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Textile Research Journal


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Investigation on improving banana fiber ! The Author(s) 2019


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fineness for textile application DOI: 10.1177/0040517519835758
journals.sagepub.com/home/trj

S Balakrishnan1, GLD Wickramasinghe1 and


UG Samudrika Wijayapala1

Abstract
The banana is one of the most commonly consumed fruits in Sri Lanka; after the fruit is harvested, the pseudostem is
thrown down as waste. The banana pseudostem is a good source of natural fiber. The purpose of this project is to
investigate the effects of banana fiber extraction, examine treatment parameters on fiber fineness and establish suitable
methods to reduce the fineness that enable banana fibers to be used as textile materials. Ten popular Sri Lankan varieties
of banana pseudostem were selected for this study. From the mechanically extracted banana fiber of these 10 varieties,
Ambun (genome AAA) was selected for further analysis because it had the lowest fiber fineness. Four layers from the
pseudostem of Ambun were extracted and put through a fineness and single fiber strength test. Scanning electron
microscopy and fiber linear density were used to observe and determine the fineness of the enzyme and chemical treated
banana fiber. The mechanical strength of the treated banana fibers was obtained by using a universal tensile tester
machine. The test result showed the second and the third layers of the pseudostem to be the finest. The mechanically
extracted fiber of the second and third layers of the pseudostem were put through an enzyme and chemical treatment.
Results showed enzyme and chemical combined treated fibers to be the finest, with a reduced diameter from 168.4 mm
to 48.8 mm, which is about 71% reduction compared to mechanical extraction.

Keywords
pseudostems, natural fiber, banana fiber, fiber fineness

Presently, with the increasing demand for sustainable natural fiber. The fibers go as waste due to lack of suit-
fiber as raw material for textiles, industries are looking able sustainable technology for its economic utiliza-
at natural fibers. Jain et al.1 mentioned famous designers tion.6 Banana fiber can be utilized as raw material for
and renowned fashion brands are moving to sustainable the industry in a range of products like paper, card-
products by using eco-friendly fibers in the production of board, tea bags and currency notes and reinforced as
clothing and other apparel. Natural fibers have essential polymer composite in fashionable dress material.7
properties such as a ligno-cellulosic fiber, consisting of Suhaib et al.8 reported that banana fiber is an environ-
helically wound cellulose microfibrils in an amorphous mentally friendly fiber like jute fiber and it has high
matrix of lignin and hemicelluloses.2 export demand from several countries such as Japan,
Banana fruits (Musa acuminata Colla) are delicacies Australia and Germany, among others. Currently,
and an important fruit crop savored all over the world. India has exhibited a silk-grade banana fiber from a
It is a popularly grown fruit crop in tropical countries,
such as Sri Lanka, and it has growing consumer
demand.3 Banana is a fruit which is continuously and Department of Textile and Clothing Technology, University of Moratuwa,
easily available no matter what season it is.4 Sri Lanka Sri Lanka
cultivates banana in a land area of about 50,000
hectares.5 Corresponding author:
Subashini Balakrishnan, Textile Technology Department, Sri Lanka Institute
Banana cultivation also generates a huge quantity of of Textile and Apparel (SLITA), Kandawala Estate, No-02 Gen. Sir John
biomass all of which goes as agricultural waste and Kotelawala Road, Ratmalana, Colombo, Western 10390, Sri Lanka.
pseudostem and peduncle are the potential sources of Email: subaedu88@gmail.com
2 Textile Research Journal 0(00)

