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Plant Safety and Layout
Plant Safety and Layout
Plant Safety and Layout
From Figure 6.1, it shows that the first thing in hazard identification and risk
assessment is to describe the system. From the description of the process, the hazards are
identified. The questions that must be asked includes what are the hazards, what can go
wrong and how, what are the chances and what are the consequences (Crawl &.Louvar,
2011).
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System Description
Hazard Identification
Scenario Identification
Risk Determination
Modify:
-Process or Plant
No -Process Operation
Risk and/or
o -Emergency Response
Hazard
Acceptance -Other
Yes
Figure 6.1: Hazard Identification and Risk Assessment. (Crawl &.Louvar, 2011)
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Crawl &.Louvar (2011), had discussed some methods for hazard identification
and risk assessment, includes:
1. Process hazards checklist: This is a list of items and possible problems in the
process that must be checked.
2. Hazards Survey: This can be as simple as an inventory of hazardous materials.
3. Hazards and operability (HAZOP) studies: Various events are suggested for a
specific piece of equipment and procedures.
4. Safety review: Less formal type of HAZOP study which is highly dependent on
the experience and synergism of the group reviewing the process.
The descriptions of the process for the production of 10, 000 tonnes of octanol are
deeply discussed in Chapter 1. Ziegler process is chosen and the description includes the
pressure and temperature was available. The detail information on chemical and physical
properties of sources is one of the measurements that also can be considered to control
and minimize the risk. It is discussed clearly in Section 6.3.
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6.1 HAZARDS AND OPERABILITY (HAZOP) STUDIES
The main objectives of HAZOP are to identify hazards and resolve the hazards.
The design area and design equipment that have the probability of occurring an accident
must be recognized first. HAZOP is important to familiarize the study team with the
information available which provided a systematic study of a serious hazard potential
area. When applied to a process design or an operating plant, it indicates potential
hazards that may arise from the intended designs. Thus, a HAZOP study is very crucial
part for a design project especially for a chemical plant likes octanol plant.
The concept of a HAZOP study first appeared with the aim of identifying possible
hazards present in the facilities that manage highly hazardous materials. According to
Dunjo et al., (2010), HAZOP studies evolved from the Imperial Chemical Industries
technique formulated in the mid of 1960s. Then, one decade later HAZOP was published
formally as a discipline procedure. It is used to identify deviations from the design intent.
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According to Hoyland & Rausand (2009), there are four types of HAZOP which are;
For a large process, HAZOP Study might take several months of biweekly meetings to
complete HAZOP study. Figure 6.2 shows the overall procedural steps in a HAZOP
study.
After the team meeting and project for the HAZOP study is identified, then the
Lead Process Engineer must be informed in order that he can plan for it. Thus, he or she
could have a very detail understanding of the process being reviewed. One individual
must be trained HAZOP Study Leader and serves as HAZOP Study Chairperson. In the
case of a new plant like this octanol plant, he should not have been involved in the design
of the plant and usually Consultant Engineer from outside is brought in for the duty.
Ask for the copies of the P and ID at least a week ahead of the study. The P and ID are
checked so that;
a. The person who are listed in the HAZOP schedule are the right members to attend
the HAZOP Study.
b. It is a continuous process. Additional documents and additional work for Study
Leader is needed to obtained for a batch process.
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c. For a new project, the P and ID must be ready to be HAZOPed.
For an existing plant, P and ID must be up to date with an accurate representation
of the plant.
d. An understandable drawing so that the Leader gets a good overall grasp of the
overall process.
e. If there are non-standard symbols used on the P and ID, symbol is used for
reference.
Pre-Hazop Meeting
A copy of P and ID with the division into short sections can be prepared for the meeting.
Study Leader is encouraged to have a discussion regarding to P and ID that have divided
into short session with Process Engineer, to assure himself has a good grasp of what the
process is all about. Another copy of P and ID also must be prepared as a clean drawing.
It is also known as “HAZOP Master”
Study Leader who is the Chairman will start the three hours meeting by calling on
Process Engineer to give the overall description and the design intent for each P and ID.
The Study Leader then defines each of section to be studies in detail by reading out the
guide word. He also marks up the HAZOP Master in red when any change need to be
made.
Technical Secretary will fill the Report Form. The form and HAZOP Master will
be checked by the Study Leader to ensure the actions are clearly stated and the scope of
each section is completely defined. Sometimes, Study Leader may also act as Technical
Secretary.
