Draft Biodiesel Manual - 19 04 2019

INDUSTRY MANUAL ON OPERATIONS, QUALITY & SAFETY FOR
BIODIESEL (B100) & HSD-BIODIESEL BLENDS(B5 & B6-B20)

2019
An Industry group under the convenorship of GM-QC, HPC Mktg. worked collectively to bring
out subject Industry Manual. As a part of this exercise, various meetings with the Industry
members were held.
The group has deliberated in great detail and has drawn up this manual containing in the
following pages, to be implemented by all Oil Industry.
Group Members
Sr. Name Designation
No.
1.
2.
3.
4.
5.
6.
7.
8.
9.
10.
11.
Page 2 of 41
INDUSTRY MANUAL ON OPERATIONS, QUALITY & SAFETY FOR
2019
AMENDMENT RECORD
AMENDMENTS SECTION/ EMBODIED DATE
NUMBER DATE PAGE BY
Page 3 of 41
Foreword
BIODIESEL (B100) is a fuel manufactured from vegetable oils , recycled cooking oil as well
as animal fats. .The fuel typically contains different types of fatty acids that are chemically
transformed into Fatty Acid Alkyl Esters.
Different fractions of each type of Fatty Acid Alkyl Esters/FAME present in various
feedstocks influence some of the properties of the fuel.
High levels of saturates (C14:0, C16:0, C18:0) from pure BIODIESEL (B100) improve Cetane
number, reduce NOx, and improve stability. This also raises the cloud point. However more
poly-unsaturates (C18:2, C18:3) in B100 will reduce cloud point & Cetane number, reduce
stability (unless stability additives are used), and raise NOx. Resultant B100 substantially
reduces unburnt Hydro Carbon, CO and particulate matter. It has almost no sulphur, no
aromatics and about 10% built in oxygen; helps in ensuring complete combustion.
The B100 conforms to the requirements stipulated in BIS specification IS 15607: 2016 and is
given as Annexure I.
B100 is environment friendly fuel and therefore it is blended in HSD manufactured as per
IS: 1460, up to a maximum of 5% v/v to formulate B5 . Specification for 6%(B6) to 20%(B20)
Biodiesel v/v blended with HSD is published in IS 16531:2016 and is given as Annexure II.
While practising the laid down procedures, various laws / statutory requirements pertaining
to handling, storage, dispensing, purchase, sale, safety etc. need to be adhered to. All
practices in handling Biodiesel and its blends as per the petroleum rules/act, shall be
followed.
The Manual provides guidelines based on proven Industry practices developed over a period
of time in this field.
Section 1……………………………………………………………………………………………..1
Introduction
Section 2 ............................................................................................................................ 2
Terminology
Section 3 ............................................................................................................................ 3
Salient Features of B100
Section 4 ............................................................................................................................ 4
Quality of B100
Section 5 ............................................................................................................................ 6
Receipt of B100
Section 6……………………………………………………………………………………………..8
Storage and Handling of B100
Section 7 ........................................................................................................................ .10

Colour Coding for B100
Section 8 ……………………………………………………………………………….................11
Quality Monitoring for B100
Section 9 .......................................................................................................................... 12
Blending of B100 in HSD and Quality Control Checks
Section 10 ........................................................................................................................ 15
Tank Trucks for Transportation of HSD-Biodiesel Blends
Section 11 ........................................................................................................................ 16
Handling of HSD --Biodiesel Blends at Retail Outlets
Section 12 ........................................................................................................................ 18
Safety
Section 13 ........................................................................................................................ 20
Additional Precautions
Annexure-I: ………………………………………………………………………………..……..21
Specification of Biodiesel B100- IS 15607:2016
Annexure-II:…....................................................................................................................30
Specification of HSD -Biodiesel Blend B6-B20( IS 16531:2016)
Annexure-III: ………………………………………………………………………………..…..…22
Type Approval format
Annexure-IV: ………………………………………………………………………………..…..…22
QC Checks on Tank truck Receipt - Format for Locations
Annexure-V: ………………….……………………………………………………………..…….23
Pre-receipt test report format for Laboratory
Annexure-VI:….....................................................................................................................27
Tank truck Inspection/Cleaning Certificate for use of B100
Annexure-VII:.......…...……………………………………………………………………………..24
BIODIESEL MSDS
INDUSTRY MANUAL ON OPERATIONS, QUALITY & SAFETY
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Section No.1 Section Name: Introduction Clause 1.1 to 1.3.
1. Introduction:
1.1 BIODIESEL (B100) is a renewable fuel manufactured from vegetable oils , recycled
cooking oil as well as animal fats. It is environment friendly fuel and is being used for
blending with HSD which brings down the consumption of conventional HSD.
Automotive diesel fuel specification ( IS: 1460) permits FAME Content , 7 % max, v/v
both for Bharat Stage IV & VI grade fuels. Earlier biodiesel blending in HSD was
permitted upto 5 % v/v. Subsequently, the specification for blending of Biodiesel in
the range of 6 % to 20 % v/v have been formulated .
B100 is heavier than HSD. Suitable methodologies such as online blending, splash
blending , in tank blending may be used . It shall be ensured that the blended product
is homogeneous.
1.2 The basic practices of handling B5 as well as B6 to B20 remains the same . The
procedures outlined in this manual are only the minimum requirements in order to
ensure quality of B100 and its blends.
1.3 This manual supersedes earlier communications regarding handling of Biodiesel.

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Section No.2 Section Name: Terminology Clause 2.1 to 2.5
2. Terminology
2.1 BIODIESEL (B100):
A fuel comprised of mono-alkyl esters of long chain fatty acids derived from vegetable
oils, Used Cooking Oil or animal fats, designated hereinafter as B100 conforming to
BIS specification IS 15607:2016 as given in Annexure I.
2.2 High Speed Diesel Oil (HSD)
Hydrocarbon Oils derived from light or middle petroleum distillate fuels, which may
contain fuel additives in an appropriate concentration in order to improve the
performance and quality of the fuel without known harmful side effects, conforming to
IS: 1460 specifications.
2.3 BIODIESEL blended HSD:
A blend of BIODIESEL (B100) with High-Speed Diesel at recommended dosage.
2.4 BIODIESEL BLENDS :-
a) B5 :-
HSD blended with up to 5% v/v max of BIODIESEL (B100) conforming to IS:

1460.
b) B6-B20:-
HSD blended with 6 % up to 20% v/v max of BIODIESEL (B100) conforming to IS:
16531:2016.
.
2.5 Fatty Acid Alkyl Ester:
BIODIESEL (B100) contains Fatty Acid Alkyl Ester (Methyl / Ethyl) and each of the
alkyl ester present in various feed stocks influence some of the properties of the fuel.
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Section Name: Salient features

