Hasil Praktikum

Diketahui :

 Data Pembakuan
- Mg Asam oksalat 1 = 50,2 mg
- Mg Asam oksalat 2 = 50,5 mg
- BM Asam oksalat = 126
- Volume NaOH 1 = 9,8 mL
- Volume NaOH 2 = 9,6 mL
 Data Titarsi Sampel
( 1 x ECC )
- Mg yang di ECC = 100 mg
- Volume NaOH hasil titrasi ECC = 6,5 mL
- BM Asam salisilat = 138,1
( 3 x ECC )
- Mg yang di ECC = 100 mg
- Volume NaOH hasil titrasi ECC = 8,3 mL
- BM Asam salisilat = 138,1

Pembakuan
- BM Asam oksalat = 126
- Valensi oksalat = 2

BM 126
BE = e =¿ 2 =¿ 63

mg Asamoksalat 1
 NNaOH 1 = BE x V . NaOH 1
50,2
= 63 x 9,8
50,2
= 617 , 4
= 0,081 N

mg Asam oksalat 2
 NNaOH2 = BE x V . NaOH 2
50,5
= 63 x 9,6
50,5
= 604,8
= 0,083 N
 N 1+ N 2 0,081+ 0,083 0,164
Nrata-rata = 2
=
2
=
2
=¿ 0,082 N

Titrasi Sampel 1x ECC

1. Reaksi

O OH O ONa

OH OH

+ NaOH + H2O

2. mgrek NaOH = NNaOH x Volume NaOH

= 0,082 x 6,5
= 0,533
koef
3. mgrek Asam salisilat = x mgrek NaOH
koef
1
= 1 x 0,533
= 0,533
4. mg Asam salisilat = mgrek Asam salisilat x BM
= 0,533 x 138,1
= 73,6073 mg
mg Asam salisilat
5. % kadar = x 100%
mg sampel
73,6073mg
= x 100 %
100 mg
= 73,6073 %

Titrasi sampel 3x ECC

1. Reaksi

O OH O ONa

OH OH

+ NaOH + H2O

2. mgrek NaOH = NNaOH x Volume NaOH

= 0,082 x 8,3
= 0,6806
koef
3. mgrek Asam salisilat = x mgrek NaOH
koef
 1
= x 0,6806
1
= 0,6806
4. mg Asam salisilat = mgrek Asam salisilat x BM
= 0,6806 X 138,1
= 93,99086 mg
mg Asam salisilat
5. % kadar = x 100 %
mg sampel
93,99086 mg
= x 100 %
100 mg
= 93,99086 %