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Evaluationof ASTMD6200
Evaluationof ASTMD6200
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An evaluation of ASTM D6200
Article · November 2017
DOI: 10.1520/MPC20170006
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An Evaluation of ASTM D 6200
Criteria for Cooling Curves
Experimental
Discussion
Conclusions
Introduction
• Cooling curves increasing used
New applications
Existing operations – Replacement Oil
Existing Oil – Quality Assurance
AMS 2759/1 – Quarterly
NADCAP – Quarterly
CQI-9 – Bi-Annually
• ASTM D6200 (ISO 9950) is basic method used
ASTM D6200
• Inconel 600 Probe
13 mm diameter
160 mm long
T/C inserted at center
850°C
• Quenchant
1-2 liters (2 liters
recommended)
Temperature variable (60°C
typical)
No agitation
• Transfer
Automated
Manual
ASTM D6200
ASTM D6200
ASTM D6200 Bias and Precision
Production Laboratory
User Data
data set integrity check
100
80
Population
60
40
20
0
60 65 70 75 80 85 90 95 100 105 110 115 120
Maxium Cooling Rate, °C/s
45
40
35
30
Population
25
20
15
10
0
552 560 568 576 584 592 600 608 616 624 632 640 648
Temperature at Maxium Cooling Rate, °C
70
60
50
Population
40
30
20
10
0
667 675 683 691 699 707 715 723 731 739 747 755 763
Temperature at the Start of Boiling, °C
35
30
25
Population
20
15
10
0
320 325 330 335 340 345 350 355 360 365 370 375 380
Temperature at the Start of Convection, °C
40
35
30
Population
25
20
15
10
0
4.7 5.0 5.3 5.6 5.9 6.2 6.5 6.8 7.1 7.4 7.7 8.0 8.3
Cooling Rate at 300°C, °C/s
60
50
Population
40
30
20
10
0
5.6 6.0 6.4 6.8 7.2 7.6 8.0 8.4 8.8 9.2 9.6 10.0 10.4
Time to 600°C, seconds
70
60
50
Population
40
30
20
10
0
8.5 9.0 9.5 10.0 10.5 11.0 11.5 12.0 12.5 13.0 13.5 14.0 14.5
Time to 400°C, seconds
50
40
Population
30
20
10
0
32.5 35.0 37.5 40.0 42.5 45.0 47.5 50.0 52.5 55.0 57.5 60.0 62.5
Time to 200°C, seconds
ASTM D6200
Average 97.3 619.2 6.1 6.6 10.9 45.0
Variation (2σ) 8.6 25.3 1.5 1.4 2.1 10.1
Minimum 88.7 593.89 N/A N/A 4.59 5.21 8.79 34.93
Maximum 105.9 644.49 N/A N/A 7.65 8.01 12.99 55.13
Summary Data
800
700
600
500
Temperature, °C
400
300
200
100
0
Maximum Cooling Rate Temp. at Max. Cooling Rate Temp at Start of Boiling Temp at Start of Convection
Laboratory Data Production Data User Data ASTM D6200
Summary Data
60
50
40
Time, Seconds
30
20
10
0
Cooling Rate at 300°C Time to 600°C Time to 400°C Time to 200°C
Laboratory Data Production Data User Data ASTM D6200
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Conclusions
• ASTM Specification
evaluated
Found to be adequate for
new oils
Not adequate for used oils
• Specification is too tight
to make good/bad
decisions on used single
oil
• Will result in excessive
audit bait