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International Journal of Rock Mechanics and Mining Sciences 36 (1999) 291±306

INTERNATIONAL SOCIETY FOR ROCK MECHANICS


COMMISSION ON SWELLING ROCKS AND COMMISSION
ON TESTING METHODS

SUGGESTED METHODS FOR LABORATORY TESTING OF SWELLING ROCKS

CONTENTS

1. Introduction . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 293
2. Part 1: suggested methods for sampling, storage and preparation of test
specimens . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 294
3. Part 2: suggested method for determining axial swelling stress . . . . . . . . . . . . . . . 295
4. Part 3: suggested method for determining axial and radial free swelling strain. . . 299
5. Part 4: suggested method for determining axial swelling stress as a function of
axial swelling strain . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 302
6. Final comments . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 305

Co-ordinator
F.T. Madsen (Switzerland)

0148-9062/99/$ - see front matter # 1999 Elsevier Science Ltd. All rights reserved.
PII: S 0 1 4 8 - 9 0 6 2 ( 9 9 ) 0 0 0 0 5 - 4
F.T. Madsen / International Journal of Rock Mechanics and Mining Sciences 36 (1999) 291±306 293

Suggested methods for laboratory testing of swelling rocks

F.T. Madsen a
Accepted 2 January 1999

ISRM SUGGESTED METHODS (SMs): SECOND SERIES

A Second Series of Suggested Methods is being produced by the ISRM Commission on Testing Methods from 1998 onwards.
In this Second Series, for each SM two versions are published:

1. A Draft SM written by the Working Group Co-ordinator(s);


2. A Final SM also produced by the Working Group Co-ordinator but with amendments resulting from the Draft SM review by
the Working Group Members and other comments received after publication of the Draft SM.

A suite of the new Suggested Methods is currently being published in this Journal. These started with an Indentation
Hardness Index SM written by T. Szwedzicki and published in June 1998. Several more will be published in 1999.
However, the following SM results from a Working Group of 14 members, is already in the ®fth draft stage and thus can be
considered to be in its ®nal form.

Please send written comments on this SM to the


President of the ISRM Commission on Testing Methods:
Professor J A Hudson, 7 The Quadrangle,
Welwyn Garden City, Herts AL8 6SG, UK

1. Introduction This particular document treats laboratory testing of


argillaceous swelling rocks and swelling rocks contain-
The engineering problems caused by swelling rocks ing clay and anhydrite and consist of four parts:
are widely recognized, as is the need to test these rocks
to determine the type and extent of their swelling Part 1: sampling, storage and preparation of test
behavior and to measure this for purposes of design. specimens
The ISRM Commission on Swelling Rock was Part 2: determining the axial swelling stress
formed in 1980 to provide a systematic treatment of Part 3: determining the axial and radial free swelling
the swelling rock problem. It is emphasized that the strain
purpose of `suggested methods' is to specify rock test- Part 4: determining axial swelling stress as a func-
ing procedures and to achieve some degree of stan- tion of axial swelling strain
dardization without inhibiting the development of
improvement of techniques. This is particularly perti- These `suggested methods' are intended to replace
nent in the case of swelling rocks which, because of and update those published in [1]. It is important to
their variability, often require special non-standard note the di€erence in procedure of specimen testing for
treatment during both specimen preparation and test-
argillaceous and for clay±anhydrite rocks as the swel-
ing which di€ers from what is proposed here.
ling mechanism is of di€erent nature.
The tests described here are intended for practical
a
Geotechnical Engineering, Laboratory for Clay Mineralogy, Swiss use. For research on swelling behavior, other tests may
Federal Institute for Technology, CH-8093, Zurich, Switzerland. have to be used.
294 F.T. Madsen / International Journal of Rock Mechanics and Mining Sciences 36 (1999) 291±306

