ues Desk Date_L/ I /91 Laboratory Instructor Separation of the | 2 Pre-lab Components of a Mixture Questions Before beginning this experiment in the laboratory, you should be able to answer the following questions. 1, Classify each of the following as a pure substance or a mixture; if tis a mixture, state whether itis heterogeneous ‘or homogeneous: (a) concrete, (b) tomato juice, (c) marble, (d) seawater, and (e) iron. \)Haaroqeneaus WK UC D)Mereroencet ) . A}homogevenlus wrrxture C)~ure SubSromer 2. Suggest a way to determine whether a colorless liquid is pure water ora salt solution without tasting it. ~ Sait Sarton Will racl c c pure LOW Wirevee 0 \ tx 4, Define the progess of sublimation. coe : oan \ é ord YD ° € aPpe torte OF A 5, How do decantation and filtration differ? Which should be faster? A AeCawtawon 15% ry nik So as do He < Ak tne Doron Wile rarlw Us oa f o ay ol\\ A to Cy 6. Why shoutd you never place a hot object on tie pan ofa balance? LT will ative meccorme wv Copyright © 2018 Pearson Eduction, le 226 Repost Sheet + Separation of the Components of a Mixture TH AS ep a Wie ie nS eam mS 8. A mixture was found to contain 1.05 g of SiO3, 0.69 g of cellulose, and 1.82 g of calcium carbonate. V percentage of calcium carbonate is in the mixture? 9, How could you separate a mixture of acetone and c-naphthol? Consult Table 2.1 for physical properties. 10. How could you separate zine chloride from Si0;? 11. A student found that her mixture was 13% NH,Cl, 18% NaCl, and 75% SiO, are correct, what did she most likely do incorrectly in her experiment? Assuming that her caleulat Nel 12, Why is the NaCl extracted with water three times as opposed to only once? \ Copyright © 2018 Pearson Education, Ine.Name us PS Desk Date A . Laboratory Instructor Unknown no. REPORT SHEET | EXPERIMENT Separation of the | 2 Components of a Mixture Determination of Mass Percent of Ammonium Chloride Mass of evaporating dish and original sample Mass of evaporating dish Mass of original sample Mass of evaporating dish after subliming NH,CI Mass of NHCI Percent of NH,CI (show calculations) Determination of Mass Percent of Sodium Chloride Mass of evaporating dish, watch glass, and NaCl Mass of evaporating dish and watch glass Mass of NaCl Percent of NaCl (show calculations) Determination of Mass Percent of Silicon Dioxide Mass of evaporating dish and SiO. g Mass of evaporating dish 2.2 2 Mass of SiO, Percent of SiO, (show calculations) SUT 62.31 2 \ 7¢ Copyright © 2018 Pearson Education, lsMixture tion of the Components of D. n of Percent Recovery Mass of original sample Mass of determined (NH,CI+NaC1+$i03) »|2 > 652, + 11S = Differences in these weights 1.S4-L16 e Percent recovery of matter = Satter reaver 9944 — Paes Sha. g orginal sample ‘Account for your errors. QUESTIONS 1, Could the separation in this experiment have been done in a different order? For example, if the mixture ‘was first extracted with water and then both the extract and the insoluble residue were heated to dryness, could you determine the amounts of NaCl, NH,Cl, and SiO, originally present? Why or why not? Consult a handbook to answer these questions. J 2. How could you separate barium sulfate, BaSO,, from NaCl? j mar \ Ox k worry c ‘ FY \ 3. How could you separate magnesium chloride, MgCl, from silver chloride, AgCI? How could you separate tellurium dioxide, TeO,, from SiO, Fl\iwatcow. 101 5. How could you separate lauric acid from c-naphthol? (See Table 3.1.) Copyright © 2018 Pearson Education, Ine.