Section No.3 of BIODIESEL (B100) Clause 3
3. Salient features of BIODIESEL (B100):-
BIODIESEL is a fuel manufactured from vegetable oils, recycled cooking oil or fats.
The fuel typically contains different types of Fatty Acid Alkyl (Methyl / Ethyl) Esters,
conforming to BIS document IS 15607 :2016.
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Section Name: Quality of

Section No.4 BIODIESEL (B100) Clause 4.1 to 4.2
4. Quality of BIODIESEL (B100):
4.1 Description & requirements:
The material shall be a Clear, homogenous liquid, free from suspended matters and
consisting essentially of Fatty Acid Alkyl Esters. The material shall also comply with
the requirements as given below in Table 1:
TABLE 1
Sr. Characteristics Requirement Method of Test Ref to
No. IS
15607:2016 Other [P:] of
Methods IS 1448
i) Density1 at 15°C, Kg/m3. 860 – 900 ISO 3675 P: 16 /

ISO 12185 P: 32
ASTM D 4052
ii) Kinematic Viscosity at 40°C, Cst 3.5 – 5.0 ISO 3104 P: 25
iii) Flash Point (PMCC)2 °C, min 101 ISO 2719 P: 21
iv) Sulphur3, mg/kg, max. 10.0 ASTM D 5453/ P: 83
ISO 20846/
ISO 20884/
ISO 13032
v) Carbon Residue (Ramsbottom)4, % 0.05 ASTM D 4530 -
by mass, max. ISO 10370
vi) Sulphated Ash, % by mass, max. 0.02 ISO 3987 -
vii) Water content5, mg/kg, max. 500 ISO 12937 P: 40
ISO 3733
ISO 6296
viii) Total contamination, mg/kg, max. 24 EN 12662 -
ix) Copper corrosion, 3 hrs at 50°C, max 1 ISO 2160 P: 15
x) Cetane No., min 51 ISO 5165 P: 9
xi) Acid Value, mg KOH/g, max 0.50 EN 14104/ P: 1/ Sec 111
ASTM D 974
xii) Methanol2, % by mass, max 0.20 EN 14110 -
xiii) Ester Content, % by mass, min 96.5 EN 14103 -
xiv) Monoglycerides6 content, % by mass, 0.7 D 6584 /
max. EN 14105
xv) Diglycerides6 content, % by mass, 0.2 D 6584 /
max. EN 14105
xvi) Triglycerides6 content, % by mass, 0.2 D 6584 /
max. EN 14105
xvii) Free Glycerol7, % by mass, max 0.02 ASTM D 6584/ -
EN 14105/
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EN 14106
xviii) Total Glycerol6, % by mass, max 0.25 ASTM D 6584/ -
EN 14105
xix) Phosphorous8, mg/kg, max 4.0 ASTM D 4951/ -
EN 14107
xx) Sodium + Potassium9, mg/kg, max 5.0 EN 14108/ -
EN 14109/
EN 14538
xxi) Calcium + Magnesium, mg/kg, max. 5.0 EN 14538 -
xxii) Iodine value10, gm Iodine/100 gm, 120 EN 14111/ -
max. EN 16300
xxiii) Oxidation stability, at 110°C hrs, min. 8 EN 14112/ -
EN 15751
xxiv) CFPP, 0C, max. EN 16329/ P 110
D 6371
a) Winter (Nov. to Feb.) +6.0
b) Summer (Other months) +18.0
xxv) Linolenic acid methyl ester, 12.0 EN 14103

% m/m, max.
xxvi) Polyunsaturated (>4 double bonds) 1.0 EN 15779
methyl ester, % m/m, max.
1) In case of dispute ISO 12185 shall be the refree method.

2) In case flash point is more than 130°C then testing and reporting of methanol content may not be
required.
3) In case of dispute ISO20846 or ISO 20884 shall be the refree method.
4) Carbon residue shall be run on 100 percent sample.
6) In case of dispute EN14105 shall be the refree method.
11) In case of dispute [P:1/Sec 1] shall be the refree method.
4.2 Significance of Characteristics – B100:
Appearance - BIODIESEL should be clear, although it may come in a variety of

colours. BIODIESEL colour does not predict fuel quality. A milky layer of material on
the bottom of a fuel container can have several meanings. If the fuel was frozen or
chilled, the layer may contain the saturated Alkyl Esters with high cloud points. If the
material returns to a clear form after heating to 40 °C, it is probably composed of
BIODIESEL saturates. If the material remains milky or jelly-like at 40 °C, it may be
poorly processed and is contaminated with the fuel residues, water, or other
contaminants.
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Flash point – It is typically high. Alkyl Esters are not volatile. The fall in flash point
signifies that the manufacturer has not removed excess alcohol used in the
manufacturing process. Accordingly the residual alcohol in the fuel is a safety issue
because very small amounts of alcohol reduces the flash point. Alcohol can also affect
fuel pumps, seals, elastomers, and can result in poor combustion properties.
Sulphated ash – The test ensures the removal of all the manufacturing catalysts.
High levels of manufacturing catalysts in the fuel can result in injector deposits or filter
plugging.
Acid Number – Acid number will become elevated if the fuel ages, or if it was not
properly manufactured. Higher Acid numbers is associated with fuel system deposits
and reduces the life of fuel pumps and filters.
Free and total glycerine – The numbers measure the complete conversion of the
fats and oils into Alkyl Esters. If these numbers are too high, the manufacturing
process is inadequate and engine fouling can occur. Fuel that exceeds the free and
total glycerine limit should not be used.
Oxidative Stability - High acid numbers coupled with high viscosity numbers indicate
a degraded fuel.
Sulphur – BIODIESEL generally contains less than 10 ppm sulphur.
Cetane Number – BIODIESEL requires the Cetane Number test because the
calculated Cetane Index provides inaccurate results.
Aromatics – Aromatics test for diesel fuel will provide inaccurate results for bio diesel.
BIODIESEL does not contain any aromatics.
Currently, fuel quality of BIODIESEL can be tested before it is blended, but not after
it is blended with diesel fuel. Once BIODIESEL is blended, it is very difficult to
determine if it was a good quality fuel to begin with. Therefore, it is essential that
organisation actually blending the BIODIESEL into the Diesel fuel ensures that the
BIODIESEL fully meets the specifications.
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Section Name: Receipt of

