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Is 542 1968 PDF
Is 542 1968 PDF
Is 542 1968 PDF
Indian Standard
SPECIFICATION FOR
COCONUT OIL j
UDC 665.353.6
" CoPY;111tI1973
BUREAU or INDIA-N '8TAND~RDS
~AK BHAVAN, 9 BAHADUll SHAH ZAlARMAllO
NEW DELID 110002
0,2 November 1888
1•• M2-I.
Indian Standard
SPECIFICATION FOR
COCONUT OIL
(Second Revision)
Oils and Oil.eed. Sectional Committee, CAFOO 5
CIWrIIIa &/wUlltn.,
DaJ. S. BADAMI Swutik ou Milia Ltd, Bombay
MmtlNrs
S8RI V. A. PAtUER (AllmMt, to
DrJ. S. Badami)
Dn K. T. ACHAYA. Reponal R~h Laboratory (CSIR.). Hyderabad
DB G. LAUBMJ_AKAY"K.. (AlII,""")
SKRt V. P. AAAIft'ANAR"YAlfAtf Directorate or Marketin & IDlpeCtion (Miniatry 01
Food, Aariculture. Community DevrlopmeDt ~
Co-operation ) t NalPur
Smu V. CSAlO>RAMOULY ( Ai"".,,,. )
SHRI R. C. DAB GUPTA National Test HOUle, Calcutta
SaRI N. DS8IXACHAB. The Tala Oil Milia (10 Ltd, Bombay
DB B. G. GUNn. (Alima"")
DR K. C. Gtn~ATI Indian Agricultural Research lrutitute, New Delhi.
atUl Indian Councilor Apicultural aaearda,
New Delhi
SRRI H. P. GUPTA. East India Oil Millen AIIociation, Calcutta
SaRI R. R. MUUADJ (Alt"".u)
DR G. S. HATT1AlfGni Mindustan Lever Ltd, lIombay
SftRI K. P. JAJit Directorate orsu.... ~ V. . . .tt (Miniitry or rood,
Apiculture, Community ~Iopmmt • Oo-ope-
ration), New Delhi
&Rftl F. G. T. MRM• • ( AI""..,,)
DR S. M. KAJJ ltalab Private Ltd, Bombay
8R.IJ. C. DEY (AI",,,tll,)
(CAlcutta)
8H"R1 S. S. tlOlJ.VAR (.4""",")
( Madra)
SHft! N. S. MAINI Re,ional 08iee. Oilleeda Developmmt (Miniltry or
PoocI, Apiculture, Community Deftlopmeat •
Co-operation ), Hyderabad
S... HA'RIIW 8ftMr (Allmllt")
Dn R. D. NARA.(I Cenrral C'..ommittee for Pood Standard. (Ministry or
HNlth' Family Planning), New DeIhl
SOl D. S. CRADH" (AI'"...',)
( C.IiDM • ,." 2 )
4 _ __
e-rnn
Da G. S. HA'l'TIANnIlJ Hindustan Lever Ltd, Bombay
Mma'trJ
SURt V. U. MARBALLt (All""tJII to
Dr G. S. Hattianpi )
Da K. T. ACRAYA Relional Rewarch l~boratory (aSIR), Hyderabad
DR G. LAX.RJllflfARAYAJJA ( ~Il"" .." )
S••I OoJlOLOHAlfD J. AOA.RWAL Bombay OilRed. and Oil. Exchange Ltd, Bonlbay
SRRI C. V. MAR1W ALA ( AI,.",." ) ,
SWIU V. P. ANANTANA"AYAKA1f Dirrctorate of Mark..ting It Inspection (Ministry of
Food, Alriculturt', C'.ommunity Dcveolopmmt Ie
Co-opnation ), N&fIPur
8.BI V. CUAlCDUKOULY (Al'nut,)
S.I\I DHORJATI PUIAD SHAftA- C.tclItta Chemi('al CeO Ltd, C..leutra
C1IARYYA
SaRI AWIL KUMA'R MAa,mr-
D.... (~lmIUlU)
DR H. Il. CAliA Indian In.titute of Science, Ban.alore
DR It. C. DA:NDOlfA. The But Asiatic Co (lndia) Pvt Ltd, Madru
SIJU N. D.IKACHA'& The Ta.. on Mill. Co Ltd, Bomt.y
DR B. G. Ot1JfDB ( AI,,,..,,)
2
M. ."s Rqw,smlill'
S.as S. C. aBO•• Indian Soap and Toiletries M.ktT.' AIIOciatlon,
Calcutta
Ilia! P. G. T. MIl. . . . Directorate or 8\11IlT It Vanaapati ( Ministry or Food,
Agricultule, CommuDity Development A
CQ-operation ), New Delhi
s..r-au. Kla.oa. (141"""")
8. .1 B. S. MODI The Vanaapati Manuracturen' Association of India.
