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Improved Viscoelastic Model For Laminate Composite Under Static and Dynamic Loadings
Improved Viscoelastic Model For Laminate Composite Under Static and Dynamic Loadings
COMPOSITE
Article M AT E R I A L S
Journal of Composite Materials
47(14) 1717–1727
! The Author(s) 2012
Improved viscoelastic model for laminate Reprints and permissions:
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composite under static and dynamic DOI: 10.1177/0021998312451294
jcm.sagepub.com
loadings
Abstract
Organic matrix composite materials are rate-dependent. Approaches exist for static and for dynamic cases but not for
both. In the present study, a viscoelastic spectral model, classically used for low strain rates, was successfully identified on
dynamic test data as being suitable for high strain rates. The associated identified model was no longer available for low
strain rates. An improved formulation of the model was devised, to be representative for both high and low strain rates.
Results exhibited the desired rate dependence and good agreement with experimental data.
Keywords
Laminate composite, non-linear behaviour, strain rate dependence
efficient one for the structural parts FE computation elementary viscous mechanisms i , associated with a
in the industry. The ONERA progressive failure relaxation time i and a weight i :
model has been enriched by a failure model,21 ageing
effects22 and multiscale effects.23 Most of these enrich- : X : : 1
"ve ¼ gðÞ i and i ¼ ði gðÞSR : i Þ ð2Þ
ments are not affected by the improved formulation i
i
presented in the Multispectrum model section of this
paper. The purpose of the present study is to model with g() a non-linear function and SR the viscous com-
variations in the apparent tangent modulus of a pliance, which are defined in the sequel. This model can
½45 s laminate behaviour by considering the visco- be seen as a generalization of rheological models with
elastic behaviour of the ply before damage apparition. an important number of springs and dashpots. The
This model is presented in the sequel. weight and relaxation times of each elementary viscous
In the Reference model section, the reference model mechanism (i , i ) define the temporal spectrum. These
is introduced and analysed. In particular, the require- relaxation times are the classical ones from rheological
ments and limits of identification of the reference model models. To be representative, the model needs a large
on dynamic data are highlighted. In the Proposal for number of viscous mechanisms to be considered (in the
an improved formulation section, a multispectrum rest of this paper 200 mechanisms are arbitrarily used).
formulation is presented which achieves a more pre- In order to simplify identification of the temporal
dictive viscoelastic model for a large range of loading spectrum, a Gaussian spectrum form (equation (3)) is
rates. used.
i
The reference model i ¼ expðiÞ and i ¼ P
i
The ONERA progressive failure model is a mesoscopic i
!
model, based on knowledge of the ply behaviour. 1 i nc 2
Consequently, the model is based on a change of with i ¼ pffiffiffi exp ð3Þ
n0 n0
scale method, in this case classical laminate theory
(CLT), and a ply behaviour description. The choice of The spectrum is based on only two parameters:
pffiffiffi nc
non-linear viscoelastic behaviour for the ply (explained the mean of the gaussian spectrum and n0 ¼ 2sd with
and described in the sequel) requires a non-linear exten- sd the standard deviation. The described spectrum has
sion of the CLT. been successfully used in Maire16 to model the visco-
elastic behaviour of glass fiber reinforced polymer
(GFRP) during creep test. In order also to simplify
Ply behaviour identification, the viscous compliance is taken as a func-
The purpose of this study is to model the mechanical tion of the elastic compliance S0 . In this model, only
response of organic matrix composite materials under viscosity in transverse and shear directions is con-
loadings of various strain rates. We will specially focus sidered (11 ¼ 0):
on the variation in the tangent shear modulus G12 in a 0 1
½45 s laminate, which is known to be rate-dependent. 0 0 0
One way taking this phenomenon into account is to B C
SR ¼ B
@0 22 S022 0 C
A ð4Þ
introduce a function f to describe the evolution of the
:
modulus, G12 ¼ f ð"Þ, as, for example, in Song et al.24 0 0 66 S066
The choice of f is not simple and generally not physic-
ally based. Another way, considered in the present Finally, to describe creep tests, the following non-
paper, is to use a viscoelastic behaviour for the uni- linear function g() is introduced18:
directional ply. In the following work, a viscoelastic pffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffin
spectral model taken from Maire16 is used. The visco- gðÞ ¼ 1 þ t : SR : ð5Þ
elastic behaviour of the ply, in the local basis, can be
written as:
This viscoelastic model is claimed to need only two
tests to identify all viscous parameters (nc , n0 , 22 , 66 ,
¼ C0 : ð" "ve Þ ð1Þ
and n): a multiple step creep test on a ½45 s laminate
and a single creep test on a ½90 laminate.