Section No.5 BIODIESEL (B100) Clause 5.1 to 5.3
5. Receipt of BIODIESEL B100:
5.1 Type Approval:
5.1.1 Vendor should obtain a Type approval of B100 from the Oil Company/BIS as a part
of procurement process based on the statement on Raw material, process, quality
monitoring, storage & handling facilities and procedures available with him.
5.1.2 The Type Approval will have the validity for one year. In case of change in raw material
or process the vendor should obtain fresh type approval and accordingly the quality
will be firmed up.
5.1.3 Vendor will submit samples in duplicate i.e. 2 sets of 2X2 litre samples for each type
of Biodiesel variant to OMC or the required quantity to BIS. One set of samples shall
be used for testing and other for retention.
5.1.4 The sample will be subjected to full specification test on characteristics mentioned in
table 1. Based on the test report, the characteristic requirement will be firmed up to
draw the Type Approval. A format for Type Approval is enclosed as Annexure III.
5.1.5 The manufacturer will rely on the Type Approval while comparing the batch test
results at the time of manufacturing of B100. The permissible limit for all the test
parameters shall be the reproducibility of the subject test method but within the limit
of the IS specification
5.1.6 The locations will rely on the Manufacturer’s cetificate while comparing the batch test
results at the time of receipt of B100.The permissible variance for density will be +/-
2.0 kg/m3 @ 15 °C and for the rest of the parameters it will be the reproducibility of
the subject test method but within the limit of the IS specification.
5.1.7 The test report of manufacturer shall contain details of Type Approval.
5.2 Transportation of Biodiesel B100
5.2.1 Hoses and seals should be compatible with B100 . It is preferred that B100 should
be transported in warm condition (around 27°C) for immediate delivery/decantation
and blending.
5.3 Receipt
5.3.1 B100 shall be received at Terminal /Depots from the approved vendors in tank trucks.
All care shall be taken to prevent ingress of water into the compartments during
transportation. Trucks which had carried B100/HSD /HSD-Biodiesel Blends in the
previous trip should only be used for carrying B100. Tanks in Tank Trucks should be
made of Aluminium, Mild Steel or Stainless Steel. Vehicles with Epoxy Coating should
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not be used for transportation of B100. The tank trucks having any other inner coating
must be compatible with B100. Proper inspection and tank cleaning certificate should
be available with truck as per the format in Annexure VI
5.3.2 before taking it for loading. It must be ensured that there is no residual water even in
traces in the truck before loading B 100.
5.3.3 The consignment of B100 must carry Type Approval Quality Certificate along with
manufacturing batch certificate conforming to IS 15607 :2016. The vendor shall
provide the details such as the Batch number, certified Batch Quantity etc. in the
batch certificate.
5.3.4 On arrival, Check seals and quantity of the product.

5.3.5 The observed density at ambient temperature may be converted to 15 deg.C. by
using ASTM Table 53-B.
Sampling shall be done after draining pipeline quantity by opening the master
valves. Clean Aluminium/ Stainless Steel containers shall be used for storage of
B100 samples.
5.3.6 a. Top and bottom samples from individual tank truck compartments shall be drawn
and checked for appearance and density test.
b. If the samples meet appearance test as bright & clear free from visible impurities,
suspended matter , haze and the density variation of each sample tested is within +/-
2.0 Kg/M3 with respect to Manufacturer certified density, proportionate composite of
all samples (Two sets -1 X 1 lit each) shall be made by the location
c. The samples shall be jointly sealed, labelled & signed by the authorized
representative of the transporter and the receiving officer of the OMC. Out of two sets,
one set of TT sample shall be sent to nearest lab for testing and other set shall be
retained for 30 days.
d. The entire operation mentioned above shall be done in the least possible time since
Biodiesel has tendency to absorb atmospheric moisture upon longer exposure.
5.3.6 A composite sample of upto 5 TTs of the same supplier and batch shall be prepared
by Lab for testing the parameters listed below :-
1. Appearance
2. Density at 150 C.
3. KV at 400 C.
4. Flash Point
5. Water content
6. Copper strip corrosion
7. Acid value
8. CFPP
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The above tests are to be conducted as per IS 15607 : 2016.

Acid value : Manual titration method IS 1448, P-2 may be used wherever
potentiometric titrator is not available
Water Content: Karl Fischer Coulometric titration technique is to be used ( ISO

12937).
5.3.7 However, in case of failure of composite sample in any of the test parameter(s),
individual TT shall be tested for the failed parameter and report released accordingly.
The TTs which are not meeting the specification in any of the above parameters would
be rejected
5.3.8 In case, any Oil Company is not having lab facility at the Biodiesel receiving location,
necessary testing assistance shall be provided by nearby OMC lab at Industry agreed
rate.
5.3.9 The TT shall be decanted if the product is meeting above eight parameters in the lab
Test.
5.3.10 B100 consignment is to be stored in a dedicated storage tank( U/G or A/G) with
dedicated facilities.
5.3.11 The unloading operations shall be carried out through special rubber or any other
compatible hoses (Teflon, Nylon 6/6, Viton A 401 –C, Viton GFLT, Flouro-silicon).
Nitrile Rubber is not compatible with B100. Utmost precaution needs to be taken to
ensure that there is no ingress of water. Both the ends of the hoses after use shall
be capped. 80 mesh strainers (mild steel/stainless steel) shall be provided before the
pump / tank inlet as the case may be. All safety precautions shall be taken as that
required for storing excluded product.
5.3.12 The location shall maintain a Batch-Control Logbook tank-wise for receipt of B100 in
the storage tank as per the following format
Batch Control Log Book Location :
Despatch Details Receipt Details
S. Supplier’s Despatch details Supplier Type Approval Supplier’s Location Sign
No Name Batch No. Test Report BatchTest Batch No.
Date quantity Date quantity
No. Report No.
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Section Name: Storage and

