Professional Documents
Culture Documents
Mitra 2016
Mitra 2016
PII: S0263-2241(15)00548-5
DOI: http://dx.doi.org/10.1016/j.measurement.2015.10.014
Reference: MEASUR 3626
Please cite this article as: S. Mitra, P. Kumar, K. Srinivasan, P. Dutta, Instrumentation and Control of a two-stage
4-bed Silica gel + Water Adsorption Cooling cum Desalination system, Measurement (2015), doi: http://dx.doi.org/
10.1016/j.measurement.2015.10.014
This is a PDF file of an unedited manuscript that has been accepted for publication. As a service to our customers
we are providing this early version of the manuscript. The manuscript will undergo copyediting, typesetting, and
review of the resulting proof before it is published in its final form. Please note that during the production process
errors may be discovered which could affect the content, and all legal disclaimers that apply to the journal pertain.
Instrumentation and Control of a two-stage 4-bed Silica gel + Water Adsorption
Abstract
This paper presents the instrumentation and control architecture for a laboratory based
two-stage 4-bed silica gel + water adsorption system. The system consists of primarily two
fluids: refrigerant (water vapour) and heat transfer fluid (water) flowing through various
components. Heat input to the system is simulated using multiple heaters and ambient air is
used as the heat sink. The laboratory setup incorporates a real time National Instruments (NI)
controller to control several digital and analog valves, heaters, pumps and fans along with
simultaneous data acquisition from various flow, pressure and temperature sensors. The paper
also presents in detail the various automated and manual tasks required for successful
operation of the system. Finally the system pressure and temperature dynamics are reported
potable water and even minimal refrigeration in several rural areas of developing countries.
The challenges faced are i) absence/unreliability of grid electric supply for operating other
methods of desalination, ii) drought of soft water for cooling needs when water cooled
systems are used and iii) absence of skilled manpower to maintain desalination/chiller units.
On the other hand, these areas are endowed with abundant solar energy and other forms of
low grade thermal energy such as from biomass. Being heat driven, an adsorption cooling
cum desalination system can potentially meet the dual needs and there is well developed
state-of-the-art for this method [1–11]. This method is based on cyclic heating and cooling of
an adsorption bed to realize pressure lifts from evaporating to condenser pressures. The
guiding principles for the present system are i) design with only air cooled heat rejection
systems, ii) realistic performance assessment, however low it may be, by generous
instrumentation and iii) evolving an automated control logic that takes care of routine
operation. The parasitic electrical load can be met from localized source like photovoltaic
panels.
Prior art of adsorption desalination is rich with both computational and experimental
studies for multi-bed single-stage systems. There are also a few studies on multi-staging of
adsorption systems [12–17]. Conclusive outcome of these studies is that the system
performance is a strong function of pressure lifts, temperature swings and cycle times.
However, in all these studies, details of instrumentation and control were given only a limited
stress. Majority of the literature on control and automation for refrigeration system pertains to
implemented in the present system due to the inherent difference in operational time scales.
Recently, a study [27] describing the automation of single-stage 2-bed solar driven activated
carbon + ammonia adsorption system has been presented. The study presents an account of
valve operation logic with little focus on instrumentation and control architecture required to
implement it.
This paper aims at presenting a detailed description of instrumentation and control for a
two-stage 4-bed silica gel + water adsorption chiller and desalination system. Components of
mechanical hardware are designed to operate the system in multiple modes such as
importance (closed cycle operation). The guiding principles of design described earlier were
inevitable when tropical arid zone operations are imminent. Although, several models do
predict that single-stage operation does not give sufficient throughput [15–17], there has been
premise. The system control logic along with its modality of implementation using an
integrated controller and data acquisition system (DAQ) is presented in detail. Further,
various manual and automated operational steps required for the system operation are
described. The system has been operated for various conditions and some representative
results which enable an assessment of the system potential are presented in this work.
2. THERMAL COMPRESSION
At the outset, it is emphasized that neither stages of the adsorption cooling cum
desalination system takes part in actual desalination process and it acts merely as a
compressor for water vapour generated in the evaporator to raise the pressure to a level
no contamination due to the adsorbent (silica gel). For the cooling part, refrigeration is
obtained by evaporating brackish/saline water at a pressure commensurate with temperature
at which refrigeration is required (typically 5–10°C). This low pressure vapour is compressed
via thermal compression route using the pressure-temperature-uptake relations of silica gel +
water. The compression of low pressure water vapour from evaporator (typically ~ 1 kPa) to
condenser pressure (around ~7 kPa) is achieved virtually without the use of any moving
parts. The motive energy for this thermal compression is low-grade heat (<100°C) which may
be derivable from simple flat plate solar collectors or low grade thermal energy such as waste
heat. The following section provides a brief overview of the processes involved in such a
system.
