Metodología: SAAM SM 5540C

Responsable: Santiago Amaya

Maximo %error permitido: 10.00

Condición Blancos
Conc. Esperada
Mn Cd Pb Se Zn Be
1 1.856535656216 0.607455 2.121608 1.145699 0.45585 1.292757
2 1.772626325852 0.437756 2.556954 0.93761 0.34663 0.319183
3 1.227145362273 0.636786 4.153556 0.973898 0.029112 0.34629
4 1.049629425523 0.525378 1.752909 0.999242 0.205949 0.303217
5 1.301587529297 0.325376 2.112815 0.988818 0.283116 0.360864
6 1.701475580362 0.802079 1.635564 1.023933 0.446352 0.354845
7 1.230008522543 0.479018 0.333777 0.973182 0.17805 0.269195
8
9
10
Datos

11
12
13
14
15
16
17
18
19
20
21
22
x 1.448 0.545 2.095 1.006 0.278 0.589
Descriptiva

s 0.3196 0.1543 1.1462 0.0670 0.1538 0.4898

s2 0.1022 0.0238 1.3137 0.0045 0.0236 0.2399
%CV 22.067 28.324 54.701 6.663 55.333 83.230
%Error #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0!
n datos 7 7 7 7 7 7
Dato Xmin 1.050 0.325 0.334 0.938 0.029 0.269
Rechazo

Dato Xmax 1.857 0.802 4.154 1.146 0.456 1.293

Tbajo 1.25 1.42 1.54 1.02 1.62 0.65
Talto 1.28 1.67 1.80 2.08 1.16 1.44
Trechazo 1.94 1.94 1.94 1.94 1.94 1.94
Dato R1 1.8475453708201 0.17319 5.271561 5.570832 2.21989 1.461698
Descartados

Dato R2
Dato R3
Dato R4
Dato R5
Total Datos 8 8 8 8 8 8

LDI 2.4073 1.0078 5.5338 1.2072 0.7391 2.0579

Detección
Detección LCMest 4.6447 2.0880 13.5569 1.6764 1.8154 5.4866

LDIprom 7.2394
LCMest,prom 6.7632

GAM-FR-28 V05 2019-04-07 Página 2 de 3

 Plantilla d

As Fe Cu Co Ba Cr Al Ni Ag
4.395818 5.351083 1.567694 0.918743 1.451228 11.41042 29.29335 1.931305 0.587925
4.434086 3.416843 1.637222 0.517835 1.356849 10.87643 27.86294 1.428912 1.160064
6.041277 3.314442 1.626727 0.550341 1.154797 10.43389 26.63898 1.457004 0.702257
6.194464 2.244921 1.428639 0.22528 1.154797 10.34962 27.13544 1.339691 2.641852
0.468732 4.554631 1.723804 0.550341 1.230566 11.35828 28.03498 1.515818 3.090522
5.516608 2.290433 1.46537 0.151509 1.590804 11.03218 25.21594 1.908264 0.534336
0.540843 2.426967 1.297545 0.639595 1.473826 10.70346 26.26786 1.307286 1.450604

3.942 3.371 1.392 0.508 1.345 10.881 27.207 1.555 1.453

2.4508 1.2010 0.4263 0.2571 0.1702 0.4173 1.3318 0.2586 1.0277
6.0066 1.4423 0.1817 0.0661 0.0290 0.1741 1.7738 0.0669 1.0561
62.177 35.623 30.615 50.652 12.660 3.835 4.895 16.623 70.751
#DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0!
7 7 7 7 7 7 7 7 7
0.469 2.245 1.298 0.152 1.155 10.350 25.216 1.307 0.534
6.194 5.351 1.724 0.919 1.591 11.410 29.293 1.931 3.091
1.42 0.94 0.22 1.39 1.12 1.27 1.50 0.96 0.89
0.92 1.65 0.78 1.60 1.45 1.27 1.57 1.45 1.59
1.94 1.94 1.94 1.94 1.94 1.94 1.94 1.94 1.94
0.055195 0.391951 0.962084 3.386774 11.47867 3.422236 3.488088

