Safety Rupture Disc Assemblies Operating Instruction Manual: General Instructions

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231M

Safety Rupture Disc Assemblies


Operating Instruction Manual

Safety rupture discs are installed in Parr laboratory pressure should not exceed 90% of their design
reactors and pressure vessels to protect the equip- burst pressure. This guidance was developed to
ment and the operator from unexpected overpressure. protect these discs from the effects of repeated
These safety devices are made in several styles, each pressure pulsing. While no cycle life is guaranteed,
designed to match the size constraints and the relief discs held to this 90% limit may be expected to
flow requirements of the reactor or vessel on which it withstand 5,000 pressurization cycles. For most
is used. Each assembly consists of a domed, frangible Parr Pressure Vessels 5,000 cycles represents many
metal disc clamped firmly against a carefully machined years of service.
orifice through which the disc will rupture and release
pressure/material from the vessel if the internal pres- It should be noted that the burst pressure tolerance
sure reaches a pre-determined burst range. All assem- of these discs is ± 5%. So to take a disc to 90% of its
blies have either a safety tee or provision for attaching design may in fact be taking it to 95% of its actual
extension piping or tubing to carry any discharge to a burst pressure. This does not leave much room for
safe area if the rupture disc should burst. The different pressure excursions.
rupture disc assemblies used in Parr equipment are
illustrated with listings of the particular units in which
The 600 psi discs are the lowest rating offered in
each is installed. The rupture disc installed in each Parr
the 526HC Series discs and in the 708HC Series,
reactor or pressure vessel will function as an effective
800 psi is the lowest available rating. If lower relief
safety device when used as directed.
pressures are desired or required, the user should
It is essential that the user of this equipment read and install a spring - loaded relief valve on the vessel to
observe the following instructions. Rupture discs are of serve as a primary relief device, leaving the rupture
such simple construction that the user will often take disc in the system as the fail-safe protection in case
them for granted. Potential hazards can occur from: im- the mechanical relief valve does not function as
proper disc selection, improper installation, improper intended.
maintenance, improper usage, overfilling, over pressur-
izing, and from failure to provide adequate venting. Standard rupture discs can be furnished with a
declaration of conformity showing burst pressures
at room temperature. At temperature rupture discs
GENERAL INSTRUCTIONS can also be furnished with a declaration of confor-
mity showing burst pressures at room and elevated
1. Retain the disc identification tag. temperatures. Custom discs made of other than
All rupture discs are furnished with a metal tag standard materials or burst ratings can be provided
which identifies the burst rating of the disc at a within the limits of available materials and size
particular temperature as well as the material of the constraints. A minimum of three discs is usually
disc. When a complete reactor system or general required for a special order.
purpose vessel is furnished with a rupture disc,
these tags are attached to the safety head body 3. Select a suitable disc material.
prior to shipment. The disc must be made of a material which is com-
patible with the environment in which it is used.
When installing a replacement disc, the new tag This is particularly important when a reactor is used
should be attached to the safety head body. It is for several different purposes. A disc that may have
important that these tags remain on the apparatus been satisfactory for an original application may
so that both present and future operators will be not be suitable in a different situation. The Alloy
aware of the disc rating. 600 series discs usually installed in Parr pressure
equipment will resist most chemical vapors, yet it
2. Select the proper burst rating. cannot be assumed that an Alloy 600 disc will be
Our standard rupture discs are made of thin metal suitable for all applications. Strong mineral acids,
foils which are domed. The discs are installed with strong organic acids and wet halogens will attack
the inside of the dome (concave side) exposed to Alloy 600 to varying degrees. If corrosion becomes
the pressure. The general guidance for rupture discs a problem, gold facing or alternate disc materials
of this design is that their maximum operating are available.

