REPORT

Removal of Underground Storage Tanks

6556 E. McNichols Property
Detroit, Michigan

July 5, 2018 NTH Project No. 62-170450-03

NTH Consultants, Ltd.

41780 Six Mile Rd., Suite 200
Northville, MI 48168
 TABLE OF CONTENTS

Page No.

1.0 INTRODUCTION 1

2.0 INITIAL REGULATORY FILINGS 1

3.0 SUMMARY OF UST REMOVAL ACTIVITIES 2

4.0 DOCUMENTATION OF RELEASE AND REMOVAL 2

APPENDICES

SITE AND UST LOCATION PLAN, FIGURE 1 APPENDIX A

REGULATORY DOCUMENTS APPENDIX B

WASTE DISPOSAL DOCUMENTATION APPENDIX C

LABORATORY DATA APPENDIX D

O:\Active PROJ\62-170450_6556 E. McNichols Property\730 - Reports\03\001-0705-LTR-RPT.doc -i-

 1.0 INTRODUCTION

NTH Consultants, Ltd. (NTH) was retained by 6556 McNichols LLC to provide
environmental consulting services related to removal of three underground storage tanks
(USTs) from the 6556 East McNichols Road property in Detroit, Michigan.

NTH completed a Phase I Environmental Site Assessment (ESA) for the property, dated
January 5, 2018. The Phase I ESA identified three USTs under the canopy area near the
southwest corner of the building. Review of the UST Facility File obtained from the
Michigan Department of Licensing and Regulatory Affairs (LARA) indicated that the USTs
were each 1,000 gallons in capacity and were installed in 1957. The USTs were reported to
contain cutting oil, lubrication oil and waste oil, and remained in use until the early 1990s.

Prior to removal, the USTs were gauged and each contained approximately two feet of liquid.
The approximate locations of the USTs are indicated on Figure 1 in Appendix A. A site
showing the property layout is included as Figure 2 in Appendix A.

On February 5, 2018, HM Environmental Services, Inc. (HM) submitted a composite sample

of the UST contents to be analyzed for waste characterization parameters for offsite disposal
purposes. Results of laboratory analysis determined that waste from the USTs would be
considered hazardous due to the presence of vinyl chloride. A copy of the laboratory
analytical report is presented in Appendix D.

2.0 INITIAL REGULATORY FILINGS

On April 23, 2018, NTH submitted an Intent of Removal form for the USTs to the LARA.
The Intent of Removal form also registered 6556 McNichols LLC as the new owner of the
USTs. LARA responded by email on April 24, 2018, approving the tank removal activities to
commence after May 24, 2018. Copies of the Intent of Removal form and LARA response
are included in Appendix B.

O:\Active PROJ\62-170450_6556 E. McNichols Property\730 - Reports\03\001-0705-LTR-RPT.doc -1-

 3.0 SUMMARY OF FIELD ACTIVITIES

On May 29, 2018, NTH visited the site to observe HM remove the USTs. The USTs were of
single-wall steel construction. Prior to excavation, HM used a vacuum truck to remove
residual liquid from the USTs. Once the USTs were exposed, HM created an opening in the
top of each UST. Oily sludge remaining in the bottom of each UST was placed into drums.
The UST interiors were then cleaned using water spray. HM used an excavator to remove the
USTs from the ground. Multiple corrosion holes were visible in the bottom of each UST.
Stained soil with petroleum odors was observed in the excavation.

Approximately 800 gallons of liquid were removed and transported to Environmental Geo-
Technologies LLC of Romulus, Michigan for disposal. Copies of the disposal manifests are
included in Appendix C. The USTs were transported to McNichols Scrap Iron and Metal
Company upon removal.

Prior to backfilling, three floor samples were collected, one from beneath each fill port as
depicted on Figure 1. These samples were not analyzed as the analysis was not expected to
yield additional relevant data based on the known contents of the USTs and results of
previous Phase II ESA. The UST excavation was backfilled with excavated soil followed by
a layer of crushed stone.