2. Part 1: suggested methods for sampling, storage and (d) Block sampling is another possibility. The
preparation of test specimens dimensions of the block sample are to be sucient for
preparation of at least three undisturbed specimens,
2.1. Scope and contain enough additional material for identi®-
cation tests.
1. These suggested methods describe techniques for (e) The cores or blocks are to be logged by a geol-
sampling, storing and preparing specimens for labora- ogist and photographed. In rocks containing clay and
tory swelling tests of argillaceous rocks and rocks con- sulphate minerals (anhydrite and gypsum), fabric and
taining clay and anhydrite1. the clay±sulphate minerals ratio is of special interest as
both are related to the swelling parameters. Prior to
2.2. Sampling logging, the cores or blocks are to be cleaned by
removing the mud cake. Their condition, such as
2. (a) To obtain meaningful results from swelling mechanical breakage, presence of mud cake on the sur-
tests, the samples2 are to have, as far as possible, the faces of the core or block, and presence of seams shall
same density and water content as those in situ at the be noted. Natural ®ssures, if any, are to be clearly
time of sampling. identi®ed.
(b) Rock samples are to be collected preferably from (f) The samples are then to be wrapped with a
core borings. Borings should be performed with air waterproof liner such as a thin plastic sheet, followed
pressure or, with an antiswelling admixture (such as by aluminum foil and sealed with a mixture consisting
Antisol) in the cooling (¯ushing) water, whichever is of 75% paran and 25% beeswax. The time between
best to keep the sample as close to its natural state as sampling and sealing should be as short as possible.
possible. (g) The sealed cores or blocks are to be labelled giv-
(c) Coring is to be accomplished using either a ing details of the sampling location, depth and el-
double tube or triple tube core barrel. The core diam- evation.
eter should be at least NX but preferably closer to 100 (h) To reduce breakage of cores or blocks during
mm. The sample length shall be sucient to prepare at transportation from the ®eld site to the testing labora-
least three undisturbed specimens, and contain enough tory, the samples are to be placed in containers, and
additional material for identi®cation tests. the space between cores and the container wall is to be
®lled with suitable material such as straw, shredded
foam or paper.
1
Depending on the depth below surface this type of rock may also (i) Samples are to be protected from frost and
contain gypsum. Normally, as these rocks originate in an evaporitic extreme heat at all times during sampling and trans-
environment other salts such as halite [NaCl] and dolomite portation. Sample temperature is to remain in the
[CaMg(CO3)2] are also present.
2
For the purpose of these suggested methods, the term `sample'
range 5±308C.
refers to the drill core, the block or other representative piece of
rock received in the laboratory, while the term `specimen' refers to 2.3. Storage of samples
the individual test specimen prepared from the sample.
3
Rocks containing clay and anhydrite (CaSO4) may also contain 3. (a) Storage time should be minimized.
gypsum (CaSO42H2O). At least this will be the case after the swel-
ling tests have been performed. For rocks containing gypsum the
(b) Storage in a constant temperature room (208C)
normally used method for determining the water content by drying is preferred.
the specimen at 1058C will produce erratic results. This is so because (c) The samples must not be exposed to direct sun-
not only pore water and water connected to clay particles is removed light.
from the specimen but also some of the crystal water of the gypsum. (d) If long-term storage is necessary, humidity in the
Using the following method for determining the water content in
two steps has several advantages. In the ®rst step pore water and
storage room should be such as to minimize any
water connected to the clay particles is removed by drying the moisture change of the samples.
crushed specimen over P2O5 in a desiccator for 3 days. The water
content determined in this way is equal to the normally used water 2.4. Specimen preparation
content in soil and rock mechanics. The water content is calculated
as: w%=((M2ÿMP)/MP)100, where: M2 is the mass of specimen
after testing, before drying over P2O5 and MP the mass of specimen
4. (a) The sampling logs and photographs are to be
after drying over P2O5. In the next step the specimen is heated in an examined to select cores or blocks that will yield
oven for 24 h at 2008C. During this procedure the gypsum releases required sizes, shapes and numbers of specimens.
all crystal water. The gypsum crystal-water content is calculated as: (b) Multiple specimens are to be prepared from the
w%gypsum=((MPÿMG)/MG)100, where: MP is the mass of speci- same sample. At least two are used for testing and one
men after drying over P2O5 and MG the mass of specimen after dry-
ing at 2008C. It is then possible to calculate the amount of gypsum
as a reference specimen for determination of water
(weight %) in the specimen as: gypsum %=(1 mol gypsum/2 mol content3, grain density, density and degree of satur-
water)w%gypsum, gypsum%=4.78w%gypsum. ation. The particular number of specimens for each of
F.T. Madsen / International Journal of Rock Mechanics and Mining Sciences 36 (1999) 291±306 295

the tests depends on the availability of material and on


the testing program Ð see Section 1. One undisturbed
specimen should be kept in storage for mineralogical
investigations.
(c) Specimens are to be prepared as rapidly as poss-
ible. If machining (cutting, recoring to a smaller diam-
eter) of the specimen is required this must be done
with air-cooling or with an antiswelling medium (such
as Antisol) in the cooling water, whichever is best to
keep the specimen as close to its natural condition as
possible. In general recoring is to be avoided. For
swelling rocks that can break easily, the special pro-
cedure described in Appendix A is to be used.
Remaining samples must be properly sealed again
according to 2(f).
(d) The specimens required for the tests described in
Parts 2, 3 and 4 (Sections 3±5) below are to be in the
shape of a right circular disc. Experience has shown
that for specimen diameters between 50 and 100 mm,
a thickness between 20 and 30 mm is most suitable.
The test described in Part 3 Section 4 can also be per-
formed with other specimen shapes, such as entirely
irregular pieces which have undergone no preparation
Fig. 1. Apparatus for measuring the axial swelling stress: (1) stain-
at all. The apparatus and procedure have then to be less-steel ring, (2) porous metal plates, (3) stainless-steel loading
adapted to such specimen shapes. plate, (4) container, (5) dial gages (attached to the bottom of con-
tainer (4), attachment not shown), (6) load measuring device, (7)
rigid frame and (8) loading piston, (9) stainless steel plate.
3. Part 2: suggested method for determining axial
swelling stress 3.2. Apparatus