where is the Cauchy stress, C0 the elastic tensor, " the The model has been successfully used to described
total strain and "ve the viscous strain. In such an the behaviour of UD and woven plies. In the sequel,
approach, the viscous strain is taken as the sum of regarding available experimental dynamic data, only
experimental environment remain on the high-speed To compare the experimental data with numerical
curve. In the previous section of this paper, it was results, two error estimators were introduced:
proved that the upper asymptotic limit of the model
is G12 . In order to be predictive in a large range of exp ðiÞ num ðiÞ
dynamic rates, this G12 value has to be identified on Error1 ¼ mean ð6Þ
exp ðiÞ
the highest possible speed test, which would give the
higher tangent modulus. For this reason, the vibrating exp ðiÞ num ðiÞ
sensor could be a problem for the present identification. Error2 ¼ max ð7Þ
i exp ðiÞ
The identification of the viscous parameters of the
model was performed with Matlab Optimisation
ToolboxÕ . Three of the four test curves are used: 4 m/ with exp ðiÞ the stress from experimental data and num ðiÞ
s, 0.1 m/s and 5 mm/min. Six parameters have to be the prediction of the stress, both at a given point i. Values
identified: G12 , 66 , nc , n0 , and n. Elastic properties for these quantities are given in Figure 4. The three curves
in directions 1 and 2 are already known: in light grey are those used to perform the identification.
E11 ¼ E22 ¼ 63,000 MPa and 12 ¼ 0:1 (manufacturer’s Both error indicators are lower than 10% for the 0.1 m/s
data). and 5 mm/min tests. The 4 m/s curve is worse, probably
because of the experimental disturbances, but the mean
error is limited to 10%. The curve in dark grey, corres-
Results of the dynamic identification ponding to the 500 mm/min test, can be used to check if
Several runs of computation were performed using dif- the model can be predictive, as these experimental data
ferent sets of initial parameters. Results globally con- were not used for identification: both estimators are
verged on the solution given in Table 1. These results lower than 10% in this case.
confirm that a spectrum with lower relaxation times is To conclude, the model can be identified on dynamic
required to represent the dynamic tests. Figure 3 com- tests and can be predictive for behaviour in a range of
pares the identified dynamic spectrum with a classical speeds fixed by identification tests.
one. A compilation of identified spectrum parameters
from the literature was performed to define this clas-
Static test prediction with dynamic parameters
sical static spectrum. The results indicate that the relax-
ation times involved in dynamic tests are lower than Experimental data on G939/M18 carbon/epoxy lamin-
those in static tests. In the region close to log()¼0, ate are available at different static loading rates in
there are some relaxation times, which are involved in Graindorge,27 but the ONERA model was not used in
both static and dynamic tests. In fact, the 5 mm/min that study, so the spectral and static parameters are not
test, used for the identification procedure for dynamic available there. Moreover, with the available data, a
data, is the bridge value between dynamic and static static identification cannot be considered, since there is
tests. The identified viscous parameters are of a usual
order of magnitude when compared to the literature.21 μ
Dynamic spectrum Static spectrum
Only the G12 value appears to be quite high, which may
be due to the experimental disturbance at highest 0.1
speeds, described in the previous paragraph (the tan-
gent modulus in the experimental data was closed to
10,000 MPa at the beginning of the 4 m/s test). On the
other hand, the identified value of G12 is the tangent
modulus expected for a very high speed test:
:
" ¼ 105 s1 . Experimental results at such a strain rate
level are not available, so that it is difficult to assess this
value.
log(τ )
Table 1. Mechanical properties of the G939/M18 after opti-
misation on ONERA Lille dynamic tests only –30 –20 –10 0 10 20 30
σ [MPa]
90
80
70
60
50
40
30
ε
0
0 1 2 3 4 5 6 7
−3
x 10
Figure 4. Comparison between experimental data (dots) and numerical results (plain curves) for dynamic test on G939/M18. The
light grey curves are those used for identification of the model and the dark grey curve estimates the prediction capability of the
model.
σ̃12
0.9
0.8
0.7
0.6 Experiments
0.5 σ̇12 = 5MPa/s
σ̇12 = 0.5MPa/s
0.4 σ̇12 = 0.05MPa/s
0.3 Numerical
σ̇12 = 5MPa/s
0.2 σ̇12 = 0.5MPa/s
σ̇12 = 0.05MPa/s
0.1
2ε12
0
0 0.002 0.004 0.006 0.008 0.01 0.012 0.014 0.016 0.018
27
Figure 6. Comparison between static experimental data from Graindorge and the prediction of the model identified in dynamic
mode.