Parr Instrument Company www.parrinst.com


Safety Rupture Disc Assemblies
The series 581HC discs for use in a 1/4” orifice are 7. Protect against loud noise.
Alloy 600 with a gold facing. This option is not When a rupture disc bursts the instantaneous expul-
available for the 1/2” orifice series 708HC discs due sion of gases and vapors at sonic velocities creates
to their configuration. a loud noise which may damage the hearing of any
individual in the general vicinity of the apparatus.
Alternate materials such as Alloy C-276 and Tanta- Extension tubing will minimize this report, but indi-
lum are available for either series disc for certain vidual ear protectors may be the only effective way
ranges which varies with the different materials. to fully protect individuals from this hazard. Because
of this potential hazard it is always best to operate a
4. Allow for temperature effect. pressure reactor in an isolated area and to keep all
The burst pressure for any metal rupture disc will unnecessary personnel away from the equipment
drop as the temperature is raised, although Alloy while it is under pressure.
600 discs are much more stable in this respect than
most other disc materials. An Alloy 600 disc will 8. Install replacement discs carefully.
retain about 90 percent of its rating when heated Before installing a replacement disc, ensure rup-
from 22 °C to 500 °C. Alloy C276 discs are compa- ture disc opening is clean and free from debris.
rable to Alloy 600 temperature for stability. Rupture When replacing a rupture disc, the domed side
discs made of other materials, such as Tantalum, of the disc must project toward the outlet or
will have entirely different temperature-pressure discharge end of the assembly. If there is a choice
profiles, usually losing strength much more rapidly between a sharp edge and a rounded edge on
at elevated temperature. the orifice ring which bears against the domed
side of the disc, place the rounded edge – not
5. Be alert to damage from over pressure. the sharp edge – against the disc. Apply a light
Under normal operating conditions where the coating of a thread lubricant (such as Parr 424HC2
pressure applied to a disc never exceeds 90 per- anti-seize lube) to the surface of the orifice ring
cent of the burst rating there should be little or no which contacts the body plug, top and bottom
deterioration in the ability of the disc to function as sealing surfaces of rupture disc, and to the faces
intended (unless it is affected by corrosion or other of the orifice cone which seals the assembly into
external factors). the pressure vessel or fitting. The installation will
be easier if you invert the assembly and the head
6. Provide safe venting. before screwing the parts into place and tightening
The user must assume full responsibility for in- the compression body.
stalling an adequate and safe venting system to
remove any toxic, flammable or volatile materials 9. Rupture Discs rated at elevated temperatures:
which would be released if the rupture disc should The burst pressure of rupture discs rated at elevated
burst. Consideration must also be given to any temperatures will increase when used at tempera-
flying particles, disc fragments or reaction materials tures lower than the specification. The percentage
which might be carried with the discharge. Contact increase in strength of the disc will be dependent on
Parr technical staff for use of knock-out pots. The the temperature profile of the material of the disc.
discharge port from the rupture disc must always be As such, rupture discs rated at elevated tempera-
directed away from all operating personnel and pref- tures may no longer provide suitable over-pressure
erably, extension piping should be attached to the protection at lower temperatures. The user is advised
safety head to carry any discharge to a fume hood to exercise due diligence when using rupture discs
or to any other area where vapors can be released rated at elevated temperatures.
safely. Connectors are available on the A888HC2
rupture disc assembly for attaching 1/4” NPT
female, 1/4” NPT male, or 3/8” OD tubing to carry
any discharge to a safe outlet. Be sure to anchor the Customer Service
discharge end of the extension tubing securely. Questions concerning the installation or operation of
this instrument can be answered by the Parr Customer
The A707HC2 and A1417HC rupture disc assem- Service Department:
blies installed on one gallon and larger reactors
have a straight discharge with a 1/2” NPT male 1-309-762-7716 • 1-800-872-7720
pipe thread to which extension tubing should be Fax: 1-309-762-9453
attached. Any extension piping attached to this E-mail: parr@parrinst.com • www.parrinst.com
assembly must also be anchored securely.

2 Parr Instrument Company


Safety Rupture Disc Assemblies
Torque Requirements for Standard 1/4” Torque Requirements for Standard 1/2” Torque Requirements for Standard 1/2”
Discs Installed on A888HC2 Assembly † Discs Installed on A707HC2 Assembly † Discs Installed on A1417HC Assembly †
Part Burst Pressure Torque Part Burst Pressure Torque Part Burst Pressure Torque
Number (PSI) (Ft-Lbs) Number (PSI) (Ft-Lbs) Number (PSI) (Ft-Lbs)
600 to 1000 33 800 to 1000 20 500 to 1000 38

1415 HC SERIES
708 HC SERIES
526 HC / 581 HC SERIES

>1000 to 2000 33 >1000 to 1500 25 >1000 to 2000 52


>2000 to 3000 33 >1500 to 2000 30 >2000 to 3000 66
>3000 to 4000 33 >2000 to 2500 35 >3000 to 4000 81
>4000 to 5000 33 >2500 to 3000 40 >4000 to 5000 96
>5000 to 6000 33
>6000 to 8000 33 † For
Rupture Discs constructed of materials other than Alloy C276 or Alloy 600, check supplemental
>8000 to 10000 39 operating instructions furnished with your order or contact Parr Customer Service Deptartment.