Bombay
Da It. S. MUATI Tunpbhadra Industries Ltd, Kurnonl
DB H. G, R.. Il.DDT Directorate General or Technical Development.• New
Delhi .
S••I L. R. SUD Ministry of nefrnre ( R &: D )
c.w..."
Da 8. M. PATJ:L l{indtL~tan J ever Ltd, Bombay
M";,b,,,
SRRI V. P. AMAlft'AKARAYANAlfDirectorate or Marketing It Inspcctien (Ministry nf
Food, Agriculture, Community Development &:
('~.o~ralion ), Nagpur
S••I V. CHAN'DRA.1I0'OLY (AllmuJU)
8.a. P. V. GUIAKATKI Khadi and \'illage Industries Commission, Bombay
S8Jtl V. D. HXRVATTK (A/Urate)
DR J. O. KANE In penonal capuity (ntpartrlUnt tJ/Ch,mi,,,1 r,cluuJJn(J.
. UniNtsilJ n.[ Bomb".1. BtmabIl.1)
SZC'RM'ARY ~ntral Committee for Food Standard~ (Mini.try of
Health It Family Planning), New Delhi
AaIII'l'AKT SBCRftAftY ( AI""..,,)
SRa, P. P. SHARMA . Solvent Fdtracton' AA.~iati()n or India, Bombay
SHal L. D. NANAVATl ( AI",,,ou) "
S••I SHIVJlAJ SARA-OUR IncUan Vegetable Product" Ltd. Iletmhay
S.R' I. D. 51.0M Ministry of J.)eitnce ( R It I)
·Methods of sarnphng and test for oils and fats: Part 2 Purity test.
(CAFDC 5)
AMENDMENT NO. 3 DECEMBER 1995
TO
IS 542: 1968 SPECIFICATION FOR COCONUf OIL
( SecondRevision)
( Page 4, Foreword, clause 0.4 ) - Add the following clause 0.5 after
clause 0.4 and renumber the subsequent clause:
'0.5 A scheme for labelling environment friendly products to be known as ECO
Mark bas been introduced at tbe instance of the Ministry of Environment and
Forests ( MEF). The ECO Mark shall be administered by the Bureau of Indian
Standards ( BIS ) under tbe BIS Act, 1986 as per the Resolution No. 71 dated 20
February 1991 88 published in the Gazette of the Government of India vide GSR
85(E) dated 21 February 1991. For 8 product to be eligible for marking with the
ECO Mark it shall also carry the Standard Mark of BIS for quality besides
meeting additional optional environment friendly ( EF ) requirements. The EF
requirements for coconut oil, raw and refined are therefore being included
through an amendment.
This amendment is based on the Gazette Notification No. 678 dated 30 August
1994 for Labelling Edible Oils, Tea and Coffee as environment friendly
products, published by the Ministry of Environment and Forests.'
(Page S, clause 4.4 ) - Add the following clauses after clause 4.4:
'4.5 Optional Requirements for ECO Mark
4.!.1 GeneralRequirements
4.!.1.1 The product shall conform to the requirements of quality prescribed
under clauses 4.1 to 4.4.
4.5.1.2 The manutacturers sball. produce to BIS environmental consent
clearance from the concerned State Pollution Control Board ~s per the nonns laid
down under the Water ( Prevention and Control 01 Pollution) Act, 1974;
Air ( Prevention and Control of Pollution ) Act, 1981; Water ( Prevention and
Control01Pollution) CessAct, 1977 respectively, along with the autbbrizltion,
if required under the Environment ( Protection) Act, 1986, while applying for
ECOMark.
4.5.~ Specific Requirements
1
Amend No. J to IS 54Z : 19"
43.%.1 Theproduct shall not contain anatoxin, more than 5 mg/kg, when tested
by tbe method prescribed in Appendix A.
4.5.1.% The pesticide residues, if any, shall not exceed the tolerance liouts as
prescribed in the Prevention of Food Adulteration Act, 1954 and Rules Ilude
thereunder.
4.5.2.3 Only permitted antioxidants not exceeding the quantities specified
against each as prescribed under the Prevention of FoodAdulteration Act, 1954
and Rules Dlide thereunder, shall be used, if required.
4.s.%.4 The product shall not contain any of the toxic metals in excess of the
quantities prescribed in Table 2.
