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Norma Copa Ford Astm.d1200.1970 PDF
Norma Copa Ford Astm.d1200.1970 PDF
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Document Name: ASTM D1200: Viscosity of Paints, Varnishes and
Lacquers by Ford Viscosity Cup
CFR Section(s): 49 CFR 171.8
Official Incorporator:
THE EXECUTIVE DIRECTOR
OFFICE OF THE FEDERAL REGISTER
WASHINGTON, D.C.
~~r~ Designation: D 1200 -70
175
D 1200
that the individual cup receives. If the cup preferred method is to overfill the cup and
varies more than 10 percent from standard, it scrape off the excess with a straightedge.
should not be used. Measure the time from the moment efflux
starts until the first break in the stream.
7. Conditioning 8.5 If the cup has been established to be
7.1 Since most materials are non-New- nonstandard when calibrated as described in
tonian in nature it is necessary to establish an the Appendix, apply the percentage difference
agitation and rest period history before the to the measured seconds in order to get the
viscosity determination is made. correct viscosity in Ford cup seconds.
7.2 Bring the material to a temperature a
few degrees below that desired and then agi- 9. Care of Cup
tate vigorously on a reciprocating shaker in a 9.1 Following each determination, clean the
pint can % full for 10 min. Allow to stand cup by the use of a suitable solvent and a soft
undisturbed while adjusting further to the de- brush. Under no conditions should metal
sired temperature. Make the viscosity deter- cleaning tools be brought into contact with the
mination at end of the lO-min period. instrument. Particular care must be exercised
in cleaning the orifice to avoid any film de-
8. Procedure posit or nicks on the inside walls.
8.1 Make viscosity determinations in a
room free from drafts and rapid changes in 10. Report
temperature. For the highest degree of accu- 10.1 Report the efflux time to the nearest
racy the room temperature should be between 0.2 s for the cup orifice combination (for ex-
20 and 30 C (68 and 86 F). Determinations ample, Viscosity 23.2 s with No.4 Ford cup),
should be made at a temperature below the the temperature as measured in the efflux
dew point of the atmosphere surrounding the stream, and the immediate history of agitation
apparatus. and rest prior to the measurement.
8.2 Choose the proper cup so that the time
of efflux will be between 20 and 100 s for cups 11. Precision
No.3 and 4 and between 40 and 100 s for cup 11.1 On the basis of a study in which eight
No.2 (Fig. 2). cooperators from six different laboratories
8.3 Level the instrument so that the cup compared measurements of oils ranging in
may be filled level full without meniscus or viscosity from 35 cSt to 130 cSt, using each of
overflow at one side. these cups, the standard deviations between
8.4 Determine the time in seconds of efflux laboratories was less than 2 percent for all the
as follows: Close the orifice with the finger cups, and the standard deviation within labo-
and fill the cup with the prepared sample. The ratories was less than 0.5 percent.
176
~~r~ D 1200
40 0
I-
(J)
w
'"o 30 0 ./
I-
(J)
>=
z
V
w
u ~
/ i,...
200
,..- ~o·
7 :....--
l- L
*- - -
ii;
o
u 100
./ ~
9.5 mm-24 N.F. 2 Tap
Orifice
(J)
:;; 1/ / ' . /
//
FORD VISCOSITY OUP
o 10 20 30 40 50 60 70 80 90 100 110
TIME, SECONDS
2.527 mm+---l-l I
!H
wv
It')
~1
r\B
9.5mm-24N.F. 2 Thd
e
¥[;~ -I
U=i I-
!-8.S';m1 '" A
. N
No.2 Orifice No.3 Orifice, A=3.404 mm
No.4 Orifice, A=4.1I5mm
FIG. I Ford Viscosity Cup and Orifices.
APPENDIX
AU The orifice of the Ford cup is commonly dure detailed in Section 8, ensuring that the temper-
made of brass or some other corrosion-resistant ature of the cup and liquid remain within the above
material which is subject to wear with use and limits during the time of flow as determined by a
cleaning. A small change in diameter of the orifice thermometer in the efflux stream.
becomes significant in the results obtained with the A 1.4 The following formulae are. used to convert
use of this type of viscosity-measuring apparatus. the time of flow in seconds to kinematic viscosity:
A 1.2 Certified kinematic viscosity standards are
available from the Cannon Instrument Co., P.O. Centistokes (No.' 2 orifice) = 2.3881 - 0.00712
Box, State College, Pa. 16801 (Note AI). For par- 57.008
ticular oils applicable use with the Ford Cups refer Centistokes (No.3 orifice) = 2.3141 - 15.200
to Table A 1. Oils available from other sources, Centistokes (N o. 4 orifice) = 3.8461 - 17.300
having known kinematic viscosities, may also be where 1 = temperature, deg C.
used. A1.5 The difference between the certified viscosity
and the determined viscosity, multiplied by 100 and
NOTE A I-The viscosity standards are available
only as I-pt samples. divided by the certified viscosity will give the per-
centage variation of the cup from standard. A per-
A 1.3 Select the appropriate liquid viscosity centage correction can be applied to the seconds
standard for the cup to be calibrated. Bring this cup flow when the cup is in normal use. If the cup varies
and the liquid viscosity standard to a constant tem- more than 10 percent from standard, it is recom-
perature of 25 ± 0.1 C (77 ± 0.2 F). Determine the mended that the orifice be replaced and that the cup
time of efflux to the nearest 0.2 s using the proce- be recalibrated.
177
~~1~ 0 1200
2 25 to 120 S-20 35
3 40 to 220 S-60 120
4 70 to 370 S-60 120
a Exact viscosities are supplied with the oil samples.
By publication of this standard no position is taken with respect to the validity of any patent rights in connection there-
with, and the American Society for Testing and Materials does not undertake to insure anyone utilizing the standard
against liability for infringement of any Leiters Patent nor assume any such liability.
178