a.

Penetapan Kadar Sampel

% Kadar Sampel

y = 0.0019x + 0.15
0.421 = 0.0019+ 0.15
0.421 – 0.15 = 0.0019x
0.271 = 0.0019x
0.271
x=
0.0019
x = 142,6315 x faktor pengenceran
x = 142,6315 x 25
x = 3565,7875 ppm
mg Analit
3565,7875
mg analit = x 50 = 178,285 mg/ 50 mL
1000

% Kadar Ciprofloxacin HCl

g analit
% kadar Ciprofloxaccinj HCl= x 100%
g sampel

0.1782
= x 100%
2
= 8,91 %

BM Ciprofloxacin
Kadar Ciprofloxacin = x berat Ciprofloxacin HCl
BM Ciprofloxacin HCl
331,4
= 385,8 x 0,1782gram

= 0,1530 gram
0,1530
% Kadar Ciprofloxacin = x 100% = 7,65 %
2