TABLE Z LIMITS FORTOXIC METAL.fit
( Page S, clause 5.1 ) - Add the following new clause 5.1.1 after clause
5.1:
'5.1.1 For ECO Mark the product shall be packed in such packages which are
made from recyclable ( tbat is which can be re-processed to manufacture Iny
useful product) or biodegradable materials.'
( Page 5, clause 6.1 ) - Add the followil\g new clause 6.1.1 after clause
'.1:
"6.1.1 For ECO Mark the containers shall be marked with the following
information:
I) Ust of identified critical ingredients in descending order of quantity,
percent by mass, which shall include 'made fronl coconut';
b) The brief criteria for whicb tbe producthas been labelled for Eoo Mark;
and
c) Shelf life of the plOduet.·'
2
Amend No.3 to IS 541 : 1968
(Page 7, clause 8.% ) - Add the following Appepdix after clause 8.%:
'APPENDIX A
(Clause 4.5.2.1 )
DETERMINATION OF AFLATOXIN
A ..l REAGENTS
A-I.I Acetone, 70 Percent - 700 mlacetone in 300 ml distilled water.
A·l.1 Aeetonet %0 Percent - 200 81) acetone in 800 ml distilled water.
A·I.3 Lead Acetate, ZO Percent - 200 g neutral acetate in distilled water and
3 ml glacial acetic acid, diluted to one litre.
A-1, PROCEDURE
A-Z.l Dissolve 30 g sample in 100 ml hexane.
A..Z.z Extract with 3 x 50 lui 70 percent acetone.
A·Z.3 To the extract add 60 ml distilled water and 20 mllead acetate.
A-Z.4 Boil to reduce volume to 150 mi. Cool to about 20°C.
A-Z.! Filter and wash with 20 percent acetone.
A-Z.' Extract filtrate and washings with 3 )( SO ml chloroform.
A·Z.7 Pass chloroform layer through anhydrous sodium sulphate.
.A·Z..8 Concentrate to SO mland spot on TLC plate.
A·3 CALCULATION
· .nnrJlu..
Aftatoxm, &U&,-t'J =V #
x 1 000
X S
vxm
where
V =volume of extract in ml,
v =volume of extract giving minilllumobservable tluorescence in Jj,1,
m II: mass of sample in g, and
s =standard toxin giving minimum observable fluomsce~ce in ~g.'
(FAD44)
3
AMENDMENT NO. 4 MARCH 2002
TO
IS 542: 1968 SPECIFICATION FOR COCONUT OIL
( Second Re,illon )
( Amendment /\'0. 3, page 2, clause 4.5.2.1] - Substitute '5 J.lg/kg' for '5
mg/kg '.
(FAD44 )
Indian Standard
SPECIFICATION FOR
COCONUT OIL
(Second Revision)
o. FOREWORD
0.1 This Indian Standard (Second Revision) was adopted by the Indian
Standards Institution on 28 August 1968, after the draft finalized by the
Oils and Oilseeds Sectional Committee had been approved by the Chemical
Division Council and the Agricultural and Food Products Division Council.
0.2 India ranks among the largest coconut producing countries of the
world. The chief coconut growing states in India are Madras, Kerala,
. Mysore, Orissa, and West Bengal. Considerable quantities of coconut oil,
both in the raw and refined state, are used in India for edible purposes and
for margarine and bakery fatl. Furthermore, the oil finds wide use in the
manufacture of soaps and various types of cosmetic and toilet preparations.
The requirements for various grades of the oil have, therefore, been SO pres-
cribed in this standard that these grades are suitable for the foregoing
purposes. The oil is also used for pharmaceutical purposes.
0.3 This standard was originally issued in 1954. In ita first revision issued
in 1963, the limits of acid value, colour and the moisture and insoluble
impurities were modified in the light of experience. As the standard
covered only the expressed type of oil, and since there was an urgent need
for formulation of an Indian Standard for the so!vent-extracted type,
15:3471·1966* was issued al an emergency standard based on the data
made available to the ad hoe Consultative Group let up for the purpose.
After having decided to normalise this emergency standard the need for
rationalizing the grades of the oil covered in these standards was keenly
felt. Thls second revision of IS: 542..1954 hal been prepared amalgarnatinJr
its.earlier revision and 18:3471·1966*. As a consequence, IS: 3471·1966i
now stands withdrawn.