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Meeting of Company‟s Identify the Project Identify the Lead
Safety Team for the HAZOP Study Process Engineer
Select the
Define the purpose HAZOP Team
and scope of HAZOP Leader
Pre-HAZOP Meeting
Inform Everyone
Concerned
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In conducting the HAZOP Study, the guide words will be applied to the process
parameter to suggest possible deviations. Process parameters may generally be classified
into the following groups:
Guide words :Simple words that are used to generate thought about the way
deviations from the intended operating conditions in HAZOP
study. 10 guides words recommended are given in Table 6.1.
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Table 6.1: Guide Words Used for the HAZOP Procedure
Guide Words Meaning Comments
No, Not, None The complete negation of the No part of the design intention is
intention achieved, but nothing else happens.
More, Higher, Quantitative increase Applies to quantities such as flow rate
Greater and temperature and to the activities
such as heating and reaction.
Less, Lower Quantitative decrease Applies to quantities such as flow rate
and temperature and to the activities
such as heating and reaction.
As well as Qualitative increase All the design and operating intentions
are achieved along with some additional
activities, such as contamination of
process streams.
Part of Qualitative decrease Only some of the design intentions are
achieved, some are not.
Reverse The logical opposite of Most applicable to activities such as low
or chemical reaction. Also applicable to
substances , for example poison instead
of antidote.
Other than Complete substitution No part of the original intentions is
achieved-the original intention is
replaced by smething else.
Sooner than Too early or in the wrong Applies to process steps or actions.
order
Later than Too late or in the wrong Applies to process steps or actions.
order
Where else In additional locations Applies to process locations, or
locations in operating procedures.
(Crawl &.Louvar, 2011)
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For the production of 10, 000 tonnes of octanol, Process HAZOP type was chosen instead
of the other types of HAZOP. All of the concepts and knowledge in conducting HAZOP
were applied. The following HAZOP procedure has been followed and the HAZOP
Study is shown in Section 6.2.
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6.2 HAZOP STUDY IN OCTANOL PLANT
Project Name: Production of 10,000 Tonnes of Octanol Per Year Date: 10/12/2017 Page 1 of 6
Part Considered: Mixer M-100 Drawing No: M-100
No Study Node Process Guide word Possible Causes Consequences Recommended Action
Parameter
1 Stream 1 Flow No Pipe leakage Incomplete Install flow sensor
Low pressure mixing Install pump
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6.2.2 Heat Exchanger E-100
Project Name: Production of 10,000 Tonnes of Octanol Per Year Date: 10/12/2017 Page 2 of 6
Part Considered: Shell and tube heat exchanger Drawing No: E-100
No Study Node Process Guide word Possible Causes Consequences Recommended Action
Parameter
1 Tubes side Flow Less Pipe blockage Temperature of High temperature
process fluid alarm
remains Flow sensor
constant
more Failure of inlet Temperature for Install temperature
cooling water the output indicator before
valve to close process will be and after process
too low and after process
fluid line.
Flow sensor
Pressure high Failure of Bursting of tube Install high
process fluid pressure alarm
valve
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6.2.3 Exothermic Reactor R-100
Project Name: Production of 10,000 Tonnes of Octanol Per Year Date: 10/12/2017 Page 3 of 6
Part Considered: Exothermic Reactor Drawing No: R-100
No Study Node Process Guide word Possible Causes Consequences Recommended Action
Parameter
1 Cooling coil Flow No Failure of inlet Process fluid Install temperature
cooling water temperature is indicator before and
valve to open not lowered after the process
accordingly fluid line
more Control valve Too much Instruct operators
failure cooling, on procedure
operator fails to reactor cool
take action on
alarm
reverse Failure of water Less cooling Install check valve
source resulting possible
in backward runaway
reaction
2 Vessel Temperature High Uncontrolled Possible of Temperature alarm
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exothermixreacti explosion and
on rupture of
vessel
Project Name: Production of 10,000 Tonnes of Octanol Per Year Date: 10/12/2017 Page 4 of 6
Part Considered: Distillation Column Drawing No: T-100
No Study Node Process Guide word Possible Causes Consequences Recommended Action
Parameter
1 Distillation Flow Less Pipe blockage Column dry out Install low level
column Tube leakage Possible alarm
and blocking dangerous Check maintenance
concentration schedule
No operation Emergency plant
shut down
More Flooding in Install high level
column alarm
Change in Check maintenance
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product quality schedule
Level High Output pipe Overpressure of Install high level
blockage reflux drum drum
Condensed Scheduling
liquid flow back inspection
to distillation
low Pipe partial Back flow of Install valve
clogged and material
leakage
Temperature High Overheating Off specification Install temperature
product sensor
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6.2.5 Separator V-100
Project Name: Production of 10,000 Tonnes of Octanol Per Year Date: 10/12/2017 Page 6 of 6
Part Considered: Separator Drawing No: V-100
No Study Node Process Guide word Possible Causes Consequences Recommended Action
Parameter
1 Stream 27 Flow Less Pipe leakage Amount to be Install flow sensor
separate is Improve the
less material
Low of construction of the
product pipe.