4.0 DOCUMENTATION OF RELEASE AND REMOVAL

Based on visual and olfactory evidence observed during the UST removals, a release to the
environment was evident. As such, NTH submitted a Confirmed Release Report to LARA.
The report was submitted at 11:19 am on May 30, 2018. LARA assigned confirmed release
number C-0087-18. A copy of the Release Report is included in Appendix B.

O:\Active PROJ\62-170450_6556 E. McNichols Property\730 - Reports\03\001-0705-LTR-RPT.doc -2-

To document removal of the USTs to LARA, NTH also completed an amended Registration
of Underground Storage Tanks form. This form was submitted to LARA on June 26, 2018.
A copy of the amended registration form is also included in Appendix B.

NTH submitted a Baseline Environmental Assessment (BEA) report to MDEQ on behalf of

the current property owner, 6556 McNichols LLC, within 45 days of property acquisition. As
such, the current property owner is not liable for remediating the contamination associated
with the former UST and is not required to pursue Part 213 UST closure activities as they
were not the owner/operator of the former USTs. However, the current owner has due care
obligations under Section 7(a) of Part 201 rules.

O:\Active PROJ\62-170450_6556 E. McNichols Property\730 - Reports\03\001-0705-LTR-RPT.doc -3-

APPENDIX A
// SITE & UST LOCATION PLAN
 N

LEGEND

NTH PROJECT No.: CAD FILE NAME:

FIGURE:
SITE AND UST LOCATION PLAN

1
DESIGNED BY: PLOT DATE:
NTH Consultants, Ltd.
DRAWN BY: DRAWING SCALE: Infrastructure Engineering
and Environmental Services 6556 E MCNICHOLS RD
CHECKED BY: INCEPTION DATE:
DETROIT, MICHIGAN
 McNICHOLS ROAD (6 MILE ROAD)
N

GIRARDIN STREET

LEGEND

NTH PROJECT No.: CAD FILE NAME:

FIGURE:
SITE PLAN

2
DESIGNED BY: PLOT DATE:
NTH Consultants, Ltd.
DRAWN BY: DRAWING SCALE: Infrastructure Engineering
and Environmental Services 6556 E. McNICHOLS ROAD
CHECKED BY: INCEPTION DATE:
DETROIT, MICHIGAN
APPENDIX B
// REGULATORY DOCUMENTS
 Department of Licensing and Regulatory Affairs, Bureau of Fire Services, Storage Tank Division
P.O. Box 30033, Lansing, MI 48909
Phone 517-241-8847, Fax 517-332-1428

RELEASE REPORT: SUSPECTED CONFIRMED BFS USE ONLY

THIS INFORMATION IS REQUIRED UNDER 1994 PA 451, AS AMENDED (Act 451). FACILITY ID NUMBER ENTRY DATE
FAILURE TO COMPLY WITH THE PROVISIONS OF THIS ACT MAY RESULT IN A
MISDEMEANOR AND/OR CIVIL PENALTIES NOT TO EXCEED $5000 PER DAY, PER
TANK.
INSTRUCTIONS: This form applies to releases of petroleum and hazardous UPGRADE/CANCEL DATE INCIDENT NUMBER
substances from underground storage tanks regulated under Part 211,
Underground Storage Tanks, of the Natural Resources and Environmental DATE REPORTED TIME REPORTED
Protection Act, 1994 PA 451, as amended (PA 451).
AM PM
The owner or operator must report suspected and confirmed releases to the Bureau of
REPORTED BY: FAX E-MAIL REGULAR MAIL
Fire Services (BFS) within 24 hours of discovery. The report may be made by a
consultant on behalf of the owner/operator. FAX this form to 517-332-1428 or call
517-335-7210. All information on this form must be provided regardless of whether the
release is reported by telephone or FAX. For further information see page 2.
Signature