0.4 The requirements laid down in this standard for the expressed type of
the ail correspond to the specifications prescribed by the Directorate of
~farketing and Inspection in their Vegetable Oils Grading and Marking
3
llulel, 1955. For the purpose of regulating the quality of the 101v( ".t-
extracted type of this oil, the concerned Indian Standard on the solvent-
extracted type or the oil which is incorporated now had been adopted in
the relevant schedule of the Solvent-Extracted Oil, De-oiled Mt\,al and
Edible Flour (CQntrol) Order, 1967. In so far al the edible grades are
concerned, this standard takes care of the provisions of the Prevention Af
Food Adulteration Rule., 1954, as modified from time to time.
U For the purpose of deciding whether a particular requirement of this
in,
ltandard i. complied with, the final value, observed or calculated, express-
the result of a test or analysis, shall be rounded off in accordance
With 18:2-1960·. The number oflignificant places retained in the rounded
off value lhould be the same .1 that of the specified value in this standard.
I. ICOPB
1.1 Thilltandard preacnDea the requirements and the methods of sampling
and test for coconut oil used for edible and industrial purposes.
. 2. TZRMINOLOGY
2.1 For ~he purpole of thil standard, the definitions given under 2 of
18:548-1964t and a110 thole given below, shall apply.
2.1.1 RlfittldCoeo,"" Oil- Coconut nil obtained by the process of expres-
,ion or 101vent extraction which hal been refined by neutralization with
alkali, bleached with bleaching earth or activated carbon or both, and
deodorized with Iteam, no other chemical agents being used.
2.1.2 hi·"fillltl CueOtlrl' 0;1- Coconut oU obtained by the process of
101veDt extraction which ha. been neutralized with alkali, and with or
without bleachinl with bleachins earth or activated carbon or both, no
other chemical agerttl beins used,
S. TYPBI AND GIlADES
1.1 The material shall he of the following types and Rradea:
a) Ex/Wusttl
Refined Grade,
Grade lA (Raw»)
Grade IB (Raw), and
Grade 2 (Raw).
..... for fOUDClbw off numerical valuet (,..iIM).
rot
tMethrxla of ampIiJII and tat oil. and rats (,..;,.).
4
b) SOi,,,,,, Exlraeted
Refined Grade,
Semi-refined Grade, and
Grade 1 (Raw).
3.1.1 The Refined Grades of the expressed and solvent-extracted types
and the Raw Grades lA and lB of the expressed type are suitable for
direct edible consumption.
3.1.2 Raw Grade 2 of the expressed type and the other two grades of the
solvent-extracted type are suitable for hydrogenation, refining and other
industrial uses, and not for direct edible consumption.
4. REQ,UlREMENTS
4.1 o.aerlpdoD- The material shall be obtained from good quality coco-
nut cake or from clean and sound copra Cocos nucif,,(J Linn., fame Palmle,
by a process of expression, .
4.1.1 Solvent-extracted oil shall be obtained from the oieaginoul
material using solvent hexane conforming to IS: 3470-1966*.
4.2 The material shall be clear and free from rancidity, adulterants, sedi-
ment suspended and other foreign matter, separated water, and added
colouring and flavourlng substances.
4.2.1 The clarity of the material shall be judged by the absence of turbi-
dity after keeping the filtered sample at 30°C for 24 hours,
4.3 Admi.tare with Other ons - The material shall be free from
admixture with other oils, when tested according to the methods pre..
crihed under 20 of IS: 548-1964t_
4.4 'The material shall also comply with the requirements given in Table 1.
5. PACKING
.5.1 The material shall be supplied in suitable well-closed container, as
agreed to between the purchaser and the supplier.
6. MARKING
6.1 The containers shall be marked with the name, including the type and
grade, and weight of the material in the container; manufacturer's name
and trade-mark, if any: batch number; and the year of manufacture.
. ·~pt'cili(".tinn (Ir hexane, food Rrade.·
tt\{rthodl of ..."pling and fe-51 fill' ()il8 and fatl (r,vj,s,~).
TAnB I a&Q,lJIaDIDITIlOa COCONUT OIL •.....
(a.- 4.4 all 8.1 ) ~
SL CHA RAC'TZJlJITJC R..Qt7IBZKD1T8 wo. ~ MftBOD OJ' ...•
No. -..A.-_ _ _ _ _- - - , Ta-r) JlUTO
I
ExpraIed SolYalt-Exttacted
, . . . . - -_ _-..A-_ _ _ _ _ ~ r----.A.--~
7
BUREAU OF INDIAN STANDARDS
Headq.."".:
Manlk Shlvln, 8 81hldurShih ZItIr Mlrg, NEW OELHI11 0002
T~ ..:23230131.23233375,23238402 Fax:81+01123239398.23238382
I- Mill: InfoObll.org.tn -website: http:/twww.bll.org.ln
c.n"", UbotItory: rellpho".
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RAJKOT 380002
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