Clear ASIA OFFICE CClearsynth Labs Utd, ASIA R&D CENTRE, ‘Clearsynth Research Centre Clearsynth Canada Inc. 17, Lotus business Pai Plot No. 172,104, 2396 Speakman Orive, Off New Link Rd, Andheri (W) Malapur, Hyderabad 500076 Lab suite NODE, wiesssougn, GD rspwing Resear — Mumia -s00083 nao Telangana nia Ontario USK 103, Canada : aa Tetvai 22 soso Trotaosriss9e evi aee 723.0060 CERTIFICATE OF ANALYSIS Product Name \Valproic Acid DS IChemical Name PPropy-3,3,3-d3ypentanoie-5,5,6-d5 Aad [Synonyms Not available CAS # [67745-18-4 (Catalogue # :S-0-02947 Batch ® [CS-SI-AAA-0100-02 Molecular formula ICcHisOa Molecular weight _ [150.25 Date of Analysis 16/09/2016 Retest Date 6/09/2021 [Storage conditions [Store at refrigerator(2-8°C) for long term storage DL . 7 2 ° ~o Test ‘Specification Result [Appearance Colouriess liquid rolourless Tquid [Solubility ‘Soluble in Chloroform [In Chloroform TH NMR spectrum ‘Confirm Structure [Confirms Isotopic enrichmentioy @ NMR) Not Less than 95% 99.39% Purity by GC Notes than 90 % (98.46% [=-This material complies Shoop 06/11/2020 Reviewed & Approved by (QC Analytical ) L Sucks i 06/11/2020 Reviewed & Approved by ( Quality Assurance ) ‘The r-tost datas assigned based onthe Hteralure avaiable. The balances used are catrated with weights traceable to the National standards NIST. ‘Quality Accreditations 0 9003:2015 150 14001:2015] OHSAS 18001:2007 ISO Guide 242009] ISO/IEC 17025:2005 Info@elearsynth.com | werw.clearsyath.com | Worldwide Helpline No +1.800.650.239 | CIN U2s100MH2010°LC201433, "The ‘Catalyst’ in making your research work" NORTH AMERICAN R&O CENTREda T z © ¥ s cacao PRY Vi :Aa pezkreuy or es 4e31D @Dat GAS CHROMATOGRAPHY ANALYSIS CS-SI-AAA0100-02 Chanel 2=2 RESULTS Samp 1 pow to x Ijin Date: Q8/672016 194217 Ison Metod: etal metodh Rintimetminy 30000 inarumen ig Yanan acsson-2 10 “0 10 © ° s 5 ‘0 Peat Peak Name xe 1 2 : ‘ 5 $ 7 2-4Propy-d2\Penianoies3Acid/ ACTS Totals Avabzed by 11 ¢ stfu lrore 09/16/2016 Cale Dae: Times Caleulation Method: leulated Instrument (Cale: Run Mode: Peak Measurement: Peak Area Cateulation Type: Result (%) 0.0491 0.1432 0.0193 0.1234 0.0257 11750 98.4648 190.0001 oc (09/16/2016 11:43:24 5 Varian GC3300-2 Analysis Percent » as Ret Time Peak Area (ni (counts) 3.265 Bn 3.395 4005 3.540 338 3.982 3450 4267 718 7.890 32881 8876 2753007 2795041 Clear. Astarimethod\ge2-method. mth toutes wiath 12 (see) 23 24 00 20 25 48. Mt revowednys 2