PERSON REPORTING RELEASE COMPANY (IF NOT OWNER/OPERATOR) AREA CODE & TELEPHONE NUMBER
Ashley Lesser NTH Consultants, Ltd. (248) 553-6300
TANK REMOVAL CONTRACTOR CONTRACTOR CONTACT CONTRACTOR AREA CODE & TELEPHONE NUMBER
HM Environmental Services Inc. Bob Borst (586) 469-0041
I. OWNERSHIP OF TANKS II. LOCATION OF TANKS
NAME OF OWNER (CORPORATION, INDIVIDUAL, ETC.) FACILITY NAME OR COMPANY SITE IDENTIFIER
6556 McNichols LLC 6556 McNichols Site
STREET ADDRESS STREET ADDRESS (P.O. Box Not Acceptable)
1437 Woodward Avenue, Apt. 414 6556 E. McNichols Road
CITY STATE ZIP CODE CITY COUNTY STATE ZIP CODE
Detroit MI 48226 Detroit Wayne MI 48212
AREA CODE & TELEPHONE NUMBER AREA CODE & TELEPHONE NUMBER
(248) 770-5097 N/A (unoccupied site)
DATE RELEASE DISCOVERED: May 29, 2018 CONTACT PERSON FOR LOCATION
TIME RELEASE DISCOVERED: 12:10 AM PM Cort Kwiecinski
TANK NUMBER1 (if known) 1 / UTK-042218-15 2 / UTK-055115-15 3 / UTK-055118-15
SIZE OF TANK (gallons) 1,000 1,000 1,000
SUBSTANCE RELEASED Used Oil Used Oil Used Oil
CONSTRUCTION OF TANK Steel Steel Steel
REASON FOR RELEASE Corrosion of tank Corrosion of tank Corrosion of tank

CAUSE OF RELEASE Tank Tank Tank Tank Tank

(Check all that apply) Piping Piping Piping Piping Piping
Spill Protection Spill Protection Spill Protection Spill Protection Spill Protection
Overfill Protection Overfill Protection Overfill Protection Overfill Protection Overfill Protection
Dispenser Dispenser Dispenser Dispenser Dispenser
Unknown Unknown Unknown Unknown Unknown
IM-10 IM-10 IM-10 IM-10 IM-10
Other (provide details Other (provide details in Other (provide details in Other (provide details in Other (provide details in
in comments) comments) comments) comments) comments)

HOW WAS LEAK Tank Removal Tank Removal Tank Removal Tank Removal Tank Removal
DETECTED Inventory Records Inventory Records Inventory Records Inventory Records Inventory Records
(Check all that apply) Repairs Repairs Repairs Repairs Repairs
Stained Soil Stained Soil Stained Soil Stained Soil Stained Soil
Petroleum Odors Petroleum Odors Petroleum Odors Petroleum Odors Petroleum Odors
Analytical Data Analytical Data Analytical Data Analytical Data Analytical Data
Free Product and/or Free Product and/or Oil Free Product and/or Oil Free Product and/or Oil Free Product and/or Oil
Oil Sheen in Sheen in Groundwater Sheen in Groundwater Sheen in Groundwater Sheen in Groundwater
Groundwater
COMMENTS (attach additional sheets if necessary): Facility ID: 00019920. Corrosion holes were noted on all 3 USTs.

1
Copy this page for additional tanks if needed. Page 1 of 2 BFS-3826 (Rev 12/17)
 Department of Licensing and Regulatory Affairs, Bureau of Fire Services, Storage Tank Division
REGISTRATION OF UNDERGROUND STORAGE TANKS
The information in this form is required under “Part 211, Underground Storage Tank Regulations, of the Natural Resources and Environmental Protection Act,
1994 PA 451, as amended.” Any owner who knowingly fails to notify or submits false information shall be subject to a misdemeanor and/or civil penalties not
to exceed $5,000 per day for each tank for which notification is not given or for which false information is submitted.
If sending form, mail to: LARA, Bureau of Fire Services, Storage Tank Division, FACILITY
P.O. Box 30033, Lansing, MI 48909
NEW REGISTRATION ID NUMBER
If sending form OVERNIGHT: LARA, Bureau of Fire Services, Storage Tank (if known)
AMENDED INFORMATION Division, 3101 Technology Blvd, Suite H, Lansing, MI 48910
00019920
(for Registered USTs Only)