3.1. Scope The apparatus6 is to include the following as sche-


matically shown in Fig. 1.
1. The test is intended to measure the time depen- 2. (a) A stainless steel ring ((1) in Fig. 1), for rigid
dent axial swelling stress of a radially con®ned rock radial restraint of the specimen. The inner surface of
specimen when immersed in water4. If possible the the ring is to be polished and smooth. The wall thick-
maximum swelling stress is to be determined5. ness of the ring depends on its other dimensions and
has to be calculated based on those dimensions and
the maximum lateral stress to be expected. Not more
than 10ÿ4 radial strain is allowed. Thicknesses between
4
For argillaceous rocks, distilled water is normally used. Water 5 and 10 mm are usually satisfactory. Several rings
from the sampling site, or water with a special chemical composition should be available to ®t all desired specimen dimen-
may also be used. For rocks containing clay and anhydrite using dis- sions.
tilled water may cause uncontrolled dissolution of sulphates in the (b) Two porous plates ((2) in Fig. 1). The porous
specimen. Normally a calcium-sulphate solution of 2.4 g CaSO4 per l
distilled water is used to minimize dissolution of the sulphate from
plates should be made of high modulus material.
within the specimen into the container water. Porous stainless steel plates are most suitable.
5
In the swelling process of clay±anhydrite rocks two di€erent swel- Alternatively, stainless steel plates into which a num-
ling mechanisms are involved: the swelling of clay due to hydration ber of small holes (dia 0.1 mm) have been drilled are
of clay particles (an osmotic process) and the swelling due to trans- also suitable. In the latter case, small channels con-
formation of anhydrite into gypsum (chemical process which involves
dissolution and precipitation). Normally clay swelling takes place in
necting the small holes to the water supply are
the ®rst days after immersion in water or calcium-sulphate solution, required.
whereas anhydrite±gypsum swelling goes on for years. (c) One porous plate is to be on top of the specimen
6
Since nearly every institution working on swelling rocks has and the other at its bottom. The lower plate is to have
developed its own apparatus for measuring the swelling stress, the a diameter of approx. 5 mm greater than the outer di-
apparatus described here is only an example. The advantage of this
apparatus is the possibility to use steel rings of various diameters,
ameter of the specimen ring, and the upper plate has
depending on the diameter of the specimen. This reduces time and to be of a size just ®tting the inside of the ring without
e€ort for preparation and lessens the risk of disturbing the specimen. restraining its movement.
296 F.T. Madsen / International Journal of Rock Mechanics and Mining Sciences 36 (1999) 291±306