Fig. 1 shows a schematic representation of the thermal compression cycle for silica gel
+ water adsorption cooling cum desalination system. The adsorber bed can be construed as a
heat exchanger filled with silica gel granules in contact with heat exchanging coils through
which heat transfer fluid (water) passes. This coil serves as a common passage for both
heating (to build the pressure after adsorption and for desorption) and cooling (for removing
heat of adsorption and reducing the pressure after desorption). External to the bed, closed
circuits of cooling and heating water are different. The bed has two vapour valves each for
inlet and outlet of water vapour. Thermal compression process also has four processes which
are broadly analogous to those in a mechanical compressor and are described below:
1) Adsorption: The low pressure vapour enters the bed from a vapour inlet port and gets
required to pass cold water through the coil to remove the heat of adsorption. This
process is continued for a time period given by tads; beyond which the bed cannot
2) Preheating: The bed is now isolated by closing both the vapour valves and the water
circuit is switched to hot water flow. This heats the bed and starts desorption. Since the
vapour valves are closed, this leads to an increase in pressure of the bed. This process is
continued till the required pressure build-up is achieved which requires time of tph. This
is similar to compression.
3) Desorption: After achieving high pressure in the bed the vapour outlet valve is opened
and hot water flow through the coil is continued to expel as much of water vapour
possible subject to equilibrium uptake state. This continues for a specific period (tdes)
beyond which the bed cannot desorb any more vapour which is analogous to discharge.
4) Precooling: The precooling phase is needed to bring the bed pressure back to slightly
less than the evaporator pressure just like the re-expansion process in a mechanical
compressor. During this process both the vapour valves are closed and the water circuit
is switched to cold water flow though the coils. Sensible cooling of adsorbent is
accompanied by some re-adsorption of vapour in the void volume reducing the bed
pressure. This process continues for time tpc, at which the bed pressure reaches its initial
the duration of each of the four processes in thermal compression cycle varies from 100 to
1000 s because of differential thermal performance of the silica gel beds and kinetics of
adsorption in each process. From operational point of view the following constraints are
imposed:
Equal times are enforced on adsorption and desorption processes; preheating and
precooling (henceforth called as switching). Therefore, the entire cycle now features only two
time scales: adsorption time (tads) and switching time (tsw). This simplifies the control logic
for valve operation. An adsorption cooling cum desalination system consists of multiple of
such beds, each going through the cycles with a certain phase shift from one another such that
there is a continuous throughput. Subsequent sections will describe the system architecture
and the control logic for two-stage 4-bed adsorption cooling cum desalination system.
3. SYSTEM DESCRIPTION
Fig. 2 shows the process and instrumentation diagram of the system discussed in this
study. There are 4-beds in stage-1 (Bed 1-1 to 1-4) and stage-2 (Bed 2-1 to 2-4). Multi-
staging is required when a single-stage cannot provide enough pressure lift needed to achieve
condenser pressure, however provision has been made to bypass the upper stage if large
pressure lifts are not required (such as desalination without cooling). Fig. 3 shows the
Each bed is equipped with its own set of valves, pressure and temperature sensors and
water flow meters. The entire piping layout of the system can be divided into two categories,
namely vapour and water circuits. There are separate pumps and heat exchangers in the cold
and hot water circuits. The following section describes the components and the
The evaporator generates low pressure water vapour which passes through two stages
of adsorbers, intermediate plenums and finally condensed at higher pressure and collected in
a tank. Instrumentation and control hardware for each of these components are described
below:
3.1.1 Evaporators
Brackish water flash evaporates outside copper tubes to generate water vapour. There
are two evaporators (Evap-1, Evap-2) in series each catering to a pair of adsorbers. The
brackish water is filled in the evaporators manually for the experimental prototype. Manually
operated vacuum sealed ball valves (MV1, MV2) close the inlet water port in each
evaporator. The two evaporators are connected by a pipe which has an electro-pneumatically
actuated valve (SV 17). This is a normally closed (NC) type valve and requires the supply of
24 VDC (digital control) and 6–8 bar air pressure for operation. The response time of
actuation is <800 ms. SV17 is used to connect to the vacuum pump for initial evacuation and
de-aeration of brackish water. The brackish water and vapour temperature in each evaporator
are measured by using two T-type thermocouples (TC). The thermocouples are calibrated in
the range of 5–85°C using a NIST traceable temperature calibrator and the expected
measured using a 0.1–50 kPa absolute pressure sensor (P1, P2). Table 1 and 2 list the
3.1.2 Adsorbers
Each adsorber has two vapour ports with a pneumatically actuated vapour valve on each of
them (SV1, SV2; SV3, SV4; and so on). These NC valves are similar to the one on the
evaporator (SV 17). For bed temperature measurement, two TCs with Swagelok vacuum
compatible fittings are placed at different depths within the adsorber assembly and the
average of the two is used to represent the bed temperature. The vapour pressure in each
adsorber is measured with an absolute pressure sensor similar to the one mounted on the
The plenums play dual role as vapor distribution channels for the beds and as pressure
dampers during switching of vapor valves. Thermodynamic states of water vapour in it are
assessed with two TCs (T13, T14; T23, T24) mounted equidistant from the central plane
along with a pressure sensor (P7; P12) mounted at the centre of it. The plenum-1 (Fig. 2) has
both stage-1 and stage-2 adsorbers connected to it. Hence, it is also used as the common
manifold to connect all the adsorbers to the vacuum pump at the beginning by using a
manually operated butterfly valve (BV2). Further, both the plenums are connected to the
condenser via vapor valves (SV18; SV19) such that upper stage can be bypassed if needed.