NUMBER OF TANKS AT FACILITY: _0_____ NUMBER OF CONTINUATION SHEETS ATTACHED: _2_____

I. OWNERSHIP OF TANKS II. LOCATION OF TANKS

IF THIS IS A NEW OWNER’S ADDRESS, PLEASE CHECK IF INFORMATION IS THE SAME AS SECTION I, PLEASE CHECK
OWNER NAME (Corporation/Individual, etc.) FACILITY NAME OR SITE IDENTIFIER
6556 McNichols LLC 6556 McNichols
MAILING ADDRESS STREET ADDRESS (P.O. Box Not Acceptable)
1437 Woodward Ave., Apt 414 6556 E. McNichols
CITY STATE ZIP CITY STATE ZIP
Detroit MI 48226 Detroit MI 48212
COUNTRY (Please Specify) COUNTY
USA OTHER ___________________________ Wayne
AREA CODE & PHONE NUMBER AREA CODE & PHONE NUMBER
( 248 ) 770-5097 ( ) N/A – Vacant

III. TYPE OF OWNER

FEDERAL COMMERCIAL
STATE GOVERNMENT PRIVATE
LOCAL GOVERNMENT ARE TANKS LOCATED ON LAND WITHIN A RESERVATION? YES NO
IF TANKS ARE LOCATED WITHIN A RESERVATION, DOES A NATIVE AMERICAN TRIBE OWN TANKS? YES NO
IF TANKS ARE OWNED BY A TRIBE, NAME OF TRIBE: ____________________________________________

IV. TYPE OF FACILITY

PUBLIC GAS STATION LOCAL GOVERNMENT CONTRACTOR
PRIVATE GAS STATION STATE GOVERNMENT TRUCKING/TRANSPORT
MARINE GAS STATION FEDERAL/NON-MILITARY UTILITIES
PETROLEUM DISTRIBUTOR FEDERAL-MILITARY RESIDENTIAL
AIRLINE AND/OR AIRCRAFT OWNER COMMERCIAL FARM
AUTO DEALERSHIP INDUSTRIAL OTHER (Explain)____________________
RAILROAD HOSPITAL

V. CONTACT PERSON
Name Job Title Area Code & Phone No.
Cort Kwiecinski ( 248 ) 770-5097
Class A operator: Name: Company Area Code & Phone No.
N/A – No USTs Present
Class B operator: Name: Company Area Code & Phone No.
N/A – No USTs Present
VI. CERTIFICATION
I CERTIFY UNDER PENALTY OF LAW THAT I HAVE PERSONALLY EXAMINED AND AM FAMILIAR WITH THE INFORMATION SUBMITTED IN THIS FORM AND ALL
ATTACHED DOCUMENTS AND THAT I HAVE VERIFIED THAT THE INFORMATION IS TRUE, ACCURATE, AND COMPLETE.
NAME AND OFFICIAL TITLE OF OWNER OR OWNERS’ AUTHORIZED REPRESENTATIVE SIGNATURE DATE
Ashley Lesser, NTH Consultants, Ltd. 6/25/18
Page 2 of 6 BFS-3821 (Rev 12/17)
 VII. DESCRIPTION OF UNDERGROUND STORAGE TANKS
(Complete the following pages for each tank at this location. Copy these pages for additional tanks if needed.)
TANK IDENTIFICATION NUMBER 1 / UTK-042218-15 2 / UTK-055115-15 3 / UTK-055118-15

1. STATUS OF TANKS (Check One)

CURRENTLY IN USE
TEMPORARILY OUT OF USE
AMENDMENT OF INFORMATION
(If tanks are removed/closed, complete Section VIII)

2. DATE OF INSTALLATION (Month/Day/Year) 6/24/1958 6/24/1958 6/24/1958

3. ESTIMATED TOTAL CAPACITY (Gallons) 1,000 1,000 1,000

VIII. TANKS OUT-OF-USE OR CHANGE-IN-SERVICE (Skip this section if this does not apply and go to Section IX.)
NOTE: A SITE ASSESSMENT MUST BE COMPLETED UNLESS YOU REPORT A CONFIRMED RELEASE

1. CLOSING OF TANK Unknown Unknown Unknown

A. ESTIMATED DATE LAST USED
(Month/Day/Year)

B. ESTIMATED DATE TANK WAS 5/29/2018 5/29/2018 5/29/2018

REMOVED/CLOSED-IN-PLACE or
CHANGE-IN-SERVICE (Month/Day/Year)