Proposal for an improved formulation Table 2. Mechanical properties of the G939/M18 after opti-
misation on dynamic tests for a large spectrum (nC ¼ 0)
Mono-spectrum model
G12 n0 n 66
The first possibility would be to find a single large spec-
trum that involves static and dynamic relaxation times. 31,875 MPa 20.5 2.08 0.37 3.65
Analysing Figure 3, the choice of a spectrum centred on
nc ¼ 0 appears to be interesting for such an objective.
Identification on dynamic tests can then be performed, satisfactory, which leads us to propose the modified
as previously, in order to identify n0 , 66 , and n. The ‘‘multispectrum’’ model, described in the following
results of identification are presented in Table 2. A paragraph.
comparison between numerical results and experimen-
tal data is presented in Figure 7. The values of the par-
Multispectrum model
ameters are quite classical, except for G12 . Its high value
is due to the fact that it corresponds to the apparent The proposed solution is to use a multi-gaussian spec-
modulus for "_ ¼ 1015 s1 . The value of n0 , which is close trum (Figure 8). The idea is to superimpose a dynamic
to 20, induces a range of strain rates with sensitivity gaussian spectrum (ndyna
c and ndyna
0 ), identified on
"_ 2 ½1015 s1 ; 1015 s1 . A very large range of rates, dynamic data, and a static gaussian spectrum (nstat
c and
particularly a large range of unwanted rates in dynamic nstat
0 ) identified on static data, all the other viscous par-
mode, is then covered. ameters being unique. Equation (3) has to be re-written
In terms of error indicators, given in Figure 7, these in order to take account of this superimposition:
new results are worse than those from the previous
dynamic identification. Moreover, the prediction of i dyna i stat
the apparent modulus is also worse. This can be seen i ¼ expðiÞ and i ¼ P dyna þ P stat
i i
in the zoom made in the dotted line frame. With that i i
large spectrum model, the errors on the prediction of 2 !
k 1 i nkc
the apparent modulus are close to 7%, 27%, 30% and with i ¼ k pffiffiffi exp ð8Þ
n0 nk0
33% for, respectively, the 4 m/s, 0.1 m/s, 500 mm/min
and 5 mm/min curve, while the error is, respectively,
5%, 15%, 6% and 4% with the spectrum identified
with dynamic data. To be representative, the model needs, as previously,
Clearly a monospectrum model, based on dynamic a reasonable number of viscous mechanisms to be
tests, static tests or both together, is not taken into account. The other equations and variables
30
20
10
0
σ [MPa] 0 1 2 −3
x 10
90
80
70
60
50
40
30
Figure 7. Comparison between experimental data (dots) and numerical results (plain curves) for dynamic tests on G939/M18 with a
large spectrum. Light grey curves are those used for the identification of the model and the dark curve (500 mm/min) estimates the
prediction capability of the model. A zoom on the beginning of the plot highlights the prediction of the apparent tangent modulus.
of the model remain the same (equations (1), (2), (4) µ Multi Gaussian spectrum
and (5)). The main result of this new formulation is to Dynamic spectrum
0.1 Static spectrum
introduce two sets of asymptotes for the viscoelastic
behaviour. This idea will be highlighted with the virtual
test in the sequel.
σ [MPa]
μ
400
0.1 Dynamic spectrum
350
150
100
log (τ )
50
ε
–30 –20 –10 0 10 20 30
0
0 2 4 6 8 10 –3
x10
σ [MPa]
μ
400
0.1 Static spectrum
350
300
ε̇ = 1 s−1
ε̇ = 10−1 s −1
250 ε̇ = 10−3 s−1
ε̇ = 10−7 s−1
200 ε̇ = 10−8 s−1
150
100
log (τ )
50
ε
–30 –20 –10 0 10 20 30
0
0 2 4 6 8 10 –3
x10
σ [MPa]
100
log (τ ) 50
ε
–30 –20 –10 0 10 20 30
0
0 2 4 6 8 10 –3
x10
Figure 9. Results of the virtual test for the multi-gaussian spectrum model.
(Figure 9) are compared to the earlier model, identified spectrum. This allows the variation in apparent modu-
on dynamic or static data. The parameters used for lus to be described for a range of loading rates between
these tests are summarised in Table 3. They concatenate 108 s1 and 108 s1 .
the viscous parameters previously identified with the This virtual study indicates that the multi-gaussian
dynamic test (Results of the dynamic identification sec- spectrum model exhibits a satisfying dependence on
tion) with standard literature values for the static loading rates in the range of speeds from dynamic
spectrum. tests to creep tests, where a single ‘‘large’’ spectrum
The model with only the dynamic spectrum exhibits failed.