(d) A stainless-steel loading plate ((3) in Fig. 1) of where the ambient temperature can be maintained con-
the same bottom diameter as the upper porous plate, stant at 20228C.
but slightly conically shaped, and placed on top of the (b) The thickness h0 of the specimen which was pre-
porous plate. The loading plate has to be thick enough pared as described in Part 1 (Section 2, Specimen prep-
to ensure rigid strain application; for specimen diam- aration) is to be measured in at least three locations
eters of between 50 and 100 mm a 10-mm thick plate between specimen ends, to an accuracy of 20.1 mm.
is adequate. (c) The specimen diameter d is to be measured at
(e) A rigid frame ((7) in Fig. 1) with a loading device least at three locations along the circumference.
capable of continuous adjustment. Measuring accuracy is again to be better than 20.1
(f) A loading piston or rod ((8) in Fig. 1) with a mm.
hemispherical end or a separate sphere to rest on the (d) The mass of the specimen M1 is to be determined
loading plate. to 0.1 g.
(g) Two mm dial gauges ((5) in Fig. 1) with a sensi- (e) The specimen ring is to be cleaned and its mass
tivity of 2.5 mm to measure the axial swelling or com- M0 determined.
pressive displacement of the specimen. The dial gauges (f) The specimen is inserted into the ring. The speci-
are attached to the bottom of the container (4). men must ®t snugly into the ring.
(h) A sti€ load measuring device7 ((6) in Fig. 1), for (g) The apparatus is assembled. The ring with the
instance an electromechanical load cell capable of specimen is placed on the lower porous plate, followed
measuring to an accuracy of 20.5% of the maximum by the upper porous plate and the steel loading plate.
rating of the load measuring device. The plate is placed with the smaller diameter facing
(i) A container ((4) in Fig. 1) (dia 15 cm) for the upwards. The piston is brought into contact with the
specimen assembly, and ®lled with water to a level top plate and centered.
above the top of the specimen. (h) A seating load corresponding to an axial stress
of 25 kPa is to be applied. The initial readings of the
3.3. Procedure micrometer dial gages are noted.
(i) The container is ®lled with water to cover the top
3. (a) The test is to be conducted in an environment porous plate.
(j) The container is covered with a plastic disc to
minimize evaporation of the container water.
7
Normally, load cells of a capacity of 20 kN and de¯ecting less (k) The axial force N and the axial displacement d
than 10ÿ8 are suitable. For very high swelling stresses, load cells of are measured and recorded as a function of elapsed
50 kN may be required. The accuracy of 0.5% is related to the maxi- time t8.
mum rating of the load cell. (l) Depending on the mineralogical composition of
8
In argillaceous rocks rapid changes in strain take place during
the ®rst hours. Also, most of the changes usually occur within the
the specimen small amounts of strain are to be com-
®rst few days, and the total test duration strongly depends on the pensated in a stepwise manner by increasing the axial
dimensions of the specimen. On the contrary, the transformation of force9. The steps should be kept as small as possible.
anhydrite into gypsum is a rather slow process and the determination (m) The test should be continued until the maximum
of the maximum swelling stress may take several years. These facts axial force developed by the specimen can be deter-
should be considered when scheduling the test.
9
The swelling heave (axial strain) due to clay swelling is reversible
mined or estimated.
and for specimens containing only clay minerals (no anhydrite and (n) The ring with the specimen is then to be
gypsum) the original thickness of the specimen may be kept constant removed from the container (after removing of the
by increasing the axial stress. The steps should be kept as small as container-water and unloading), the excess water
possible, particularly toward the end of the test (see Fig. 2b); this is wiped o€ and the mass M2 determined. For strongly
necessary to obtain an accurate measurement of the maximum axial
force and thus maximum axial swelling stress. An axial strain of
swelling rock, the water is drained o€ before unload-
0.05% in the last increment is usually adequate. The transformation ing. At this stage the specimen condition is logged.
of anhydrite into gypsum cannot be reversed by increasing the axial (o) If the tested rock is purely argillaceous (no gyp-
stress (at least not for the range of stresses which normally occurs in sum), the specimen with the ring is heated in an oven
tunnelling problems). For rocks containing anhydrite the axial strain to constant mass at a temperature of 105228C. The
of the specimen caused by transformation of anhydrite into gypsum
is not to be compensated as a compensation will lead to an unreason-
specimen with the ring is allowed to cool in a dessica-
able high swelling stress. In some cases it may however be sensible to tor. The oven-dry mass M3 is determined.
compensate the strain occurring during the ®rst days of the test as Alternatively the specimen can be oven heated without
this is usually caused by the clay-swelling process. After this time the ring10.
however, no compensation is to be made. (p) If the tested rock contains clay and anhydrite/
10
In all tests, an alternative approach is to remove a part of the
specimen before drying to determine its mineralogical composition.
gypsum, a part of the specimen is used for the determi-
The mass M2 and M3 determination applies then to the remainder of nation of the water content after testing as earlier
the specimen. described.
F.T. Madsen / International Journal of Rock Mechanics and Mining Sciences 36 (1999) 291±306 297

Fig. 2. (a) Plot of axial stress vs. time of argillaceous rock. s =maximum axial stress. (b) Plot of axial stress vs. compensated axial swelling
strain of argillaceous rock. s =maximum axial stress.
298 F.T. Madsen / International Journal of Rock Mechanics and Mining Sciences 36 (1999) 291±306

Fig. 3. (a) Plot of axial stress vs. time of clay±sulphate (anhydrite) rock. (b) Plot of axial swelling strain due to noncompensation of the specimen
height vs. time of clay±sulphate (anhydrite) rock.
F.T. Madsen / International Journal of Rock Mechanics and Mining Sciences 36 (1999) 291±306 299

3.4. Calculations

4. (a) The following test parameters are calculated:


the area of cross section of the specimen A; the axial
stress s; the compensated swelling strains eclay and the
noncompensated swelling strains egypsum.
(b) The area of cross-section A of the specimen is
calculated as

pd2
Aˆ ,
4
where d is the specimen diameter.
(c) The axial stress s is calculated as

N
sˆ ,
A
where N is the measured axial force.
(d) The compensated clay swelling strain increment
Declay is calculated as