8 7 8 8 8 8 7 8 8

11.2942 6.9742 2.6712 1.2791 1.8554 12.1325 31.2026 2.3312 4.5355

28.4500 15.3810 5.6551 3.0791 3.0471 15.0535 40.5254 4.1412 11.7292
 Plantilla de Elaboración Análisis LDI y LCM

Fecha Elaboración:
Unidades Conc.:

Maximo %CV permitido: 15.00

LCM
6.000
Sb Tl Hg (KMNO3) Hg (HNO3) Hg (HCl) P Mn
4.916063 1.329531 0.00930609 0.741129 0.99149 1.18159990277242 6.042013
5.799408 2.023317 0.067081623 0.201891 0.702612 1.50609258224653 6.143108
6.01935 0.718525 0.105598614 0.209654 1.173467 1.03052967669896 6.1459963
0.34896 5.114828 0.144115597 0.40298 1.193973 1.21512824376321 5.9721222
1.151589 4.880832 0.17362462 0.619135 1.203333 1.22823127357571 5.9854083
1.839196 3.308323 0.231753498 0.741129 1.145558 0.859034139447203 5.8623678
1.455824 6.100329 0.240408093 0.510027 1.251147 1.08486871209783 5.8744985
5.9791305

3.076 3.354 0.100 0.486 1.015 1.158 6.001

2.4070 2.0733 0.0646 0.2498 0.2275 0.2004 0.1067
5.7935 4.2985 0.0042 0.0624 0.0518 0.0401 0.0114
78.256 61.821 64.663 51.391 22.406 17.305 1.778
#DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! 0.010
7 7 7 7 7 7 8
0.349 0.719 0.009 0.202 0.703 0.859 5.862
6.019 6.100 0.240 0.741 1.251 1.506 6.146
1.13 1.27 1.40 1.14 1.37 1.49 1.30
1.22 1.32 2.17 1.02 1.04 1.74 1.36
1.94 1.94 1.94 1.94 1.94 1.94 2.03
7.305114 1E-04 0.10559861 3.03289056 0.859034139447203

8 7 8 8 8 8 8
1.7590
10.2967 9.5735 0.2938 1.2352 1.6979 3.1617
27.1454 24.0865 0.7462 2.9835 3.2905 3.1617
tn-1,99 3.500
LCMdet 6.3740
 Anotaciones:
11/22/2019 *Recuerde que el nivel de confianza para la prueba t (a) está definido para un 99% de confianza
ppb *Recuerde que la cantidad de datos rechazados no debe ser mayor a 5 para un conjunto de 22 datos, mante
*Recuerde que las celdas en fondo rojo indican alguna condición negativa, mientras las celdas en fondo verde
*El límite de cuantificación estimado se da a partir de los ensayos con blancos, el determinado es el evaluado

LCM LCM LCM LCM LCM LCM LCM LCM

6.000 6.000 6.000 6.000 6.000 6.000 6.000 6.000
Cd Pb Se Zn Be As Fe Cu
5.6167985 5.9365652 5.8647611 5.940933 5.8223032 5.2331052 5.9678475 5.592437
5.9975958 6.1292604 6.2521269 6.147424 5.84794 6.2401185 5.7475777 5.4546932
5.9581057 5.5693145 5.8176988 6.0795781 5.8367188 6.9637849 6.9892005 5.6186739
5.4129006 5.9199721 6.1599755 6.0462741 5.8371283 6.8914182 5.4845114 5.3523692
6.0494868 6.0605822 6.3179493 5.9796661 5.7167255 6.9599561 5.0807241 5.6450276
6.1699861 6.0282687 5.4622576 6.3257986 5.6292491 7.2319242 6.0321357 5.2679155
6.3275622 6.254463 6.4101007 6.0957216 5.7384307 6.1440518 6.222418 5.9514311
6.2456844 5.8020745 5.2467035 5.9735568 5.8273814 5.8544456 6.0869648