Handling of B100 and Bio-Diesel
Section No.6 blends Clause 6.1 to 6.15
6. Storage and Handling of B100 and Bio-Diesel blends:
a) B-100
6.1 The selection of material for the construction of the storage and handling facilities
should be such that it is compatible to both fuel and the material used for storage and
handling facilities. It is recommended that integrity of all materials coming in to contact
with the fuel will be verified with ‘Soak testing’ or any other suitable method as per
standard engineering practice.
6.2 B100 will degrade, soften or seep through some hoses, gaskets, seals, elastomers,
glues and plastics with prolonged exposure.
6.3 Nozzles, fittings, connectors, piping, pump and impellers may be of best suitable
material compatible with B100 as recommended for the storage tanks.
6.4 Zinc, Brass, Bronze, Tin, Lead and Copper are some of the sensitive materials known
to be degraded while in contact with B100. Lead solders and zinc linings should be
avoided, as should copper pipes, brass regulators and copper fittings.
6.5 Stainless Steel, mild steel or Aluminium has shown acceptable resistance to corrosion
by B100.
6.6 Non-metallic materials that degrade when in contact with B100 include Nitrile Rubber,
Natural Rubber, Polypropylene, Tygon, Polyurethane, Polyvinyl Chlorides and hence
their contact with B-100 should be avoided.
6.7 Non-metallic materials that have been successfully used with B100 include Viton,
Teflon, Fluorosilicon / Fluorinated plastics & Nylon.
6.8 It is advisable to monitor and visually inspect the equipment regularly for leaks seeps
and seal decompositions
6.9 Epicoating is not recommended for the tanks proposed for storage of B100.
6.10 Epicoating recommended in storage tank for general hydrocarbons may not be
compatible for system handling B100 & B5. Compatibility may be ensured before any
application or use.
6.11 The storage tanks and allied facilities for B100 shall be positively segregated. The
tank shall be absolutely free from water at all times.
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6.12 B100 storage tanks shall be cleaned once in two years or more frequently depending
on the need. Tank cleaning certificate shall be maintained as per Appendix 8 of IQCM.
Date of tank cleaning and due date of next tank cleaning shall be prominently painted
on the tank at a suitable place. For Under Ground Tanks, such details shall be
displayed on a suitable display board adjacent to the tank. In case of any exigency a
one time of extension of max. 3months can be granted with recommendation from
Operations department and approval from QA/ QC department.
6.13 All level / TMB samples after receipt of first parcel in a newly commissioned tank /
after tank cleaning shall be sent to laboratory for necessary Tests on parameters
mentioned in Annexure V against the specifications of B100. The product from the
tank shall be released only if the Laboratory confirms that the product meets
requirement in respect of the tests carried out as per IS 15607 :2016.
6.14 In case of dormancy of B100 for 6 months, the sample shall be checked for 8
parameters(Annexure V) and oxidation stability test additionally.
b) BIO-DIESEL BLENDS:
6.15 Various Bio-Diesel blends can also be stored in AG/UG tanks. However, care should
be taken for ensuring homogeneity of the product. This is important as the density of
Bio-Diesel is higher than HSD. Suitable churning facility/ blending facility required to
be provided. Water presence and moisture ingress shall be avoided.
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Section Name Colour Coding

Section No.7 for B100 Clause 7
7.Colour Coding for B100 :
7.1 The colour band for B100 on the pipeline shall be Turquoise Blue (No. 102 of IS 5,
2007). The procedure for Colour Coding shall be in accordance with Clause 4.3 of
Industry Quality Control Manual for Non-Aviation Products (IQCM).
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Section Name: Quality

Monitoring for B100 and
Section No.8 Biodiesel Blends Clause 8.1 to 8.2
8. Quality Monitoring for B100 and Biodiesel Blends:
8.1 One litre composite sample of B100 from the storage tank(s) shall be collected in
dedicated Aluminium or Stainless Steel for Monitoring Tests and sent to the nearest
Laboratory once in a month. These samples shall be tested for 8 parameters
mentioned in Annexure V against the specifications of B100.
8.2 HSD-Biodiesel blend samples shall be tested for monthly monitoring test. Retention
process as per IQCM shall be followed.
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Section Name: Blending of B100

in HSD and Quality Control
Section No.9 Checks Clause 9.1 to 9.2
9. Blending of B100 in HSD and Quality Control Checks :
9.1 At Depot / Installation / Terminal:-
9.1.1 It is necessary that adequate care be taken to ensure the correct blending of B100
with HSD.
9.1.2 Manufacturing specification of HSD at Refinery end to be kept such that the end
product from Marketing after blending 5% v/v max B100 into HSD remains within
specification IS 1460.and after blending 6 % v/v to 20 % v/v remains within
specification IS 16531-2016.
9.1.3 Procedure for Blending B100 in HSD:
There are mainly three options available and practised for blending B100 in HSD
i.e. On-line blending, in-tank blending and Splash blending.
a. On-line Blending:
In this case, B100 is added slowly and continuously into the moving stream of
HSD via a smaller line inserted or ‘Y’ in a larger pipe at the loading gantry. B100
can also be added in small slug or pulsed quantities spread evenly throughout the
time HSD is being loaded. B100 and HSD get mixed by the turbulent movement
that occurs once the fuel is loaded into its receiving tank truck/tank wagon. This is
similar to the way additives are blended into HSD and is commonly used
at locations.
b. In-tank blending:
In tank blending shall be applicable for pipeline receiving location. In this operation,
Bio-Diesel is stored at location in dedicated tanks with facility for pumping metered
quantity such as batch controllers/ Mass Flow Meters, Pipelines etc. Pre calculated
quantity of B100 is based on the total quantity expected to be available in the HSD
tank after receipt. The injection point of Bio-Diesel in HSD receipt line should be as
far away as possible from the receiving tank inlet.
It shall be ensured that the receiving HSD tank as well as incoming HSD parcel is
free from water.
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Batch controller/Mass Flow Controller shall be used to monitor requisite quantity of

Bio-Diesel injected in HSD. It shall be ensured that on completion of the operation,
the pipeline is left with HSD only and no bio diesel is available. The storage tank
should have facility for churning either through circulation or through jet mixer. After
completion of operation, TMB samples shall be checked for density to verify
homogeneity of product. In case the product is non-homogeneous, the product
needs to be circulated till homogeneity is established. It is preferable to carry out in
tank blending operation in empty tank or with minimum stock.
c. Splash Blending:
In this blending, both the products Bio Diesel and HSD are loaded sequentially in
the tank truck. Product mixing occurs as the fuel is agitated during the
transportation and delivery of the Biodiesel blend to the end user.Being slightly
heavier than conventional distillates, we recommend that Biodiesel be loaded
as per the following sequence:
Top loading TT facility:

HSD followed by Bio Diesel
Bottom loading TT facility:

Bio Diesel followed by HSD
9.1.4 Notwithstanding the method adopted, to ensure uniform blending of B100 with
HSD, it shall be carried out through a closed system, with proper interlocks, while
maintaining efficacy of mixing B100 in the right proportion of 5% v/v max or 6 % v/v
upto 20 % v/v as per specification. This can be ascertained at least for first few
batches employing test method given in Annexe- A of the BIS specification for HSD
viz. IS 1460.
9.1.5 A 80 mesh strainer shall be provided on the delivery side of B100 storage tank.
9.1.6 The following QC checks are recommended for quality monitoring after blending
B100 in HSD:
A top, middle, and bottom sample of the tank can be taken and analysed for the
percent B100 by measuring the density. This can be done with any of the
conventional means of measuring density that are readily available (i.e. digital
density meter, hydrometer). If the values do not vary by more than 3.0 kg/m3 at 15°C
from top to bottom, the mixture is adequate.
If the homogeneity as above is not achieved, the fuel will require agitation to mix
thoroughly.
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9.1.7 Samples shall be drawn, tested and retained as per the procedure mentioned below
a) At locations Sampling procedure as outlined in IQCM for HSD will be followed
for B5 & B6-B20..
b) Parameters covered under MDG for HSD will be followed in case of MDG samples
of B5 & B6-B20.
9.1.7 Biodiesel content in HSD-Biodiesel Blends is to be verified as per procedure outlined

in Annex- A of IS 1460. In case Biodiesel content in HSD exceeds / is less than the
permissible level, corrective steps are to be taken immediately.
9.1.8 Retention of the HSD-Biodiesel sample from TLF shall be ensured as per IQCM
requirements (before commencement of loading in each shift and whenever there is
a switchover of tank).
9.2 Test / Facilities required for testing B100 and HSD. :
9.2.1 At Depot / Installation:
Facilities required for the field test of B100 Quality:

 Hydrometers,
 Thermometers,
 Glass Cylinders,
 ASTM 53-B density conversion table
 Cooling facility (Optional)
9.2.2 At QC Labs:
i) B100 to be tested for the parameters shown in Annexure V. The quantity of B100
in blended HSD can be ascertained as per the method given under Annex-Aof
IS 1460.
ii) Contamination / suspected adulteration or deviation in B100 may be verified by

carrying out full specification test as given in IS 15607:2017.
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Section Name: Despatch of

Section No.10 B100 blended HSD Clause 10
10 Despatch of B100 blended HSD:
10.1 Tank trucks used for transportation of HSD can be used for carrying Biodiesel
blends. Trucks to be inspected for presence of water before loading. Adequate care
shall be taken to ensure that the tank truck fittings are absolutely tight to eliminate
ingress of water.
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Section Name Handling of B100

Section No.11 blended HSD at Retail Outlets Clause 11.1 to 11.4
11 Handling of B100 blended HSD at Retail Outlets:
11.1 Underground Tanks, Dispensers and Fittings
11.1.1 Storage tank shall be suitable for Class “B” product and pipeline fittings shall be tight
and the threaded connections if any shall be tightened with the help of PTFE tapes.
Bolted connections shall be provided with proper gaskets. Storage tanks shall be
thoroughly cleaned ensuring absence of any traces of water before commissioning
into HSD- Biodiesel blend service. Fill cap and dip cap fittings shall be water tight
and have suitable gaskets / packing to prevent entry of moisture. The fill / dip caps
shall be raised sufficiently high above the ground level. In case these are situated in
chambers, the chambers shall be constructed in a manner so as to avoid entry of
water into the tank and the caps positioned sufficiently above the bottom of the
chamber.
11.1.2 The presence of any water in the underground tank shall be checked by using water-
finding paste everyday. During the rainy season the water shall be promptly removed
from the tank.
11.1.3 Utmost precaution needs to be taken to ensure that there is no ingress of water or
moisture in the storage tanks
11.1.4 Sampling procedures at the Retail Outlets would be the same as mentioned in the
Marketing Discipline Guidelines.
11.1.5 Dispensing Units are typically manufactured with Steel, Cast Iron, Aluminium, Brass,
Bronze and sometimes Stainless Steel components. B100 blended HSD should not
pose problem with any of these metals. Normal dispensing hoses can be used for
B100 blended HSD
11.2 Receipt of B100 blended HSD:
11.2.1 The procedure will remain same as is being followed for un-blended HSD.
11.2.2 During rainy seasons, wherever the canopy is available, the tank lorry shall be
checked under the canopy, to avoid ingress of water. Tarpaulin cover shall be used
during tank lorry discharge. The dip cap of underground tanks shall be kept closed
during tank lorry unloading operation.
11.3 Colour coding for dispensing pumps for B100 blended HSD:
The colour coding for the dispensing pumps used for B100 blended HSD remains
same as that of un-blended HSD.
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11.4 Fire fighting system :
The most accepted system is Dry Chemical Powder (DCP), which works as
effectively on B100 blended HSD fire as being used for HSD fire. The personnel
should be informed about the properties of B100 blended HSD and safe practices
for operating, fuelling etc.
All staff in the Retail Outlets must be trained in handling any emergencies.
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Section No.12 Section Name Safety Clause 12.1 to 12.19
12.Safety:
12.1 B100 is not covered under Petroleum Act/Rules. B100 is not easily flammable liquid
and has a flash point of >101°C. It requires fire-fighting facilities like CO2/Dry
Chemical Powder (DCP) fire extinguishers.
12.2 Earthing and Bonding procedure shall be followed as being done for Petroleum
products.
12.3 B100 material safety data sheet is enclosed in Annexure VII:
12.4 Extinguishing media :
Carbon di-oxide, Dry Chemical Powder, Foam & water spray (Fog) for small fires.
12.5 Special fire-fighting procedures:
Use necessary protective equipment & breathing apparatus as would normally be

used when fighting fires where there may be danger of breathing hazardous products
during combustion.
12.6 Unusual fire and explosion hazards:
Oil soaked rags are flammable if not handled properly
12.7 Stability:
Product is stable and hazardous polymerisation will not occur
12.8 Conditions to avoid in normal use (incompatibility, material to avoid) :
May react with oxidizing material
12.9 Hazardous decomposition or by- products :
Combustion may produce COx, NOx and thick smoke. Hazardous polymerisation will
not occur.
12.10 Health hazards :
Routes of entry is through inhalation / skin contact / ingestion
12.11 Toxicity: Moderate
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12.12 Signs and symptoms of exposure:
May cause dizziness, irritation and nausea.
12.13 Emergency and safety procedures:
If swallowed, induce vomiting. If inhaled, remove person to fresh air. Give artificial
respiration if breathing has stopped and call a physician.
If splashed in eyes or on skin, splash water /wash immediately with soap and water.
12.14 Precautions for safe handling and use:
In case spilled or released out , eliminate all sources of ignition. Small spills should
be flushed with large quantities of water. Large spills should be collected for waste
disposal.
12.15 Waste disposal methods:
Company’s procedure for waste disposal shall be followed.
12.16 Precautions to be taken in handling and storage:
 Store in closed containers between 15 – 50 ° C

 Keep away from oxidising agents, excessive heat and ignition sources.
 Use with adequate ventilation;
 Use explosion-proof electrical equipment and
 Non-sparking tools.
12.17 Protective Controlled measures:
Air supplied mask to be used for a high concentration as a respiratory precaution. Use
protective rubber gloves and goggles for eyes. Eye bath and Safety shower is
recommended as outer protective equipment.
12.18 Salient features:
Carcinogenic compounds are not present in pure B100.
12.19 Environmental impact of B100 blended HSD:
 B100 blended HSD vehicle reduces most of the exhaust emissions.