separator machine, which can be utilized in handicrafts pseudostem can be used as a source of natural fiber, as
and textile industries. Banana fiber is easily blended an alternative or blended with synthetic fibers such as
with cotton or other man-made fibers to produce appa- nylon and polyester, among others.15 Ray et al.16
rel products.1 However, in Sri Lanka there is no signifi- revealed three kinds of mechanical banana fiber extrac-
cant investigation work done on banana fiber for textile tion methods, namely, manual stripping, Bacnis
application. To provide the sustainable textile raw method and Loenit method. The banana stem extrac-
material supply, many natural fibers have been identi- tion machine reduces work and increases fiber gener-
fied and investigated to evaluate their suitability for ation by 20–25 times when compared with the manual
textile applications. process.8,17 Jacob et al.18 reported that an unrefined
This research work is to extract banana fiber from the catalyst was utilized for banana fiber treatment of
Sri Lankan plant varieties that are abundantly available crude enzyme (pectinase) and the treated fiber was
island wide. Furthermore, banana fibers are used as a observed to be appropriate for banana fiber treatment
source for making products such as handicrafts and to impact the detachment of fine fiber. The combined
paper. This paper investigates the banana fiber extrac- treatment of NaOH, H2O2 and Na2CO3 increased the
tion and treatment methods to improve fiber fineness to fineness (5.8 tex) of the banana fibers and the single yarn
produce fiber suitable for textiles. strength and tensile strength were decreased by increas-
ing the concentration of the chemicals.19 This study
aimed to evaluate the layer-wise properties, namely
Objectives of the research fiber linear density, fineness and strength. This paper
This research paper is therefore seeking to explore and investigates the factors influencing the quality of the
investigate the following objectives: fiber and which layers are good for extraction of fine
fiber. This area of research is already progressing in
. To investigate the effect of banana fiber extraction India20,21 and Spain,22 but has not yet been done with
and treatment parameters on fiber fineness. Sri Lankan varieties. Based on the literature, this paper
. To develop suitable methods to reduce the fineness concentrates on reducing the fineness of the banana fiber
of banana fibers for textile materials. for textile application.

Literature review Materials and methods


Banana fiber is easily blended with cotton or other
Selection of banana varieties
man-made fibers to produce fabrics.9 The natural Popular varieties of banana in Sri Lanka, namely Ambul
fibers are accessible economically, in plenitude, being (Mysore type, AAB group), Kolikuttu (AAB), from the
biodegradable, recyclable and of low thickness, and Cavendish subgroup Anamalu (AAA), Rathambala/
have inspired numerous specialists throughout the Rath kehel (AAA) and Ambun or Amban (AAA),
world to investigate their application potential in dif- Atamuru (ABB), Seenikesel (ABB), Alu kesel (ABB),
ferent modern divisions.10 Poowalu (AB) and Suwandel (AB), were selected for
Banana pseudostem is abundant and banana fibers this research study. Banana pseudostem was collected
can be easily gathered in Sri Lanka.11 M. cavendishii, from dry, intermediate and wet zones and its fibers were
M. paradisiaca and M. sapientum are a few widely mechanically extracted for further processing.
grown common species of musa. M. cavendishii is
known as pure triploid acuminate genome AAA
group. M. paradisiaca and M. sapientum species are
Methods of extraction and treatment
known as triploid acuminate AAB group.12 As indi- Mechanical extraction: decortication. Banana pseudostem
cated in the report of the International Board for fibers were extracted by using a decorticator machine
Plant Genetic Resources (descriptor list for bananas), or defibering machine. By using the decorticator crush-
the banana genomic constitutions of Kolikuttu (AAB), ing action the pulpy material was removed. After the
Ambul (Mysore type, AAB group), from the Cavendish extraction, the fibers were washed and allowed to dry.
subgroup Anamalu (AAA), Rath kehel (AAA) and Gentle combing was done to remove excess pith from
Ambun (AAA), Atamuru (ABB), Seenikesel (ABB), the fibers. Washing was done by immersing the fibers in
Alu kesel (ABB), Poowalu (AB) and Suwandel (AB) the large centrifugal washing machine and allowed to
varieties are found in Sri Lanka.13 dry. The extracted fibers were observed to be in long
Banana farming generates large quantities of ped- strands and slightly dull yellowish in color. Once the
uncle and pseudostem due to lack of suitable sustain- banana stems were mechanically extracted, extracted
able technology for its economic utilization.14 Banana banana fiber samples were treated with chemicals and
Balakrishnan et al. 3

enzymes to evaluate their physical characterizations. using equation one (1), where T is the average fiber
Mechanically extracted banana fiber cut into 25-cm linear density, dtex, D is the average fiber linear den-
lengths were used for physico-biological, physico-che- sity, denier, W is the mass of bundle specimen, mg, L is
mical and physico-enzyme and chemical combined the length of bundle specimen, mm, and N is the
treatments. number of fibers in the bundle specimen.