The condenser is an air-cooled finned copper tube heat exchanger with two vapour
inlets, one from each stage, and a condensate outlet. At any given moment only one vapour
inlet valve (SV18/SV19) is opened. The condenser also has provision for vapour temperature
(T25) and pressure measurements (P13) like other components mentioned above.
The condensate gets collected in a tank having 1 mm least count graduation scale. The
condensate is desalinated water which is still below atmospheric pressure in the collection
tank. This water is taken out by breaking its vacuum in the prototype. In a production system
the condensate can be pumped out using a positive pressure head pump.
Water is used as heat transfer fluid in this system and it flows in closed loop. There are
three water circuits for chilled, cold and hot water flow (Fig. 2). The evaporator generates the
cooling effect due to evaporation and water to be chilled provides the cooling load. The cold
water circuit is used to remove heat from the adsorber beds of both the stages during
precooling and adsorption processes. The cold water then rejects this heat to the ambient
through an air cooler. The hot water circuit is divided into two parts, one for each stage. This
water circuit supplies heat to the adsorber beds during preheating and desorption. The hot
water temperature is maintained by three 2 kW heaters. Thus, water circuits consist of the
following major components: evaporator, adsorbers, cold/hot water tanks and air-cooler.
3.2.1 Evaporators
The evaporators are connected to chilled water circuit. A constant temperature bath is
used as a source for steady flow at constant inlet temperature and also a receiver for chilled
water from the evaporator. The water inlet temperature to the first evaporator and outlet
temperature from second evaporator are measured using TCs. A manual ball valve (MV5) is
placed at the outlet to regulate the water flow rate of the circuit. It is also equipped with a 0–
3.2.2 Adsorbers
Adsorbers have a water header to evenly distribute the flow into 15 heat exchanging
copper tubes. A detailed description of the adsorber design can be found in previous paper
[29]. Water flows through the bed in two passes and returns back to the header. At the inlet
and outlet two 3-way pneumatically operated ball valves (WV1, WV2; WV3, WV4; and so
on) are placed to switch between cold and hot water. Each ball valve is operated by 6–8 bar
air pressure controlled by 24 VDC pilot operated solenoid valve. In normal condition the 3-
way ball valve connects to the cold water circuit and upon actuation it switches to the hot
water circuit. Further, the water flow rate through the heat exchanging tubes is controlled so
that each adsorber has near identical water flow rate. This is achieved by using a motorized
flow control valve (FCV1, FCV2; FCV3, FCV4; and so on) on the return line of both hot and
cold water circuits of each adsorber. The motor requires 4–20 mA current input with a
resolution of 0.5 mA. At 20 mA input signal, the motor completely closes the ball valve and
at 4 mA it completely opens it. Water flow rate is measured using 0–100 Lpm flow sensor
There are two hot and one cold water tanks which serve as thermal storage and
expansion tanks for their respective flow circuits. The cold/hot water tanks are equipped with
temperature sensors. Although the system is designed to work with solar hot water, to test the
prototype, electrical heaters in hot water tanks are used as heat source. Since the performance
analysis is required as a function of source temperature, individual heater on/off controls are
A commercially available finned tube heat exchanger is customized for rejecting the
heat of adsorption and precooling. The cold water loop rejects the heat in air cooler which
uses a 220 W fan running continuously during the steady operation of the system. The
consequence of using the air cooler is that it raises the temperature of heat rejection to about
5–10°C above the dry bulb temperature as compared to 3–5°C above the wet bulb
temperature if a cooling tower was used . The choice of air cooler has been deliberate
Data acquisition and control is accomplished using National Instruments (NI) PXIe
8115 real time controller. The NI controller is equipped with digital and analog input/output
cards for data acquisition and control. The control and data acquisition architecture is as
shown in Fig.4a). Fig. 4b) shows the photograph of internal details of the control panel. The
NI cards required for the actuation of various valves and sensors are listed out in Table 1 and
2. The control logic is developed using NI Labview® software (version 2012). The control
algorithm is deployed on the standalone controller and logs the data on its local hard disk. A
Pressure and flow sensors provide 4–20 mA analog input (AI) directly to the NI PXI
6239 card. Data is acquired at 1000 samples/s per channel (parallel manner) and averaged out
for every 1 s window to filter out high frequency noise. This is fast enough due to the large
system thermal inertia and process times associated with thermal compression processes. The
4.2 Thermocouple
T-type thermocouples are terminated directly to the PXIe 4353 card having 24 bit
resolution. The card has on-board reference junction compensation. The maximum sampling
rate of the card is 90 samples/s per channel scanned simultaneously. However, for the present
All on/off valves are controlled by the PXI 6512 digital output (DO) card. The 24 VDC
digital outputs to all the valves are provided using relays (Fig. 4a). This is due to the low
current capacity (<75 mA/channel) of the DO card which is less than the required current
(>100 mA) for the valves to operate. Further, the addition of relays acts as isolation for the
controller card.