produced
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6.3 EMERGENCY RESPONSE PLAN
The performances goal of the programs need to study in order for ERP can be
develop. Then, the risk evaluation which involving recognized the hazard or threat
scenarios also need to be studied. It is compulsory to consider all the resources of
incident stabilization including people, equipment available as well as the system. Held
conversation with public emergency services in order to know the response time to the
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facility in case of emergency happen. Rules or regulations need to determine if it is
required in order to apply plan emergency planning at the facility. Afterward, before
planning for hazard and threat-specific emergency procedure, protective actions for life
safety required to develop first. In order to stabilize incidents regarding to hazards at the
facility, public emergency services must be synchronized with emergency planning.
Employees need to well-trained to fulfill roles and responsibility throughout emergency
occurrence and finally, make easy exercise to practice ERP. Effect from the accident can
be reduce with appropriate responses during emergency occur and understanding of
hazard is truly required.
One of the initiatives in order to minimize loss of life and other damage property
during emergency is through the following items which are required at the control centre:
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6.3.1 Hazard Identification
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In contact with water
releases flammable gases
which may ignite
Spontaneously.
Causes severe skin burns
and eye damage.
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May cause drowsiness or
dizziness
May displace oxygen and
cause rapid suffocation
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Moving parts of
machinery such as
pinch
Vehicles such as
forklifts
Slips, trips and falls
at work such as at
uneven floor
surfaces
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Fire Hazard Fire hazards take account A simple source of
of all types of live flames, ignition can caused
due to sparks, hot objects, build-up waste to
and chemicals that are cause fire rapidly
possible for ignition, or Due to the damaged
that can provoke a fire to electrical
become big and equipment are one
uncontrolled. It can kill or of the most
seriously injure employees common fire types
or visitors and can damage
or destroy buildings,
equipment and stock.
1. Fire
Fire is a hazard that can give threat to the lives or health and safety of relevant persons,
damage to or loss of property and severe interruption to normal business activities or
opportunities. Fires related to flammable liquids and gases are often related to chemical
plant and can be disastrous. Yet, this accident can be escaped by hazard identification,
proper storage of chemical liquids and control of all ignition sources. Personal protective
equipment must be used when handling chemicals.
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2. Explosion
An explosion is rapid increase in volume and release of energy in an extreme manner,
usually with the generation of high temperature and release of gases. In this plant
explosion due to ignition, it occur when open vigorous flame and spark of heat presence.
Other than that, the ignition of flammable liquids, rupturing of compressed gas cylinders,
maintenance and laboratory activities, dust, and terrorist activities are a few examples
that can cause explosion. An explosion is classified as low or high explosive according to
its rate of burn. Low explosive burn rapidly while high explosives are detonates.
Explosion can cause risk to health which are smoke inhalation, lung and hearing damage,
trauma and burns due to the force and heat of the blast. Structural damage to the facilities,
equipment damage and loss of process are other hazards of an explosion.
3. Chemical spill
A chemical spill is known as a hazardous chemical which are uncontrolled release either
as a solid, liquid or a gas. For reducing the potential for chemical spills, all worksites
need to implement methods and have a plan regarding to chemical spills, regardless of
the type or quantity of hazardous chemical involved (“Keck Graduate Institutes”, 2017).
Quickly respond and effectively managing a spill is very significant to be incorporated in
any safety program of a chemical plant. Workers and other property ought to be protected
as well as the environment from any chemical spill occurrence. For facilities and plants
that store great amounts of multiple chemicals on site or have infrequent or frequent leaks
from heavy equipment, the prevention very important. (“Premier Magnesia”, 2017).
