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PM/ 2074/ 2

Aug 2020

PRODUCT MANUAL
FORREADY MIXED PAINT, AIR DRYING, RED OXIDE – ZINC CHROME, PRIMING
ACCORDING TO IS 2074: 2015

This Product Manual shall be used as reference material by all Regional/Branch Offices & licensees to
ensure coherence of practice and transparency in operation of certification under Scheme-I of Bureau
of Indian Standards (Conformity Assessment) Regulations, 2018 for various products. The document
may also be used by prospective applicants desirous of obtaining BIS certification licence/certificate.
1. Product : IS 2074 : 2015
READY MIXED PAINT, AIR DRYING, RED OXIDE – ZINC
Title :
CHROME, PRIMING
No. of Amendments : 1

2. Sampling Guidelines:
a) Raw material : Pigments and driers shall be as per cl. 5 of IS 2074:2015
There are no different varieties mentioned in the Indian
b) Grouping guidelines : Standard, so no grouping guidelines required.

c) Sample Size : 4x500ml

3. List of Test Equipment : Please refer ANNEX –A

Scheme of Inspection and


4. : Please refer ANNEX –B
Testing

5. Possible tests in a day :


Consistency , mass, Flash point , Finish , Drying Time , Viscosity, Colour, Volume solids, Scratch
Hardness, Bend Test
6. Scope of the Licence :

“Licence is granted to use Standard Mark as per IS 2074:2015with the following scope:
READY MIXED PAINT, AIR DRYING, RED OXIDE – ZINC CHROME,
Name of the product
PRIMING

BUREAU OF INDIAN STANDARDS


Manak Bhawan, 9, Bahadur Shah Zafar Marg,
New Delhi – 110002
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ANNEX A

List of Test Equipment

Major test equipment required to test as per the Indian Standard

S. Tests used in with Clause Chemicals Equipments


No Reference
1 Composition Dilute Sulphuric Acid Stirer glass rod
5.1 Potassium Iodide Solution water-bath, separarting
Standard Sodium funnel
Thiosulphate Filter paper (Whatman No.
Starch Solution 42)
Potassium Ferricyanide conical flask.
Solution Titration stand with pippete
Ammonium Bifluoride Petri Dish
Sodium Hydroxide Solution conical flask , weighing
Alcohol , Glacial acetic acid balance
Petroleum Hydrocarbon distillation unit
solvent oven , test tube
Phenol Porcelain Tile
Bromine Evaporating Dish

2 Total Non volatile content Benzene , Methyl alcohol Centrifugal machine


5.1 water-bath
Analytical balance
oven , petri dish

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3 Zinc oxide content Chromic Dilute Sulphuric Acid Stirrer glass rod
anhydride content Potassium Iodide Solution water-bath, separating
(5.1.1) Standard Sodium funnel
Thiosulphate Filter paper (Whatman No.
Starch Solution 42)
Potassium Ferricyanide conical flask.
Solution Titration stand with pippete
Ammonium Bifluoride Petri Dish
Sodium Hydroxide Solution conical flask , weighing
Alcohol , Glacial acetic acid balance
Petroleum Hydrocarbon distillation unit
solvent oven , test tube
Phenol Porcelain Tile
Bromine Evaporating Dish

4 Red Oxide (5.1.1) Standard Potassium water-bath


Dichromate Solution Hot Plate
Stannous Chloride Solution Filter paper (Whatman
Hydrochloric Acid-R No. 30 )
Dilute Sulphuric Acid Hot Plate
Phosphoric Acid

Saturated Aqueous Solution


of Mercuric Chloride
Diphenylamine Indicator
5 Lead restriction (clause 5.5) Analytical balance
Filter paper (Whatman No.
42)
Oven, Centrifuge
Toulene
Benzene

6 Consistency (5.6 & table 1 ) Palette Knife or Metal Rod


Glass Panels
Viscosity ((5.6 & table 1 ) Flow cup , thermometer ,
Flow Cup method stand , stop watch
Glas plate
Viscometer method Viscometer
Beaker , Thermometer ,
weights

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7 Mass in Kg / litre Thermo meter


(5.6 & table 1 ) Weight per 10 Litre Cup
(Pyknometer)