C. TANK WAS REMOVED FROM GROUND

D. TANK FILLED WITH INERT
MATERIAL (Sand, Concrete, etc.)
●DESCRIBE TYPE OF FILL USED _______ ________ ________ ___ ___ ___ ___ ___
●REASON TANK WAS NOT REMOVED _______ ________ ________ ___ ___ ___ ___ ___
__ __ __ __ __
(Specify in comments area)
___ ___ ___ ___ ___
2. CHANGE-IN-SERVICE

IX. SUBSTANCE STORED

1. SUBSTANCE CURRENTLY OR LAST

STORED IN GREATEST QUANTITY
BY VOLUME
GASOLINE
DIESEL
GASOHOL
KEROSENE
(Not For Consumptive Use On Premises) FUEL OIL

WASTE OIL
USED OIL
HAZARDOUS SUBSTANCE
HEATING OIL
MIXTURE
TANK HAS COMPARTMENTS

OTHER (Specify in comments area)

(List substances in comments area)
CERCLA NAME AND/OR CHEMICAL ABSTRACT
SERVICE (CAS) NUMBER (if hazardous
substance stored) ________ ________ ________ ___ ___ ___ ___ ___
___ ___ ___ ___ ___
__ __ __ __ __
Page 3 of 6 BFS-3821 (Rev 12/17)
COMMENTS AND/OR CLARIFICATIONS:

_____USTs were removed from the ground on May 25, 2018. Based on visual and olfactory evidence observed during removal, a_______

confirmed release was reported (C-0087-18).___________________________________________________________________________

_______________________________________________________________________________________________________________

_______________________________________________________________________________________________________________

_______________________________________________________________________________________________________________

_______________________________________________________________________________________________________________

_______________________________________________________________________________________________________________

_______________________________________________________________________________________________________________

_______________________________________________________________________________________________________________

_______________________________________________________________________________________________________________

_______________________________________________________________________________________________________________

_______________________________________________________________________________________________________________

_______________________________________________________________________________________ ____________________________

_______________________________________________________________________________________________________________________________

_______________________________________________________________________________________________________________________________

_______________________________________________________________________________________________________________________________

_______________________________________________________________________________________________________________________________

_______________________________________________________________________________________________________________________________

_______________________________________________________________________________________________________________________________

_______________________________________________________________________________________________________________________________

_______________________________________________________________________________________________________________________________

_______________________________________________________________________________________________________________________________

_______________________________________________________________________________________________________________________________

_______________________________________________________________________________________________________________________________

_______________________________________________________________________________________________________________________________

_______________________________________________________________________________________________________________________________

_______________________________________________________________________________________

Page 6 of 6 BFS-3821 (Rev 12/17)

APPENDIX C
// WASTE DISPOSAL
DOCUMENTATION
APPENDIX D
// LABORATORY DATA
 Analytical Laboratory Report

Report ID: S87344.01(01)

Generated on 02/09/2018

Report to Report produced by

Attention: Robert Borst Merit Laboratories, Inc.
HM Environmental Services, Inc. 2680 East Lansing Drive
42826 N. Walnut East Lansing, MI 48823
Mt. Clemens, MI 48043
Phone: (517) 332-0167 FAX: (517) 332-6333
Phone: 586-469-0041 FAX: 586-469-1014
Email: bborst@hmenv.com Contacts for report questions:
John Laverty (johnlaverty@meritlabs.com)
Barbara Ball (bball@meritlabs.com)
Addtional Contacts: John Kemp

Report Summary
Lab Sample ID(s): S87344.01-S87344.02
Project: Christoph Holdings LLC
Collected Date: 02/05/2018
Submitted Date/Time: 02/05/2018 13:51
Sampled by: Unknown
P.O. #:

Table of Contents
Cover Page (Page 1)
General Report Notes (Page 2)
Report Narrative (Page 2)
Laboratory Certifications (Page 3)
Qualifier Descriptions (Page 3)
Glossary of Abbreviations (Page 3)
Method Summary (Page 4)
Sample Summary (Page 5)