This valve requires 24 VDC (0.2–0.8 A) for operation and 4-20 mA current for control.
The operating current is actuated by PXI 6512 DO card and the control current is provided by
The digital output to switch high power AC equipment namely pumps, heaters and heat
exchanger fans is provided by a set of isolation relays, contactors (24 VDC coils) and
overload relays (OLR). Fig. 5 shows the typical wiring diagram. The DO card switches the
relays thereby providing current for the actuation of contactors. The contactors then switch
high power AC to individual components. All the low voltage (24 VDC) cables to the field
are shielded to prevent any electrical interference from the high power (AC) cables.
5. SYSTEM OPERATION
The system operation involves various steps in which certain steps are accomplished
manually and rest is automated. The controller runs the NI Labview ® code which implements
the logic as mentioned in this section. The various activities to be followed in sequence are:
a) Start up
d) Bed evacuation
The start-up comprises of few automated and manual tasks. However, the steady
system operation is completely automated with user intervention requiring to stop the system.
The step of removal of desalinated water and bed evacuation are completely manual
5.1 Start up
Initially brackish water is filled in the evaporator using a manual inlet valve (MV1 or
MV2). Salinity content of feed water is measured with handheld total dissolved solid (TDS)
meter with a range of 0–9999 ppm (±2% of measured value or 1 ppm whichever is higher). A
level indicator is provided to guide the maximum level of filling. After filling the evaporators
the manual valves are closed manually. Subsequent to this process the start-up phase of the
system is initiated.
The start-up comprises of two key activities: de-gassing of evaporator and warming up
hot water source. Since the evaporator is opened to atmosphere when brackish water is filled,
gases present in water. A rotary vacuum pump is used to accomplish these tasks.
Concurrently the chilled water pump (M4) is run with the constant temperature bath
temperature set to cooling mode having a set point temperature of 5°C. During this process it
is desired to remove only the air/non-condensable from the evaporator. However, as the
minimized by simultaneously reducing the temperature of brackish water. The final target
pressure by this process is 0.9 kPa, corresponding to saturation pressure of water at 5°C.
After achieving this steady state, holding time of 60 min is provided to evacuate any
dissolved gases present in water. The vapour valve SV17 is activated by manual input from
Labview® interface. The valve is opened and closed intermittently by the user so as to prevent
Meanwhile the heaters are simultaneously switched on to heat up the water in the tanks
to the user defined set point heat source temperature. This is accomplished in an automatic
mode and the logic for heater control is given by the flowchart shown in Fig. 6.
The Labview® code employs the entire logic of manual digital output control and
automated heater control in the form of parallel loops shown schematically in Fig. 7. Further,
the user needs to operate the valve SV17 manually based on temperature and pressure
readings of evaporators. Hence, for this purpose the temperature and pressure data are
After the start-up phase, the system is ready for steady operation in automated mode.
The constant temperature bath is now set into heating mode to serve as cooling load for the
evaporator. The user starts the system operation from the PC with various inputs as shown in
Fig. 8. The entire operating sequence runs till user interrupts. The controller automatically
supervises the operation of valves, heaters, acquires and logs the data obtained from various
sensors. The entire control and data acquisition is implemented through parallel loops (Fig.
8), similar to that in start-up phase. Priorities are assigned to each loop to help the controller
decide loop execution priority in case of clash. The loops are shown in decreasing order of
their priority with highest priority assigned to the digital output loop and least priority to the
There are 8 beds to be operated in tandem as per the timing scheme shown in Fig. 9.
The entire cycle time can be divided into six states where each state corresponds to a time
slot. The user inputs are the two variables tads and tsw based on which the time slots are
calculated. During each time slot, beds undergo different processes corresponding to different
valve positions. The entire valve logic for all the beds are mapped to each of this state and fed
to the controller as a binary array. The controller automatically actuates the corresponding
relays which in turn actuates the valves, as shown in Fig. 4a. The binary array for each state
is tabulated in table 3. The controller goes through each of these states in a cyclic manner and
hence implements the logic in the form of state-machine as represented in Fig. 10.
The flow control valve is provided a pre-set current input value for position control.