Physico-biological treatment. Mechanically extracted fibers Td ¼ 1000WðL  NÞ ð1Þ


were treated with 5% concentrations of enzyme at a
temperature of 55 C in acid medium. pH was con- Fiber fineness/surface characteristics or scanning
trolled between 2.5 and 3.5 for the enzyme treatment.
The liquor ratio of 1:50 was used for the treatment. The
electron microscopy analysis
treated banana fiber samples were then thoroughly Scanning electron microscopy (SEM) was used to ana-
washed using running water and dried in the oven. lyze the exterior properties of the fibers. SEM was used
to observe the diameter results to evaluate the fineness
Physico-chemical treatment. Mechanically extracted fibers of the fiber. It was analyzed by calculating fiber thick-
were treated with 6% bleaching agents (hydrogen per- ness (diameter) at five different places with a magnifi-
oxide), 2% sodium silicate, 3% caustic soda and 0.2% cation factor of 1500. This paper assumes that the
wetting agent at a temperature of 95 C for 2 hours. The cross-section of banana fiber is approximately circular
treatment’s liquor ratio is 1:50. The treated banana based on the finding reported by Mukhopadhyay et al.2
fiber samples were then thoroughly washed using run- The fiber diameter was observed under SEM micro-
ning water and dried in the oven. scope as the average of five diameter measurements
taken at different locations along the treated and
Physico-enzyme and chemical combined untreated fiber.
treatment. Mechanically extracted fibers were treated
with 5% concentrations of pectinase enzyme at a tem-
perature of 45–55 C. pH was controlled between 2.5
Fourier transform infrared analysis
and 3.5 for the enzyme treatment. The liquor ratio of A Fourier transform infrared (FTIR) Bruker TENSOR
1:50 was used for the treatment. The treated banana 27 spectrophotometer was used to determine the spec-
fiber samples were thoroughly washed using running trum of each treated and untreated sample. A 4000–
water and dried in the oven. After that, the enzyme- 600 cm1 transmission range of mode was used for the
treated samples were treated with concentrations of 6% testing. FTIR analysis of banana fibers was done to
hydrogen peroxide, 2% sodium silicate, 3% caustic study the components and its spectrum depicts O – H
soda and 0.2% wetting agent at a temperature of stretch, free hydroxyl, O- H stretch, H- bond, - CH2 -
95 C for 2 hours. The liquor ratio of 1:50 was used CH2 -, -C C – and C- H alkenes compound gatherings
for the treatment. These combination-treated banana that are available in the untreated banana fiber.
fiber samples were then thoroughly washed using run-
ning water and dried in the oven.
Conditioning
All test specimens (untreated and treated banana fiber)
Testing of banana fibers were conditioned in the standard atmosphere for test-
ing, which is 21  1 C and 65  2% relative humidity.
Tensile strength
The electro-mechanical Instron universal tensile tester
Results and discussion
machine was used in this experiment. Tensile test speci-
mens were made in accordance with ASTM D3822 stand- Figure 1 shows the fiber fineness results of mechanically
ard to measure the single fiber strength. The breaking extracted fiber from 10 types of banana varieties. Rath
force of individual specimens was recorded to three sig- kehel fiber shows the greatest fiber fineness value and
nificant digits as read directly from the tension testing Ambun (AAA genome) fiber the lowest compared to
machine expressed in centinewton or gf. the other varieties. In order to study the finer fiber and
single fiber strength testing results, this research work
selected Ambun, Kolikuttu, Ambul, Atamuru and
Fiber linear density
Poowalu varieties for further testing.
Single fibers in a bundle were calculated from mass and Table 1 gives the standard deviation and coefficient
length measurements on the untreated and treated of variation of fiber diameter from 10 selected banana
bundle. The average fiber linear density was calculated varieties.
4 Textile Research Journal 0(00)