Maya Murshak
Technical Director

Report to HM Environmental Services, Inc. Page 1 of 8 Generated on 02/09/2018

Project: Christoph Holdings LLC Report ID: S87344.01(01)
 Analytical Laboratory Report

General Report Notes

Analytical results relate only to the samples tested, in the condition received by the laboratory.
Methods may be modified for improved performance.
Results reported on a dry weight basis where applicable.
'Not detected' indicates that parameter was not found at a level equal to or greater than the reporting limit (RL).
40 CFR Part 136 Table II Required Containers, Preservation Techniques and Holding Times for the Clean Water Act specify that samples
for acrolein and acrylonitrile need to be preserved at a pH in the range of 4 to 5 or if not preserved, analyzed within 3 days of sampling.
QA/QC corresponding to this analytical report is a separate document with the same Merit ID reference and is available upon request.
Full accreditation certificates are available upon request. Starred (*) analytes are not NELAP accredited.
Samples are held by the lab for 30 days from the final report date unless a written request to hold longer is provided by the client.
Report shall not be reproduced except in full, without the written approval of Merit Laboratories, Inc.
Limits for drinking water samples, are listed as the MCL Limits (Maximum Contaminant Level Concentrations)

Report Narrative
There is no additional narrative for this analytical report

Report to HM Environmental Services, Inc. Page 2 of 8 Generated on 02/09/2018

Project: Christoph Holdings LLC Report ID: S87344.01(01)
 Analytical Laboratory Report

Laboratory Certifications
Authority Certification ID
Michigan DEQ #9956
DOD ELAP/ISO 17025 #69699
WBENC #2005110032
Ohio VAP #CL0002
Indiana DOH #C-MI-07
New York NELAC #11814
North Carolina DENR #680
North Carolina DOH #26702
Alaska CSLAP #17-001

Qualifier Descriptions
Qualifier Description
! Result is outside of stated limit criteria
B Compound also found in associated method blank
E Concentration exceeds calibration range
F Analysis run outside of holding time
G Estimated result due to extraction run outside of holding time
H Sample submitted and run outside of holding time
I Matrix interference with internal standard
J Estimated value less than reporting limit, but greater than MDL
L Elevated reporting limit due to low sample amount
M Result reported to MDL not RDL
O Analysis performed by outside laboratory. See attached report.
R Preliminary result
S Surrogate recovery outside of control limits
T No correction for total solids
X Elevated reporting limit due to matrix interference
Y Elevated reporting limit due to high target concentration
b Value detected less than reporting limit, but greater than MDL
e Reported value estimated due to interference
j Analyte also found in associated method blank
p Benzo(b)Fluoranthene and Benzo(k)Fluoranthene integrated as one peak.
x Preserved from bulk sample

Glossary of Abbreviations
Abbreviation Description
RL/RDL Reporting Limit
MDL Method Detection Limit
MS Matrix Spike
MSD Matrix Spike Duplicate
SW EPA SW 846 (Soil and Wastewater) Methods
E EPA Methods
SM Standard Methods

Report to HM Environmental Services, Inc. Page 3 of 8 Generated on 02/09/2018

Project: Christoph Holdings LLC Report ID: S87344.01(01)
 Analytical Laboratory Report

Method Summary
Method Version
ASTMD3278 - 96 ASTM Method D3278 - 96(2011)
SW1311 SW 846 Method 1311 Revision 0 July 1992
SW3015A SW 846 Method 3015A Revision 1 February 2007
SW3510C SW 846 Method 3510C Revision 3 December 1996
SW3550C SW 846 Method 3550C Revision 3 February 2007
SW5030C/8260C SW 846 Method 8260C Revision 3 August 2006 / 5030C Revision 3 May 2003
SW6020A SW 846 Method 6020A Revision 1 February 2007
SW7471B SW 846 Method 7471B Revision 2 February 2007
SW8082A SW 846 Method 8082A Revision 1 February 2007
SW8270D SW 846 Method 8270D Revision 4 February 2007
SW9010B SW 846 Method 9010B Revision 2 December 1996
SW9030B SW 846 Method 9030B Revision 2 December 1996
SW9045D SW 846 Method 9045D Revision 4 November 2004