8 Drying Time Mild steel panel , Brush ,


(5.6 & table 1 ) conditioning chamber
Stop watch ,ballotinigarded,
Panel stand

9 Finish Mild steel panel, Brush&


(5.6 & table 1 ) panel stand

10 Fineness of grind Heghman Grinding gauze ,


(5.6 & table 1 ) scraper
11 colour Mild steel panel, Brush&
(5.6 & table 1 ) panel stand
Oven , Humidity Chamber ,
thickness gauge
Color matching table ,
reference Table

12 Fexibility and adhesion Bending Mandrel 6.25mm,


(5.6 & table 1 ) Humidity chamber
Bend Test Tim panel , Brush, panel Stand

Scratch Hardness Automatic hardness Tester


(load 1000gm) with needle
Mild steel panel, Brush&
panel stand
Oven , Humidity Chamber
13 Flash Point Abels Flash point apparatus
(5.6 & table 1 ) Thermometer

14 Volume Solids Volume solid disk ,


(5.6 & table 1 ) Analytical Balance , Beaker
Mass per liter cup Oven
15 Resistance to Humidity Distill water Metal Panels, Hot Plate

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Resistance If humiduty under Corrosion Cabinet,Humidity


condition chamber
of condensation Rotating panerrack , Oven
(5.6 & table 1 )
Resistance to sea water molten wax Salt Spray apparatus
(5.6 & table 1 ) mild steel panel
Micrometer

RESISTANCE TO SALT SPRAY spray solution Spray cabinet


(5.6 & table 1 ) mild steel panel
cotton wool
Collecting device
16 Accelerated storage Oven
(5.6 & table 1 ) Metal container 500 Ml
Ford cup
Gloss meter

17 Keeping Properties Spatula


Weighing balance
Nylon Brush

The above list is indicative only and may not be treated as exhaustive.

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Annex- B
Scheme of Inspection And Testing

1. LABORATORY - A laboratory shall be maintained which shall be suitably equipped (as per the
requirement given in column 2 of Table 1) and staffed, where different tests given in the specification
shall be carried out in accordance with the methods given in the specification.
1.1The manufacturer shall prepare a calibration plan for the test equipments.

2. TEST RECORDS –The manufacturer shall maintain test records for the tests carried out to establish
conformity.

3. PACKING AND MARKING–The Standard Mark, as given in the Schedule of the license shall be printed
on each container and on the label applied to the container; provided always that the material in each
container on which this Mark is thus applied conforms to every requirement of the specification.

3.1 Packing and Marking shall be done as per the requirements of the standard. In addition, the
following details shall be marked on labels affixed to each container:
i) Licence No. (CM/L……………)
ii) BIS website details: ‘For BIS certification details please visit www.bis.gov.in’ .

4. CONTROL UNIT – For the purpose of this scheme, the entire quantity of the product produced in a
batch mixer at a time shall constitute a control unit.

5. LEVELS OF CONTROL- The test and inspection as indicated in Table 1 and at the levels of control
specified therein,shall be carried out on the whole production of the factory which is covered by this
Scheme of testing and appropriate records and charts maintained in accordance with paragraph 2
above.

5.1 All the production which conforms to the Indian Standard and covered by this license shall be
marked with the BISStandard Mark.

6. REJECTIONS– Disposal of non-conforming product shall be done in such a way so as to ensure that
there is no violation of provisions of BIS Act, 2016 and shall be made as per relevant provisions of the
extant law for disposal of such products. A separate record shall be maintained giving information on
quantity and control unit number, relating to all such rejections/defective/sub-standard material of the
production not conforming to the requirements of the Specification and the method of its disposal.
Such material shall in no case be stored together with that conforming to the Specification. The
Standard Mark (if already applied) on rejected material should be defaced.