Figure 2 shows that the greatest amount of the single and 6) taken from the four layers of the pseudostem
fiber strength is achieved by Atamuru, Puwalu and fiber. Banana fibers show uneven joints, obvious slubs,
Ambun fibers. According to the results, Ambun fiber the joint distances of which are long. The mechanically
is more suitable for extracting very fine fiber. Hence, extracted banana fiber appearance is not very clean and
these fibers were used in the chemical and enzyme smooth (very rough) compared with the other treated
treatments. fibers.
Table 2 shows the standard deviation and coefficient
of variation of single fiber strength from five selected
banana varieties.
Surface morphological analysis
Scanning electron micrograph results of the surface of
Analysis of layer-wise Ambun banana fiber’s mechanically extracted Ambun banana fiber layer-wise
mechanical properties
Table 3 shows mechanical properties of Ambun banana 400

Fibre Strength(gf)
fibers. It was observed that the second and third layers 300 1. Kolikuttu
of Ambun banana fibers are finer than the first and 2. Ambul
fourth layers. The results showed that the average fine- 200 3. Atamuru
4. Puwalu
ness of the second layer is 25 tex and the diameter value 100 5. Ambun
is 79.8 mm. The test result showed the middle layers
(second and third) to be the finest. 0
1 2 3 4 5
Banana varieties
Microscopy analysis
Figure 2. Single fiber strength of mechanically extracted fibers
Light microscopic analysis of banana fibers was per-
from five selected varieties.
formed to study the structure of banana fibers with
different magnifications. Significant differences in the
morphology of the fibers (longitudinal views) were
not visible in the microscopic images (Figures 3, 4, 5 Table 2. Standard deviation and coefficient of variation of single
fiber strength from five selected varieties

Banana varieties 1 2 3 4 5

Standard deviation 0.368 1.140 0.517 0.608 0.114


Coefficient 0.154 0.894 0.216 0.254 0.298
of variation

Table 3. Mechanical properties of Ambun banana pseudostem


fiber

1st 2nd 3rd 4th


Test method layer layer layer layer

Fiber linear density (tex) 30 25 25 27


Fiber diameter (mm) 206.3 79.8 78.02 159.6
Single fiber strength (N) 2.78 2.67 2.65 2.54
Figure 1. Diameter of mechanically extracted fibers from 10
Elongation (%) 1.10 1.20 1.10 1.50
selected varieties.

Table 1. Standard deviation and coefficient of variation of fiber diameter from 10 selected varieties

Banana varieties 1 2 3 4 5 6 7 8 9 10

Standard deviation 0.868 1.35 1.725 0.993 0.895 1.477 1.817 2.985 2.641 2.108
Coefficient of variation 1.226 1.82 2.976 0.987 0.381 1.181 0.571 1.915 1.976 1.945
Balakrishnan et al. 5

Figure 3. Microscopic view of the first layer.

Figure 4. Microscopic view of the second layer.

Figure 5. Microscopic view of the third layer.

Figure 6. Microscopic view of the fourth layer.

are shown in Figure 7; the irregular surface with impu- fiber improves the fiber surface adhesive characteristics
rities due to the microfibrils appeared to be parallel to by the chemical treatment and enzyme treatment for
the fiber’s axis. removing natural (lignin and hemicelluloses) and artifi-
Treated Ambun fiber specimens are shown in cial impurities. However, fibrillation also started
Figures 8 and 9. A rough surface topography of the (Figures 8 and 9).
6 Textile Research Journal 0(00)

Figure 7. SEM view of Ambun layer.

Figure 8. SEM view of physico-biologically treated fiber.


