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Research Center for Metrology-

Indonesian Institute of Sciences

Jaminan Ketertelusuran
METROLOGI Massa
di INDONESIA

Sosialisasi Metrologi
Tangerang Selatan, 4 Desember 2018

by Renanta Hayu
Kegiatan METROLOGI

Realisasi satuan SI, Pengukuran di Industri, Pengukuran dalam transaksi


pemeliharaan dan proses produksi perdagangan,perlindungan
diseminasi SNSU kesehatan
METROLOGI TERAPAN /
METROLOGI ILMIAH METROLOGI INDUSTRI METROLOGI LEGAL

Research Center for Metrology - Indonesian Institute of Sciences | Measurement for Happiness...
Measurement Traceability

sifat dari hasil pengukuran yang dapat dihubungkan ke


acuan tertentu, melalui rantai kalibrasi yang tak
terputus yang terdokumentasi,yang masing-masing
berkontribusi terhadap ketidakpastian pengukuran

property of a measurement result whereby the result


can be related to a reference through a documented
unbroken chain of calibrations, each contributing to
the measurement uncertainty

International Vocabulary of Metrology – VIM 2008: 2.41

Research Center for Metrology - Indonesian Institute of Sciences | Measurement for Happiness...
kilogram
4E-8
3E-7
A K

o definisi dapat
rusak atau dirusak 8E-7
o akumulasi debu
o harus dibersihkan
mol s
o tidak dapat
o memiliki
digunakan secara 3E-15 awalan “kilo”
rutin (karena takut
o definisi
rusak)
sebagai
o definisi berubah
barang
69 μg/100 th
1E-4 o ada sejak
o hanya dapat
1889
diakses di BIPM
cd m o tiga besaran
dasar
lainnya
1E-12 bergantung
kg
?
Research Center for Metrology - Indonesian Institute of Sciences | Measurement for Happiness...
kilogram

1889  before 20 May 2019

“The kilogram is the unit of mass, it is equal to the


mass of the international prototype kilogram”

Material : 90% Pt and 10% Ir, density :


21500 kg/m³ ,cylindrical with diameter:
39 mm, height 39 mm.

Location:
Bureau international des poids et
measure ( BIPM ), Sevres, France

Research Center for Metrology - Indonesian Institute of Sciences | Measurement for Happiness...
CMC’s in Mass Measurement

Research Center for Metrology - Indonesian Institute of Sciences | Measurement for Happiness...
Definition of kg

International prototype of kg
1 kg Platinum Iridium (PtIr)

Copy of 1 kg
International Prototype No 25 Stainless Steel No 112492
1kg 5 µg (k=1)
1kg 14 µg (k=1)

1 kg Set of E1 Weights
Stainless Steel No 74

1 kg 30 µg (k=1)
1kg 16 µg (k=1)
1 mg – 50 kg 0.5 µg – 1.1 mg (k=2)

Set of E2, F1, F2,M1,M2,M3 Weights


and Weighing Machines

Research Center for Metrology - Indonesian Institute of Sciences | Measurement for Happiness...
Extraordinary Calibration
• IPK disimpan di BIPM sejak 1889
• IPK hanya digunakan dalam dua kali pengukuran yaitu
‘second ‘ dan ‘third’ periodic verification (2ndPV dan
3rdPV)
• Hasil 3rdPV : Salinan IPK massanya berubah terhadap
IPK sebesar 69 g per 100 tahun • Untuk mengantisipasi redefinisi kg
• 2013, CIPM menyetujui pengukuran IPK dan semua
salinannya (extraordinary calibration)
• Periode pelaksanaan akhir 2013  2014
• Hasil : terdapat pergeseran sebesar 35 g
• BIPM mengeluarkan amandemen semua sertifikat yang
pernah dikeluarkan sepanjang tahun 1992  2014
termasuk sertifikat E0 milik Puslit Metrologi LIPI
• CCM merekomendasikan setiap NMI untuk
mengevaluasi efek pergeseran

Research Center for Metrology - Indonesian Institute of Sciences | Measurement for Happiness...
Statistitical Process Control (E0 75)

skema diseminasi massa


nilai massa E0 92 (BIPM)

999.999 280

999.999 260

True mass /g
999.999 240

999.999 220

999.999 200

2012 2015 2017


Calibration Interval
True mass Mean UWL LWL UCL LCL

nilai massa E0 74 Control chart E0 75


Research Center for Metrology - Indonesian Institute of Sciences | Measurement for Happiness...
Statistical Process Control (E1 199)
Control Chart of 199-1kg

999.999 98

Conventional Mass /g
999.999 96

999.999 94

999.999 92

999.999 90

2013 Calibration Interval 2016

pergeseran nilai massa E1 Conv. Mass Mean UWL LWL UCL LCL
Control Chart of 199-0,001g

0.000 999 6

Conventional Mass /g
0.000 999 5

0.000 999 4

0.000 999 3

2013 Calibration Interval 2016


Statistical process control to monitor the impacts of extraordinary calibrations result on the mass Conv. Mass Mean UWL LWL UCL LCL

dissemination
IOP Conf. Series: Journal of Physics: Conf. Series 1065 (2018) 042046 Control chart E1 199
doi:10.1088/1742-6596/1065/4/042046
Research Center for Metrology - Indonesian Institute of Sciences | Measurement for Happiness...
Redefinisi kg

Since 20 May 2019

The kilogram (kg) is defined by taking the fixed numerical value of the Planck
constant h to be 6.626 070 15 x 10-34 when expressed in the unit J s, which is
equal to kgm2s-1,where the metre and the second are defined in terms of c
and v.

Research Center for Metrology - Indonesian Institute of Sciences | Measurement for Happiness...
Rantai ketertelusuran

Research Center for Metrology - Indonesian Institute of Sciences | Measurement for Happiness...
Old and New Mass Measurement Traceability

M Stock, S Davidson, H Fang, M Milton, E de Mirandes, P Richard


and C Sutton, “Maintaining and disseminating the kilogram
following its redefinition,”Metrologia, Vol.54, pp. 98–107, 2017.

Research Center for Metrology - Indonesian Institute of Sciences | Measurement for Happiness...
Old and New Mass Measurement Traceability

Research Center for Metrology - Indonesian Institute of Sciences | Measurement for Happiness...
Rencana

Diseminasi anak
timbangan dan
timbangan

Diseminasi PtIr /
E0 (di udara dan
vakum)

Pengukuran silicon
sphere tertelusur
ke definisi kg yang
baru

Research Center for Metrology - Indonesian Institute of Sciences | Measurement for Happiness...
Kesimpulan
• Sejak 1889, IPK telah dipakai sebagai realisasi kilogram
• Pengukuran konstanta Avogadro,NA, dan konstanta Planck,h, menggunakan
tehnologi canggih telah berhasil mengukur kedua konstanta tersebut dengan
ketidakpastian yang jauh lebih baik dari ’long term mass stability’ IPK
• Redefinisi kg memungkinkan untuk mengukur besaran massa, gaya dan torsi
dalam nominal kecil secara langsung
• Redefinisi SI akan berlaku efektif sejak 20 Mei 2019

Research Center for Metrology - Indonesian Institute of Sciences | Measurement for Happiness...
Thank You

Research Center for Metrology - Indonesian Institute of Sciences | Measurement for Happiness...

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