a dependence at loading rates between 108 s1 and
108 s1 (Figure 9). The model with only the static spec-
trum exhibits a dependence at loading rates between
Discussion on the virtual test results
108 s1 and 1 s1 . The multispectrum model with both Quantitative comparisons with experimental results are
static and dynamic spectrums exhibits a dependence at for the moment not available. Nevertheless, a qualita-
loading rates between 108 s1 and 108 s1 , which is the tive comparison of the multi-gaussian spectrum model
union of the two previous interval of dependence. This with the experimental G939/M18 results is possible.
result permits to support the concept of the two sets of The aim is to check whether the behaviour is now
asymptotes. In fact, the dynamic spectrum defines two rate-dependent with respect to the tests by
asymptotes (purely elastic and viscous) as well as the Graindorge.27 The parameters used for this test are
static spectrum. For the multi-gaussian spectrum, two summarized in Table 3. Results are presented in
grey levels were used to plot results, to see the loading Figure 10. As in Static test prediction with dynamic
rates linked to the dynamic spectrum and the loading parameters section, the stress is normalised to make
rates linked to the static spectrum. The new formula- model and test results comparable. The predicted
tion uses the viscous asymptote of the dynamic spec- behaviour is now clearly rate-dependent on the full
trum as the ‘‘purely elastic’’ asymptote for the static rate range investigated.
Dynamic experimental results are compared to the
prediction of the multispectrum model (Figure 11), with
Table 3. Value of multispectrum model parameters used for
the same set of viscous parameters (Table 3). Light grey
the virtual test: nstat stat
0 and nc are standard values from the
literature
curves have been used for the dynamic identification
(Results of the dynamic identification section) G12 ,
G12 ndyna
0 ndyna
c nstat
0 nstat
c n 66 ndyna
c , ndyna
0 , 66 , and n. The dark grey curve can be
used as a prediction case. Dynamic results with the
15,800 MPa 5.6 9.25 5 8 0.8 2.5 3.2
multispectrum model are subject to minor
∼
σ12
0.9
0.8
0.7
0.6 Experiments
σ̇12 = 5MPa/s
0.5
σ̇12 = 0.5MPa/s
σ̇12 = 0.05MPa/s
0.4
0.3 Numerical
σ˙ 12 = 5MPa/s
0.2 σ˙ 12 = 0.5ΜPa/s
σ̇12 = 0.05MPa/s
0.1
2ε 12
0
0 0.002 0.004 0.006 0.008 0.01 0.012 0.014 0.016 0.018
Figure 10. Comparison between static experimental data from Graindorge27 and the prediction of the model with the
multi-gaussian spectrum.
σ [MPa]
90
80
70
60
50
40
30
20
4 m/s 0.1 m/s 500 mm/min 5 mm/min
Error 1 10% 5% 6% 5%
10 Error 2 29% 11% 10% 12%
ε
0
0 1 2 3 4 5 6 7
−3
x 10
Figure 11. Comparison between experimental data (dots) and numerical results with a multispectrum model (plain curves) for
dynamic tests on G939/M18. Light grey curves are those used for previous identification of the dynamic mono-spectrum model and
dark grey curves estimates predictions from the model.
modifications as compared to those obtained with the static tests. An improved multispectrum formulation
dynamic mono-spectrum (Figure 4). This is related to of this model was then presented and evaluated.
the small overlap area between the static and the The capability of the new formulation was demon-
dynamic spectra, as shown in Figure 8. Results with strated by virtual tests and qualitative comparison
this multi-spectrum model are significantly better than with experimental data.
those with the large mono-spectrum model (Figure 7), A dedicated experimental campaign remains to be
since strain rate effects are effective for both the high performed on a standard CFRP material in order to
strain rate and static cases. fully validate this improved formulation for a wide
These results confirm the capability of the multi- range of loadings. The campaign will also allow results
gaussian spectrum to be representative over a large to be assessed for unidirectional tape materials. Last,
range of strain rates. This viscoelastic behaviour others works are also under progress on M21 material
should therefore be more suitable for dynamic, static samples to investigate if the multispectrum formulation
and creep tests on composite laminates. would also prove relevant for the pure epoxy constituent.
Conclusion Funding
This work was supported by DGA (French Ministry of
The purpose of the present study was to model the
Defense).
effect of strain rates on aeronautical CFRP composite
laminates behaviour, with special attention to variation
in the tangent shear modulus G12 of a ½45 s laminate, Acknowledgements
which was shown to be rate-dependent. The authors gratefully acknowledge funding from the DGA
A viscoelastic spectral model was used to model the (French Ministry of Defense) for this work.
laminate ply behaviour. The reference model was iden-
tified on dynamic tests as being suitable for high Conflict of Interest
strain rates. However, it was no longer predictive for None declared.