset image (in Fig. 5b) shows the magnified view of the
a wider heat affected zone which became clearer after etching. On
rectangle exhibiting the precipitates present at the grain boundary of
contrary, SSFSW joint showed more uniform stir zone and small
the CHAZ (HAZ of conventional FSW). Fig. 5c is showing the EDS
‘shoulder affected region’ as compared to the conventional FSW. A quite
analysis of the precipitate present in the CHAZ indicated by the arrow.
large stirred region developed at the upper part of nugget zone than the
Large amount of copper along with the aluminium was observed in
pin stirred region due to the presence of the rotating sub-shoulder
these precipitates, suggesting the presence of the Al2Cu as second phase
(Fig. 2d). Sliding of the stationary shoulder did not affect the cross-
particles.
section of the SSFSW joint and therefore, no evidence of macrostructure
Nugget zone of the SSFSW joint (SSNZ) also showed (Fig. 6a) fine
change due to sliding of stationary shoulder was observed.
precipitates. Heat affected zone of the SSFSW joint (SSHAZ) is showing
precipitates arranged along the grain boundary (Fig. 6b). Inset image
3.3. Microstructure (in Fig. 6b) shows precipitates present at the grain boundary of the
SSHAZ. Fig. 6c is showing the EDS area analysis of the SSHAZ shown in
Optical micrographs were taken from the various regions of con- the Fig. 6b. Copper was found as the major alloying element in the
ventional and stationary shoulder friction stir weld joints at different aluminium matrix.
magnifications. Images from the NZ/TMAZ interface, NZ and HAZ of Further, strengthening precipitates present in the conventional FSW
the conventional FSW and SSFSW joints are shown in Figs. 3 and 4, joint and SSFSW joint were studied using transmission electron mi-
respectively. Nugget Zone/TMAZ interface of the conventional FSW croscopy. TEM images of NZ and HAZ of conventional FSW joint are
joint is more clear (Fig. 3a) while in case of SSFSW joint, NZ/TMAZ shown in Fig. 8a and b, respectively. Strengthening precipitates ob-
interface is mixed (Fig. 4a). The α-Al grain size of NZ and HAZ of the served in the matrix of NZ and HAZ of conventional FSW joint were
conventional FSW joint was 7.17 ± 1.07 μm and 143.2 ± 16.61 μm, found to be in the range of 60 nm – 83 nm, and 94 nm – 197 nm, re-
respectively (Fig. 3b and c). The α-Al grain size of NZ and HAZ of the spectively. TEM images of NZ and HAZ of SSFSW joint are shown in
SSFSW joint was 5.62 ± 0.66 μm and 127.5 ± 26.17 μm, respectively

Fig. 3. Microstructure of conventional FSW joint a) NZ/TMAZ interface, b) NZ, and c) HAZ.

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S. Sinhmar and D.K. Dwivedi Journal of Materials Processing Tech. 277 (2020) 116482

Fig. 4. Microstructure of SSFSW joint a) NZ/TMAZ interface, b) nugget zone, and c) HAZ.