The water flow rate required through each bed is fixed and hence the valve positions once set
need not be changed during the entire system operation. Thus, a pre-set logic is ideal for such
application. The numerical value of current provided by the controller to each valve is
tabulated in table 4. The required hot water flow rate through each adsorber is 25 Lpm and
cold water flow rate is 33 Lpm. The current values provided to each valve are selected to
maintain the desired water flow rates with an uncertainty of ±1 Lpm. The current value
required by each valve varies marginally for same flow rate due to variable pipeline lengths
and flow resistances of the water circuit; these values are arrived at by a trial and error
method. The values are calibrated for the current setup for each operational parameter and
therefore cannot be generalized. However, in a functional system the data acquired from
water gets accumulated in the collection tank, which is accompanied by a glass level
indicator. The average rate of desalinated water production is obtained by manually reading
the water level at the start and end of a cycle time. The measurements are performed for 3
collection tank is isolated from the condenser by closing the valve MV3 and the drain valve
MV4 is opened thereby breaking the vacuum in the chamber and allowing the desalinated
water to flow out. Once the tank is emptied the drain valve MV4 is closed and vacuum pump
is connected to the chamber through the butterfly valve BV3. After evacuation, the collection
tank is disconnected from vacuum pump by closing BV3 and then reconnected to the
condenser by opening MV3. This entire process may be carried out even when rest of the
system is operating. The TDS content of the collected desalinated water is measured. In a
production model, the draining of desalinated water may be automated by use of a condensate
After the system is stopped, the beds are brought back to initial dry condition before the
next experiment is started. The moisture present within the silica gel beds are drawn out by
passing hot water (at 85°C) through each of them while simultaneously evacuating it by the
vacuum pump. At any given instant only one bed is connected to the vacuum pump (through
plenum-1) in order to minimize the vapour load on it. This process is carried out one by one
6. EXPERIMENTAL RESULTS
The entire description above is for 4-bed mode; however, the number of beds can be
reduced by suitably disconnecting the water and vapour flow to selected adsorbers. Hence,
the 4-bed/stage system can be run in 2-, 3- or 4-bed modes. The results presented in the
subsequent sections are for 2-bed mode of operation to prove the efficacy of instrumentation
and control system. The detailed performance results are already published elsewhere [28,
29].
For the 2-bed mode operation, the beds 1-1 and 1-3 from stage-1, beds 2-1 and 2-3
from stage-2 (shown in Fig. 2) are disconnected. Fig. 11 a) and b) show the transients of
water flow rate to the bed, the inlet water temperature and bed temperature. Only one bed
(bed 1-2, 2-2) is shown from each stage to represent the transient responses. The pair of water
valves (e.g. WV1, WV2) on each bed switches between hot and cold water flow whereas the
flow rates are set by pair of flow control valves (eg. FCV1, FCV2). The switch between the
cold to hot water and vice versa is near instantaneous, as the valve switching time is <1 s.
However, the water inlet temperature takes significantly longer time to respond due to large
thermal inertia of the metallic water passages and water already present in the adsorber
header and heat exchanger tubes. The silica gel bed temperature rise/drop is even slower
because of its own thermal capacitance and hence it is evident that bed thermal dynamics is
the most important feature of adsorber beds. The pressure swing is obtained as a consequence
of near isosteric heating/cooling brought about by temperature swing of silica gel bed. Stage-
1 lifts the pressure from evaporator pressure (pevap) to inter-stage pressure (pint) and stage-2
beds should operate between inter-stage pressure to condenser pressure (pcond ). Fig. 12 a) and
b) show the pressure transients and compares them to water flow switching. It is observed
that the time for pressure rise in bed is significantly slower than the switching time of the
vapour valves (<800 ms). This is inferred from a steep change in the flow rate whereas the
pressure rise/fall occur over a finite time marked by preheating/precooling durations in the
reaffirms the choice of 1 s window for moving average filter during acquisition of pressure
data. It also proves that the entire system response is not limited by the overall response time
temperature swing of the beds are significantly slower than pressure swing, as noticed from
the time of rise/fall of temperatures and pressures. This is due to a larger bed thermal inertia
At the end of preheating of bed 1-2 and precooling of bed 2-2 the beds across the stages
interact and mass transfer occurs. During this process bed 1-2 discharges vapour which gets
drawn in by bed 2-2. Hence, in order to maintain forward flow the pressure of bed 1-2 at the
end of preheating should be marginally higher than pressure at the end of precooling process
of bed 2-2. Fig. 13 shows the pressure rise curves for bed 1-2 during preheating and pressure
fall curves for bed 2-2 during precooling process for 1 kPa evaporator pressure having three
half cycle times and constant switching time of 200 s. It is evident that the switching time of
200 s ensures that the pressure in bed 1-2 after preheating process is marginally higher than
that of bed 2-2 after precooling process, thereby preventing any back flow. It is observed that
as the half cycle time increases the pressure swing becomes faster causing a small jump in
pressure curves as the two beds interconnect. This may be prevented by having a variable
switching time, however in order to simplify the control logic a constant value is used
irrespective of the half cycle times. In fact it can be seen from Fig. 13 that within few seconds
the pressures equalizes between the two beds to a pressure corresponding to inter-stage
pressure.
The performance indicators for this system are desalinated water throughput, cooling
capacity and the coefficient of performance (COP). The desalinated water throughput is
Cooling capacity is derived directly from desalinated water throughput and heat of
vaporization at evaporator condition described in Ref. [28, 29]. COP is defined as the ratio of
cooling capacity and heat input the adsorber bed. For estimating heat input the logged
electrical heater pulses are integrated over the cycle times and an average value is used. Fig.
