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PHASE 6 PRACTICAL  Summary

COMPONENT - PART 1. REVIEW OF


DEVELOPMENT OF THE LABORATORY ANALYSIS
ALTERNATE PRACTICAL TECHNIQUES
COMPONENT COURSE
DESIGN OF DRINKING - ALKALINITY ANALYSIS:
PLANTS "Alkalinity is specified as the ability
of water to neutralize acids, in
Colombia Resolution 2115 of 2007
STUDENT:
of the Ministry of Social Protection,
DIANA MARCELA RODRIGUEZ Environment, Housing and Territorial
CODE 1121418340
Development establishes the
maximum admissible value of
CaCO3 of 200 mg / L" (University
North of Barranquilla) 1. In the
GROUP: 358040_
explanatory video, Methyl Orange,
0.02N sulfuric acid (H2SO4) is used
as an indicator as a titrant to
TUTOR: determine the alkalinity of the
WILSON AVILA AVILA sample, in which the amount of
sulfuric acid used in the solution is
measured until the color change is
obtained to orange, it tends to be very
subtle.
NATIONAL UNIVERSITY OPEN AND
DISTANCE (UNAD)
PROGRAM: ENVIRONMENTAL - JUGS TEST: 1000 ml of residual
ENGINEERING water was observed in each biker,
COURSE: DESIGN OF DRINKING
PLANTS then they were placed in the
ACACÍAS META flocculator, then 1% aluminum
2020
sulfate was added in different doses
to each jug using dosages of 20 ppm,
40 ppm, 60 ppm and 80 ppm, the characteristics allow us to define their
Which are placed at a fast speed in a safety for human consumption, which is
short time and then at a slow speed essential for our lives and the
for a long time in order to achieve the development of our daily physical
desired flocs and then proceed to functions.
settle the mixtures to achieve
Taking into account the above, according
sedimentation. Then, a sample of the
to the development of this activity we
water resulting from the
reinforce the understanding acquired in
sedimentation is taken and the
the revision of the theory of the course,
turbidity is measured, using the
through the analysis of a case study.
turbidimeter.
Where a surface water sample was
characterized, to which the pH, alkalinity,
CASE STUDY:
color and turbidity were evaluated, after
A surface water sample was characterized being subjected to the jar test, where two
to carry out the jar test in a water coagulants (aluminum sulfate and ferric
purification plant using two coagulants, chloride) were added in different
aluminum sulfate and ferric chloride in concentrations to your treatment.
doses ranging from 10 ppm to 1000 ppm.

The guide gives us the pH, Color and


PURPOSE OF THE PRACTICE
turbidity data of the initial sample and the
final sample, respectively, in 4 tests  Reinforce the knowledge acquired

(20ppm, 40 ppm, 60ppm and 80ppm), by the student of the present

which were calculated according to the course, in the theory provided,

definition of ppm, density and coagulant combining it with practical

concentration. knowledge through a practical


activity in a with a score of 90
 INTRODUCTION
points; as a complementary tool in
For the Design of Water Treatment Plants the student's higher education.
it is essential to understand different
aspects and characteristics of water, the  Strengthen the knowledge of
measurement and change of these English as a second language by
appropriating the terminology and
applying the knowledge acquired Sulfato de aluminio: Tomar
con una pipeta 17.5 ml de
in the research. Preparación de reactivos sulfato y disolver en agua
corriente hasta aforar un litro
en un matraz de bola
 Strengthen the knowledge
acquired by the student of this
Nitrato de plata: Moler 5 gr
course, in the theory provided, Polímero: Pesar 1 gr de de cristales de Nitratos de
polímero, colocarlo en un Plata y secar durante 2 hrs.
through practical design exercises vaso de precipitado con agua Pesar en la balanza
de corriente y disolver. Aforar aproximadamente 5.1 gr de
Phase 5 with a score of 60 points hasta un litro en un matraz los cristales pulverizados de
that will be executed within the de bola. Nitratos de plata, disolver en
2000 ml de agua destilada
Evaluation and Monitoring
EDTA: Secar
Environment of the course; in aproximadamente 18 gr de
cristales de EDTA a 140°C en Hidróxido de sodio: Pesar
order to acquire skills in horno durante 2 hrs. Pesar aproximadamente 40 gr de
aproximadamente y con hidróxido de sodio en
calculating structures and dosages precisión 15 gr. Vaciar al lentejas y disolver en 1000 ml
of a PTAP. matraz aforado de 2 Lt y de agua destilada.
aforar con agua destilada
hasta 4 Lts.