Report to HM Environmental Services, Inc. Page 4 of 8 Generated on 02/09/2018

Project: Christoph Holdings LLC Report ID: S87344.01(01)
 Analytical Laboratory Report

Sample Summary (2 samples)

Sample ID Sample Tag Matrix Collected Date/Time
S87344.01 Water & Oil (Water Layer) Liquid 02/05/18 10:30
S87344.02 Water & Oil (Oil Layer) Oil 02/05/18 10:30

Report to HM Environmental Services, Inc. Page 5 of 8 Generated on 02/09/2018

Project: Christoph Holdings LLC Report ID: S87344.01(01)
 Analytical Laboratory Report

Lab Sample ID: S87344.01

Sample Tag: Water & Oil (Water Layer)
Collected Date/Time: 02/05/2018 10:30
Matrix: Liquid
COC Reference: 106170

Sample Containers
# Type Preservative(s) Refrigerated? Arrival Temp. (C) Thermometer #
1 32oz Glass None Yes 4.6 IR

Analysis Results Units RL Method Run Date/Time Tech Limits Flags

Extraction / Prep.
Mercury Digestion* Completed SW7471B 02/08/18 10:15 JRH
Metal Digestion Completed SW3015A 02/07/18 11:00 CCM
TCLP Zero Headspace Ext. <0.5% SW1311 02/06/18 11:35 JBL
TCLP/SPLP BNA Extraction Completed SW3510C 02/07/18 14:00 PLB

TCLP Extraction
Inital Sample pH <0.5% SW1311 02/06/18 11:35-02/06 JBL
pH after 3.5 ml HCl <0.5% SW1311 02/06/18 11:35-02/06 JBL
% Solids <0.5% SW1311 02/06/18 11:35-02/06 JBL
Sample Used g <0.5% SW1311 02/06/18 11:35-02/06 JBL
Final Volume mL <0.5% SW1311 02/06/18 11:35-02/06 JBL
TCLP Extraction Fluid <0.5% SW1311 02/06/18 11:35-02/06 JBL
Final Extract pH <0.5% SW1311 02/06/18 11:35-02/06 JBL

Inorganics
Flash Point* Not detected oF 180 ASTMD3278 - 96 02/07/18 16:55 PL <140
pH/ Corrosivity* 5.29 STD Units 0.01 SW9045D 02/08/18 18:54 ASB 2-12.5
Reactive Cyanide* Not detected mg/kg 0.5 SW9010B 02/08/18 13:22 JDP
Reactive Sulfide* Not detected mg/kg 2.0 SW9030B 02/08/18 11:20 JDP

Metals
Arsenic, TCLP Not detected mg/L 0.02 SW6020A 02/07/18 13:45 CCM 5.0
Barium, TCLP 0.41 mg/L 0.05 SW6020A 02/07/18 13:45 CCM 100.0
Cadmium, TCLP Not detected mg/L 0.005 SW6020A 02/07/18 13:45 CCM 1.0
Chromium, TCLP Not detected mg/L 0.05 SW6020A 02/07/18 13:45 CCM 5.0
Lead, TCLP Not detected mg/L 0.03 SW6020A 02/07/18 13:45 CCM 5.0
Mercury, TCLP* Not detected mg/L 0.0005 SW7471B 02/08/18 12:46 JRH 0.2
Selenium, TCLP Not detected mg/L 0.05 SW6020A 02/07/18 13:45 CCM 1.0
Silver, TCLP Not detected mg/L 0.005 SW6020A 02/07/18 13:45 CCM 5.0