14 a)–c) show the system performance extracted from experimental data for various half
cycle times for 1 kPa evaporator pressure. It is evident from the figure that half cycle time of
1800 s is the optimum operating point with respect to system throughput; however an
optimum is not obtained with respect to COP which is typical of most adsorption cooling
The foregoing results conclusively prove that to standardize the operational sequence of
adsorption chillers, unlike mechanical counterparts, operate over long time constants. Despite
exhaustive modeling there are several features such as thermal inertia and thermal wave
phenomena [27] due to water passages switching from cold to hot and vice versa, which are
not amenable to precise modeling. There is no option other than assessing the overall
performance through a detailed experimental investigation. This has been the main objective
Once the operation is standardized, a production model that uses the same adsorbent-
adsorbate pair need not have this level of sophistication in instrumentation. For example, the
flow meters can be completely dispensed with. Except for a few pressure sensors (one for
each stage) and a few thermocouples, others can be avoided. Flow control valves can be
discarded by suitable design of piping to maintain desired flow rate. The control system can
be embedded into a small module as is done for other types of refrigeration systems. A salient
outcome is that, the system operation is sufficiently immune to precision and time constants
7. CONCLUSION
bed silica gel + water adsorption chiller-cum-desalination system has been presented in
detail. The adsorption cooling cum desalination system requires the operation of multiple
actuators in tandem with each other while simultaneously acquiring data from multiple
sensors. In the present system entire instrumentation and control architecture is integrated
into a single controller running prioritized programs in parallel. The instrumentation and
control architecture discussed in this study is for a two-stage 4-bed mode however the system
may be operated in single/two-stage system with 2-, 3- and 4-bed modes. Hence, this
adjusting for number of stages and beds. The results for the system when operated as two-
The system dynamics curves show that the water and vapour valves operational time is
significantly faster than the bed temperature and pressure dynamics and hence the system
response is not limited by the instrumentation and control hardware. A constant switching
time is selected to simplify the control logic which creates marginal inter-stage pressure
deviation for various half cycle times. The bed performance results show that there exists an
References
[1] C. Hildbrand, P. Dind, M. Pons, and F. Buchter, “A new solar powered adsorption
refrigerator with high performance,” Sol. Energ., vol. 77, no. 3, pp. 311–318, Sept.
2004.
[2] Y.L. Liu, R.Z. Wang, and Z.Z. Xia, “Experimental study on a continuous adsorption
water chiller with novel design,” Int. J. Refrig., vol. 28, no. 2, pp. 218–230, March
2005.
[3] X. Wang, and K.C. Ng, “Experimental investigation of an adsorption desalination plant
using low-temperature waste heat,” Appl. Therm. Eng., vol. 25, no. 17–18, pp. 2780–
[4] D.C. Wang, Z.Z. Xia, J.Y. Wu, R.Z. Wang, H. Zhai, and W.D. Dou, “Study of a novel
silica-gel adsorption chiller. Part I. Design and performance prediction,” Int. J. Refrig.,
[5] K. Thu, K.C. Ng, B.B. Saha, A. Chakraborty and S. Koyama, “Operational strategy of
adsorption desalination systems,” Int. J. Heat Mass Tran., vol. 52, no.7–8, 1811–1816,
March 2009.
[6] K.C. Ng, K. Thu, A. Chakraborty, B.B. Saha, and W.G. Chun, “Solar-assisted dual-
effect adsorption cycle for the production of cooling effect and potable water,” Int. J.
powered adsorption air-conditioning system,” in Proc. Int. Conf. Mater. Renew. Energ.
[8] L. Wang, X. Bu, and W. Ma, “Preparation and performance testing of silica gel/
calcium chloride composite adsorbents for waste heat adsorption refrigeration,” World
[9] K. Thu, A. Chakraborty, Y.D. Kim, A. Myat, B.B. Saha, and K.C. Ng, “Numerical
[10] K.C. Ng, K. Thu, Y. Kim, A. Chakraborty, and G. Amy, “Adsorption desalination: An
emerging low-cost thermal desalination method,” Desalination, vol. 308, pp. 161–179,
Jan. 2013.
[11] S. Mitra, K. Srinivasan, P. Kumar, S.S. Murthy, and P. Dutta, “Solar driven adsorption
[12] B.B. Saha, A. Akisawa, and T. Kashiwagi, “Silica gel water advanced adsorption
refrigeration cycles,” in Proc. Inter. Energ. Conv. Eng. Conf., 27 Jul–1 Aug 1997, vol.
2, pp. 1258–1264.
[14] B.B. Saha, A. Akisawa, and T. Kashiwagi, “Solar/waste heat driven two-stage
adsorption chiller: the prototype,” Renew. Energ., vol. 23, no. 1, pp. 93–101, May
2001.
[15] B.B. Saha, S. Koyama, T. Kashiwagi, A. Akisawa, K.C. Ng, and H.T. Chua, “Waste
adsorber system,” Appl. Therm. Eng., vol. 72, no. 2, pp. 283–288, Nov. 2014.
[17] S. Mitra, P. Kumar, K. Srinivasan, and P. Dutta, “Silica gel + water adsorber chiller and
desalination system: a transient heat transfer study,” ASME J. Therm. Sci. Eng. Appl.,
(in press).