Fig. 9a and b, respectively. Strengthening precipitates observed in the Contribution in the heat generation by the different parts of the tool
matrix of NZ and HAZ of SSFSW joint were in the range of was investigated. Tool geometry based analysis was presented using
35 nm – 65 nm, and 61 nm – 124 nm, respectively. Thus, size of the ratio of heat generation by surface of different part of the tool (e.g.
strengthening precipitates in the SSFSW joint is finer than the con- shoulder, vertical surface of pin, pin tip) to the total heat generation
ventional FSW joint. Precipitate density (number of precipitates per (Schmidt et al., 2004). Ratio of the heat generation is given as:
unit area) in the NZ and HAZ of conventional FSW joint is 89 pre-
(RS3 − RP3)(1 + tanα )
cipitates/μm2 and 40 precipitates/μm2, respectively. Similarly, pre- QS =
cipitate density in the NZ and HAZ of SSFSW joint in 122 precipitates/ (RS3 − RP3)(1 + tanα ) + RP3 + 3RP2 HP (1)
μm2 and 67 precipitates/μm2, respectively. Density of the fine
3RP2 HP
strengthening precipitates in the NZ and HAZ of SSFSW (Fig. 9) was QPS =
(RS3 − RP3)(1 + tanα ) + RP3 + 3RP2 HP (2)
higher than the respective zone of the conventional FSW joint (Fig. 8).
Strengthening precipitates present in the HAZ of the conventional FSW RP3
joint were coarser and low dense than the HAZ of the SSFSW joint and QPT =
(RS3 − RP3)(1 + tanα ) + RP3 + 3RP2 HP (3)
this is discussed in ‘Discussion’ section in detail.
where, QS, QPS and QPT are showing the contribution of the shoulder,
3.4. Weld thermal cycle vertical surface of pin and bottom of pin tip to the heat generation,
respectively. Radius of the shoulder (RS), radius of the pin (RP) and
Weld thermal cycle was measured at 5 mm and 10 mm distance height of the pin (HP) were taken in ‘m’, whereas angle of concavity of
from the center of weld during welding using both type of tools and the the shoulder (α) was taken in ‘degree’. Radius of the pin was considered
peak temperature was also recorded. Thermocouple wires were not from the middle because of its trapezoidal shape. Radius of sub-
embedded at the center of the weld to avoid the damage of wire by shoulder was considered to calculate the contribution of stationary
rotating pin. So, the wire was inserted into the nearest possible region shoulder tool in heat generation. Values of the different parameters
of the nugget zone. Weld thermal cycle observed for the conventional considered in above equations along with the results are shown in the
friction stir welding is shown in Fig. 10a. Peak temperatures recorded Table 2.
during conventional FSW joint at 5 mm and 10 mm distance from the
center of the weld were 445 °C and 355 °C, respectively. Weld thermal 3.5. Microhardness
cycle observed for the SSFSW is shown in Fig. 10b. Peak temperatures
recorded in SSFSW joint at 5 mm and 10 mm distance from the center of Microhardness distribution across the transverse cross-section of the
the weld were 360 °C and 282 °C, respectively. Initially, at plunging both weld joints are shown in Fig. 11. Reduction in the hardness of the
stage of conventional FSW (see Fig. 10a) the rate of increase in tem- weld zone as compared to the base metal was observed in case of the
perature at thermocouple wire location was almost same at 5 mm and both (conventional and SSFSW) weld joints. Average hardness of the NZ
10 mm (approximately up to the 175 °C). In case of SSFSW, the rate of of the conventional FSW and SSFSW joint was 79 HV and 85 HV, re-
increase in temperature during plunging of the tool pin at 10 mm dis- spectively. Minimum hardness observed in the conventional FSW and
tance was lower than at the 5 mm distance due to use of stationary SSFSW joint was 73 HV and 80 HV, respectively. Minimum hardness
shoulder (see Fig. 10b). So, absence of frictional effect of large rotating zone in the conventional weld joint was observed in the HAZ, away
shoulder as in case of conventional FSW can be observed. Peak tem- from the NZ while in case of the SSFSW joint it was observed at the NZ/
perature attained at 5 mm and 10 mm distance away from the center of TMAZ interface. Further, low hardness region found in the conventional
the weld was higher for conventional FSW joint than SSFSW joint. weld joint was wider than the SSFSW joint. A steep increase in the

Fig. 5. FESEM images of conventional FSW joint a) NZ, b) HAZ, and c) EDS analysis of a particle in inset of ‘b’.

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S. Sinhmar and D.K. Dwivedi Journal of Materials Processing Tech. 277 (2020) 116482

Fig. 6. FESEM images of SSFSW joint a) NZ, b) HAZ, and c) EDS analysis of whole area shown in ‘b’.

also studied. Ultimate tensile strength, yield strength and percentage


elongation observed in the conventional FSW joint and SSFSW joint are
shown in Table 3. Stationary shoulder FSW weld joint showed slightly
higher strength than the conventional FSW joint. However, the differ-
ence in elongation of both welds joint was marginal. Stress strain curve
(Fig. 12) is showing the comparative UTS and % elongation of the both
type of weld joints. Images of few fractured samples of conventional
FSW and SSFSW are also shown in Fig. 12. Fracture location of the
conventional FSW joint was far away from the NZ and it was in the
HAZ, whereas the fracture location of the SSFSW joints was at the NZ/
TMAZ interface. These results are in agreement with the minimum
hardness region. The fracture location site moved from the HAZ of the
conventional FSW joint to the NZ/TMAZ interface in case of the SSFSW
joint. Fractographs of the fractured surface of conventional FSW and
SSFSW joints are shown in Fig. 13(a–d). Large size dimples were ob-
served in conventional FSW joint (Fig. 13b), whereas small size dimples
were witnessed in SSFSW joint (Fig. 13d).

