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  • Tilahun

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    Emanuel Senbeto
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    The document reports results from measurements of magnetic properties, X-ray diffraction, and scanning electron microscopy of samples with varying composition x. Magnetic measurements show increasing magnetization and coercivity with x. XRD results list peak positions, widths, and d-spacings for each sample, with shifts indicating changing crystal structure with x. Lattice parameters a, b, and c calculated from XRD decrease with increasing x. SEM images show changes in morphology with increasing x.

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    The document reports results from measurements of magnetic properties, X-ray diffraction, and scanning electron microscopy of samples with varying composition x. Magnetic measurements show increasing magnetization and coercivity with x. XRD results list peak positions, widths, and d-spacings for each sample, with shifts indicating changing crystal structure with x. Lattice parameters a, b, and c calculated from XRD decrease with increasing x. SEM images show changes in morphology with increasing x.

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    © All Rights Reserved
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    8 views9 pages

    Tilahun

    Uploaded by

    Emanuel Senbeto
    The document reports results from measurements of magnetic properties, X-ray diffraction, and scanning electron microscopy of samples with varying composition x. Magnetic measurements show increasing magnetization and coercivity with x. XRD results list peak positions, widths, and d-spacings for each sample, with shifts indicating changing crystal structure with x. Lattice parameters a, b, and c calculated from XRD decrease with increasing x. SEM images show changes in morphology with increasing x.

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    © All Rights Reserved
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    of 9

    x Ms (emu/g) Mr(emu/g) Hc (G)

    0 0.0623 0.0543 -312.09, 310.269


    0.1 10.39 2.242 -483.612
    0.2 11.392 3.482 -366.423, 383.232
    XRD Result

    For x=0

    Pos. FWHM d-
    [°2Th.] [°2Th.] spacing
    [Å]
    22.4448 0.3149 3.96129
    32.1303 0.251 2.78588
    39.604 0.4723 2.27569
    44.8913 0.4723 1.97748
    51.5352 0.4723 1.7734
    57.1108 0.3936 1.61281
    For x=0.1

    Pos. FWHM d-
    [°2Th.] [°2Th.] spacing
    [Å]
    22.6448 0.2949 3.89143
    33.4343 0.255 2.88786
    39.754 0.4876 2.37669
    45.7913 0.4625 1.87838
    51.8852 0.4813 1.6844
    57.6708 0.3166 1.66281
    For x=0.2

    Pos. FWHM d-
    [°2Th.] [°2Th.] spacing
    [Å]
    22.9448 0.3049 3.89143
    33.4343 0.262 2.78884
    39.956 0.4966 2.36679
    45.8843 0.4735 1.79848
    51.9761 0.4955 1.6734
    57.7308 0.3276 1.67172
    Crystal lattice parameters

    x a=b c
    0 0.5784 nm 1.3936 nm
    0.1 0.5678 nm 1.3717 nm
    0.2 0.5572 nm 1.3529 nm

    SEM result

    For x=0
    For x=0.1
    For x=0.2

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