[18] M. Becker, D. Oestreich, H. Hasse, and L. Litz, “Fuzzy control for temperature and
humidity in refrigeration systems,” in Proc. Third IEEE Conf. Control Appl., 24-26
[19] S.A. Tassou, and T.Q. Qureshi, “Performance of a variable-speed inverter/motor drive
for refrigeration applications,” Comput. Contr. Eng. J., vol. 5, no. 4, pp.193–199, Aug.
1994.
[20] H. Rasmussen, and L.F.S. Larsen, “Non-linear and adaptive control of a refrigeration
system,” IET Contr. Theor. Appl., vol. 5, no. 2, pp. 364–378, Jan. 2011.
[21] I.M. MacLeod, and A. Stothert, “Distributed intelligent control for a mine refrigeration
system,” IEEE Contr. Syst. Mag., vol. 18, no. 2, pp. 31–38, Apr. 1998.
[22] L.S. Larsen, C. Thybo, J. Stoustrup, and H. Rasmussen, “Control methods utilizing
[23] J. Primozic, and R. Svecko, “Control in refrigeration systems,” in Proc. IEEE Int. Conf.
[24] N. Jain, Li. Bin, M. Keir, B. Hencey, and A. Alleyne, “Decentralized Feedback
using PI controller and predictive control,” in Proc. 15th Int. Conf. Sci. Tech. Autom.
direct load control of refrigeration systems,” IET Contr. Theor. Appl., vol. 9, no. 7, pp.
[27] A.El Fadar, A. Haddi, M. Becherif, and J. Jay, “Automation of a solar adsorption
refrigeration system,” in Proc. Int. Conf. Renew. Sust. Energ,, 7-9 March 2013, pp.
118–122.
air cooled two-stage multi-bed silica gel + water adsorption system,” Int. J. Refrig.
(under review).
Low pressure High pressure
steam in steam out
BED 2-3
BED 2-2
BED 2-1
SV18
T26
P11
P10
P8
P9
T22 T20 T18 T16
MV4
P14
DESALINATED
T44 T43 T42 T39 T38 T37
T41 T40 WATER
F8 F7 F6 F5
WV15 WV13 WV11 WV9
MV7
T46
FCV16 WV16 FCV15 FCV14 WV14 FCV13 FCV12 WV12 FCV11 FCV10 WV10 FCV9
M2
HOT
T13 P7 T14
WATER
BV2 H6 H5
PLENUM-1
H4
AIR COOLER
T47
T11 T9 T7 T5
BED 1-4
BED 1-3
BED 1-2
BED 1-1
COLD M3
Fn1
WATER
P6
P5
P4
P3
T12 T10 T8 T6
MV8
F4 F3 F2 F1
WV7 WV5 WV3 WV1
T45
MV6
FCV8 WV8 FCV7 FCV6 WV6 FCV5 FCV4 WV4 FCV3 FCV2 WV2 FCV1
M1
MV1 HOT
MV2 WATER
SV17 H3 H2
T4 P2 P1 T2 BRACKISH
BRACKISH WATER H1
WATER T28 T27
P Pressure sensor P
Chilled water circuit Butterfly valves (manual) BV
Fig. 2: Process instrumentation diagram for the adsorption cum desalination system
Vapour valve Plenum-2
Plenum-1
Vapour pipeline
Hot water pipeline
Flowmeter
Chilled water line
Constant
Evaporator
temperature bath
Stage-2 Stage-1
Adsorber beds Adsorber beds
High speed
network
FLOW
SENSORS RELAY ARRAY
DIGITAL
CONTROL VAPOURVALVES
Sensor
panel switch
DIGITAL CONTACTORS
CONTROL +
OVERLOAD RELAYS
Control MCB
PXIe
Transformer
panel switch
HEATERS
Bus Bar
PUMPS
AC Mains FANS
Control
Transformer
Terminal
Blocks Bus Bar
NI Cards
24VDC
NI PXIe Supply 3 phase
Controller & DAQ MCCB
Y-phase
B-phase
+24 VDC
Fuse MCB
RELAY
DIGITAL
OUTPUT
CONTACTOR
24 VDC
-24 VDC Coil
OLR
AC equipment
Fig. 5: Wiring diagram for actuating high power equipment using digital output card
START STOP
Is Yes
diff >2.5 ? Operate 3 heaters
No
Is Yes
diff >1.5 ? Operate 2 heaters
No
Is Yes
diff >(−0.5) ? Operate 1 heater
No
Heaters OFF
START
Analog input loop
Inputs: (Flow & pressure sensors)
i. Adsorption time STOP
ii. Switching time Hardware/Software
iii. Hot water set point Temperature interrupt
iv. Data logging interval acquisition loop
v. Preset flow control
Feedback
valve positions
t sw Adsorption
Stage-1 BED 4
Stage-2 BED 1
Stage-2 BED 2
Stage-2 BED 3
Stage-2 BED 4
STOP
Initialize time; t = 0
t = t+1
No
Yes Yes
t < tsw? STATE 1 STOP pressed ?