Fig. 7. XRD analysis of NZ and HAZ of conventional FSW and SSFSW joint. 3.7. Toughness study

hardness was observed on moving away from the TMAZ/HAZ interface Charpy impact test (V-notch) was performed to measure the impact
in case of the SSFSW joint. Conventional FSW heat affected zone toughness of NZ and HAZ of the conventional FSW and SSFSW joint.
showed gradual increase in the microhardness on moving away from Results were compared with the toughness of base metal. Toughness of
minimum hardness region toward the base metal. Heat affected zone in the NZ and HAZ of the both weld joints along with the base metals is
case of the conventional FSW joint was wider than SSFSW joint as shown in Table 4. There was not much difference in the toughness
suggested by softening (hardness drop). Nugget zone and HAZ of the values of both (conventional and SSFSW) weld joints. However, sig-
SSFSW joint showed higher microhardness as compared to the con- nificant improvement in the toughness of the weld joint was observed
ventional FSW joint. as compared to the base metal. Fractographs of the toughness test
sample of NZ and HAZ of the conventional FSW joint and SSFSW joint
along with the base metal are shown in Fig. 14(a–e). Photographs of the
3.6. Tensile test toughness test samples of NZ of conventional FSW and SSFSW joints
after fracture are shown in Fig. 14f. Low magnification image of the
Tensile properties of the conventional FSW and SSFSW joint were fractured surface is shown in inset of each fractograph. Presence of the

Fig. 8. TEM images of conventional FSW joint a) nugget zone, and b) heat affected zone.

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S. Sinhmar and D.K. Dwivedi Journal of Materials Processing Tech. 277 (2020) 116482

Fig. 9. TEM images of SSFSW joint a) nugget zone, and b) heat affected zone.

dimples in the fractographs indicates the ductile fracture behavior of Table 2


the weld joint and base metal. Value of the variable considered in heat generation equation, and heat con-
tribution by surfaces.
Variable RS (CFSW) RS (SSFSW) RP HP αCFSW αSSFSW
4. Discussion
−3 −3 −3 −3
8 × 10 m 4 × 10 m 2.25 × 10 m 5.8 × 10 m 5° 0°
Present SSFSW tool was designed with the ability of automatic re-
moval of the plasticized material during the welding. It is suitable for Heat Contribution Conventional FSW (%) Stationary shoulder FSW (%)
long run weld without heating problem. Rotating shoulder of the con-
Shoulder 84 35
ventional FSW tool directly affects the stirring of the weld joint. Stirred
Pin surface 14 58
region in the macrostructure (Fig. 2c) covered a large area from the top Pin tip 2 7
section, while this region seems to be uniform in case of SSFSW joint
(Fig. 2d). Rotating shoulder resulted into high heat generation due to
the friction in case of the conventional FSW. Contribution of the
shoulder in heat generation was higher (84%) than the other parts of
the conventional FSW tool while in case of the stationary shoulder tool
(Table 2) higher heat was generated by the pin surface (58%). Sub-
shoulder of the stationary shoulder tool was also considered, and found
responsible for the partial heat generation (35%). Rotating shoulder
was found to be a major source of heat generation in case of conven-
tional FSW joint while same was not true for the SSFSW joint. This
prevented stationary shoulder from unnecessary flow of the material
which in turn resulted into more symmetrical joint. Bottom tip of the
pin generated only small amount of the heat in both type of weld joints.
Plastic deformation caused by the friction of the rotating shoulder re-
sulted into the higher peak temperature in conventional FSW joint.
Large difference was observed in the peak temperature of the conven-
tional FSW joint and the SSFSW joint.
High heat input affected the microstructure of the conventional FSW
Fig. 11. Microhardness profile of conventional FSW joint and SSFSW joint.
joint and resulted in to the grain growth. Dissolution and coarsening of
the second phase particles was observed in the conventional FSW joint.

Fig. 10. Weld thermal cycle of a) conventional FSW joint, and b) SSFSW joint.