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IS 2074:2015
READY MIXED PAINT, AIR DRYING, RED OXIDE –
ZINC CHROME, PRIMING
TABLE 1 LEVELS OF CONTROL
(Cl.5 of Scheme of Testing and Inspection)

(1) (2) (3)


Test equipment
Test Details Levels of Control
requirement
Test Method R: required (or)
S: Sub-contracting
No. of
Cl. Requirement Clause Reference Frequency Remarks
permitted Sample

Composition 5.1 IS 2074:2015 R One Fifth Control Unit In case of failure of any sample in
5.1 these requirements (every 5th
Non-volatile Vehicle content control unit tests), that control
- IS 101(Pt8/Sec2) R One -do-
(Applicable in defence supply)
unit shall be considered unfit for
(a) Zinc oxidecontent
Chromic anhydride content Annex B -do- R One -do- the purpose of marking. After
(b) Synthetic red oxides of iron or taking needful corrective actions,
natural red oxides of iron or a sample from every subsequent
mixture of both which shall 6 IS 6947(pt2) R One -do- control unit shall be tested and
5.1.1 correspond to red oxide (as Fe2O3),
% by mass regular frequency (every five
control units) shall be resumed
- - R One -do- only when samples from 2
(c) Suitable Extenders
consecutive control units pass.
5.1.2 Volatile vehicle 5.1.2 IS 2074: 2015 R One -do-
Suitability for use with oleoresins If any sample fails in these
syntheticand nitrocellulose based requirements (each control unit
5.2 undercoats, surfaces, fillers and 5.2 IS 2074: 2015 R One Every Control Unit test), that control unit shall be
putty considered unfit for the purpose of
5.3 Compatibility with Thinner 5.3 IS 2074:2015 R One -do- marking. After taking needful
5.4 Freedom from Objectionable -do- R One corrective actions, sample from
Impurities -do-
5.5 Lead Restriction IS 101(Pt 8/Sec 5) R One every subsequent control unit shall
-do-

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be tested and regular frequency
5.6 & shall be resumed only when samples
Table 1 from 2 consecutive control units
pass.
IS 2074:2015
(a) Consistency One
Annex C IS 101(Part R -do- -do-
i) 1/Sec 5)
(b) Viscosity by ford cup IS 101 (Pt 1.Sec 5) One
R -do-
no. 4at 27±2oC -do-

ii) Mass in kg /10 litre IS 101(Pt 1/Sec 7) R one Every Control


Unit -do-
Drying time, h, IS 101 (Pt3/Sec1):
iii a) Surfacedry R One -do- -do-
1986
b) Harddry
IS 101 (Pt.3/Sec -do-
iv) 4)
a) Finish - R one -do-

b) Gloss60° IS 101(Pt 4/Sec -do-


- 4):88 R one -do-

v) Fineness of grind, microns IS 101(Pt.3/Sec 5) R One -do- -do-


IS 101(Pt 4/Sec
vi) Colour R One -do- -do-
2):88
Flexibility and Adhesion:
a) Bend test (with 6.25
vii) mmdia mandrel and in R One -do- -do-
Cl2 IS 101 (Pt.5/Sec2)
type 1 apparatus)
b) Scratch hardness
(load1000g) Cl3 IS 101 (Pt 5/Sec2)
viii) Flash point IS 101 (Pt 1/Sec6) R One -do- -do-
ix) Volume solids, percent, Min IS 101(Pt 8/Sec 6) R One -do- -do-
Resistance if humidity under
x) condition of condensation

a) Resistance to humidity Cl 2 IS 101 (Pt6/Sec1) S Every 10th Control


One unit If any sample fails in these
b) Resistance to sea water. Annex D IS 2074:2015 R One -do- requirements (every 10th control

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(applicable for marine unit tests), that control unit shall be
paints only) considered unfit for the purpose of
c) Resistance to saltspray Annex E IS 2074:2015 S One -do- marking. After taking needful
xi) Accelerated storage stability test Annex F IS 2074 :2015 R One -do- corrective actions, sample from
every subsequent control unit shall
be tested and regular frequency
xii) Keeping properties. IS 101(Pt6/Sec 2) R One -do- shall be restored, only when
samples from 5 consecutive control
units pass.

Note 1: Whether test equipment is required or sub-contracting is permitted in column 2 shall be decided by the Bureau and shall be mandatory. Sub-contracting
is permitted to a laboratory recognized by the Bureau or Government laboratories empaneled by the Bureau

Note 2: Levels of control given in column 3 are only recommendatory in nature. The manufacturer may define the control unit/batch/lot and submit his own
levels of control in column 3 with proper justification to the Head BO.

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