Figure 9. SEM view of enzyme and chemical combined treated
fiber.
Balakrishnan et al. 7

The fractured surfaces of enzyme and chemical trea-


ted banana fibers of SEM images (Figures 8 and 9)
FTIR analysis
signify that the crash or surface structure changes as FTIR spectra of the four untreated layers of banana
a result of the pull out of microfibrils joined by tearing fibers are shown in Figures 10, 11, 12 and 13. The
of cell dividers and fiber surface see the morphology of absorption peaks at 1600 cm1 and 1636 cm1 are dif-
the treated fiber. Mechanical properties of banana ficult to interpret due to the presence of lignin
fibers impact on low microfibril angle and high cellulose components.
content.23 Figure 9 (enzyme and chemical combined The absorption band at 3500–3600 cm–1 region
treatment) shows the finest diameter compared to the exposed the presence of a strong hydrogen bonded
other treatments as the hemicellulose and lignin bond- hydroxyl stretching peak which was due to the presence
ing agents between the microfibrils were removed. of cellulose. The absorption band around 1400 cm–1
Bonding substances can be observed in mechanically revealed the frequency of bending vibration of CH –
extracted fiber images.24 bonds. The sharp peak at 1737 cm–1 absorption band

Figure 10. FTIR spectroscopy graph of the first layer.

Figure 11. FTIR spectroscopy graph of the second layer.


8 Textile Research Journal 0(00)

Figure 12. FTIR spectroscopy graph of the third layer.

Figure 13. FTIR spectroscopy graph of the fourth layer.

Figure 14. FTIR spectroscopy graph of physico-biologically treated fiber.


Balakrishnan et al. 9

Figure 15. FTIR spectroscopy graph of physico-chemically treated fiber.

Figure 16. FTIR spectroscopy graph of enzyme and chemical treated fiber.

revealed C¼O group. The absorption band at 1440– –C (triple bond) C-H:C-H bend and H-C¼O:C-H
1400 cm–1 region exposed the presence of O-H bend. stretch aldehydes (Source: Infrared Spectroscopy
The 770–735 cm–1 absorption bond represents C-H Absorption Table). Physico-enzyme and chemical com-
bend (meta). Figure 14 shows the absorption band at bined treated fibers’ (Figure 16) peak at 1600 cm–1 is
2850–2750 cm–1 exposed the presence of C-H aldehyde found to have disappeared which indicates lower
stretch and 2830–2695 cm–1 region exposed H-C¼O:C- lignin components.
H stretch aldehydes. Figure 15 shows the absorption From the biological and chemical treatment result, it
band at 700–610 cm–1 region exposed the presence of was observed that the fiber fineness influences the
10 Textile Research Journal 0(00)

Figure 17. Tensile strength of Ambun fiber.

180

160
1.Mechanical extraction
140
2.Physico-biological
Fibre fineness (µm)

120 treatment

100 3.Physico - chemical


treatment
80
4.Physico - enzyme and
60 chemical treatm ent

40

20

0
1 2 3 4

Figure 18. Fineness of Ambun fiber.

Table 4. Mechanical properties of mechanical extraction and treatment methods

Mechanical Physico-biological Physico-chemical Physico-enzyme and


Properties extraction treatment treatment chemical treatment

Fineness (mm) 168.4 101.45 60.5 48.8


Fiber linear density (tex) 25 21 18 5.6
Single fiber strength (gf) 2.670 3.298 2.973 2.931
Moisture content (%) 9.90 9.60 9.60 11.10
Balakrishnan et al. 11

thickness (diameter) and tensile strength properties. Declaration of conflicting interests


The fiber fineness reduced after biological and chemical The authors declared no potential conflicts of interest with
treatments. Physico-biological treatment shows a respect to the research, authorship and/or publication of this
higher strength value compared to the other treatments. article.
Physico-chemical treatment and physico-enzyme and
chemical combined treatment results show fiber fine- Funding
ness is reduced and single fiber strength of the
The authors disclosed receipt of the following financial sup-
Ambun fibers (Figures 17 and 18) is increased due to port and necessary facilities for the research, authorship and/
the alkali treatment. Physico-enzyme and chemical or publication of this article: the Ministry of Industry and
combined treated fiber diameter (mm) is the lowest com- Commerce Sri Lanka and Sri Lanka Institute of Textile and
pared to the other treatments (Figure 18). Apparel.
Treatment of enzyme and 6% hydrogen peroxide,
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