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S. Sinhmar and D.K. Dwivedi Journal of Materials Processing Tech. 277 (2020) 116482

Table 3 Table 4
Tensile properties of conventional FSW joint and SSFSW joint. Impact toughness value (J) of the conventional FSW joint and SSFSW joint.
Type of Ultimate tensile strength Yield strength Elongation (%) Type of welding Nugget zone Heat affected zone
welding (MPa) (MPa)
CFSW 16 J 11 J
CFSW 274 158 11.51 SSFSW 15 J 12 J
SSFSW 298 180 12.23 Base metal 6J –

size shows higher microhardness as given by the ‘Hall-Petch relation-


ship’ (Sinhmar and Dwivedi, 2018). Presence of precipitates also helped
to improve the microhardness. Hence, the SSFSW joint showed higher
microhardness than the conventional FSW joint.
Nugget zone of the both type of weld joints showed higher tensile
strength than the HAZ. In both type of the joints, fracture location was
outside of the NZ. Fracture location can be correlated with the micro-
hardness of the weld joints. Tensile test samples obtained from the
conventional FSW joint were fractured from the HAZ, far away from the
NZ/TMAZ interface. This location was the softest region of the con-
ventional FSW joint observed from the microhardness profile (Fig. 11).
On the other hand, tensile sample obtained from the SSFSW joint was
fractured from the NZ/TMAZ interface. This location was the softest/
weakest region of the SSFSW joint observed from the microhardness
profile (Fig. 11). Fine precipitates improve the tensile strength. Pre-
sence of fine precipitates impedes the dislocation movement through
Fig. 12. Stress stain curve of conventional FSW and SSFSW joint with fractured pinning effect at grain boundary during the tensile test (Aydin et al.,
samples.
2010). These factors improved the tensile strength of the SSFSW joint.
Fractograph of the SSFSW joint showed small dimples as compared to
On the other hand, sliding of the stationary shoulder generated less heat the conventional joint, which suggested the higher strength and duc-
and that was not enough to make any major microstructural change in tility offered by the joint.
the SSFSW joint. Heat generation was limited to the nugget zone and Charpy impact test showed that the toughness of the NZ was higher
nearby region, which in turn resulted into the narrow heat affected for the both type of weld joints as compared to the HAZ. Significant
zone of the SSFSW joint. Wider heat affected zone was evident from the improvement in the impact toughness was observed in the weld zone
microhardness profile of the conventional FSW joint (Fig. 11). Soft re- than the base metal. Factors like yield strength, percentage elongation,
gion was wider due to the influence of rotating shoulder into the heat recrystallization and presence of second phase particles affect the im-
generation. However, in case of SSFSW joint the soft region was re- pact toughness. Reduction in the yield strength and increase in the
stricted to the NZ/TMAZ interface. Sub-shoulder of the rotating tool of percentage elongation lead to the high impact toughness (Tajally et al.,
the SSFSW was expected to be active in this region. There was a minute 2010). Similarly, recrystallization also helps to improve the impact
gap between the rotating sub-shoulder and the stationary shoulder of toughness. Recrystallization in the nugget zone of the weld joints
the SSFSW tool. Plasticized material moves through this gap into the during the friction stir welding leads to the higher impact toughness
upward direction from this region. Stationary shoulder FSW joint than the HAZ and base metal. On the other hand, yield strength of the
showed finer grain size of α-Al and precipitates. Generally, small grain AA2014 base metal is quite higher and percentage elongation is lower

Fig. 13. Tensile fractographs of conventional FSW joint at a) lower magnification, b) higher magnification; and SSFSW joint at c) lower magnification, and d) higher
magnification.

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S. Sinhmar and D.K. Dwivedi Journal of Materials Processing Tech. 277 (2020) 116482

Fig. 14. Impact toughness fractographs of a) NZ of CFSW, b) HAZ of CFSW, c) NZ of SSFSW, d) HAZ of SSFSW, e) base metal, and f) fractured samples of NZ of
conventional FSW and SSFSW. Low magnification image of the fractured surface is shown in inset.

than the conventional and stationary shoulder weld joints. These factors Acknowledgements
adversely affected the impact toughness of the base metal. Tensile
properties of AA2014 base metal were reported in previous work The authors would like to acknowledge the help from Dr. Sunny
(Sinhmar and Dwivedi, 2017). Difference in the percentage elongation Zafar (IIT-Mandi) for preparation of TEM samples.
of the both weld joint was insignificant (Table 3). Similarly, difference
in the toughness of the HAZ of the both weld joint was small. Ductility References
and toughness of the SSFSW joint was found higher than the conven-
tional FSW joint. Moreover, concentrated material flow reduced the arc Ahmed, M.M.Z., Wynne, B.P., Rainforth, W.M., Threadgill, P.L., 2011. Through-thickness
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