PARR RUPTURE DISC SERIES


Series 526HC Discs for 1/4” Orifice (For A888HC2 Assembly)
Part Number Burst Rating (psi) Max. Operating Pressure (psi) Temperature Material CE
526HCP6YA 600 540 22 °C Alum/FEP Y
526HCPD 1000 900 22 °C Alloy 600 Y
526HCP10CH 1000 900 22 °C Alloy C276 Y
526HCP11AD 1150 1035 22 °C T316 Y
526HCP11CT 1150 1035 22 °C Alloy 600 Y
526HCP12CT 1200 1080 22 °C Alloy 600 Y
526HCP14CT 1400 1260 22 °C Alloy 600 Y
526HCP14CH 1400 1260 22 °C Alloy C276 Y
526HCP15CT 1500 1350 22 °C Alloy 600 Y
526HCP15CH 1500 1350 22 °C Alloy C276 Y
526HCP17CT 1700 1530 22 °C Alloy 600 Y
526HCP19CT 1900 1710 22 °C Alloy 600 Y
526HCPF 2000 1800 22 °C Alloy 600 Y
526HCP20CH 2000 1800 22 °C Alloy C276 Y
526HCP22CT 2200 1980 22 °C Alloy 600 Y
526HCPG 3000 2700 22 °C Alloy 600 Y
526HCP29CH 2900 2610 22 °C Alloy C276 Y
526HCP29CT 2900 2610 22 °C Alloy 600 Y
526HCP30CH 3000 2700 22 °C Alloy C276 Y
526HCP40CT 4000 3600 22 °C Alloy 600 Y
526HCP45CT 4500 4050 22 °C Alloy 600 Y
526HCP45CH 4500 4050 22 °C Alloy C276 Y
526HCPH 5000 4500 22 °C Alloy 600 Y
526HCP50CH 5000 4500 22 °C Alloy C276 Y
526HCP52CT 5250 4725 22 °C Alloy 600 Y
526HCP60CT 6000 5400 22 °C Alloy 600 Y
526HCPJ 8000 7200 22 °C Alloy 600 Y
526HCP80CH 8000 7200 22 °C Alloy C276 Y
526HCP85CH 8500 7650 22 °C Alloy C276 Y
526HCP85CT 8500 7650 22 °C Alloy 600 Y
526HCP100CT 10,000 9000 22 °C Alloy 600 Y

www.parrinst.com 3
Safety Rupture Disc Assemblies
Series 526HC Discs for 1/4” Orifice (For A888HC2 Assembly) (Continued)
Part Number Burst Rating (psi) Max. Operating Pressure (psi) Temperature Material CE
526HCP10CTYZ35 1000 900 350 ºC Alloy 600 Y
526HCP10CTYZ50 1000 900 500 ºC Alloy 600 Y
526HCP19CTYZ35 1900 1710 350 ºC Alloy 600 Y
526HCP19CTYZ50 1900 1710 500 ºC Alloy 600 Y
526HCP20CHYZ50 2000 1800 500 ºC Alloy C276 Y
526HCP20CTYZ35 2000 1800 350 ºC Alloy 600 Y
526HCP20CTYZ50 2000 1800 500 ºC Alloy 600 Y
526HCP29CHYZ30 2900 2610 300 ºC Alloy C276 Y
526HCP29CTYZ35 2900 2610 350 ºC Alloy 600 Y
526HCP29CHYZ35 2900 2610 350 ºC Alloy C276 Y
526HCP30CHYZ35 3000 2700 350 ºC Alloy C276 Y
526HCP30CTYZ35 3000 2700 350 ºC Alloy 600 Y
526HCP30CHYZ50 3000 2700 500 ºC Alloy C276 Y
526HCP30CTYZ50 3000 2700 500 ºC Alloy 600 Y
526HCP42CTYZ60 4200 3780 600 ºC Alloy 600 Y
526HCP44CTYZ50 4400 3960 500 ºC Alloy 600 Y
526HCP50CHYZ35 5000 4500 350 ºC Alloy C276 Y
526HCP50CHYZ35 5000 4500 350 ºC Alloy C276 Y
526HCP50CHYZ50 5000 4500 500 ºC Alloy C276 Y
526HCP50CTYZ35 5000 4500 350 ºC Alloy 600 Y
526HCP50CTYZ50 5000 4500 500 ºC Alloy 600 Y
526HCP59CTYZ50 5900 5310 500 ºC Alloy 600 Y
526HCP80CTYZ50 8000 7200 500 ºC Alloy 600 Y
526HCP94CHYZ35 9400 8460 350 ºC Alloy C276 Y
526HCP10CR ‡ 1000 900 22 °C Tantalum Y
‡ Maximum operating pressure will vary dramatically with increase in temperature.