5.972 5.963 5.941 6.074 5.782 6.523 5.922 5.621

0.3131 0.2104 0.4207 0.1235 0.0789 0.6965 0.5577 0.2809
0.0980 0.0443 0.1770 0.0153 0.0062 0.4852 0.3111 0.0789
5.242 3.528 7.081 2.033 1.364 10.677 9.418 4.997
0.462 0.624 0.976 1.227 3.634 8.725 1.294 6.314
8 8 8 8 8 7 8 8
5.413 5.569 5.247 5.941 5.629 5.233 5.081 5.268
6.328 6.254 6.410 6.326 5.848 7.232 6.989 6.087
1.79 1.87 1.65 1.07 1.94 1.85 1.51 1.26
1.13 1.39 1.11 2.04 0.84 1.02 1.91 1.66
2.03 2.03 2.03 2.03 2.03 1.94 2.03 2.03

8 8 8 8 8 7 8 8
3.500 3.500 3.500 3.500 3.500 3.710 3.500 3.500
7.0680 6.6989 7.4140 6.5059 6.0581 9.1076 7.8745 6.6042
 Corporación Autónoma Regional de Cundinamarca
Dirección de Laboratorio e Innovación Ambiental

ra un 99% de confianza
ra un conjunto de 22 datos, manteniendo proporcionalidad
mientras las celdas en fondo verde indican aceptación de los criterios
cos, el determinado es el evaluado a partir de estándares

LCM LCM LCM LCM LCM LCM LCM LCM

6.000 6.000 6.000 6.000 6.000 6.000 8.000 600.000
Co Ba Cr Al Ni Ag Sb Tl
5.5996163 5.8417403 6.0205019 5.8241115 5.7102281 6.1106778 8.07719 543.08764
5.7520208 5.7229468 5.8482678 5.7121644 6.2494294 6.5140684 8.0249752 535.6447
5.7771352 5.9276574 5.9859359 5.4193795 5.6716001 5.8735117 8.10565 594.51106
5.6201702 5.7309225 5.8323362 5.1265946 5.9917192 6.1377443 9.0211695 640.77271
5.8461999 5.7336175 5.8171565 6.8316359 5.7635229 6.5509185 7.320319 544.47521
5.6693083 6.2606147 5.928649 5.9877266 6.6089148 6.4295219 7.5470991 542.62268
6.08971 6.1761298 6.0584619 6.1899335 5.6222939 6.3004155 8.7509932 563.81232
5.664777 5.5977534 5.842805 5.9969967 5.7501433 5.8135684 7.9153609 606.62957

5.752 5.874 5.917 5.886 5.921 6.216 8.095 571.444

0.1597 0.2342 0.0949 0.5124 0.3456 0.2804 0.5639 38.3191
0.0255 0.0549 0.0090 0.2625 0.1194 0.0786 0.3180 1468.3549
2.777 3.987 1.603 8.705 5.836 4.510 6.966 6.706
4.127 2.101 1.387 1.899 1.317 3.605 1.192 4.759
8 8 8 8 8 8 8 8
5.600 5.598 5.817 5.127 5.622 5.814 7.320 535.645
6.090 6.261 6.058 6.832 6.609 6.551 9.021 640.773
0.96 1.18 1.05 1.48 0.86 1.44 1.37 0.93
2.11 1.65 1.49 1.85 1.99 1.19 1.64 1.81
2.03 2.03 2.03 2.03 2.03 2.03 2.03 2.03

8 8 8 8 8 8 8 8
3.500 3.500 3.500 3.500 3.500 3.500 3.500 3.500
6.3114 6.6937 6.2487 7.6794 7.1305 7.1975 10.0691 705.5614
 LCM LCM
600.000 6.000
P Hg
525.97845 5.48629427
591.8004 5.594141483
637.07504 5.836798191
525.11868 5.890722275
664.78579 5.971608639
529.42461 6.025531769
562.00448 5.836798191
608.64565 5.257456303

580.604 5.737
53.7389 0.2659
2887.8697 0.0707
9.256 4.635
3.233 4.376
8 8
525.119 5.257
664.786 6.026
1.03 1.80
1.57 1.08
2.03 2.03

8 8
 3.500 3.500
768.6903 6.6682