 Compared with HSD vehicle, the B100 blended HSD vehicle produces lower
hydrocarbon, carbon monoxide and carbon dioxide emissions.
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Section Name Additional

Section No.13 Precautions Clause 13
13. Additional Precautions :
13.1 Additional Precautions and First Aid
Don’ts First Aid measures

1 Prolonged exposure to high Move person to an open area. Give artificial
concentration should be avoided respiration in case of breathing problem. Get
medical attention.
2 Ingestion/swallowing should be Induce vomiting immediately as directed by
avoided medical practitioner.
3 Skin contact should be avoided to Immediately flush skin with plenty of water for
prevent absorption of toxic at least 15 minutes. Remove all contaminated
compound into body. clothing and shoes. Wash & clean clothing &
shoes before reuse.
4 Splashes and eye contact should Immediately flush eyes with plenty of clean
be avoided. running water for at least 15 minutes, moving
lower and upper eye lids occasionally.
5 In case of spill do not use recover liquid in appropriate container or
combustive materials such as absorb with inert material like Paper towels,
sawdust etc. Do not flush to Oil dry sand or dirt.
sewage system. Remove all
sources of ignition through
appropriate protective equipment.
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Annexure –I
Specification for B100- IS 15607:2016
Sr. Characteristics Requirement Method of Test Ref to

No. IS
15607:2016 Other [P:] of
Methods IS 1448

ISO 12185 P: 32
ASTM D 4052
iv) Sulphur3, mg/kg, max. 10.0 ASTM D 5453/ P: 83
ISO 20846/
ISO 20884/
ISO 13032
v) Carbon Residue (Ramsbottom)4, % 0.05 ASTM D 4530 -
by mass, max. ISO 10370
ISO 3733
ISO 6296
ix) Copper corrosion, 3 hrs at 50°C, max 1 ISO 2160 P: 15
xi) Acid Value, mg KOH/g, max 0.50 EN 14104/ P: 1/ Sec 111
ASTM D 974
xiv) Monoglycerides6 content, % by mass, 0.7 D 6584 /
max. EN 14105
max. EN 14105
max. EN 14105
xvii) Free Glycerol7, % by mass, max 0.02 ASTM D 6584/ -
EN 14105/
EN 14106
xviii) Total Glycerol6, % by mass, max 0.25 ASTM D 6584/ -
EN 14105
xix) Phosphorous8, mg/kg, max 4.0 ASTM D 4951/ -
EN 14107
EN 14109/
EN 14538
xxi) Calcium + Magnesium, mg/kg, max. 5.0 EN 14538 -
[Type here]
FOR
2019

max. EN 16300
xxiii) Oxidation stability, at 110°C hrs, min. 8 EN 14112/ -
EN 15751
D 6371
c) Winter (Nov. to Feb.) +6.0
d) Summer (Other months) +18.0

% m/m, max.
xxvi) Polyunsaturated (>4 double bonds) 1.0 EN 15779
methyl ester, % m/m, max.

2) In case flash point is more than 130°C then testing and reporting of methanol content may not
be required.
[Type here]
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2019
ANNEXURE II
Specification for B6-B20 - (IS 16531:2016)
Sl. Characteristics Requirements Method of Test, Ref to

No
ISO/ASTM D/ [P:] of 1448/
IP/EN /Annex
i) Density 1) at 150C ISO 12185/3675 [P:16]/[P : 32 ]
(kg/m3) / D 4052
820-860
ii) Kinematic viscosity. ISO3104 [P:25]

@ 400C (cSt) 2.0 -4.62
iii) Flash point, Abel [P : 20]

(0C) Min
35
iv) Sulphur2) (mg/kg), D 4294/D
Max 5453/ISO 20846/
ISO 20884/ISO
BS III 350 13032
BS IV 50
v) Carbon Residue D 4530/ ISO [P : 8]
(Ramsbottom) 3 on 0.3 10370
10% residue ,%
mass) Max
vi) Ash content (% ISO 6245 [ P : 4/Sec 1]
mass) Max 0.01
vii) Water , ppm, Max ISO 6296 /ISO [ P : 40 ]
12937
260
viii) Cu corrosion, 3h @ ISO 2160 [P : 15 ]

0
50 C , Max 1
ix) Cetane No4), Min ISO 5165 [P:9]
51
4)
x) Cetane index , Min ISO
46 4264/D4737
xi) PAH, m/m Max EN 12916/
11 IP391
xii) Lubricity , wear scar ISO12156-1
Diameter(wsd1.4) at
Page 4 of 41
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60 deg C, micron, Max 460

xiii) Acid No , mg of ISO 7537 [P: 1/Sec1]
KOH/gm Max 0.2
xiv) Oxidation stability , at EN15751

110°C, h, Min 20
xv) Distillation , percent ISO 3405 P:18
0
recovery at 360 C 95
Min.
xvi) Biodiesel Content , EN 14078 Annex B of
percent,v/v 6-20 IS 1460 : 2005
xvii) Pour point5) , Max D5949 / [P : 10/Sec 2]
Winter D5950/
Summar 30C D5985/ISO
3016
150C
xviii) Cold filter plugging
point(CFPP5) Max
[P:110]
Winter 60C EN
Summar 180C 16329/D6371
xix) Total contamination, EN12662
mg/kg Max 24

2) In case flash point is more than 130°C then testing and reporting of methanol content
may not be required.
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Annexure III
Type approval of Biodiesel B-100(Requirement as per IS 15607:2016)
Name Of the Vendor : Date of Application:

Reference :
Validity :
Sr. Characteristics Requireme Method of Test Ref to Type

No. nt Value
IS s
15607:2016 Other [P:] of
Methods IS 1448

ISO 12185 P: 32
ASTM D 4052
iv) Sulphur3, mg/kg, max. 10.0 ASTM D P: 83
5453/ ISO
20846/ ISO
20884/ ISO
13032
v) Carbon Residue (Ramsbottom)4, 0.05 ASTM D 4530 -
% by mass, max. ISO 10370
ISO 3733
ISO 6296
ix) Copper corrosion, 3 hrs at 50°C, 1 ISO 2160 P: 15
max
xi) Acid Value, mg KOH/g, max 0.50 EN 14104/ P: 1/ Sec
ASTM D 974 111
xiv) Monoglycerides6 content, % by 0.7 D 6584 /
mass, max. EN 14105
max. EN 14105
max. EN 14105
xvii) Free Glycerol7, % by mass, max 0.02 ASTM D -
6584/ EN
14105/
EN 14106
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xviii) Total Glycerol6, % by mass, max 0.25 ASTM D -

6584/ EN
14105
xix) Phosphorous8, mg/kg, max 4.0 ASTM D -
4951/ EN
14107
EN 14109/
EN 14538
xxi) Calcium + Magnesium, mg/kg, 5.0 EN 14538 -
max.
max. EN 16300
xxiii) Oxidation stability, at 110°C hrs, 8 EN 14112/ -
min. EN 15751

D 6371
a) Winter (Nov. to Feb.) +6.0
b) Summer (Other months) +18.0

% m/m, max.
xxvi) Polyunsaturated (>4 double 1.0 EN 15779
bonds) methyl ester, % m/m, max.

2) In case flash point is more than 130°C then testing and reporting of methanol content
may not be required.
ANNEXURE IV
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QC CHECKS BY LOCATION FOR RECEIPT OF BIODIESEL B-100 TANK TRUCKS
Truck No.
Supplier's Quality Certificate
details
Date & Time of samples drawn
Date tested
Samples drawn by
Testing carried out by
RESULTS
TESTS METHOD Limits Top Bottom
C1 T C1 B C2 T C2 B C3 T C3 B C4 T C4 B C5 T C5 B composite Composite
Bright &
clear, free
from visible
1. Appearance Visual impurities,
suspended
matter and
haze.
2. Density @15°C kg/m3 IS 1448:P16 860 - 900
Remarks :
Signature of Location Officer
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Annexure –V
Format for Pre–receipt Test
Sample ID No. : Date of Report :

Quantity represented: Date sample is drawn:
Source of Sample: Date of Receipt:
Type of Sample:
Sample Drawn By:
Sr. Characteristics Requirement Method of Test Ref to Typ Supplier Lab Variatio
No as per IS e Batch Values ns
15607:2016 Val Test between
(3) ues Values (7) & (8)
(1) (2) Other [P:] of
Methods IS 1448
(4) (5) (6) (7) (8)
i) Appearance Bright & Clear
ii) Density at 15°C, 860 - 900 ISO 3675 P: 16 /
Kg/m3. ISO 12185 P: 32
ASTM D 4052
iii) Kinematic 2.5 – 6.0 ISO 3104 P: 25
Viscosity at 40°C,
cSt
iv) Flash Point 101 ISO 2719 P: 21
(PMCC) °C, min
v) Water content, 500 ISO 12937 P: 40
mg/kg, max. ISO 3733
ISO 6296
vi) Copper corrosion, 1 ISO 2160 P: 15
3 hrs at 50°C, max
vii) Acid Value, mg 0.50 D 664 P: 1/ Sec 1
KOH/g, max
viii) CFPP , °C Max EN16329/ [P:110]
a) winter +6 D6371
(Nov to +18
Feb)
b) summer
Other
months)
Remarks:
Signature of the QC/QA Officer
Page 9 of 41
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Annexure VI
TANK TRUCK INSPECTION / CLEANING CERTIFICATE

FOR USE OF BIODIESEL B100.
This is to certify that tank truck no. ------------- carrying capacity -------------KL was
previously on the service of product-----------. The tank truck is upgraded, inspected
from inside and found empty and dry. The tank truck is fit to load Biodiesel B100.
Date of inspection
Name & Signature of the inspecting Authority
Page 10 of 41
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Annexure-VII
BIODIESEL (B100) MATERIAL SAFETY DATA SHEET
Chemical Product / General Product Name: BIODIESEL (B100) Synonyms: Methyl

Soyate, Rapeseed Methyl Ester (RME), Methyl Tallowate Product Description: Methyl
esters from lipid sources CAS Number: Methyl Soyate: 67784-80-9; RME: 73891-99-3;
Methyl Tallowate: 61788-71-2
Composition/Information on Ingredients
This product contains no hazardous materials.
Hazards Identification Potential Health Effects:

INHALATION: Negligible unless heated to produce vapors. Vapors or finely misted
materials may irritate the mucous membranes and cause irritation, dizziness, and nausea.
Remove to fresh air.
EYE CONTACT: May cause irritation. Irrigate eye with water for at least 15 to 20 minutes.
Seek medical attention if symptoms persist.
SKIN CONTACT: Prolonged or repeated contact is not likely to cause significant skin
irritation. Material is sometimes encountered at elevated temperatures. Thermal burns are
possible.
INGESTION: No hazards anticipated from ingestion incidental to industrial exposure.
First Aid Measures
EYES: Irrigate eyes with a heavy stream of water for at least 15 to 20 minutes.
SKIN: Wash exposed areas of the body with soap and water.
INHALATION: Remove from area of exposure; seek medical attention if symptoms

persist.
INGESTION: Give one or two glasses of water to drink. If gastro-intestinal symptoms

develop, consult medical personnel. (Never give anything by mouth to an unconscious
person.)
Fire Fighting Measures
Flash Point (Method Used): 101°C min.
Flammability Limits: None known
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EXTINGUISHING MEDIA: Dry chemical, Foam (AFFF), CO2, water spray (fog). Water
stream may splash the burning liquid and spread fire.
SPECIAL FIRE FIGHTING PROCEDURES: Use water spray to cool drums exposed to
fire.
UNUSUAL FIRE AND EXPLOSION HAZARDS: Oil soaked rags can cause spontaneous
combustion if not handled properly. Before disposal, wash rags with soap and water and
dry in well ventilated area. Firefighters should use self-contained breathing apparatus to
avoid exposure to smoke and vapor.
Accidental Release Measures / Spill Clean-Up Procedures

Remove sources of ignition, contain spill to smallest area possible. Stop leak if possible.
Pick up small spills with absorbent materials such as paper towels, “Oil Dry”, sand or dirt.
Recover large spills for salvage or disposal. Wash hard surfaces with safety solvent or
detergent to remove remaining oil film. Greasy nature will result in a slippery surface.
Handling and Storage