Series 581HC Discs for 1/4” Orifice (For A888HC2 Assembly)


Part Number Burst Rating (psi) Max. Operating Pressure (psi) Temperature Material CE
581HCP08CT 800 720 22 °C Gold Faced Alloy 200 Y
581HCPD 1000 900 22 °C Gold Faced Alloy 600 Y
581HCP12CT 1200 1080 22 °C Gold Faced Alloy 600 Y
581HCP14CT 1400 1260 22 °C Gold Faced Alloy 600 Y
581HCP16CT 1600 1440 22 °C Gold Faced Alloy 600 Y
581HCP18CT 1800 1620 22 °C Gold Faced Alloy 600 Y
581HCPF 2000 1800 22 °C Gold Faced Alloy 600 Y
581HCP27CT 2700 2430 22 °C Gold Faced Alloy 600 Y
581HCPG 3000 2700 22 °C Gold Faced Alloy 600 Y
581HCPH 5000 4500 22 °C Gold Faced Alloy 600 Y
581HCP52CT 5250 4725 22 °C Gold Faced Alloy 600 Y
581HCP60CT 6000 5400 22 °C Gold Faced Alloy 600 Y
581HCPJ 8000 7200 22 °C Gold Faced Alloy 600 Y
581HCP10CTYZ35 1000 900 350 ºC Gold Faced Alloy 600 Y
581HCP20CTYZ35 2000 1800 350 ºC Gold Faced Alloy 600 Y

4 Parr Instrument Company


Safety Rupture Disc Assemblies
Series 708HC Discs for 1/2” Orifice (For A707HC2 Assembly)
Part Number Burst Rating Max. Operating Pressure Temperature Material CE
708HCP08CH 800 720 22 °C Alloy C276 Y
708HCP10CH 1000 900 22 °C Alloy C276 Y
708HCP10CT 1000 900 22 °C Alloy 600 Y
708HCP10CTYZ35 1000 900 350 °C Alloy 600 Y
708HCP10CTYZ50 1000 900 500 ºC Alloy 600 Y
708HCP16CT 1600 1440 22 °C Alloy 600 Y
708HCP19CT 1900 1710 22 °C Alloy 600 Y
708HCP19CTYZ35 1900 1710 350 °C Alloy 600 Y
708HCP20CH 2000 1800 22 °C Alloy C276 Y
708HCP20CT 2000 1800 22 °C Alloy 600 Y
708HCP20CTYZ35 2000 1800 350 °C Alloy 600 Y
708HCP22CT 2200 1980 22 °C Alloy 600 Y
708HCP30CT 3000 2700 22 °C Alloy 600 Y
708HCP10CR ‡ 1000 900 22 °C Tantalum N
708HCP20CR ‡ 2000 1800 22 °C Tantalum N
708HCP30CR ‡ 3000 2700 22 °C Tantalum N
‡ Maximum operating pressure will vary dramatically with increase in temperature.

Series 1415HC Discs for 1/2” Orifice (For A1417HC Assembly)


Part Number Burst Rating Max. Operating Pressure Temperature Material CE
1415HCP10CT 1000 900 22 °C Alloy 600 Y
1415HCP20CT 2000 1800 22 °C Alloy 600 Y
1415HCP30CT 3000 2700 22 °C Alloy 600 Y
1415HCP32CT 3200 2880 22 °C Alloy 600 Y
1415HCP45CT 4500 4050 22 °C Alloy 600 Y
1415HCP20CTYZ50 2000 1800 500 ºC Alloy 600 Y
1415HCP30CHYZ50 3000 2700 500 ºC Alloy C276 Y
1415HCP30CTYZ50 3000 2700 500 ºC Alloy 600 Y

www.parrinst.com 5
Safety Rupture Disc Assemblies
SAFETY RUPTURE DISC ASSEMBLIES FOR PARR APPARATUS

A888HC2*

Orifice diameter: 0.25 inch 1/4” NPT(M)


526HC/581HC
Thread size: 5/8-18 inch
RUPTURE DISC
REF
Use on Reactor Models
4523 – 4526 1&2L
433HC4
4531 – 4536 1&2L SAFETY HEAD
4561 – 4568 100 - 600 mL OUTLET
4575 – 4576 250 & 500 mL 527HC
4591 – 4598 25, 50, 100 mL ORIFICE RING
5000 (MRS) 45 & 75 mL
**49HC2
5101 – 5112 160 mL - 1.5 L ORIFICE CONE
4544 – 4547 600 & 1200 mL
4571 – 4578 1000 & 1800 mL
5511 – 5525 25 - 600 mL
4316 – 4317 Gage Block Assembly

Use on Cell Disruption Vessels


4635 – 4636 920 & 1850 mL

* Use 526HC or 581HC Series disc


** Orifice cones available in special materials

Connectors for the A888HC2


366VBAD Hex Coupling, I/4 NPT(F)
288VBAD Connectors, Male 3/8T – I/4 NPT 288VBAD
302VBAD Connectors, Female 3/8T – I/4 NPT

302VBAD 366VBAD

A888HC2
A888HC2

A888HC2 Rupture Disc Assembly A888HC2 Rupture Disc Assembly


Shown with 1/4 NPT female Shown with 1/4 NPT female
connector to 3/8” OD tubing hex coupling and 1/4 NPT male
connector to 3/8” OD tubing

6 Parr Instrument Company


Safety Rupture Disc Assemblies
A888HC*

Orifice diameter: 0.25 inch


Thread size: 5/8-18 inch 526HC/581HC
RUPTURE DISC
Alternate Rupture Disc Assembly REF
Contact Parr Customer Service Department for
more information 604HC
SAFETY TEE
* Use 526HC or 581HC Series disc
** Orifice cones available in special materials 527HC
ORIFICE RING

**49HC2
ORIFICE CONE

A707HC2*

Orifice Diameter: 0.50 inch 708HC


RUPTURE DISC
1/2” NPT(M)
Thread size: 1/2” NPT Thread REF

Use on Reactor Models 759HC2


PIPE OUTLET
4551 – 4554 1 & 2 gallon
4555 – 4558 2.6 & 5 gallon
760HC
Use on Cell Disruption Vessels ORIFICE RING
4637 – 4638 1 & 2 gallon
**761HC
* Use 708HC Series rupture disc SAFETY HEAD BODY
** Safety head bodies available in special material

A1417HC*

Orifice Diameter: 0.50 inch


1/2” NPT(M)
Thread Size: 1-20 inch 1415HC
RUPTURE DISC
REF
Use on Reactor Models
4581 – 4584 1 & 1.5 gallon 759HC2
PIPE OUTLET
* Use 1415HC Series rupture disc
** Orifice rings available in special material
1416HC
BACKUP ORIFICE

**760HC
ORIFICE RING

ASSEMBLY INSTRUCTIONS:
1) INSTALL 760HC ORIFICE RING W/TAPER AS SHOWN
2) INSTALL 1415HC STYLE RUPTURE DISC W/BUBBLEwAS
wSHOWN
w.pa rrinst.com 7
3) INSTALL 1416HC BACKUP ORIFICE W/5 TAPER NEXT TO
RUPTURE DISC R1
4) INSTALL 759HC2 PIPE OUTLET TO COMPLETE ASSEMBLY
231M R17 11/08/16

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