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  • Bab Iv Hasil Pengamatan: Kurva Baku

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    The document reports the results of observations from an experiment involving paracetamol and EDTA solutions. It includes tables showing the absorbance measurements of standard paracetamol solutions at different concentrations, sample solutions of paracetamol and NaEDTA at various amounts, and a blank solution. Graphs are presented of the calibration curves for paracetamol and paracetamol with NaEDTA. Calculations are shown for making standard solutions of different concentrations and for determining the concentrations of samples based on their absorbance values and the calibration curves.

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    The document reports the results of observations from an experiment involving paracetamol and EDTA solutions. It includes tables showing the absorbance measurements of standard paracetamol solutions at different concentrations, sample solutions of paracetamol and NaEDTA at various amounts, and a blank solution. Graphs are presented of the calibration curves for paracetamol and paracetamol with NaEDTA. Calculations are shown for making standard solutions of different concentrations and for determining the concentrations of samples based on their absorbance values and the calibration curves.

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    15 views5 pages

    Bab Iv Hasil Pengamatan: Kurva Baku

    Uploaded by

    Dela djamaludin
    The document reports the results of observations from an experiment involving paracetamol and EDTA solutions. It includes tables showing the absorbance measurements of standard paracetamol solutions at different concentrations, sample solutions of paracetamol and NaEDTA at various amounts, and a blank solution. Graphs are presented of the calibration curves for paracetamol and paracetamol with NaEDTA. Calculations are shown for making standard solutions of different concentrations and for determining the concentrations of samples based on their absorbance values and the calibration curves.

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    of 5

    BAB IV

    HASIL PENGAMATAN

    4.1 Tabel Pengamatan


    4.1.1 Larutan Standar

    No Sampel Absorban (nm)


    1. Parasetamol 10 ppm 0,201
    2. Parasetamol 20 ppm 0,251
    3. Parasetamol 30 ppm 0,360
    4.1.2 Larutan Sampel

    No Sampel Absorban (nm)


    1. Pct + NaEDTA 0,2 gr 0,301
    2. Pct + NaEDTA 0,4 gr 0,410
    3. Pct + NaEDTA 0,6 gr 0,501
    4.1.3 Larutan Blangko

    No Sampel Absorban (nm)


    1. Aquadest 0,00
    4.1.4 Grafik Kurva Baku Parasetamol

    KURVA BAKU
    0.4
    0.35
    0.3 f(x) = 0.01 x + 0.11
    R² = 0.96
    ABSORBAN

    0.25
    0.2
    0.15 Linear ()
    0.1
    0.05
    0
    5 10 15 20 25 30 35
    KONSENTRASI

    4.1.5 Grafik Kurva Baku Na EDTA + Parasetamol

    14
    KURVA BAKU
    0.6
    0.5
    f(x) = 0.5 x + 0.2
    0.4 R² = 1
    ABSORBAN

    0.3
    Linear ()
    0.2
    0.1
    0
    0.15 0.2 0.25 0.3 0.35 0.4 0.45 0.5 0.55 0.6 0.65
    KONSENTRASI

    4.1 Perhitungan
    4.2.1 Perhitungan pengenceran
     Pengenceran 1000 ppm
    1000 × X = 1.000.000 × 0.01 gr
    1000 × X = 10.000/1000
    X = 10 ml
     Pengenceran untuk 100 ppm
    M1× V1 = M2 × V2
    1000 × V1 = 100 × 10
    V1 = 100 × 10 / 1000
    V1 = 1 ml
     Pengenceran untuk 10 ppm
    M1 × V1 = M2 × V2
    100 × V1 = 10 × 10
    V1 = 10 × 10 / 100
    V1 = 1 ml
     Pengenceran untuk 20 ppm
    M1 × V1 = M2 × V2
    100 × V1= 20 × 10
    V1 = 20 × 10 / 100

    16
    V1 = 2 ml
     Pengenceran untuk 30 ppm
    M1 × V1 = M2× V2
    100 × V1= 30 × 10
    V1 = 30 × 10 / 100
    V1 = 3 ml
    4.2.2 Perhitungan konsentrasi
    a. Larutan standar
     Larutan pct 10 ppm
    Dik : a = 0,111
    bx = 0,008
    Penye : y = bx + a
    0,201 = 0,008x + 0,111
    0,201-0,111 = 0,008x
    0,09 = 0,008x
    x = 0,09 / 0,008 = 11,25 ml
     Larutan pct 20 ppm
    Dik : a = 0,111
    bx = 0,008
    Penye : y = bx + a
    0,251 = 0,008x + 0,111
    0,251-0,111 = 0,008x
    0,14 = 0,008x
    x = 0,14 / 0,008 = 17,5 ml
     Larutan pct 30 ppm
    Dik : a = 0, 111
    bx = 0,008
    Penye : y = bx + a
    0,360 = 0,008x + 0,111
    0,360-0,111 = 0,008x
    0,249 = 0,008x

    16
    x = 0,249 / 0,008 = 31,125 ml
    b. Larutan sampel
     Pct 10 ppm + NaEDTA 0,2 gr
    Dik : a = 0,204
    bx = 0,5
    Penye : y = bx + a
    0,301 = 0,5x + 0,204
    0,301-0,204 = 0,5x
    0,097 = 0,5x
    x = 0,097 / 0,5 = 0,194 ml
     Pct 20 ppm + NaEDTA 0,4 gr
    Dik : a = 0,204
    bx = 0,5
    Penye : y = bx + a
    0,410 = 0,5x + 0,204
    0,410-0,204 = 0,5x
    0,206 = 0,5x
    x = 0,206 / 0,5= 0,412 ml
     Pct 30 ppm + NaEDTA 0,6 gr
    Dik : a = 0,204
    bx = 0,5
    Penye : y = bx + a
    0,501 = 0,5x + 0,204
    0,501-0,204 = 0,5x
    0,297 = 0,5x
    x = 0,297 / 0,5 = 0,594 ml

    16
    16

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