Store in closed containers between 15°C and 50°C. Keep away from oxidizing agents,
excessive heat, and ignition sources. Store and use in well ventilated areas. Do not store
or use near heat, spark, or flame, store out of sun. Do not puncture, drag, or slide this
container. Drum is not a pressure vessel; never use pressure to empty.
Exposure Control /Personal Protection
RESPIRATORY PROTECTION: If vapors or mists are generated, wear a NIOSH

approved organic vapor/mist respirator.
PROTECTIVE CLOTHING: Safety glasses, goggles, or face shield recommended to

protect eyes from mists or splashing. PVC coated gloves recommended to prevent skin
contact.
OTHER PROTECTIVE MEASURES: Employees must practice good personal hygiene,

washing exposed areas of skin several times daily and laundering contaminated clothing
before re-use.
Physical and Chemical Properties

Boiling Point,@ 760 mm Hg:>200°C
Auto ignition temperature, deg.c. : 705 to 840
Volatiles, % by Volume: <2
Specific Gravity (H2O=1): 0.860 to 0.900
Solubility in H2O, % by Volume: insoluble
Vapor Pressure, mm Hg: <2
Evaporation Rate, Butyl Acetate=1: <1
Vapor Density, Air=1: >1
Appearance and Odour: Colourless to pale yellow liquid, mild odour
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Stability and Reactivity
GENERAL: This product is stable and hazardous polymerization will not occur.
INCOMPATIBLE MATERIALS AND CONDITIONS TO AVOID: Strong oxidizing agents
HAZARDOUS DECOMPOSITION PRODUCTS: Combustion produces carbon monoxide,

carbon dioxide along with thick smoke.
Disposal Considerations
WASTE DISPOSAL: Waste may be disposed of by a licensed waste disposal company.

Contaminated absorbent material may be disposed of in an approved landfill. Follow local,
State and Central disposal regulations.
Transport Information
UN HAZARD CLASS: N/A
NMFC (National Motor Freight Classification):
PROPER SHIPPING NAME: Fatty acid ester
IDENTIFICATION NUMBER: 144920 SHIPPING CLASSIFICATION: 65
Regulatory Information
OSHA STATUS: This product is not hazardous under the criteria of the Federal OSHA
Hazard Communication Standard 29 CFR 1910.1200. However, thermal processing and
decomposition fumes from this product may be hazardous as noted in Sections 2 and 3.
TSCA STATUS: This product is listed on TSCA.
CERCLA (Comprehensive Response Compensation and Liability Act): NOT reportable.
SARA TITLE III (Superfund Amendments and Reauthorization Act): Section 312
Extremely Hazardous Substances: None
Section 311/312 Hazard Categories: Non-hazardous under Section 311/312
Section 313 Toxic Chemicals: None
RCRA STATUS: If discarded in its purchased form, this product would not be a hazardous
waste either by listing or by characteristic. However, under RCRA, it is the responsibility
of the product user to determine at the time of disposal, whether a material containing the
product or derived from the product should be classified as a hazardous waste.
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Other Information
This information relates only to the specific material designated and may not be valid for
such material used in combination with any other materials or in any other process. Such
information is to the best of the company’s knowledge and believed accurate and reliable
as of the date indicated. However, no representation, warranty or guarantee of any kind,
express or implied, is made as to its accuracy, reliability or completeness and we assume
no responsibility for any loss, damage or expense, direct or consequential, arising out of
use. It is the user’s responsibility to satisfy himself as to the suitableness and
completeness of such information for his own particular use.
23

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INDUSTRY MANUAL ON OPERATIONS, QUALITY & SAFETY FOR

BIODIESEL (B100) & HSD-BIODIESEL BLENDS(B5 & B6-B20)

Section 7 ........................................................................................................................ .10

Section No.1 Section Name: Introduction Clause 1.1 to 1.3.

1.3 This manual supersedes earlier communications regarding handling of Biodiesel.

Section No.2 Section Name: Terminology Clause 2.1 to 2.5

2.1 BIODIESEL (B100):

2.2 High Speed Diesel Oil (HSD)

2.3 BIODIESEL blended HSD:

A blend of BIODIESEL (B100) with High-Speed Diesel at recommended dosage.

2.4 BIODIESEL BLENDS :-

HSD blended with up to 5% v/v max of BIODIESEL (B100) conforming to IS:

2.5 Fatty Acid Alkyl Ester:

Section Name: Salient features

3. Salient features of BIODIESEL (B100):-

Section Name: Quality of

4. Quality of BIODIESEL (B100):

4.1 Description & requirements:

i) Density1 at 15°C, Kg/m3. 860 – 900 ISO 3675 P: 16 /

xxv) Linolenic acid methyl ester, 12.0 EN 14103

1) In case of dispute ISO 12185 shall be the refree method.

4.2 Significance of Characteristics – B100:

Appearance - BIODIESEL should be clear, although it may come in a variety of

Sulphur – BIODIESEL generally contains less than 10 ppm sulphur.

Section Name: Receipt of

5. Receipt of BIODIESEL B100:

5.1 Type Approval:

5.2 Transportation of Biodiesel B100

5.3.4 On arrival, Check seals and quantity of the product.

The above tests are to be conducted as per IS 15607 : 2016.

Water Content: Karl Fischer Coulometric titration technique is to be used ( ISO

Section Name: Storage and

6. Storage and Handling of B100 and Bio-Diesel blends:

Section Name Colour Coding

7.Colour Coding for B100 :

Section Name: Quality

8. Quality Monitoring for B100 and Biodiesel Blends:

Section Name: Blending of B100

9. Blending of B100 in HSD and Quality Control Checks :

9.1 At Depot / Installation / Terminal:-

9.1.3 Procedure for Blending B100 in HSD:

Batch controller/Mass Flow Controller shall be used to monitor requisite quantity of

Top loading TT facility:

Bottom loading TT facility:

9.1.7 Biodiesel content in HSD-Biodiesel Blends is to be verified as per procedure outlined

9.2 Test / Facilities required for testing B100 and HSD. :

9.2.1 At Depot / Installation:

Facilities required for the field test of B100 Quality:

ii) Contamination / suspected adulteration or deviation in B100 may be verified by

Section Name: Despatch of

10 Despatch of B100 blended HSD:

Section Name Handling of B100

11 Handling of B100 blended HSD at Retail Outlets:

11.1 Underground Tanks, Dispensers and Fittings

11.2 Receipt of B100 blended HSD:

11.4 Fire fighting system :

Section No.12 Section Name Safety Clause 12.1 to 12.19

12.3 B100 material safety data sheet is enclosed in Annexure VII:

12.4 Extinguishing media :

12.5 Special fire-fighting procedures:

Use necessary protective equipment & breathing apparatus as would normally be

12.6 Unusual fire and explosion hazards: