Ethyl

Sample Sample Elapsed Sodium

Acetate
Number Time Time Hydroxide
Concentr
Concentaion
aion
[mol/dm³]
[mol/dm³]

1 01:46:11 00:00:00 0.100 0.100

6 01:51:11 00:05:00 0.100 0.100
11 01:56:11 00:10:00 0.100 0.100
16 02:01:11 00:15:00 0.100 0.100
21 02:06:11 00:20:00 0.100 0.100
26 02:11:11 00:25:00 0.100 0.100

Time (min) Measured Conductivity Conversion of NaOH Specific Rate Constant Ln K

00:00:00 8.0762 0.5400 0.0690 -2.6736
00:05:00 8.0469 0.5400 0.0700 -2.6593
00:10:00 8.0273 0.5500 0.0700 -2.6593
00:15:00 8.0273 0.5500 0.0700 -2.6593
00:20:00 9.6680 0.3200 0.0190 -3.9633
00:25:00 11.6406 0.0600 0.0020 -6.2146
 NaOH
Flowrate Flowrate Stirrer Reactor Reactor
Measured Feed
of Sodium of Ethyl Speed Temp. Volume
Conductivity Notes Concentr
Hydroxide Acetate
0 - 20 [mS] ation
[cm³/min] [cm³/min] [rpm] [°C] [dm³]
[mol/dm³]

40.0 40.0 8.08 0 34.3 1.00 0.05

40.0 40.0 8.05 0 34.2 1.00 0.05
40.0 40.0 8.03 0 34.1 1.00 0.05
40.0 40.0 8.03 0 34.1 1.00 0.05
40.0 40.0 9.67 0 34.0 1.00 0.05
40.0 40.0 11.64 0 34.1 1.00 0.05

Chart Title
1/T T K 1/K 0.0000
0.0285 35.0586 308.2086 0.00324456 0.00324400 0.00324500 0.00324600 0.00324700
0.0286 34.9609 308.1109 0.00324558 -1.0000
0.0286 34.9609 308.1109 0.00324558
-2.0000
0.0288 34.7656 307.9156 0.00324764
0.0288 34.7656 307.9156 0.00324764 -3.0000 f(x) = − 384125.484849024 x + 1243.50369761071
0.0287 34.8633 308.0133 0.00324661
-4.0000

-5.0000

-6.0000

-7.0000
 Calculate
EtAC Initial Final Final Current Current Conversi Producti
d Specific
Feed Feed NaOH NaAC NaOH NaAC on on
Final Rate
Concentr Conducti Concentr Concentr Concentr Concentr of of
Conducti Constant
ation vity ation ation ation ation NaOH NaAC
vity K
[mol/dm³] [mS] [mol/dm³] [mol/dm³] [mol/dm³] [mol/dm³] [%] [%]
[mS]

0.05 12.1 0.00 0.05 4.7 0.02 0.03 0.54 0.54 0.069
0.05 12.1 0.00 0.05 4.6 0.02 0.03 0.54 0.54 0.070
0.05 12.1 0.00 0.05 4.6 0.02 0.03 0.55 0.55 0.070
0.05 12.1 0.00 0.05 4.6 0.02 0.03 0.55 0.55 0.070
0.05 12.1 0.00 0.05 4.6 0.03 0.02 0.32 0.32 0.019
0.05 12.1 0.00 0.05 4.6 0.05 0.00 0.06 0.06 0.002

Chart Title
0.00324600 0.00324700 0.00324800

84849024 x + 1243.50369761071
 Measure
Optional Optional
ln ((a - d
Temperat Temperat
a1)/ Conducti
ure ure
(a - a0)) vity
T2 [°C] T3 [°C]
0 - 5 [mS]

-0.781 0.00 35.06 199.90

-0.786 0.00 34.96 199.90
-0.788 0.00 34.96 199.90
-0.788 0.00 34.77 199.90
-0.391 0.00 34.77 199.90
-0.063 0.00 34.86 199.90