Ddclay
Declay ˆ ,
h0
Fig. 4. Apparatus for measuring the swelling strain: (1) container, (2)
where Ddclay is the displacement increment caused by dial gauge, (3) glass plate, (4) stainless-steel band and (5) specimen.
clay swelling and h0 the original thickness of the speci-
men. men anisotropy speci®cally with respect to bedding
(e) The noncompensated anhydrite into gypsum planes and relative to in situ directions.
swelling strain increment Degypsum is calculated as (g) Dimensions of the test specimen.
(h) Density, water content, grain density and degree
Ddgypsum of saturation of the test specimen before the swelling
Degypsum ˆ ,
h0 test11.
(i) Final density, water content and degree of satur-
where Ddgypsum is the displacement increment caused ation of the test specimen after the swelling test.
by the transformation of anhydrite into gypsum and h0 (j) Test temperature.
the original thickness of the specimen. (k) Applied seating-load.
(f) Density, initial and ®nal water contents and (l) Speci®cation of water used for immersion.
degree of saturation are calculated according to [2]. (m) A plot of axial stress vs. elapsed time, such as
Fig. 2a and Fig. 3a.
3.5. Reporting of results (n) A plot of axial swelling strain vs. elapsed time,
such as Fig. 3b.
5. The test report is to include the following for Additional for argillaceous rock:
each specimen. (o) A plot of axial stress vs. compensated swelling
(a) A unique identi®cation of the sample and of strain such as Fig. 2b.
each individual specimen. (p) Total compensated swelling strain (optional).
(b) Information on geographic origin, lithology, fab-
ric and, if possible, mineralogy and pore water chem-
istry of the sample and specimen.
(c) Date and method of sampling; date(s) of testing.
4. Part 3: suggested method for determining axial and
(d) Method of sealing and storage.
radial free swelling strain
(e) Method of specimen preparation for testing.
(f) Orientation of the specimen axis relative to speci-
4.1. Scope

11
Density and water content of the test specimen are determined in 1. The test is intended to measure the axial and
the specimen next to the test specimen (having similar mineralogical radial free swelling strain developed when an uncon-
composition) in the drilling core or block. ®ned, undisturbed rock specimen is immersed in water.
300 F.T. Madsen / International Journal of Rock Mechanics and Mining Sciences 36 (1999) 291±306

4.2. Apparatus (h) The axial swelling displacement dax is recorded


as a function of time elapsed14.
2. The apparatus12 is to include the following as (i) The swelling displacement is recorded until a
schematically shown in Fig. 4: maximum (or constant) value has been reached or can
(a) A container (dia 15 cm) for the specimen ((1) in be estimates15.
Fig. 4). (j) After swelling strain is determined, and before
(b) A mm dial gauge (or equivalent) with a sensitivity the specimen is removed from the container, the
of 2.5 mm, mounted to measure the swelling displace- increase in circumference DC is measured with the
ment in the central axis of the specimen ((2) in Fig. 4). stainless-steel band.
(c) A glass plate, positioned at the point of gauging (k) The specimen is then to be removed from the
to prevent indentation of the specimen ((3) in Fig. 4). container, the excess water wiped o€, the stainless-steel
(d) A thin (0.1 mm) ¯exible, stainless steel band ((4) band removed from the specimen, and the mass M2
in Fig. 4) attached to the specimen by an elastic rubber determined. At this stage the specimen condition is
band. The steel band is calibrated at 0.1-mm intervals logged.
and is used to determine the radial swelling13 defor- (l) If the tested rock is purely argillaceous, the speci-
mation. men is heated in an oven to constant mass at a tem-
perature of 105228C. The specimen is then allowed to
cool in a dessicator. The oven-dry mass M3 is deter-
mined.
4.3. Procedure (m) If the tested rock contains clay and anhydrite/
gypsum a part of the specimen is used for the determi-
3. (a) The test is to be conducted in an environment nation of the water content after testing as described
where the ambient temperature can be maintained con- earlier.
stant at 20228C.
(b) The thickness h0 of the specimen which was pre- 4.4. Calculations
pared as described in Part 1 Section 2 is to be
measured in at least three locations between specimen 4. (a) The axial swelling strain eax and the radial
ends, to an accuracy of 20.1 mm. swelling strain erad are determined.
(c) The specimen diameter d0 is to be measured at (b) The axial swelling strain is calculated as
least at three locations along the circumference, to an
accuracy of 20.1 mm. dax
eax ˆ ,
(d) The mass of the specimen M1 is to be determined h0
to 0.1 g.
(e) The stainless-steel band is attached and the speci- where dax is the axial displacement and h0 the initial
men with the dial gauge (or equivalent) is mounted in thickness of the specimen.
the container. (c) The radial swelling strain is calculated as
(f) The container is to be ®lled with water to cover
the specimen. drad
erad ˆ ,
(g) The container is covered with a plastic disc to d0
minimize evaporation of the container water.
where d0 is the initial specimen diameter and