Organics - Semi-Volatiles
TCLP Semi Volatiles
o-Cresol* Not detected ug/L 1,000 SW8270D 02/07/18 20:57 PL 200,000
p,m-Cresol Not detected ug/L 1,000 SW8270D 02/07/18 20:57 PL 200,000
Pentachlorophenol Not detected ug/L 1,000 SW8270D 02/07/18 20:57 PL 100,000
2,4,5-Trichlorophenol Not detected ug/L 1,000 SW8270D 02/07/18 20:57 PL 400,000
2,4,6-Trichlorophenol Not detected ug/L 1,000 SW8270D 02/07/18 20:57 PL 2,000
2,4-Dinitrotoluene Not detected ug/L 90 SW8270D 02/07/18 20:57 PL 130
Hexachlorobenzene Not detected ug/L 90 SW8270D 02/07/18 20:57 PL 130
Hexachlorobutadiene Not detected ug/L 100 SW8270D 02/07/18 20:57 PL 500
Hexachloroethane Not detected ug/L 100 SW8270D 02/07/18 20:57 PL 3,000
Nitrobenzene Not detected ug/L 100 SW8270D 02/07/18 20:57 PL 2,000
Pyridine Not detected ug/L 100 SW8270D 02/07/18 20:57 PL 5,000

Report to HM Environmental Services, Inc. Page 6 of 8 Generated on 02/09/2018

Project: Christoph Holdings LLC Report ID: S87344.01(01)
 Analytical Laboratory Report

Lab Sample ID: S87344.01 (continued)

Sample Tag: Water & Oil (Water Layer)

Analysis Results Units RL Method Run Date/Time Tech Limits Flags

Organics - Volatiles (continued)
Organics - Volatiles
TCLP Volatiles
Benzene Not detected ug/L 100 SW5030C/8260C 02/07/18 13:24 JML 500
Carbon tetrachloride Not detected ug/L 100 SW5030C/8260C 02/07/18 13:24 JML 500
Chlorobenzene Not detected ug/L 100 SW5030C/8260C 02/07/18 13:24 JML 100,000
Chloroform Not detected ug/L 100 SW5030C/8260C 02/07/18 13:24 JML 6,000
1,4-Dichlorobenzene Not detected ug/L 100 SW5030C/8260C 02/07/18 13:24 JML 7,500
1,2-Dichloroethane Not detected ug/L 100 SW5030C/8260C 02/07/18 13:24 JML 500
1,1-Dichloroethene Not detected ug/L 100 SW5030C/8260C 02/07/18 13:24 JML 700
2-Butanone (MEK) Not detected ug/L 1,000 SW5030C/8260C 02/07/18 13:24 JML 200,000
Tetrachloroethene 200 ug/L 100 SW5030C/8260C 02/07/18 13:24 JML 700
Trichloroethene Not detected ug/L 100 SW5030C/8260C 02/07/18 13:24 JML 500
Vinyl chloride 1,100 ug/L 100 SW5030C/8260C 02/07/18 13:24 JML 200 !

!-Result is outside of stated limit criteria

Report to HM Environmental Services, Inc. Page 7 of 8 Generated on 02/09/2018

Project: Christoph Holdings LLC Report ID: S87344.01(01)
 Analytical Laboratory Report

Lab Sample ID: S87344.02

Sample Tag: Water & Oil (Oil Layer)
Collected Date/Time: 02/05/2018 10:30
Matrix: Oil
COC Reference: 106170

Sample Containers
# Type Preservative(s) Refrigerated? Arrival Temp. (C) Thermometer #
1 32oz Glass None Yes 4.6 IR

Analysis Results Units RL Method Run Date/Time Tech Limits Flags

Extraction / Prep.
Extraction, PCB* Completed SW3550C 02/07/18 14:30 PLB

Organics - PCBs/Pesticides
PCB List
PCB-1016* Not detected ug/kg 1,000 SW8082A 02/07/18 18:48 JAN
PCB-1242* Not detected ug/kg 1,000 SW8082A 02/07/18 18:48 JAN
PCB-1221* Not detected ug/kg 1,000 SW8082A 02/07/18 18:48 JAN
PCB-1232* Not detected ug/kg 1,000 SW8082A 02/07/18 18:48 JAN
PCB-1248* Not detected ug/kg 1,000 SW8082A 02/07/18 18:48 JAN
PCB-1254* Not detected ug/kg 1,000 SW8082A 02/07/18 18:48 JAN
PCB-1260* Not detected ug/kg 1,000 SW8082A 02/07/18 18:48 JAN

Report to HM Environmental Services, Inc. Page 8 of 8 Generated on 02/09/2018

Project: Christoph Holdings LLC Report ID: S87344.01(01)