No t = t+1
No
Yes Yes
t < tads ? STATE 2 STOP pressed ?
No t = t+1
No
Yes Yes
t < tads+ tsw? STATE 3 STOP pressed ?
No t = t+1
No
Yes Yes
t < tads+ 2tsw? STATE 4 STOP pressed ?
No t = t+1
No
Yes Yes
t < 2tads+ tsw? STATE 5 STOP pressed ?
No t = t+1
No
No Yes Yes
t < 2tads+ 2tsw? STATE 6 STOP pressed ?
60 30
50
Hot water flow 25
40
Adsorption Desorption
30 20
0 600 1200 1800 2400 3000 3600
a) Time (s)
Fig. 11 a)
90 40
Bed 2-2 inlet temp
Bed 2-2 bed temp
80 Bed 2-2 water flow
35
Temperature ( C)
60 30
50
Hot water flow 25
40
Desorption Adsorption
30 20
0 600 1200 1800 2400 3000 3600
b) Time (s)
Fig. 11 b)
Fig. 11: Temperature swings superposed on water flow dynamics for two-stage 2-bed mode
2.0 30
1.5
Hot water flow 25
pevap
1.0
Adsorption Desorption
0.5 20
0 600 1200 1800 2400 3000 3600
a) Time (s)
Fig. 12 a)
8 40
Bed 2-2 pressure
7
Bed 2-2 water flow
pcond 35
6
Flow aret (Lpm)
Pressure (kPa)
Fig. 12 b)
Fig. 12: Pressure curves superimposed on water flow dynamics for two-stage 2-bed mode
5
Pressure (kPa)
pinter
2 pevap
Beds
Bed 1-2 (Preheating)
interconnect
1
1800 1850 1900 1950 2000 2050
Time (s)
Fig. 13: Effect of half cycle time on bed pressure lifts for a constant switching time of 200 s
12
Desalinated water (L/day)
0
1200 1800 2400
a) Half cycle time (s)
Fig. 14a)
350
300
Cooling capacity (W)
250
200
150
100
50
0
1200 1800 2400
b) Half cycle time (s)
Fig. 14b)
0.20
0.15
COP
0.10
0.05
0.00
1200 1800 2400
c) Half cycle time (s)
Fig. 14c)
Fig. 14: Variation of system performance indicators with half cycle time a) Desalinated water
NI Card
Sensor Type Range Accuracy Location Output
used
(0.1–50) kPa
Pressure Capacitance ±0.05 kPa Vapour circuit 4–20 mA PXI 6239
absolute
±0.2°C
T-type Vapour and
Temperature (-250–300)°C (in range 5– μV PXIe 4353
thermocouple water circuit
85°C)
(0.1–100) Lpm ±1 % of
Flow Magneto-inductive Water circuit 4–20 mA PXI 6239
(0.1–50) Lpm measured value
BED 1-1 BED 1-2 BED 1-3 BED 1-4 BED 2-1 BED 2-2 BED 2-3 BED 2-4
WV10
WV11
WV12
WV13
WV14
WV15
WV16
SV10
SV11
SV12
SV13
SV14
SV15
SV16
WV1
WV2
WV3
WV4
WV5
WV6
WV7
WV8
WV9
SV1
SV2
SV3
SV4
SV5
SV6
SV7
SV8
SV9
STATES
State-1 1 0 0 0 0 0 0 0 0 1 1 1 0 0 1 1 0 1 1 1 0 0 1 1 1 0 0 0 0 0 0 0
State-2 1 0 0 0 1 0 0 0 0 1 1 1 0 1 1 1 0 1 1 1 0 1 1 1 1 0 0 0 1 0 0 0
State-3 0 0 1 1 1 0 0 0 0 0 0 0 0 1 1 1 0 0 0 0 0 1 1 1 0 0 1 1 1 0 0 0
State-4 0 1 1 1 0 0 1 1 1 0 0 0 0 0 0 0 1 0 0 0 0 0 0 0 0 1 1 1 0 0 1 1
State-5 0 1 1 1 0 1 1 1 1 0 0 0 1 0 0 0 1 0 0 0 1 0 0 0 0 1 1 1 0 1 1 1
State-6 0 0 0 0 0 1 0 0 0 0 1 1 1 0 0 0 0 0 1 1 1 0 0 0 0 0 0 0 0 1 1 1
Stop 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0
BED 1-3
BED 1-4
BED 1-1
BED 2-1
BED 2-2
BED 2-3
BED 2-4
Adsorbers
FCV10
FCV11
FCV12
FCV13
FCV14
FCV15
FCV16
FCV1
FCV2
FCV3
FCV4
FCV5
FCV6
FCV7
FCV8
FCV9
Valves
Cold
Cold
Cold
Cold
Cold
Cold
Cold
Cold
Hot
Hot
Hot
Hot
Hot
Hot
Hot
Hot
Water Circuit
10.0
13.5
11.0
14.5
10.0
14.0
10.0
14.0
11.5
13.5
10.5
13.5
10.0
15.0
11.0
14.5