4. Gas leak
This situation refers to the gaseous product leakage from a pipeline or other containment
into area which involve society or any other area which the gaseous product leakage
should not be exists. Flammable gases could be explode when in contact with flame or
sparks. Society or residential will have major impact due to this dangerous situation.
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6.3.3 Emergency Response Procedures
I. Find any protection from flying glass or debris such as take cover under tables,
desks or other objects immediately.
II. If found wounded person, evacuate them. However, do not move seriously
wounded persons unless they are obviously in immediate danger.
III. Evacuate and avoid using elevators
IV. The building fire alarm system needs to be activated and call emergency line 999.
V. As soon as being outside, move to an area at least 300 feet from the affected area.
VI. Workers must be careful of further possible explosions and need to avoid from go
back into the building
VII. Access the damage straightaway and restore service when the area has been
identified to be safe.
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Emergency response procedure in case of chemical spill
1. Alert other people about the situation and quarantine the spill area
I. Identified the spill material and refer to the MSDS to define the potential hazard
associated with the material.
II. Wear protective equipment such as goggles, apron, laboratory coat, gloves, shoe
covers, or respirator.
III. Remove any ignition sources, use plastic or nonmetallic cleanup equipment.
VI. Any spill chemicals need to prevent from going into the drain in order to evade
affecting environment.
I. Immediately sound the alarm when a leak is detected. Report to the person in
charge about the situation.
II. Leave the fuming hoof running and ventilate the affected area prior leaving the
area (if it safe to be done and only to the outside).
V. Turn off any ignition sources that can make situation become worst due to the gas
leak
VI. Use emergency gas masks for escapes purposes even though it only for short
periods of use.
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6.4 EMERGENCY DEVICES
Emergency alarm system Can detect and give warning to people with
visual and audio appliances when the
present of smoke, fire, carbon monoxide or
other emergencies.
The detectors will sense smoke, heat and
will activated alarms automatically or also
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can be activated through manual fire alarm
activation devices such as manual call
points or pull stations.
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6.5 PLANT LAYOUT
The efficiency of an operation process will depend on how the plant and the equipment
are laid out. Apart of safety consideration, it also affect the costs, operation, maintenance,
plant expansion and modular construction. There are two schemes for determination of
plant layout. First, The flow-through layout or flow-line pattern and second one is
grouping similar plant (Ray & sneeby, 2000). For this octanol plant, the flow-line line
pattern was chosen where the plant items are arranged in order in which they appear on
the process flow sheet. Moreover, the second type pattern is often used for larger plants.
Referring to the Site Location chapter, Tanjung Langsat Industrial Land, Johor has been
chosen as the site location for this Octanol Plant. Several factors such as raw material
supply, potential marketing area, logistics and transportation facilities, availability of
labor, availability of utilities, availability and price of land, environmental issue and local
community considerations had been compared to the other two industrial lands in
Malaysia.
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Furthermore, the octanol plant is relatively small and should not occupy more
than 5 acres and this small area is sufficient for future expansion plan. Thus, site location
is an acceptable area for the plant layout. Figure 6.3 shows the octanol plant layout. The
octanol plant is divided into several zones as follows:
Amenities
It is necessary to separate canteen facilities and administration building. Proper fire-
protections are installed. The main entrance is located near to the administration building
so that the administrative officers and business visits can be directly access to the
building. Moreover, it is the safest zone in the plant. Essential activities such as
offloading supplies and the collecting waste are away as far as possible. This zone is
strategically located upwind.
Emergency Services
Octanol is not a toxic material but it is a flammable material. Fire water tank as well as
fire emergency department are positioned to give rapid vehicle access to all parts of the
site and closed to gate to enable external aid to be brought in. This plant layout consisted
of two exits and one entrance point. The main entrance is located at non-process area
which is near to administration building. The location of evacuation and assembly point
is near to the entrance. The distance between assembly point and plant area are
reasonably close so that it is possible for personnel to evacuate as fast as possible from
the plant area in case of emergency.
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Plant Area
The plant area is about half of the plant layout. It is the heart for the octanol plant and the
most hazardous area. All of safety precautions are strictly followed. Non-workers are not
encouraged to enter this zone. The control room is located adjacent to plant area in a safer
distance to the processing unit. The control room is located reasonably close the plant
area so that the plant area can be viewed clearly from the control room so that, any
suspicious incident can be detected as early as possible. Both control room and laboratory
is built with fire-proof material. Expansion area also is provided for the future plan.
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Figure 6.3: Plant Layout of Octanol Plant
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