12 DC
This apparatus represents a possible example. If the swelling drad ˆ ,
strain has to be measured in three directions the specimens should p
preferably be cube shaped. It should be possible to mount the dial
gauges (or equivalent) in three directions. where DC is the increase in specimen circumference as
13
A number of possibilities exist to conduct both continuous and measured with the stainless-steel band (see 3f).
more precise measurements of radial strain. Given the purpose of the (d) Density, initial and ®nal water contents and
swell test, which is to provide as quick information as possible on degree of saturation are calculated according to [2].
the swelling strain, such sophistication may not be justi®ed.
14
Some swelling rocks may start to disintegrate after a short period
of immersion in water by developing open ®ssures along their bed- 4.5. Reporting of results
ding planes. In such cases, applying a small axial surcharge may be
advisable. 5. The test report is to include the following for
15
The time for reaching the ®nal (maximum) strain depends on the each specimen.
mineralogical composition of the tested specimen. For argillaceous
rock this usually takes a few days. For rocks containing anhydrite it (a) A unique identi®cation of the sample and of
may take several years to reach the ®nal strain, as the transformation each individual specimen.
of anhydrite into gypsum is a rather slow process. (b) Information on geographic origin, lithology, fab-
F.T. Madsen / International Journal of Rock Mechanics and Mining Sciences 36 (1999) 291±306 301

Fig. 5. (a) Axial swelling strain vs. time (example for an argillaceous specimen). e =maximum axial strain. (b) Axial swelling strain vs. time
(example for a clay±sulphate (anhydrite) specimen). e =maximum axial strain.
302 F.T. Madsen / International Journal of Rock Mechanics and Mining Sciences 36 (1999) 291±306

ric and, if possible, mineralogy and pore water chem-


istry of the sample and specimen.
(c) Date and method of sampling; date(s) of testing.
(d) Method of sealing and storage.
(e) Method of specimen preparation for testing.
(f) Orientation of the specimen axis relative to speci-
men anisotropy speci®cally with respect to bedding
planes and relative to in situ directions.
(g) Dimensions of the test specimen.
(h) Density water content, grain density and degree
of saturation of the test specimen before the swelling
test.
(i) Final density, water content and degree of satur-
ation of the test specimen after the swelling test.
(j) Test temperature.
(k) Applied load (if any).
(l) Speci®cation of water used for immersion.
(m) A plot of axial strain vs. elapsed time, such as
Fig. 5a or b.
(n) Maximum axial swelling strain.
(o) Maximum radial swelling strain.
(p) Volumetric strain, either computed from axial
and radial swelling strain for regularly shaped speci-
mens, or determined by the liquid displacement
method.

5. Part 4: suggested method for determining axial


swelling stress as a function of axial swelling strain Fig. 6. Apparatus for measuring the axial swelling stress as a func-
tion of axial swelling strain: (1) stainless-steel ring, (2) porous metal
plates, (3) stainless-steel loading plate, (4) container, (5) dial gauge
5.1. Scope (attached to the bottom of container (4)), attachment not shown and
(6) loading frame.
1. The test is intended to measure the axial swelling
strain necessary to reduce the axial swelling stress of a be calculated based on these dimensions and the maxi-
radially constrained rock specimen immersed in water mum lateral stress to be expected. Not more than 10ÿ4
from its maximum value to a value which is acceptable radial strain is allowed. Thicknesses of between 5 and
in the particular application. It is intended for appli- 10 mm are usually satisfactory. Several rings should be
cation to cases where analogous boundary conditions
available to ®t all desired specimen dimensions.
prevail. The test is practicable only on purely argillac-
(b) Two porous plates ((2) in Fig. 6). The porous
eous specimens.
plates should be made of a high modulus material.
Porous stainless-steel plates are most suitable.
5.2. Apparatus
Alternatively, stainless-steel plates into which a num-
2. The apparatus16 is to include the following as ber of small holes (dia 0.1 mm) have been drilled are
schematically shown in Fig. 6. also suitable. In the latter case, small channels con-
(a) A stainless-steel ring for rigid radial restraint of necting the small holes to the water supply are
the specimen ((1) in Fig. 6). The inner surface of the required.
ring is to be polished and smooth. The wall thickness (c) One porous plate is to be on top of the specimen
of the ring depends on its other dimensions and has to and the other at its bottom. The lower plate is to have
a diameter approx. 5 mm greater than the outer diam-
eter of the specimen ring, and the upper plate has to
16
The apparatus described here is essentially a modi®ed oedometer, be of a size just ®tting the inside of the ring without
as used in soil mechanics. The di€erence and advantage of this par- restraining its movement.
ticular apparatus is the possibility to use steel rings of various diam-
eters, depending on the diameter of the specimen. This reduces time
(d) A stainless-steel loading plate of the same bot-
and e€ort for specimen preparation and lessens the risk of disturbing tom diameter as the upper porous plate but slightly
the specimen. conically shaped, and placed on top of the porous
F.T. Madsen / International Journal of Rock Mechanics and Mining Sciences 36 (1999) 291±306 303

Fig. 7. Axial stress vs. total axial strain: (1) compression curve (without water supply), (2) water applied at the stress sA (in this example=2
MPa), (3) swelling at the stress sA, (4) unloading to sB (in this example=1.5 MPa), (5) swelling at the stress sB, (6) matrix deformation strain
Des and (7) swelling strain Des.

plate. The loading plate has to be thick enough to pared as described in Part 1 (Section 2, Specimen prep-
ensure rigid strain application ((3) in Fig. 6). For spe- aration) is to be measured in at least three locations
cimen diameters of between 50 and 100 mm a 10-mm between specimen ends, to an accuracy of 20.1 mm.
thick plate is adequate. An indentation in the center of (c) The specimen diameter d is to be measured in at
the plate for placing the load transfer sphere (see (e) least three locations along the circumference.
below) is required. Measuring accuracy is again to be better than 20.1
(e) A loading frame ((6) in Fig. 6), with suitable fea- mm.
tures to apply incremental loads up to a total load of (d) The mass of the specimen M1 is then to be deter-
10 kN. Direct loading or indirect loading via a lever mined to 0.1 g.
using lead plates are possibilities. The loading frame (e) The specimen ring is to be cleaned and its mass
transmits the load to the top steel plate via a 2-cm di- M0 determined.
ameter polished steel sphere. (f) The specimen is inserted into the ring. The speci-
(f) A mm dial gauge (or equivalent) with a sensitivity men must ®t snugly into the ring.
at 2.5 m attached to the bottom of container (4) an (g) The apparatus is assembled. The ring with the
mounted in such a way as to measure compression specimen is placed on the lower porous plate, followed
and swelling along the central axis of the specimen ((5) by the upper porous plate, the loading plate and the
in Fig. 6).
sphere. The load frame is then placed on the sphere.
(g) A container ((4) in Fig. 6) (dia 15 cm) for the
(h) The specimen is loaded in a stepwise manner up
specimen assembly, which is ®lled with water to a level
to a load corresponding to a desired axial stress s. A
above the top of the specimen.
stress level comparable to the overburden stress at the
sample location is reasonable. This load and the corre-
5.3. Procedure sponding ®nal compression of the specimen are
recorded (Fig. 7, curve l).
3. (a) The test is to be conducted in an environment (i) The container is the ®lled with water to cover the
where the ambient temperature can be maintained con- top porous plate.
stant at 20228C. (j) Initial swell heave is recorded (curve segment 3 in
(b) The thickness h0 of the specimen, which was pre- Fig. 7).
304 F.T. Madsen / International Journal of Rock Mechanics and Mining Sciences 36 (1999) 291±306

Fig. 8. Axial stress vs. swelling strain.

(k) The axial load is reduced in consistent decre- cool in a desiccator. The oven-dry mass, M3 is deter-
ments17. It is usual to reduce the load by 50% in each mined and recorded. Alternatively the specimen can be
step. However, other decrements can also be chosen. oven heated, without the ring.
(l) The swell heave for each load decrement is
measured until no displacement can be observed for 5.4. Calculations
the particular load decrement. The load decrement and
the displacement are recorded. 4. (a) The following test parameters are calculated:
(m) Steps (k) and (l) are repeated down to a load the area of cross section of the specimen, A, the axial
corresponding to 25 kPa18. Complete unloading is not stress s, the axial matrix deformation strain Des and
recommended because upward bulging may occur pro- axial swelling strain Des.
ducing displacements which are not representative of (b) The area of cross-section A of the specimen is
swelling. calculated as
(n) The ring with the specimen is then to be
removed from the container (after removing of the pd2
Aˆ ,
container water and unloading), the excess water 4
wiped o€ and the mass M2 determined and recorded.
where d is the specimen diameter.
For strongly swelling rock the container water is
(c) The axial stress s is calculated as
drained o€ before unloading. At this stage the speci-
men condition is logged. N
(o) The specimen with the ring is heated in an oven sˆ ,
A
to constant mass at a temperature of 105228C.
(p) The specimen and the ring and is allowed to where N is the measured axial force.
(d) The matrix deformation strain Des, which is re-
17
lated to the axial stress decrement, is calculated as:
This procedure is expected to produce lower bound swelling stres-
ses for a particular swelling strain. The method is appropriate for ds
determining heave resulting from unloading. Des ˆ ,
18
For applications in which the stress on the swelling rock is lower h0
than 25 kPa, such as foundations of light buildings or excavated
slopes, lower ®nal loads have to be selected. where ds is the instantaneous axial displacement due
F.T. Madsen / International Journal of Rock Mechanics and Mining Sciences 36 (1999) 291±306 305

to matrix deformation per decrement Ds and h0 the (h) Density, water content, grain density and degree
original thickness of the specimen. of saturation of the test specimen before the swelling
The swelling strain Des at each stress level is calcu- test.
lated as (i) Final density, water content and degree of satur-
ation of the test specimen after the swelling test.
ds (j) Test temperature.
Des ˆ ,
h0 (k) Speci®cations of water used for immersion.
where ds is the axial displacement due to swelling per (l) A plot of axial stress vs. total axial strain similar
decrement Ds and h0 the original height of the speci- to Fig. 7. The plot has to distinguish between Des ((6)
men. in Fig. 7), which is the instantaneous strain directly re-
(e) Density, initial and ®nal water contents and lated to the axial stress decrement through matrix de-
degree of saturation are calculated according to Ref. formation, and Des ((7) in Fig. 7), which is the swelling
[2]. strain caused by adsorption of water. The total strain
at a certain stress is thus
5.5. Reporting of results Detot ˆ Des ‡ Des :