 MATERIALS AND METHODS


reactivos

material de
cristaleria turo de plastio (50 pipeta tipo psteur agua destilada
ml) con perilla (ml)

sulfato de alunio
pipetas serologicas
material de plastico gradilla
y graduas

polimetro
matraz de bola celda de lectura
vasos precipitados
(1000 ml) para aspecto
nitrato de plata

vaso de
celdas de lectura
precipitación (150 edta
para turbimetro
ml)

hidroxido de sodio
RESULTS: Test 2
PARAMETER INITIAL FINAL EFFICIENCY
According to what was stated in the case SAMPLE SAMPLE
study, calculate pH 7.8 6.8 12.8%

Alkalinity
Colour 68 12 82.3%

Concentarcion H 2 SO4  volumen gastado deH 2 SO4  50000


Alcalinidad  Turbidity 5.52 1.84 66.6%
volumen de la muestra
Note Test 3
50000: CaCO3 weighs 100g, this value is
PARAMETER INITIAL FINAL EFFICIENCY
divided by the eq-g, which is two, and
SAMPLE SAMPLE
multiplied by 1000 milliequivalents. pH 7.9 5.6 29.1%
𝐴𝑙𝑐𝑎𝑙𝑖𝑛𝑖𝑑𝑎𝑑
Colour 1545 16 98.9%
0.02𝑁 ∗ 22.5𝑚𝑙𝐻2 S𝑂4 ∗ 50000
=
100𝑚𝑙 Turbidity 272 5.09 98.1%
= 225𝑁

1. Parameter Removal Percentage: Test 4


Turbidity, Color and pH PARAMETER INITIAL FINAL EFFICIENCY
SAMPLE SAMPLE
𝐸𝑓𝑖𝑐𝑖𝑒𝑛𝑐𝑖𝑎 (%) pH 8.1 4.7 41.9%
Parametro (afluente) − Parametro (efluente)
=( )
Parametro (afluente)
Colour 4475 14 99.6%
∗ 100
Turbidity 683 2.5 99.6%

Trial 1
PARAMETER INITIAL FINAL EFFICIENCY
SAMPLE SAMPLE
pH 8.7 6.8 21.8%

Colour 2. 3. 4 13 94.4%

Turbidity 24.5 1.47 94%


2. Based on the example within the  Nvueltas 
case study, the volume for each 1segundo  
 60 segundos 
reagent is calculated at the
P   * 3 *  paleta * k
5
different dosages and the table is
completed: P
G
v
Coa Conce De 20 2 6 8
gula ntrati nsi pp 0 0 0
nt on ty m p p p 100𝑅𝑃𝑀
p p p 1𝑠𝑒𝑔𝑢𝑛𝑑𝑜 ( ) = 1,66 𝑅𝑃𝑆
m m m 60𝑠𝑒𝑔𝑢𝑛𝑑𝑜𝑠
Alu 17% 1.1 0. 0. 0.
minu 2g 0.0 1 2 3 𝑘𝑔
𝑃 = 998.43 ∗ 2.53 ∗ 0.07635 𝑚 ∗ 2.3
m / 84 6 5 3 𝑚3
sulfa mL ml m m m = 0.09
te l l l
Chlo 40% 1.4 0.0 0. 0. 0. 0.09
ride 2g 2 0 0 1 𝐺=√
𝐾𝑔
iron / ml 5 8 1 0.001034 𝑚 ∗ 𝑠 ∗ 0.0008 𝑚3
mL m m m
l l l = 329.84

 Discussion
3. A comparative table must be made
with the regulations Resolution
JARS TEST
2115 of 2007 according to the Through the explanatory video it
analysis of the parameters in each
was possible to deduce that the
of the tests carried out.
flocculation of particles in the
4. Design gradients for fast mix waste water is more effective in
and slow mix will be calculated;
taking into account: the doses of 20 ppm, 40 ppm and
 H 2O  0.001034 kg / m * s 60 ppm, in the concentrations of
  998 .43kg / m 3 10 ppm and 100 ppm it is not even
  100 rpm / 40 rpm possible to observe the generation
k  2.3
of the flocs. Therefore, these
  0.0763 m
concentrations are suitable for use
v  800 ml
in wastewater treatment.
 BIBLIOGRAPHY
WITH APA RULES

1. University of the North of


Barranquilla. Chemical
characteristics of water.
Introduction and determination of
alkalinity. Recovered
fromhttps://www.youtube.com/wat
ch?v=mmkY5ET9GTM

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