5. The test report is to include the following for (m) A plot of swelling strain vs. axial stress such as
each specimen. Fig. 8. This graph is obtained by plotting the swelling
(a) A unique identi®cation of the sample and of strain, Des for the corresponding stress decrements.
each individual specimen. The resulting curve can be used to estimate the poten-
(b) Information on geographic origin, lithology, fab- tial swelling strains which need to be considered in de-
ric and, if possible, mineralogy and pore water chem- sign.
istry of the sample and specimen.
(c) Date and method of sampling; date(s) of testing.
(d) Method of sealing and storage. 6. Final comments
(e) Method of specimen preparation for testing.
(f) Orientation of the specimen axis with respect to . The methods are relatively simple and have been
specimen anisotropy, speci®cally with respect to bed- extensively used in practice.
ding planes and relative to in situ directions. . Future development of laboratory testing will be
(g) Dimensions of the test specimen. necessary, particularly regarding 3-D testing.
. The maximum possible swelling stress developing
from the transformation of anhydrite into gypsum is
not known at the present time. Swelling stresses up
to 8 MPa have been reported from laboratory tests.

Acknowledgements

The Commission members responsible for preparing


these suggested methods were: C. Amstad,
Switzerland, G. Anagnostou, Switzerland N. Bischo€,
Switzerland; H.H. Einstein, USA; E. Fecker,
Germany; L. Hauber, Switzerland; J.R. Kiehl,
Germany; D. Kirschke, Germany; F.T. Madsen,
Switzerland; G. Mesri, USA; R. NuÈesch, Switzerland;
H. Santos, Brazil; W. Steiner, Switzerland; B. VoÈgtli,
Switzerland.

Appendix A. Specimen preparation for rocks that can


easily break

(a) The intact specimen is trimmed into a sharp-


edged, approx. 65 mm diameter and 20 mm tall
Fig. 9. (1), (5)=bearings, (2)=upper adapter, (3)=trimming ring; highly-polished stainless-steel con®ning ring. The
(4)=lower adapter and (6)=specimen. sample is hand-carved in a humidity-controlled room
306 F.T. Madsen / International Journal of Rock Mechanics and Mining Sciences 36 (1999) 291±306

using sharp and pointed (for instance, Bard-Parker (e) The face of the specimen at the sharp end of the
No. 10) stainless-steel surgical blades. ring is to be cut ¯at using a sharp, straight edge.
(b) A slice approx. 30 mm thick is to be cut ¯at (f) For testing the specimen, height must be less
from an undisturbed cylindrical (or block shaped) than the ring height. A spacer approx. 5 mm thick is
sample. If necessary, the slice-ends are to be re®nished to be placed against the ¯at surface, and using the
¯at and nearly parallel to each other using a sharp, manual press the trimmed specimen is pushed out in
straight edge. the direction opposite to the one it has been pushed in.
(c) The slice is to be placed and centered on the (g) The specimen is then to be cut ¯at at this oppo-
lower adapter of a manual press (Fig. 9). The manual site end using a sharp straight edge as it extrudes out
press is modi®ed from a U-116 Field Classi®cation of the ring, such that the desired specimen thickness is
Tester (Soiltest, Inc), using two adapters and bearings reached.
so that the swelling rock slice can be rotated freely
during the trimming process.
(d) After removing any rock from outside the ring, References
the trimming ring is to be pressed down in small incre-
ments (generally less than 2 mm) using the manual [1] Suggested methods for laboratory testing of argillaceous swelling
press. Prior to each increment the part of the specimen rocks. ISRM Commission on Swelling Rocks, 1989.
[2] ISRM Commission on Standardisation of Laboratory and Field
just below the trimming ring is to be handcarved as Tests. Suggested methods for determining water content, poros-
close as possible to the ®nal dimension but without ity, density, absorption and related properties and the swelling
undercutting, so that only a thin annular layer is and slake durability index. In: Brown ET, editor. Rock charac-
removed by the advancing ring. This is to be continued terisation, testing and monitoring. Oxford: Pergamon Press, 1981
until the specimen completely occupies the 20 mm high document No. 2, First Revision.

ring.

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